ML18075A012
| ML18075A012 | |
| Person / Time | |
|---|---|
| Site: | 07000036 |
| Issue date: | 04/06/2016 |
| From: | TestAmerica Labs - St. Louis, Westinghouse |
| To: | Office of Nuclear Material Safety and Safeguards |
| Shared Package | |
| ML18074A285 | List: |
| References | |
| HEM-18-6 | |
| Download: ML18075A012 (20) | |
Text
ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-16698-1 Client Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Revision: 1 For:
Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Mr. Martin Swanson Authorized for release by:
4/6/2016 1:36:27 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
TestAmerica Job ID: 160-16698-1 Page 2 of 20 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
5 Receipt Checklists.........................................
6 Definitions/Glossary.......................................
7 Method Summary.........................................
8 Sample Summary.........................................
9 Client Sample Results......................................
10 QC Sample Results........................................
15 QC Association Summary...................................
18 Tracer Carrier Summary....................................
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16698-1 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Job ID: 160-16698-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: HDP RFP-CBA-022 (7 DAY TAT)
Report Number: 160-16698 Revision 1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client. This revision places comments for gamma spec analysis in the correct section of the narrative.
RECEIPT The samples were received on 3/28/2016 11:11 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 20.0º C.
TECHNETIUM-99 (ICPMS)
Samples L08-13-13-T-E-B-00 (160-16698-1), L08-13-14-T-E-B-00 (160-16698-2), L08-13-15-T-E-B-00 (160-16698-3),
L08-13-16-T-E-B-00 (160-16698-4) and L08-13-17-T-E-B-00 (160-16698-5) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 03/29/2016 and analyzed on 03/30/2016.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
PERCENT SOLIDS Samples L08-13-13-T-E-B-00 (160-16698-1), L08-13-14-T-E-B-00 (160-16698-2), L08-13-15-T-E-B-00 (160-16698-3),
L08-13-16-T-E-B-00 (160-16698-4) and L08-13-17-T-E-B-00 (160-16698-5) were analyzed for percent solids in accordance with EPA TestAmerica St. Louis Page 3 of 20 1
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16698-1 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Job ID: 160-16698-1 (Continued)
Laboratory: TestAmerica St. Louis (Continued)
Method 160.3 MOD. The samples were analyzed on 03/29/2016.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CESIUM-137 & OTHER GAMMA EMITTERS (GS)
Samples L08-13-13-T-E-B-00 (160-16698-1), L08-13-14-T-E-B-00 (160-16698-2), L08-13-15-T-E-B-00 (160-16698-3),
L08-13-16-T-E-B-00 (160-16698-4) and L08-13-17-T-E-B-00 (160-16698-5) were analyzed for Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 03/28/2016, and prepared and analyzed on 03/31/2016.
Preparation Batch 160-243052:
Radium-226 is reported in these samples at the client's request. Radium-226 is reported from the 609.31 keV line of bismuth-214.
Because the samples have not had a 21-day ingrowth, the activity for radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between radium-226 and bismuth-214 by the loss of radon-222 during sample preparation. L08-13-13-T-E-B-00 (160-16698-1), L08-13-14-T-E-B-00 (160-16698-2), L08-13-15-T-E-B-00 (160-16698-3),
L08-13-16-T-E-B-00 (160-16698-4), L08-13-17-T-E-B-00 (160-16698-5), (LCS 160-243052/2-A), (MB 160-243052/1-A) and (160-16698-A-1-G DU)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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10 11 12 Procedure HDP-PR-QA-006,. Chain ;;,/Custody Hematite Decommissioning Project !Revision: 4 I
Page 1 ofl l Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person fi:om each organiz.ation should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before. the sample is released for use or analysis and send the completed CoC to HDP.
Chain of Cutodv ID No. I F-032816-02 Pa2:e Project Name:
Westinghouse Electric Company Contact Person:
Clark Evers Phone Number:
314-810-3336 Sampler Name Donte Love Sample ID L08-13-13-T-E-B-OO L08-13-14-T-E-B-OO L08-13-15-T0 E-B-OO L08-13-16-T-E-B-OO L08-13-l 7-T-E-B-OO Relinquished by:
Company Name:
Received by:
Company Name:
Date Time 3/24/2016 10:20 3/24/2016 10:30 3/24/2016 10:25 3/24/2016 10:35 3/24/2016 15:00 f.,..>t!,C, Date/Time
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Date/Time 1/1
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Matrix a
0 C.J s
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Date/Tim~~~,
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, u, i-2 Laboratory Name:
TA-MO Laboratory Address:
13715 Rider Trail North
" 1----------------------,
- E Phone No..
8 314-298-8566 g Laboratory Contact Person:
,:: Ivan Vania Phone No.
708-870-8453 Turn Around Tim__e_
Rush (7 days)
Remarks LSA 08-13 Sidewall Bias LSA 08-13 Bias LSA 08-13 Bias LSA 08-13 Bias LSA 08-13 Bias 160-16698 Chain of Custody Total I
Cooler Temperature:
5 Ambient Cooler ID: I Shipper and Number:
3-28-01 Date/Time
!Comments: NIA Verified By:
3/J-e/J<,
Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-16698-1 Login Number: 16698 Question Answer Comment Creator: Dedner, Connie L List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
N/A Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time (excluding tests with immediate HTs)
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-16698-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Qualifiers Rad Qualifier Description U
Result is less than the sample detection limit.
Qualifier Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-16698-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL DOE GA-01-R Cesium-137 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 8 of 20 1
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Sample Summary TestAmerica Job ID: 160-16698-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID Client Sample ID Received Collected Matrix 160-16698-1 L08-13-13-T-E-B-00 Solid 03/24/16 10:20 03/28/16 11:11 160-16698-2 L08-13-14-T-E-B-00 Solid 03/24/16 10:30 03/28/16 11:11 160-16698-3 L08-13-15-T-E-B-00 Solid 03/24/16 10:25 03/28/16 11:11 160-16698-4 L08-13-16-T-E-B-00 Solid 03/24/16 10:35 03/28/16 11:11 160-16698-5 L08-13-17-T-E-B-00 Solid 03/24/16 15:00 03/28/16 11:11 TestAmerica St. Louis Page 9 of 20 1
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Client Sample Results TestAmerica Job ID: 160-16698-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16698-1 Client Sample ID: L08-13-13-T-E-B-00 Matrix: Solid Date Collected: 03/24/16 10:20 Date Received: 03/28/16 11:11 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.27 (2+/-)
0.244 (2+/-)
1 03/31/16 21:46 03/31/16 12:41 pCi/g 0.0983 RL MDC 0.206 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/31/16 12:41 03/31/16 21:46 1
0.123 0.0736 0.0735 U
0.0345 Americium 241 pCi/g 03/31/16 12:41 03/31/16 21:46 1
0.308 0.440 0.414 1.44 Bismuth 212 pCi/g 03/31/16 12:41 03/31/16 21:46 1
0.0958 0.169 0.141 0.883 Bismuth 214 pCi/g 03/31/16 12:41 03/31/16 21:46 1
0.0787 0.167 0.0956 1.06 Lead 212 pCi/g 03/31/16 12:41 03/31/16 21:46 1
0.0962 0.154 0.115 0.985 Lead 214 pCi/g 03/31/16 12:41 03/31/16 21:46 1
0.459 2.35 1.48 17.9 Potassium 40 pCi/g 03/31/16 12:41 03/31/16 21:46 1
1.43 0.865 0.863 U
-0.609 Protactinium 231 pCi/g 03/31/16 12:41 03/31/16 21:46 1
0.0958 1.00 0.169 0.141 0.883 Radium 226 pCi/g 03/31/16 12:41 03/31/16 21:46 1
0.972 1.00 0.351 0.336 0.998 Thorium 234 pCi/g 03/31/16 12:41 03/31/16 21:46 1
0.253 0.160 0.159 U
0.152 Uranium 235 pCi/g 03/31/16 12:41 03/31/16 21:46 1
5.63 4.14 4.11 U
4.47 Protactinium 234m pCi/g 03/31/16 12:41 03/31/16 21:46 1
0.0983 0.244 0.206 1.27 Thorium 232 Tl-208 0.362 0.0683 0.0779 0.0531 pCi/g 03/31/16 12:41 03/31/16 21:46 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16698-1 Client Sample ID: L08-13-13-T-E-B-00 Matrix: Solid Date Collected: 03/24/16 10:20 Percent Solids: 83.2 Date Received: 03/28/16 11:11 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000083 0.000068 0.000021 mg/Kg
03/29/16 06:15 03/30/16 11:14 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.43 (2+/-)
0.151 (2+/-)
1 03/30/16 11:14 03/29/16 06:15 pCi/g 0.235 1.37 RL MDC 0.0743 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 03/29/16 06:15 03/30/16 11:14 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 87 Lab Sample ID: 160-16698-2 Client Sample ID: L08-13-14-T-E-B-00 Matrix: Solid Date Collected: 03/24/16 10:30 Date Received: 03/28/16 11:11 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.05 (2+/-)
0.157 (2+/-)
1 03/31/16 21:47 03/31/16 12:41 pCi/g 0.0852 RL MDC 0.115 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/31/16 12:41 03/31/16 21:47 1
0.120 0.0719 0.0719 U
-0.0157 Americium 241 pCi/g 03/31/16 12:41 03/31/16 21:47 1
0.348 0.425 0.401 1.35 Bismuth 212 pCi/g 03/31/16 12:41 03/31/16 21:47 1
0.0587 0.117 0.0840 0.778 Bismuth 214 pCi/g 03/31/16 12:41 03/31/16 21:47 1
0.0637 0.161 0.0777 1.09 Lead 212 TestAmerica St. Louis Page 10 of 20 1
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Client Sample Results TestAmerica Job ID: 160-16698-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16698-2 Client Sample ID: L08-13-14-T-E-B-00 Matrix: Solid Date Collected: 03/24/16 10:30 Date Received: 03/28/16 11:11 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Lead 214 0.952 (2+/-)
0.129 (2+/-)
1 03/31/16 21:47 03/31/16 12:41 pCi/g 0.0625 RL MDC 0.0824 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/31/16 12:41 03/31/16 21:47 1
0.258 2.23 1.06 19.2 Potassium 40 pCi/g 03/31/16 12:41 03/31/16 21:47 1
1.01 0.210 0.207 U
0.319 Protactinium 231 pCi/g 03/31/16 12:41 03/31/16 21:47 1
0.0587 1.00 0.117 0.0840 0.778 Radium 226 pCi/g 03/31/16 12:41 03/31/16 21:47 1
0.853 1.00 0.637 0.575 2.62 Thorium 234 pCi/g 03/31/16 12:41 03/31/16 21:47 1
0.250 0.378 0.260 2.70 Uranium 235 pCi/g 03/31/16 12:41 03/31/16 21:47 1
4.53 2.60 2.56 U
4.50 Protactinium 234m pCi/g 03/31/16 12:41 03/31/16 21:47 1
0.0852 0.157 0.115 1.05 Thorium 232 Tl-208 0.330 0.0406 0.0531 0.0295 pCi/g 03/31/16 12:41 03/31/16 21:47 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16698-2 Client Sample ID: L08-13-14-T-E-B-00 Matrix: Solid Date Collected: 03/24/16 10:30 Percent Solids: 81.9 Date Received: 03/28/16 11:11 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00020 0.000070 0.000021 mg/Kg
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Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 3.48 (2+/-)
0.326 (2+/-)
1 03/30/16 11:26 03/29/16 06:15 pCi/g 0.239 1.40 RL MDC 0.0617 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 03/29/16 06:15 03/30/16 11:26 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 87 Lab Sample ID: 160-16698-3 Client Sample ID: L08-13-15-T-E-B-00 Matrix: Solid Date Collected: 03/24/16 10:25 Date Received: 03/28/16 11:11 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.950 (2+/-)
0.188 (2+/-)
1 03/31/16 21:48 03/31/16 12:41 pCi/g 0.112 RL MDC 0.161 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.0945 0.0567 0.0566 U
0.0236 Americium 241 pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.312 0.419 0.387 1.55 Bismuth 212 pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.0653 0.129 0.0968 0.825 Bismuth 214 pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.0632 0.153 0.0778 1.01 Lead 212 pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.0663 0.121 0.0788 0.882 Lead 214 pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.237 2.18 1.16 18.0 Potassium 40 pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.898 0.391 0.380 U
0.844 Protactinium 231 pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.0653 1.00 0.129 0.0968 0.825 Radium 226 pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.739 1.00 0.502 0.480 1.39 Thorium 234 TestAmerica St. Louis Page 11 of 20 1
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Client Sample Results TestAmerica Job ID: 160-16698-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16698-3 Client Sample ID: L08-13-15-T-E-B-00 Matrix: Solid Date Collected: 03/24/16 10:25 Date Received: 03/28/16 11:11 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Uranium 235 0.193 U (2+/-)
0.147 (2+/-)
1 03/31/16 21:48 03/31/16 12:41 pCi/g 0.205 RL MDC 0.146 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/31/16 12:41 03/31/16 21:48 1
5.80 3.55 3.53 U
3.24 Protactinium 234m pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.112 0.188 0.161 0.950 Thorium 232 Tl-208 0.388 0.0539 0.0673 0.0371 pCi/g 03/31/16 12:41 03/31/16 21:48 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16698-3 Client Sample ID: L08-13-15-T-E-B-00 Matrix: Solid Date Collected: 03/24/16 10:25 Percent Solids: 79.9 Date Received: 03/28/16 11:11 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00036 0.000069 0.000021 mg/Kg
03/29/16 06:15 03/30/16 11:30 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 6.23 (2+/-)
0.728 (2+/-)
1 03/30/16 11:30 03/29/16 06:15 pCi/g 0.236 1.38 RL MDC 0.448 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 03/29/16 06:15 03/30/16 11:30 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 Lab Sample ID: 160-16698-4 Client Sample ID: L08-13-16-T-E-B-00 Matrix: Solid Date Collected: 03/24/16 10:35 Date Received: 03/28/16 11:11 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.21 (2+/-)
0.184 (2+/-)
1 03/31/16 21:48 03/31/16 12:41 pCi/g 0.110 RL MDC 0.137 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.107 6.02 6.02 U
-0.00951 Americium 241 pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.412 0.480 0.458 1.39 Bismuth 212 pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.0641 0.140 0.0981 0.964 Bismuth 214 pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.0661 0.174 0.0819 1.19 Lead 212 pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.0733 0.139 0.0949 0.968 Lead 214 pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.287 2.45 1.17 21.4 Potassium 40 pCi/g 03/31/16 12:41 03/31/16 21:48 1
1.29 0.206 0.202 U
0.363 Protactinium 231 pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.0641 1.00 0.140 0.0981 0.964 Radium 226 pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.823 1.00 0.533 0.518 1.20 Thorium 234 pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.201 0.132 0.130 0.226 Uranium 235 pCi/g 03/31/16 12:41 03/31/16 21:48 1
4.76 2.98 2.97 U
3.07 Protactinium 234m pCi/g 03/31/16 12:41 03/31/16 21:48 1
0.110 0.184 0.137 1.21 Thorium 232 TestAmerica St. Louis Page 12 of 20 1
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Client Sample Results TestAmerica Job ID: 160-16698-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16698-4 Client Sample ID: L08-13-16-T-E-B-00 Matrix: Solid Date Collected: 03/24/16 10:35 Date Received: 03/28/16 11:11 Pb-210 1.77 0.707 0.737 0.827 pCi/g 03/31/16 12:41 03/31/16 21:48 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.437 0.0561 0.0719 0.0430 pCi/g 03/31/16 12:41 03/31/16 21:48 1
Lab Sample ID: 160-16698-4 Client Sample ID: L08-13-16-T-E-B-00 Matrix: Solid Date Collected: 03/24/16 10:35 Percent Solids: 78.6 Date Received: 03/28/16 11:11 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00047 0.000074 0.000022 mg/Kg
03/29/16 06:15 03/30/16 11:34 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 8.11 (2+/-)
0.767 (2+/-)
1 03/30/16 11:34 03/29/16 06:15 pCi/g 0.254 1.48 RL MDC 0.178 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 03/29/16 06:15 03/30/16 11:34 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 86 Lab Sample ID: 160-16698-5 Client Sample ID: L08-13-17-T-E-B-00 Matrix: Solid Date Collected: 03/24/16 15:00 Date Received: 03/28/16 11:11 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.03 (2+/-)
0.151 (2+/-)
1 03/31/16 21:50 03/31/16 12:41 pCi/g 0.0908 RL MDC 0.108 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/31/16 12:41 03/31/16 21:50 1
0.0883 0.0528 0.0528 U
0.0181 Americium 241 pCi/g 03/31/16 12:41 03/31/16 21:50 1
0.380 0.417 0.402 1.08 Bismuth 212 pCi/g 03/31/16 12:41 03/31/16 21:50 1
0.0704 0.124 0.0932 0.780 Bismuth 214 pCi/g 03/31/16 12:41 03/31/16 21:50 1
0.0600 0.153 0.0733 1.04 Lead 212 pCi/g 03/31/16 12:41 03/31/16 21:50 1
0.0592 0.128 0.0794 0.969 Lead 214 pCi/g 03/31/16 12:41 03/31/16 21:50 1
0.265 2.08 1.03 17.7 Potassium 40 pCi/g 03/31/16 12:41 03/31/16 21:50 1
1.13 0.690 0.687 U
-0.574 Protactinium 231 pCi/g 03/31/16 12:41 03/31/16 21:50 1
0.0704 1.00 0.124 0.0932 0.780 Radium 226 pCi/g 03/31/16 12:41 03/31/16 21:50 1
0.732 1.00 0.475 0.461 1.07 Thorium 234 pCi/g 03/31/16 12:41 03/31/16 21:50 1
0.206 0.141 0.140 U
0.103 Uranium 235 pCi/g 03/31/16 12:41 03/31/16 21:50 1
3.89 2.14 2.14 U
-0.0204 Protactinium 234m pCi/g 03/31/16 12:41 03/31/16 21:50 1
0.0908 0.151 0.108 1.03 Thorium 232 Tl-208 0.312 0.0422 0.0532 0.0344 pCi/g 03/31/16 12:41 03/31/16 21:50 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 13 of 20 1
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Client Sample Results TestAmerica Job ID: 160-16698-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16698-5 Client Sample ID: L08-13-17-T-E-B-00 Matrix: Solid Date Collected: 03/24/16 15:00 Percent Solids: 81.2 Date Received: 03/28/16 11:11 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.0015 0.000069 0.000021 mg/Kg
03/29/16 06:15 03/30/16 11:38 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 24.9 (2+/-)
2.36 (2+/-)
1 03/30/16 11:38 03/29/16 06:15 pCi/g 0.237 1.39 RL MDC 0.576 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 03/29/16 06:15 03/30/16 11:38 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 89 TestAmerica St. Louis Page 14 of 20 1
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QC Sample Results TestAmerica Job ID: 160-16698-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-242513/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242946 Prep Batch: 242513 RL MDL Technetium 99 ND 0.000053 0.000016 mg/Kg 03/29/16 06:15 03/30/16 11:07 1
MB MB Analyte Dil Fac Analyzed Prepared D
Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-242513/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242946 Prep Batch: 242513 Technetium 99 0.00119 0.00124 mg/Kg 104 80 - 120 Analyte LCS LCS D
Unit Result Qualifier
%Rec Spike Added
%Rec.
Limits Client Sample ID: L08-13-13-T-E-B-00 Lab Sample ID: 160-16698-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 242946 Prep Batch: 242513 Technetium 99 0.000083 0.00143 0.00160 mg/Kg 106 75 - 125
Analyte MS MS D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Client Sample ID: L08-13-13-T-E-B-00 Lab Sample ID: 160-16698-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 242946 Prep Batch: 242513 Technetium 99 0.000083 0.00143 0.00160 mg/Kg 106 75 - 125 0
30
Analyte MSD MSD D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Limit RPD RPD Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-242513/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242947 Prep Batch: 242513 Technetium 99 Analyte U
1 03/30/16 11:07 03/29/16 06:15 pCi/g 0.182 MDC 1.06 RL 0.0186 0.0185 (2+/-)
(2+/-)
MB 0.01873 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Carrier Re 30 - 110 03/29/16 06:15 03/30/16 11:07 1
Dil Fac Prepared Analyzed Qualifier Limits
%Yield 94 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-242513/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242947 Prep Batch: 242513 Technetium 99 Analyte 120 80 104 21.22 20.3 2.28 1.06 0.182 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 LCS Qualifier Limits
%Yield 94 LCS TestAmerica St. Louis Page 15 of 20 1
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QC Sample Results TestAmerica Job ID: 160-16698-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)
Client Sample ID: L08-13-13-T-E-B-00 Lab Sample ID: 160-16698-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 242947 Prep Batch: 242513 Technetium 99 Analyte 125 75 106 27.42 24.4 1.43 2.74 1.37 0.234 RL MDC (2+/-)
MS MS pCi/g Unit Result Qual
%Rec Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 MS Qualifier Limits
%Yield 88 MS Client Sample ID: L08-13-13-T-E-B-00 Lab Sample ID: 160-16698-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 242947 Prep Batch: 242513 Technetium 99 Analyte 1
0.01 125 75 106 27.40 24.4 1.43 2.54 1.36 0.233 RL MDC (2+/-)
MSD MSD pCi/g Unit Result Qual
%Rec Limit Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits
%Yield 88 MSD Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-243052/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 243068 Prep Batch: 243052 Actinium 228 Analyte U
1 03/31/16 20:41 03/31/16 12:41 pCi/g 0.0414 MDC RL 0.0163 0.0162 (2+/-)
(2+/-)
MB 0.01033 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
03/31/16 20:41 03/31/16 12:41 pCi/g 0.0213 0.0121 0.0121 U
0.005009 Americium 241 1
03/31/16 20:41 03/31/16 12:41 pCi/g 0.130 0.0352 0.0352 U
0.0000 Bismuth 212 1
03/31/16 20:41 03/31/16 12:41 pCi/g 0.0552 0.0712 0.0711 U
-0.01474 Bismuth 214 1
03/31/16 20:41 03/31/16 12:41 pCi/g 0.0272 0.0420 0.0420 U
-0.005071 Lead 212 1
03/31/16 20:41 03/31/16 12:41 pCi/g 0.0400 0.417 0.417 U
-0.01008 Lead 214 1
03/31/16 20:41 03/31/16 12:41 pCi/g 0.723 2.48 2.48 U
-0.06207 Potassium 40 1
03/31/16 20:41 03/31/16 12:41 pCi/g 0.341 0.186 0.186 U
0.05800 Protactinium 231 1
03/31/16 20:41 03/31/16 12:41 pCi/g 0.0552 1.00 0.0712 0.0711 U
-0.01474 Radium 226 1
03/31/16 20:41 03/31/16 12:41 pCi/g 0.286 1.00 0.00533 0.00532 U
-0.003878 Thorium 234 1
03/31/16 20:41 03/31/16 12:41 pCi/g 0.0743 0.0640 0.0640 U
-0.003477 Uranium 235 1
03/31/16 20:41 03/31/16 12:41 pCi/g 3.40 0.122 0.122 U
-0.03520 Protactinium 234m 1
03/31/16 20:41 03/31/16 12:41 pCi/g 0.0414 0.0163 0.0162 U
0.01033 Thorium 232 Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 03/31/16 12:41 03/31/16 20:41 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected TestAmerica St. Louis Page 16 of 20 1
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QC Sample Results TestAmerica Job ID: 160-16698-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-243052/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 243069 Prep Batch: 243052 Americium 241 Analyte 116 87 98 98.32 101 10.2 0.516 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 34.1 32.73 3.42 0.200 0.152 pCi/g 96 87 - 120 Cobalt 60 31.7 29.99 3.03 0.122 pCi/g 95 87 - 115 Client Sample ID: L08-13-13-T-E-B-00 Lab Sample ID: 160-16698-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 243069 Prep Batch: 243052 Actinium 228 Analyte 1
0.52 1.061 1.27 0.165 0.0688 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Americium 241 0.0345 U 0.01823 U 0.0636 0.106 pCi/g 0.12 1
Bismuth 212 1.44 1.506 0.505 0.404 pCi/g 0.07 1
Bismuth 214 0.883 0.8419 0.130 0.0640 pCi/g 0.14 1
Lead 212 1.06 1.073 0.164 0.0730 pCi/g 0.03 1
Lead 214 0.985 0.9756 0.133 0.0691 pCi/g 0.03 1
Potassium 40 17.9 17.07 2.04 0.210 pCi/g 0.19 1
Protactinium 231
-0.609 U 0.5087 U 0.265 1.13 pCi/g 0.99 1
Radium 226 0.883 0.8419 0.130 1.00 0.0640 pCi/g 0.14 1
Thorium 234 0.998 1.271 0.512 1.00 0.771 pCi/g 0.32 1
Uranium 235 0.152 U 0.07467 U 0.156 0.252 pCi/g 0.24 1
Protactinium 234m 4.47 U 2.144 U 3.06 5.14 pCi/g 0.32 1
Thorium 232 1.27 1.061 0.165 0.0688 pCi/g 0.52 1
Tl-208 1
0.20 0.3339 0.362 0.0593 0.0352 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
RER RER Total Other Detected Radionuclides TestAmerica St. Louis Page 17 of 20 1
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QC Association Summary TestAmerica Job ID: 160-16698-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Metals Prep Batch: 242513 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-16698-1 L08-13-13-T-E-B-00 Total/NA Solid None 160-16698-1 MS L08-13-13-T-E-B-00 Total/NA Solid None 160-16698-1 MSD L08-13-13-T-E-B-00 Total/NA Solid None 160-16698-2 L08-13-14-T-E-B-00 Total/NA Solid None 160-16698-3 L08-13-15-T-E-B-00 Total/NA Solid None 160-16698-4 L08-13-16-T-E-B-00 Total/NA Solid None 160-16698-5 L08-13-17-T-E-B-00 Total/NA Solid None LCS 160-242513/2-A Lab Control Sample Total/NA Solid None MB 160-242513/1-A Method Blank Total/NA Analysis Batch: 242946 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 242513 160-16698-1 L08-13-13-T-E-B-00 Total/NA Solid 6020A 242513 160-16698-1 MS L08-13-13-T-E-B-00 Total/NA Solid 6020A 242513 160-16698-1 MSD L08-13-13-T-E-B-00 Total/NA Solid 6020A 242513 160-16698-2 L08-13-14-T-E-B-00 Total/NA Solid 6020A 242513 160-16698-3 L08-13-15-T-E-B-00 Total/NA Solid 6020A 242513 160-16698-4 L08-13-16-T-E-B-00 Total/NA Solid 6020A 242513 160-16698-5 L08-13-17-T-E-B-00 Total/NA Solid 6020A 242513 LCS 160-242513/2-A Lab Control Sample Total/NA Solid 6020A 242513 MB 160-242513/1-A Method Blank Total/NA General Chemistry Analysis Batch: 242510 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-16698-1 L08-13-13-T-E-B-00 Total/NA Solid Moisture 160-16698-1 DU L08-13-13-T-E-B-00 Total/NA Solid Moisture 160-16698-2 L08-13-14-T-E-B-00 Total/NA Solid Moisture 160-16698-3 L08-13-15-T-E-B-00 Total/NA Solid Moisture 160-16698-4 L08-13-16-T-E-B-00 Total/NA Solid Moisture 160-16698-5 L08-13-17-T-E-B-00 Total/NA Rad Leach Batch: 242446 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-16698-1 L08-13-13-T-E-B-00 Total/NA Solid Dry and Grind 160-16698-1 DU L08-13-13-T-E-B-00 Total/NA Solid Dry and Grind 160-16698-2 L08-13-14-T-E-B-00 Total/NA Solid Dry and Grind 160-16698-3 L08-13-15-T-E-B-00 Total/NA Solid Dry and Grind 160-16698-4 L08-13-16-T-E-B-00 Total/NA Solid Dry and Grind 160-16698-5 L08-13-17-T-E-B-00 Total/NA Prep Batch: 242513 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-16698-1 L08-13-13-T-E-B-00 Total/NA Solid None 160-16698-1 MS L08-13-13-T-E-B-00 Total/NA Solid None 160-16698-1 MSD L08-13-13-T-E-B-00 Total/NA Solid None 160-16698-2 L08-13-14-T-E-B-00 Total/NA TestAmerica St. Louis Page 18 of 20 1
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QC Association Summary TestAmerica Job ID: 160-16698-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Rad (Continued)
Prep Batch: 242513 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-16698-3 L08-13-15-T-E-B-00 Total/NA Solid None 160-16698-4 L08-13-16-T-E-B-00 Total/NA Solid None 160-16698-5 L08-13-17-T-E-B-00 Total/NA Solid None LCS 160-242513/2-A Lab Control Sample Total/NA Solid None MB 160-242513/1-A Method Blank Total/NA Prep Batch: 243052 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 242446 160-16698-1 L08-13-13-T-E-B-00 Total/NA Solid Fill_Geo-0 242446 160-16698-1 DU L08-13-13-T-E-B-00 Total/NA Solid Fill_Geo-0 242446 160-16698-2 L08-13-14-T-E-B-00 Total/NA Solid Fill_Geo-0 242446 160-16698-3 L08-13-15-T-E-B-00 Total/NA Solid Fill_Geo-0 242446 160-16698-4 L08-13-16-T-E-B-00 Total/NA Solid Fill_Geo-0 242446 160-16698-5 L08-13-17-T-E-B-00 Total/NA Solid Fill_Geo-0 LCS 160-243052/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-243052/1-A Method Blank Total/NA TestAmerica St. Louis Page 19 of 20 1
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Tracer/Carrier Summary TestAmerica Job ID: 160-16698-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110)
Re 87 160-16698-1 Percent Yield (Acceptance Limits)
L08-13-13-T-E-B-00 88 160-16698-1 MS L08-13-13-T-E-B-00 88 160-16698-1 MSD L08-13-13-T-E-B-00 87 160-16698-2 L08-13-14-T-E-B-00 91 160-16698-3 L08-13-15-T-E-B-00 86 160-16698-4 L08-13-16-T-E-B-00 89 160-16698-5 L08-13-17-T-E-B-00 94 LCS 160-242513/2-A Lab Control Sample 94 MB 160-242513/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 20 of 20 1
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