Text

Westinghouse Hematite Decommissioning Project - Final Status Survey Final Report Volume 3, Chapter 4, Survey Area Release Record for Land Survey Area 10, Survey Unit 12, Rev. 2, J10497-2 Uds Level 2 Report Final Report
	ML18074A220
Person / Time
Site:	07000036
Issue date:	03/13/2015
From:	Barry Miller, Ridenhower R, Vania I; Perma-Fix Environmental Services, Testamerica Labs, Westinghouse
To:	; Office of Nuclear Material Safety and Safeguards
Shared Package
ML18074A285	List: ML18074A217; ML18074A218; ML18074A219; ML18074A220; ML18074A221; ML18074A222; ML18074A223; ML18074A224; ML18074A225; ML18074A227; ML18074A292; ML18074A293; ML18074A295; ML18074A296; ML18074A297; ML18074A298; ML18074A299; ML18075A008; ML18075A009; ML18075A010; ML18075A011; ML18075A012; ML18075A013; ML18075A014; ML18075A015; ML18075A016; ML18075A017;
References
	HEM-18-6
	Download: ML18074A220 (19)
	v • d • e

ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-10497-2 Client Project/Site: HDP For:

Perma-Fix Environmental Services Inc.

2800 Solway Road Knoxville, Tennessee 37931 Attn: Brian Miller Authorized for release by:

3/13/2015 9:41:31 AM Rhonda Ridenhower, Manager of Project Management rhonda.ridenhower@testamericainc.com Designee for Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP TestAmerica Job ID: 160-10497-2 Page 2 of 19 TestAmerica St. Louis 3/13/2015 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

4 Receipt Checklists.........................................

6 Definitions/Glossary.......................................

7 Method Summary.........................................

8 Sample Summary.........................................

9 Client Sample Results......................................

10 QC Sample Results........................................

17 QC Association Summary...................................

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Case Narrative Client: Perma-Fix Environmental Services Inc.

TestAmerica Job ID: 160-10497-2 Project/Site: HDP Job ID: 160-10497-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Perma-Fix Environmental Services Inc.

Project: HDP Report Number: 160-10497-2 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 02/13/2015; the samples arrived in good condition, properly preserved. The temperature of the coolers at receipt was 18.0 C.

RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)

Samples L10-12-01-B-E-S-00 (160-10497-1), L10-12-02-B-E-S-00 (160-10497-2), L10-12-03-B-E-S-00 (160-10497-3),

L10-12-04-B-E-S-00 (160-10497-4), L10-12-05-B-R-S-00 (160-10497-5), L10-12-06-B-E-S-00 (160-10497-6), L10-12-07-B-E-S-00 (160-10497-7), L10-12-08-B-R-S-00 (160-10497-8), L10-12-09-B-E-S-00 (160-10497-9), L10-12-10-B-R-S-00 (160-10497-10),

L10-12-11-B-E-S-00 (160-10497-11), L10-12-12-B-E-S-00 (160-10497-12) and L10-12-07-B-E-Q-00 (160-10497-13) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R. The samples were dried on 02/13/2015, prepared on 02/18/2015 and analyzed on 03/11/2015.

No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

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10 11 TestAmerica St Louis I

Chain of Custody Record 13715 Rider Trail North 160-10497 Chain of Custody Earth City, MO 63045 phone 314.298.8566 fax

-~~ 0 DW O NPDES D RCRA 0 Other:

Client Contact Project Manager: Brian Miller Site.Contact: Ellen Jakub Pemia-Fix Environmental Services Tel/Fax: (314) 810-3333 Lab

Contact:

Ivan Vanya 2800 Solway Road Analysis Turnaround Time Knoxville, TN 37931 0 CALENDAR DAYS O WORJ<ING DAYS

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Sample Identification Sample I Sample Date Time L 10-12-01-8-E-S-00 2/1 1/15 1042 L 10-12-02-8-E-S-OO 2/11/15 J 1048 L 10-12--03-B-E-S-OO 2111115 I 1055 L 10-12-04-B-E-S-OO 2111115 I 1059 L 10-12-05-B-R-S-OO 2111115 I. 1622 L10-12-06-B-E-S-OO 211 1115 I 1627 L 10-12~07-B-E-S-OO 2111115 I 1651 L 10-12--08-B-R-S-OO 2111115 I 1111 L 10-12-09-B-E-S-OO 2111115 I 1130 L 10-12"10-B-R-S-OO 211 1115 I 1638 L 10-12°11-B-E-S-OO 2111115 I 1644 Type (C=Comp, I I # of G=Grab)

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XI X XIX XI X XIX XIX XIX XIX XIX XIX XI X XIX Date: 02/13/2015 Carrier: Courier Test America THE LEADER IN ENVIRONMENTAL TESTING TestAmerica Laboratories, Inc.

COC No: 021315-FSS1 Page 1 of2 Sampler:

For Lab Use Oilly:

'Walk-in Client:

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Lab Sampling:

Job I SDG No.:

Sample Specific Notes:

Matt Cushman Matt Cushman Matt Cushman Matt Cushman Jahmai Williams Matt Cushman Jahmai Williams Matt Cushman Matt Cushman Jahmai Williams Jahmaf Williams Possible Hazard Identification:

Sample Disposal (.A lee may be assessed if samples are retained longer than 1 month)

Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the Comments Section if the lab is to dlspose of the sample.

0 Non-Ha:rard D Flammable D* Skin rmtant D Prnson B D Unknown J 0 Return to Gient D DispoSal by Lab D Archive fur Months

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10 11 TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 phone 314.298.8566 fax Client Contact PeF!Tla-Fix Environmental Services 2800 Solway Road Knoxville., TN 37931

{865) 690-0501 Phone (865) 539-9868 FAX Project Name: Hematite Decommissioning Project Site: Westinghouse Hematite, MO P 0#832953 Sample Identification L 10-12-07-8-E-Q-OO I'------

Chain of Custody Record TestAmerica THE LEADER IN ENVIRONMENT AL TESTlNG Regulatory Program: D DW D NP.DES D RCRA 0 Other:

TestAmerica Laboratories, Inc.

Project Manager: Brian Miller Site

Contact:

Ellen Jakub Date: 02'13/2015 COC No: 021315-FSS1 TeUFax: (314) 810-3333 Lab

Contact:

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Sample Disposal. (A fee may be assessed if samples are retained longer thaR 1 month)

Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the Comments Section if the lab is to dispose of the sample.

0 Non-Hazard O Flammable O Skin I rrttant O Poison B O Unknown 0 Return to Client 0 Disposal by Lab 0 Archive for Months Special Instructions/QC Requirements & Comments: Potential for Radiological Contamination Custody Seals Intact 0

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Login Sample Receipt Checklist Client: Perma-Fix Environmental Services Inc.

Job Number: 160-10497-2 Login Number: 10497 Question Answer Comment Creator: Clarke, Jill C List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.

True The cooler's custody seal, if present, is intact.

N/A Sample custody seals, if present, are intact.

True The cooler or samples do not appear to have been compromised or tampered with.

N/A Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

False Is the Field Sampler's name present on COC?

True There are no discrepancies between the containers received and the COC.

True Samples are received within Holding Time.

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified.

True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

N/A Residual Chlorine Checked.

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Definitions/Glossary TestAmerica Job ID: 160-10497-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Qualifiers Rad Qualifier Description U

Result is less than the sample detection limit.

Qualifier Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation

%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)

NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method Summary TestAmerica Job ID: 160-10497-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)

TAL SL Protocol

References:

DOE = U.S. Department of Energy Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 8 of 19 3/13/2015 1

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Sample Summary TestAmerica Job ID: 160-10497-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID Client Sample ID Received Collected Matrix 160-10497-1 L10-12-01-B-E-S-00 Solid 02/11/15 10:42 02/13/15 12:10 160-10497-2 L10-12-02-B-E-S-00 Solid 02/11/15 10:48 02/13/15 12:10 160-10497-3 L10-12-03-B-E-S-00 Solid 02/11/15 10:55 02/13/15 12:10 160-10497-4 L10-12-04-B-E-S-00 Solid 02/11/15 10:59 02/13/15 12:10 160-10497-5 L10-12-05-B-R-S-00 Solid 02/11/15 16:22 02/13/15 12:10 160-10497-6 L10-12-06-B-E-S-00 Solid 02/11/15 16:27 02/13/15 12:10 160-10497-7 L10-12-07-B-E-S-00 Solid 02/11/15 16:51 02/13/15 12:10 160-10497-8 L10-12-08-B-R-S-00 Solid 02/11/15 11:11 02/13/15 12:10 160-10497-9 L10-12-09-B-E-S-00 Solid 02/11/15 11:30 02/13/15 12:10 160-10497-10 L10-12-10-B-R-S-00 Solid 02/11/15 16:38 02/13/15 12:10 160-10497-11 L10-12-11-B-E-S-00 Solid 02/11/15 16:44 02/13/15 12:10 160-10497-12 L10-12-12-B-E-S-00 Solid 02/11/15 11:03 02/13/15 12:10 160-10497-13 L10-12-07-B-E-Q-00 Solid 02/11/15 16:51 02/13/15 12:10 TestAmerica St. Louis Page 9 of 19 3/13/2015 1

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Client Sample Results TestAmerica Job ID: 160-10497-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-10497-1 Client Sample ID: L10-12-01-B-E-S-00 Matrix: Solid Date Collected: 02/11/15 10:42 Date Received: 02/13/15 12:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.01 (2+/-)

0.160 (2+/-)

1 03/11/15 07:42 02/18/15 09:00 pCi/g 0.112 RL MDC 0.122 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/18/15 09:00 03/11/15 07:42 1

0.389 0.330 0.312 1.04 Bismuth 212 pCi/g 02/18/15 09:00 03/11/15 07:42 1

0.0599 0.136 0.0941 0.949 Bismuth 214 pCi/g 02/18/15 09:00 03/11/15 07:42 1

0.0711 0.144 0.0724 0.958 Lead 212 pCi/g 02/18/15 09:00 03/11/15 07:42 1

0.0800 0.144 0.0852 1.11 Lead 214 pCi/g 02/18/15 09:00 03/11/15 07:42 1

0.302 2.27 1.13 19.2 Potassium 40 pCi/g 02/18/15 09:00 03/11/15 07:42 1

1.12 0.196 0.193 U

0.312 Protactinium 231 pCi/g 02/18/15 09:00 03/11/15 07:42 1

0.0599 1.00 0.136 0.0941 0.949 Radium 226 pCi/g 02/18/15 09:00 03/11/15 07:42 1

0.112 0.160 0.122 1.01 Thorium 232 pCi/g 02/18/15 09:00 03/11/15 07:42 1

0.836 0.539 0.525 1.13 Thorium 234 pCi/g 02/18/15 09:00 03/11/15 07:42 1

0.251 0.141 0.141 U

0.0515 Uranium 235 pCi/g 02/18/15 09:00 03/11/15 07:42 1

0.110 0.0652 0.0652 U

-0.00101 Americium 241 pCi/g 02/18/15 09:00 03/11/15 07:42 1

5.03 2.86 2.86 U

-0.449 Protactinium 234m Pb-210 1.57 0.749 0.771 0.896 pCi/g 02/18/15 09:00 03/11/15 07:42 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.367 0.0477 0.0611 0.0343 pCi/g 02/18/15 09:00 03/11/15 07:42 1

Lab Sample ID: 160-10497-2 Client Sample ID: L10-12-02-B-E-S-00 Matrix: Solid Date Collected: 02/11/15 10:48 Date Received: 02/13/15 12:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.08 (2+/-)

0.198 (2+/-)

1 03/11/15 07:43 02/18/15 09:00 pCi/g 0.107 RL MDC 0.165 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/18/15 09:00 03/11/15 07:43 1

0.609 0.702 0.686 1.42 Bismuth 212 pCi/g 02/18/15 09:00 03/11/15 07:43 1

0.0935 0.160 0.130 0.904 Bismuth 214 pCi/g 02/18/15 09:00 03/11/15 07:43 1

0.0911 0.146 0.0866 0.913 Lead 212 pCi/g 02/18/15 09:00 03/11/15 07:43 1

0.0883 0.163 0.112 1.14 Lead 214 pCi/g 02/18/15 09:00 03/11/15 07:43 1

0.416 2.31 1.40 18.0 Potassium 40 pCi/g 02/18/15 09:00 03/11/15 07:43 1

1.22 0.306 0.304 U

0.324 Protactinium 231 pCi/g 02/18/15 09:00 03/11/15 07:43 1

0.0935 1.00 0.160 0.130 0.904 Radium 226 pCi/g 02/18/15 09:00 03/11/15 07:43 1

0.107 0.198 0.165 1.08 Thorium 232 pCi/g 02/18/15 09:00 03/11/15 07:43 1

0.932 0.588 0.579 0.990 Thorium 234 pCi/g 02/18/15 09:00 03/11/15 07:43 1

0.264 0.166 0.166 U

0.109 Uranium 235 pCi/g 02/18/15 09:00 03/11/15 07:43 1

0.118 0.0704 0.0704 U

0.0217 Americium 241 pCi/g 02/18/15 09:00 03/11/15 07:43 1

6.85 3.95 3.95 U

1.48 Protactinium 234m Pb-210 0.811 0.562 0.570 0.801 pCi/g 02/18/15 09:00 03/11/15 07:43 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.328 0.0594 0.0685 0.0453 pCi/g 02/18/15 09:00 03/11/15 07:43 1

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Client Sample Results TestAmerica Job ID: 160-10497-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-10497-3 Client Sample ID: L10-12-03-B-E-S-00 Matrix: Solid Date Collected: 02/11/15 10:55 Date Received: 02/13/15 12:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.47 (2+/-)

0.224 (2+/-)

1 03/11/15 08:19 02/18/15 09:00 pCi/g 0.129 RL MDC 0.168 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/18/15 09:00 03/11/15 08:19 1

0.563 0.631 0.603 1.80 Bismuth 212 pCi/g 02/18/15 09:00 03/11/15 08:19 1

0.0867 0.192 0.128 1.39 Bismuth 214 pCi/g 02/18/15 09:00 03/11/15 08:19 1

0.0934 0.204 0.0975 1.38 Lead 212 pCi/g 02/18/15 09:00 03/11/15 08:19 1

0.103 0.221 0.129 1.72 Lead 214 pCi/g 02/18/15 09:00 03/11/15 08:19 1

0.505 2.76 1.44 23.3 Potassium 40 pCi/g 02/18/15 09:00 03/11/15 08:19 1

1.37 0.265 0.261 U

0.423 Protactinium 231 pCi/g 02/18/15 09:00 03/11/15 08:19 1

0.0867 1.00 0.192 0.128 1.39 Radium 226 pCi/g 02/18/15 09:00 03/11/15 08:19 1

0.129 0.224 0.168 1.47 Thorium 232 pCi/g 02/18/15 09:00 03/11/15 08:19 1

1.06 0.384 0.361 1.25 Thorium 234 pCi/g 02/18/15 09:00 03/11/15 08:19 1

0.285 0.169 0.169 U

-0.0311 Uranium 235 pCi/g 02/18/15 09:00 03/11/15 08:19 1

0.118 0.799 0.799 U

-0.0132 Americium 241 pCi/g 02/18/15 09:00 03/11/15 08:19 1

6.60 3.94 3.94 U

2.45 Protactinium 234m Pb-210 1.53 0.811 0.831 1.03 pCi/g 02/18/15 09:00 03/11/15 08:19 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.506 0.0677 0.0854 0.0494 pCi/g 02/18/15 09:00 03/11/15 08:19 1

Lab Sample ID: 160-10497-4 Client Sample ID: L10-12-04-B-E-S-00 Matrix: Solid Date Collected: 02/11/15 10:59 Date Received: 02/13/15 12:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.41 (2+/-)

0.233 (2+/-)

1 03/11/15 09:24 02/18/15 09:00 pCi/g 0.0947 RL MDC 0.183 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/18/15 09:00 03/11/15 09:24 1

0.525 0.650 0.627 1.63 Bismuth 212 pCi/g 02/18/15 09:00 03/11/15 09:24 1

0.0788 0.170 0.119 1.16 Bismuth 214 pCi/g 02/18/15 09:00 03/11/15 09:24 1

0.0790 0.175 0.0867 1.18 Lead 212 pCi/g 02/18/15 09:00 03/11/15 09:24 1

0.0845 0.180 0.118 1.31 Lead 214 pCi/g 02/18/15 09:00 03/11/15 09:24 1

0.452 2.55 1.35 21.1 Potassium 40 pCi/g 02/18/15 09:00 03/11/15 09:24 1

0.672 0.413 0.411 U

0.355 Protactinium 231 pCi/g 02/18/15 09:00 03/11/15 09:24 1

0.0788 1.00 0.170 0.119 1.16 Radium 226 pCi/g 02/18/15 09:00 03/11/15 09:24 1

0.0947 0.233 0.183 1.41 Thorium 232 pCi/g 02/18/15 09:00 03/11/15 09:24 1

0.943 0.610 0.595 1.29 Thorium 234 pCi/g 02/18/15 09:00 03/11/15 09:24 1

0.269 0.155 0.154 U

0.146 Uranium 235 pCi/g 02/18/15 09:00 03/11/15 09:24 1

0.112 0.0670 0.0669 U

0.0284 Americium 241 pCi/g 02/18/15 09:00 03/11/15 09:24 1

6.48 3.64 3.64 U

0.00572 Protactinium 234m Pb-210 1.80 0.788 0.816 0.983 pCi/g 02/18/15 09:00 03/11/15 09:24 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.378 0.0487 0.0625 0.0345 pCi/g 02/18/15 09:00 03/11/15 09:24 1

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Client Sample Results TestAmerica Job ID: 160-10497-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-10497-5 Client Sample ID: L10-12-05-B-R-S-00 Matrix: Solid Date Collected: 02/11/15 16:22 Date Received: 02/13/15 12:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.12 (2+/-)

0.178 (2+/-)

1 03/11/15 09:25 02/18/15 09:00 pCi/g 0.139 RL MDC 0.136 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.570 0.395 0.388 0.708 Bismuth 212 pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.0774 0.185 0.132 1.25 Bismuth 214 pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.0576 0.163 0.0803 1.10 Lead 212 pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.0891 0.174 0.108 1.31 Lead 214 pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.272 2.38 1.34 19.2 Potassium 40 pCi/g 02/18/15 09:00 03/11/15 09:25 1

1.42 0.317 0.300 U

0.940 Protactinium 231 pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.0774 1.00 0.185 0.132 1.25 Radium 226 pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.139 0.178 0.136 1.12 Thorium 232 pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.903 0.360 0.326 1.46 Thorium 234 pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.197 0.151 0.147 0.308 Uranium 235 pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.119 0.0726 0.0724 U

-0.0590 Americium 241 pCi/g 02/18/15 09:00 03/11/15 09:25 1

5.69 3.51 3.50 U

3.04 Protactinium 234m Pb-210 1.10 0.582 0.596 0.822 pCi/g 02/18/15 09:00 03/11/15 09:25 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.324 0.0469 0.0577 0.0336 pCi/g 02/18/15 09:00 03/11/15 09:25 1

Lab Sample ID: 160-10497-6 Client Sample ID: L10-12-06-B-E-S-00 Matrix: Solid Date Collected: 02/11/15 16:27 Date Received: 02/13/15 12:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.981 (2+/-)

0.183 (2+/-)

1 03/11/15 09:25 02/18/15 09:00 pCi/g 0.156 RL MDC 0.153 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.647 0.437 0.431 0.719 Bismuth 212 pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.0763 0.172 0.127 1.12 Bismuth 214 pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.0946 0.142 0.0868 0.867 Lead 212 pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.0940 0.161 0.114 1.09 Lead 214 pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.507 2.24 1.38 17.2 Potassium 40 pCi/g 02/18/15 09:00 03/11/15 09:25 1

1.30 0.227 0.225 U

0.304 Protactinium 231 pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.0763 1.00 0.172 0.127 1.12 Radium 226 pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.156 0.183 0.153 0.981 Thorium 232 pCi/g 02/18/15 09:00 03/11/15 09:25 1

1.19 0.429 0.421 U

0.790 Thorium 234 pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.205 0.162 0.162 U

0.0932 Uranium 235 pCi/g 02/18/15 09:00 03/11/15 09:25 1

0.124 0.0736 0.0736 U

-0.0141 Americium 241 pCi/g 02/18/15 09:00 03/11/15 09:25 1

6.55 3.57 3.56 U

2.07 Protactinium 234m Pb-210 1.20 0.702 0.716 0.901 pCi/g 02/18/15 09:00 03/11/15 09:25 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.294 0.0600 0.0673 0.0522 pCi/g 02/18/15 09:00 03/11/15 09:25 1

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Client Sample Results TestAmerica Job ID: 160-10497-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-10497-7 Client Sample ID: L10-12-07-B-E-S-00 Matrix: Solid Date Collected: 02/11/15 16:51 Date Received: 02/13/15 12:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.31 (2+/-)

0.187 (2+/-)

1 03/11/15 09:26 02/18/15 09:00 pCi/g 0.110 RL MDC 0.133 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/18/15 09:00 03/11/15 09:26 1

0.479 0.555 0.530 1.63 Bismuth 212 pCi/g 02/18/15 09:00 03/11/15 09:26 1

0.0827 0.204 0.129 1.53 Bismuth 214 pCi/g 02/18/15 09:00 03/11/15 09:26 1

0.0795 0.179 0.0808 1.23 Lead 212 pCi/g 02/18/15 09:00 03/11/15 09:26 1

0.0902 0.204 0.113 1.62 Lead 214 pCi/g 02/18/15 09:00 03/11/15 09:26 1

0.339 2.50 1.19 21.9 Potassium 40 pCi/g 02/18/15 09:00 03/11/15 09:26 1

1.36 0.305 0.301 U

0.449 Protactinium 231 pCi/g 02/18/15 09:00 03/11/15 09:26 1

0.0827 1.00 0.204 0.129 1.53 Radium 226 pCi/g 02/18/15 09:00 03/11/15 09:26 1

0.110 0.187 0.133 1.31 Thorium 232 pCi/g 02/18/15 09:00 03/11/15 09:26 1

0.888 0.316 0.299 0.956 Thorium 234 pCi/g 02/18/15 09:00 03/11/15 09:26 1

0.275 0.167 0.166 U

0.115 Uranium 235 pCi/g 02/18/15 09:00 03/11/15 09:26 1

0.114 0.0681 0.0680 U

0.0292 Americium 241 pCi/g 02/18/15 09:00 03/11/15 09:26 1

5.45 3.51 3.43 7.51 Protactinium 234m Pb-210 2.02 0.798 0.832 0.932 pCi/g 02/18/15 09:00 03/11/15 09:26 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.441 0.0502 0.0677 0.0365 pCi/g 02/18/15 09:00 03/11/15 09:26 1

Lab Sample ID: 160-10497-8 Client Sample ID: L10-12-08-B-R-S-00 Matrix: Solid Date Collected: 02/11/15 11:11 Date Received: 02/13/15 12:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.17 (2+/-)

0.181 (2+/-)

1 03/11/15 09:28 02/18/15 09:00 pCi/g 0.133 RL MDC 0.136 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.336 0.407 0.375 1.50 Bismuth 212 pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.0600 0.177 0.109 1.34 Bismuth 214 pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.0635 0.190 0.0802 1.33 Lead 212 pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.0679 0.189 0.100 1.54 Lead 214 pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.213 2.24 1.12 19.0 Potassium 40 pCi/g 02/18/15 09:00 03/11/15 09:28 1

1.31 0.813 0.807 U

-0.868 Protactinium 231 pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.0600 1.00 0.177 0.109 1.34 Radium 226 pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.133 0.181 0.136 1.17 Thorium 232 pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.866 0.317 0.303 0.898 Thorium 234 pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.214 0.165 0.164 0.214 Uranium 235 pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.108 0.0645 0.0645 U

-0.0245 Americium 241 pCi/g 02/18/15 09:00 03/11/15 09:28 1

4.57 39.4 39.4 U

-0.530 Protactinium 234m Pb-210 1.58 0.695 0.720 0.869 pCi/g 02/18/15 09:00 03/11/15 09:28 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.414 0.0472 0.0638 0.0333 pCi/g 02/18/15 09:00 03/11/15 09:28 1

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Client Sample Results TestAmerica Job ID: 160-10497-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-10497-9 Client Sample ID: L10-12-09-B-E-S-00 Matrix: Solid Date Collected: 02/11/15 11:30 Date Received: 02/13/15 12:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.30 (2+/-)

0.234 (2+/-)

1 03/11/15 09:28 02/18/15 09:00 pCi/g 0.170 RL MDC 0.192 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.540 0.622 0.594 1.76 Bismuth 212 pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.115 0.247 0.182 1.60 Bismuth 214 pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.116 0.172 0.104 1.06 Lead 212 pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.0946 0.227 0.147 1.66 Lead 214 pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.323 2.31 1.45 17.6 Potassium 40 pCi/g 02/18/15 09:00 03/11/15 09:28 1

1.60 0.219 0.217 U

0.278 Protactinium 231 pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.115 1.00 0.247 0.182 1.60 Radium 226 pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.170 0.234 0.192 1.30 Thorium 232 pCi/g 02/18/15 09:00 03/11/15 09:28 1

1.10 0.366 0.359 U

0.674 Thorium 234 pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.317 0.177 0.177 U

0.0879 Uranium 235 pCi/g 02/18/15 09:00 03/11/15 09:28 1

0.137 0.0816 0.0816 U

-0.0252 Americium 241 pCi/g 02/18/15 09:00 03/11/15 09:28 1

12.5 5.25 5.25 U

0.000 Protactinium 234m Pb-210 1.36 0.816 0.832 1.06 pCi/g 02/18/15 09:00 03/11/15 09:28 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.452 0.0762 0.0895 0.0571 pCi/g 02/18/15 09:00 03/11/15 09:28 1

Lab Sample ID: 160-10497-10 Client Sample ID: L10-12-10-B-R-S-00 Matrix: Solid Date Collected: 02/11/15 16:38 Date Received: 02/13/15 12:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.27 (2+/-)

0.214 (2+/-)

1 03/11/15 10:28 02/18/15 09:00 pCi/g 0.0790 RL MDC 0.169 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/18/15 09:00 03/11/15 10:28 1

0.456 0.602 0.565 2.00 Bismuth 212 pCi/g 02/18/15 09:00 03/11/15 10:28 1

0.121 0.221 0.171 1.35 Bismuth 214 pCi/g 02/18/15 09:00 03/11/15 10:28 1

0.0992 0.175 0.0983 1.12 Lead 212 pCi/g 02/18/15 09:00 03/11/15 10:28 1

0.0886 0.204 0.126 1.55 Lead 214 pCi/g 02/18/15 09:00 03/11/15 10:28 1

0.333 2.36 1.43 18.3 Potassium 40 pCi/g 02/18/15 09:00 03/11/15 10:28 1

1.58 0.295 0.291 U

0.450 Protactinium 231 pCi/g 02/18/15 09:00 03/11/15 10:28 1

0.121 1.00 0.221 0.171 1.35 Radium 226 pCi/g 02/18/15 09:00 03/11/15 10:28 1

0.0790 0.214 0.169 1.27 Thorium 232 pCi/g 02/18/15 09:00 03/11/15 10:28 1

1.03 0.657 0.644 1.21 Thorium 234 pCi/g 02/18/15 09:00 03/11/15 10:28 1

0.221 0.191 0.189 0.229 Uranium 235 pCi/g 02/18/15 09:00 03/11/15 10:28 1

0.134 0.0806 0.0805 U

0.0389 Americium 241 pCi/g 02/18/15 09:00 03/11/15 10:28 1

6.47 3.77 3.76 U

1.83 Protactinium 234m Pb-210 1.49 0.757 0.777 0.944 pCi/g 02/18/15 09:00 03/11/15 10:28 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.396 0.0629 0.0752 0.0483 pCi/g 02/18/15 09:00 03/11/15 10:28 1

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Client Sample Results TestAmerica Job ID: 160-10497-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-10497-11 Client Sample ID: L10-12-11-B-E-S-00 Matrix: Solid Date Collected: 02/11/15 16:44 Date Received: 02/13/15 12:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.40 (2+/-)

0.210 (2+/-)

1 03/11/15 10:29 02/18/15 09:00 pCi/g 0.112 RL MDC 0.157 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/18/15 09:00 03/11/15 10:29 1

0.483 0.525 0.504 1.43 Bismuth 212 pCi/g 02/18/15 09:00 03/11/15 10:29 1

0.0777 0.208 0.123 1.63 Bismuth 214 pCi/g 02/18/15 09:00 03/11/15 10:29 1

0.0802 0.201 0.0842 1.41 Lead 212 pCi/g 02/18/15 09:00 03/11/15 10:29 1

0.0940 0.221 0.108 1.85 Lead 214 pCi/g 02/18/15 09:00 03/11/15 10:29 1

0.337 2.12 1.08 18.2 Potassium 40 pCi/g 02/18/15 09:00 03/11/15 10:29 1

1.36 0.242 0.236 U

0.485 Protactinium 231 pCi/g 02/18/15 09:00 03/11/15 10:29 1

0.0777 1.00 0.208 0.123 1.63 Radium 226 pCi/g 02/18/15 09:00 03/11/15 10:29 1

0.112 0.210 0.157 1.40 Thorium 232 pCi/g 02/18/15 09:00 03/11/15 10:29 1

0.895 0.577 0.561 1.28 Thorium 234 pCi/g 02/18/15 09:00 03/11/15 10:29 1

0.274 0.166 0.165 U

0.0914 Uranium 235 pCi/g 02/18/15 09:00 03/11/15 10:29 1

0.117 0.240 0.240 U

-0.0148 Americium 241 pCi/g 02/18/15 09:00 03/11/15 10:29 1

5.92 3.04 3.04 U

1.22 Protactinium 234m Pb-210 1.61 0.725 0.749 0.889 pCi/g 02/18/15 09:00 03/11/15 10:29 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.504 0.0627 0.0813 0.0452 pCi/g 02/18/15 09:00 03/11/15 10:29 1

Lab Sample ID: 160-10497-12 Client Sample ID: L10-12-12-B-E-S-00 Matrix: Solid Date Collected: 02/11/15 11:03 Date Received: 02/13/15 12:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.17 (2+/-)

0.168 (2+/-)

1 03/11/15 10:30 02/18/15 09:00 pCi/g 0.0888 RL MDC 0.118 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/18/15 09:00 03/11/15 10:30 1

0.404 0.457 0.436 1.34 Bismuth 212 pCi/g 02/18/15 09:00 03/11/15 10:30 1

0.0699 0.171 0.110 1.25 Bismuth 214 pCi/g 02/18/15 09:00 03/11/15 10:30 1

0.0633 0.173 0.0768 1.20 Lead 212 pCi/g 02/18/15 09:00 03/11/15 10:30 1

0.0839 0.176 0.0962 1.42 Lead 214 pCi/g 02/18/15 09:00 03/11/15 10:30 1

0.298 2.18 1.12 18.2 Potassium 40 pCi/g 02/18/15 09:00 03/11/15 10:30 1

1.15 0.279 0.271 U

0.585 Protactinium 231 pCi/g 02/18/15 09:00 03/11/15 10:30 1

0.0699 1.00 0.171 0.110 1.25 Radium 226 pCi/g 02/18/15 09:00 03/11/15 10:30 1

0.0888 0.168 0.118 1.17 Thorium 232 pCi/g 02/18/15 09:00 03/11/15 10:30 1

0.880 0.306 0.291 0.908 Thorium 234 pCi/g 02/18/15 09:00 03/11/15 10:30 1

0.242 0.145 0.145 U

0.132 Uranium 235 pCi/g 02/18/15 09:00 03/11/15 10:30 1

0.109 0.0647 0.0647 U

0.00212 Americium 241 pCi/g 02/18/15 09:00 03/11/15 10:30 1

5.39 2.40 2.35 U

4.61 Protactinium 234m Pb-210 1.39 0.656 0.676 0.825 pCi/g 02/18/15 09:00 03/11/15 10:30 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.415 0.0609 0.0746 0.0468 pCi/g 02/18/15 09:00 03/11/15 10:30 1

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Client Sample Results TestAmerica Job ID: 160-10497-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Lab Sample ID: 160-10497-13 Client Sample ID: L10-12-07-B-E-Q-00 Matrix: Solid Date Collected: 02/11/15 16:51 Date Received: 02/13/15 12:10 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.29 (2+/-)

0.209 (2+/-)

1 03/11/15 10:31 02/18/15 09:00 pCi/g 0.200 RL MDC 0.162 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 02/18/15 09:00 03/11/15 10:31 1

0.830 0.362 0.362 U

0.000 Bismuth 212 pCi/g 02/18/15 09:00 03/11/15 10:31 1

0.0929 0.214 0.154 1.43 Bismuth 214 pCi/g 02/18/15 09:00 03/11/15 10:31 1

0.122 0.170 0.106 1.03 Lead 212 pCi/g 02/18/15 09:00 03/11/15 10:31 1

0.103 0.212 0.146 1.48 Lead 214 pCi/g 02/18/15 09:00 03/11/15 10:31 1

0.532 2.38 1.54 17.8 Potassium 40 pCi/g 02/18/15 09:00 03/11/15 10:31 1

0.984 0.519 0.516 U

0.448 Protactinium 231 pCi/g 02/18/15 09:00 03/11/15 10:31 1

0.0929 1.00 0.214 0.154 1.43 Radium 226 pCi/g 02/18/15 09:00 03/11/15 10:31 1

0.200 0.209 0.162 1.29 Thorium 232 pCi/g 02/18/15 09:00 03/11/15 10:31 1

1.14 0.910 0.894 1.58 Thorium 234 pCi/g 02/18/15 09:00 03/11/15 10:31 1

0.313 0.188 0.188 U

0.102 Uranium 235 pCi/g 02/18/15 09:00 03/11/15 10:31 1

0.140 0.0832 0.0832 U

-0.0147 Americium 241 pCi/g 02/18/15 09:00 03/11/15 10:31 1

7.92 4.56 4.55 U

1.59 Protactinium 234m Pb-210 1.26 0.810 0.823 1.06 pCi/g 02/18/15 09:00 03/11/15 10:31 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.399 0.0714 0.0825 0.0537 pCi/g 02/18/15 09:00 03/11/15 10:31 1

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QC Sample Results TestAmerica Job ID: 160-10497-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-174642/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 178603 Prep Batch: 174642 Actinium 228 Analyte U

1 03/11/15 08:22 02/18/15 09:00 pCi/g 0.0433 MDC RL 0.0266 0.0265 (2+/-)

(2+/-)

MB 0.02039 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

03/11/15 08:22 02/18/15 09:00 pCi/g 0.173 0.0960 0.0959 U

0.03533 Bismuth 212 1

03/11/15 08:22 02/18/15 09:00 pCi/g 0.0337 0.0162 0.0162 U

0.004746 Bismuth 214 1

03/11/15 08:22 02/18/15 09:00 pCi/g 0.0239 0.0345 0.0345 U

-0.005266 Lead 212 1

03/11/15 08:22 02/18/15 09:00 pCi/g 0.0318 0.00740 0.00739 U

-0.001799 Lead 214 1

03/11/15 08:22 02/18/15 09:00 pCi/g 0.186 3.13 3.13 U

-0.07816 Potassium 40 1

03/11/15 08:22 02/18/15 09:00 pCi/g 0.348 0.189 0.189 U

0.001915 Protactinium 231 1

03/11/15 08:22 02/18/15 09:00 pCi/g 0.0337 1.00 0.0162 0.0162 U

0.004746 Radium 226 1

03/11/15 08:22 02/18/15 09:00 pCi/g 0.0433 0.0266 0.0265 U

0.02039 Thorium 232 1

03/11/15 08:22 02/18/15 09:00 pCi/g 0.240 0.0363 0.0362 U

0.02073 Thorium 234 1

03/11/15 08:22 02/18/15 09:00 pCi/g 0.0535 0.00671 0.00671 U

0.001172 Uranium 235 1

03/11/15 08:22 02/18/15 09:00 pCi/g 0.0198 0.0107 0.0107 U

0.0001022 Americium 241 1

03/11/15 08:22 02/18/15 09:00 pCi/g 1.17 0.544 0.544 U

0.07050 Protactinium 234m Other Detected Radionuclide None MB (2+/-)

(2+/-)

MDC RL pCi/g 02/18/15 09:00 03/11/15 08:22 1

MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-174642/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 178604 Prep Batch: 174642 Americium 241 Analyte 116 87 102 102.4 101 10.7 0.528 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 34.9 35.39 3.71 0.188 pCi/g 101 87 - 120 Cobalt 60 36.5 36.27 3.66 0.108 pCi/g 99 87 - 115 Client Sample ID: L10-12-01-B-E-S-00 Lab Sample ID: 160-10497-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 178599 Prep Batch: 174642 Actinium 228 Analyte 1

0.30 0.8998 1.01 0.219 0.146 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Bismuth 212 1.04 1.468 0.568 0.494 pCi/g 0.48 1

Bismuth 214 0.949 1.188 0.183 0.0701 pCi/g 0.75 1

Lead 212 0.958 0.7718 0.135 0.110 pCi/g 0.67 1

Lead 214 1.11 1.200 0.169 0.0811 pCi/g 0.27 1

Potassium 40 19.2 16.80 2.20 0.308 pCi/g 0.54 1

Protactinium 231 0.312 U

0.3627 U

0.374 1.37 pCi/g 0.09 1

Radium 226 0.949 1.188 0.183 1.00 0.0701 pCi/g 0.75 1

Thorium 232 1.01 0.8998 0.219 0.146 pCi/g 0.30 1

Thorium 234 1.13 0.3395 U

0.727 1.22 pCi/g 0.62 1

Uranium 235 0.0515 U

0.08760 U

0.0812 0.276 pCi/g 0.16 1

Americium 241

-0.00101 U

-0.01544 U

0.0651 0.110 pCi/g 0.11 1

TestAmerica St. Louis Page 17 of 19 3/13/2015 1

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QC Sample Results TestAmerica Job ID: 160-10497-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)

Client Sample ID: L10-12-01-B-E-S-00 Lab Sample ID: 160-10497-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 178599 Prep Batch: 174642 Protactinium 234m Analyte 1

0.17 U

0.5074

-0.449 U

2.67 4.91 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Pb-210 1

0.27 1.159 1.57 0.772 0.996 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

RER RER Total Other Detected Radionuclides Tl-208 0.367 0.3393 0.0712 0.0479 pCi/g 0.21 1

TestAmerica St. Louis Page 18 of 19 3/13/2015 1

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QC Association Summary TestAmerica Job ID: 160-10497-2 Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP Rad Leach Batch: 173804 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-10497-1 L10-12-01-B-E-S-00 Total/NA Solid Dry and Grind 160-10497-1 DU L10-12-01-B-E-S-00 Total/NA Solid Dry and Grind 160-10497-2 L10-12-02-B-E-S-00 Total/NA Solid Dry and Grind 160-10497-3 L10-12-03-B-E-S-00 Total/NA Solid Dry and Grind 160-10497-4 L10-12-04-B-E-S-00 Total/NA Solid Dry and Grind 160-10497-5 L10-12-05-B-R-S-00 Total/NA Solid Dry and Grind 160-10497-6 L10-12-06-B-E-S-00 Total/NA Solid Dry and Grind 160-10497-7 L10-12-07-B-E-S-00 Total/NA Solid Dry and Grind 160-10497-8 L10-12-08-B-R-S-00 Total/NA Solid Dry and Grind 160-10497-9 L10-12-09-B-E-S-00 Total/NA Solid Dry and Grind 160-10497-10 L10-12-10-B-R-S-00 Total/NA Solid Dry and Grind 160-10497-11 L10-12-11-B-E-S-00 Total/NA Solid Dry and Grind 160-10497-12 L10-12-12-B-E-S-00 Total/NA Solid Dry and Grind 160-10497-13 L10-12-07-B-E-Q-00 Total/NA Prep Batch: 174642 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 173804 160-10497-1 L10-12-01-B-E-S-00 Total/NA Solid Fill_Geo-21 173804 160-10497-1 DU L10-12-01-B-E-S-00 Total/NA Solid Fill_Geo-21 173804 160-10497-2 L10-12-02-B-E-S-00 Total/NA Solid Fill_Geo-21 173804 160-10497-3 L10-12-03-B-E-S-00 Total/NA Solid Fill_Geo-21 173804 160-10497-4 L10-12-04-B-E-S-00 Total/NA Solid Fill_Geo-21 173804 160-10497-5 L10-12-05-B-R-S-00 Total/NA Solid Fill_Geo-21 173804 160-10497-6 L10-12-06-B-E-S-00 Total/NA Solid Fill_Geo-21 173804 160-10497-7 L10-12-07-B-E-S-00 Total/NA Solid Fill_Geo-21 173804 160-10497-8 L10-12-08-B-R-S-00 Total/NA Solid Fill_Geo-21 173804 160-10497-9 L10-12-09-B-E-S-00 Total/NA Solid Fill_Geo-21 173804 160-10497-10 L10-12-10-B-R-S-00 Total/NA Solid Fill_Geo-21 173804 160-10497-11 L10-12-11-B-E-S-00 Total/NA Solid Fill_Geo-21 173804 160-10497-12 L10-12-12-B-E-S-00 Total/NA Solid Fill_Geo-21 173804 160-10497-13 L10-12-07-B-E-Q-00 Total/NA Solid Fill_Geo-21 LCS 160-174642/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-174642/1-A Method Blank Total/NA TestAmerica St. Louis Page 19 of 19 3/13/2015 1

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ML18074A220

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