Text

Westinghouse Hematite Decommissioning Project - Final Status Survey Final Report Vol. 3, Chapter 21, Survey Area Release Record for Land Survey Area 08, Survey Units 09, 12 and 13, Rev. 1, J16616-1 Uds Level 2 Report Final Report
	ML18075A008
Person / Time
Site:	07000036
Issue date:	03/29/2016
From:	; TestAmerica Labs - St. Louis, Westinghouse
To:	; Office of Nuclear Material Safety and Safeguards
Shared Package
ML18074A285	List: ML18074A217; ML18074A218; ML18074A219; ML18074A220; ML18074A221; ML18074A222; ML18074A223; ML18074A224; ML18074A225; ML18074A227; ML18074A292; ML18074A293; ML18074A295; ML18074A296; ML18074A297; ML18074A298; ML18074A299; ML18075A008; ML18075A009; ML18075A010; ML18075A011; ML18075A012; ML18075A013; ML18075A014; ML18075A015; ML18075A016; ML18075A017;
References
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	Download: ML18075A008 (37)
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ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-16616-1 Client Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

For:

Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Mr. Martin Swanson Authorized for release by:

3/29/2016 2:52:58 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

TestAmerica Job ID: 160-16616-1 Page 2 of 37 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

5 Receipt Checklists.........................................

7 Definitions/Glossary.......................................

8 Method Summary.........................................

9 Sample Summary.........................................

10 Client Sample Results......................................

11 QC Sample Results........................................

28 QC Association Summary...................................

33 Tracer Carrier Summary....................................

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16616-1 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Job ID: 160-16616-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: HDP RFP-CBA-022 (7 DAY TAT)

Report Number: 160-16616-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 3/22/2016 10:45 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperatures of the 2 coolers at receipt time were 20.0º C and 20.0º C.

TECHNETIUM-99 (ICPMS)

Samples L08-12-01-T-E-S-00 (160-16616-1), L08-12-02-T-E-S-00 (160-16616-2), L08-12-03-T-E-S-00 (160-16616-3),

L08-12-04-T-R-S-00 (160-16616-4), L08-12-05-T-E-S-00 (160-16616-5), L08-12-06-T-E-S-00 (160-16616-6), L08-12-07-T-R-S-00 (160-16616-7), L08-12-08-T-E-S-00 (160-16616-8), L08-12-09-T-R-S-00 (160-16616-9), L08-12-10-T-E-S-00 (160-16616-10),

L08-12-11-T-E-S-00 (160-16616-11), L08-12-12-T-R-S-00 (160-16616-12), L08-12-13-T-E-S-00 (160-16616-13), L08-12-14-T-R-S-00 (160-16616-14), L08-12-15-T-E-S-00 (160-16616-15), L08-12-15-T-E-Q-00 (160-16616-16), L08-12-16-T-R-S-00 (160-16616-17),

L08-12-17-T-E-S-00 (160-16616-18) and L08-12-18-T-E-B-00 (160-16616-19) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 03/23/2016 and analyzed on 03/24/2016.

The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 160-241768 and analytical batch 160-242133 were outside control limits for technetium. Sample matrix interference and/or non-homogeneity are suspected because the associated TestAmerica St. Louis Page 3 of 37 1

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16616-1 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Job ID: 160-16616-1 (Continued)

Laboratory: TestAmerica St. Louis (Continued) laboratory control sample (LCS) recovery was within acceptance limits. (160-16618-A-1-D MS) and (160-16618-A-1-E MSD)

The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 160-241768 and analytical batch 160-242134 were outside control limits for technetium. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits. (160-16618-A-1-D MS) and (160-16618-A-1-E MSD)

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

PERCENT SOLIDS Samples L08-12-01-T-E-S-00 (160-16616-1), L08-12-02-T-E-S-00 (160-16616-2), L08-12-03-T-E-S-00 (160-16616-3),

L08-12-04-T-R-S-00 (160-16616-4), L08-12-05-T-E-S-00 (160-16616-5), L08-12-06-T-E-S-00 (160-16616-6), L08-12-07-T-R-S-00 (160-16616-7), L08-12-08-T-E-S-00 (160-16616-8), L08-12-09-T-R-S-00 (160-16616-9), L08-12-10-T-E-S-00 (160-16616-10),

L08-12-11-T-E-S-00 (160-16616-11), L08-12-12-T-R-S-00 (160-16616-12), L08-12-13-T-E-S-00 (160-16616-13), L08-12-14-T-R-S-00 (160-16616-14), L08-12-15-T-E-S-00 (160-16616-15), L08-12-15-T-E-Q-00 (160-16616-16), L08-12-16-T-R-S-00 (160-16616-17),

L08-12-17-T-E-S-00 (160-16616-18) and L08-12-18-T-E-B-00 (160-16616-19) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 03/23/2016.

No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

CESIUM-137 & OTHER GAMMA EMITTERS (GS)

Samples L08-12-01-T-E-S-00 (160-16616-1), L08-12-02-T-E-S-00 (160-16616-2), L08-12-03-T-E-S-00 (160-16616-3),

L08-12-04-T-R-S-00 (160-16616-4), L08-12-05-T-E-S-00 (160-16616-5), L08-12-06-T-E-S-00 (160-16616-6), L08-12-07-T-R-S-00 (160-16616-7), L08-12-08-T-E-S-00 (160-16616-8), L08-12-09-T-R-S-00 (160-16616-9), L08-12-10-T-E-S-00 (160-16616-10),

L08-12-11-T-E-S-00 (160-16616-11), L08-12-12-T-R-S-00 (160-16616-12), L08-12-13-T-E-S-00 (160-16616-13), L08-12-14-T-R-S-00 (160-16616-14), L08-12-15-T-E-S-00 (160-16616-15), L08-12-15-T-E-Q-00 (160-16616-16), L08-12-16-T-R-S-00 (160-16616-17),

L08-12-17-T-E-S-00 (160-16616-18) and L08-12-18-T-E-B-00 (160-16616-19) were analyzed for Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 03/22/2016, prepared on 03/25/2016 and analyzed on 03/26/2016.

Preparation Batch 160-242185:

Radium-226 is reported in these samples at the client's request. Radium-226 is reported from the 609.31 keV line of bismuth-214.

Because the samples have not had 21-days of ingrowth, the activity for radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between radium-226 and bismuth-214 by the loss of radon-222 during sample preparation. The samples are reported with the MDC achieved. L08-12-01-T-E-S-00 (160-16616-1), L08-12-02-T-E-S-00 (160-16616-2),

L08-12-03-T-E-S-00 (160-16616-3), L08-12-04-T-R-S-00 (160-16616-4), L08-12-05-T-E-S-00 (160-16616-5), L08-12-06-T-E-S-00 (160-16616-6), L08-12-07-T-R-S-00 (160-16616-7), L08-12-08-T-E-S-00 (160-16616-8), L08-12-09-T-R-S-00 (160-16616-9),

L08-12-10-T-E-S-00 (160-16616-10), L08-12-11-T-E-S-00 (160-16616-11), L08-12-12-T-R-S-00 (160-16616-12), L08-12-13-T-E-S-00 (160-16616-13), L08-12-14-T-R-S-00 (160-16616-14), L08-12-15-T-E-S-00 (160-16616-15), L08-12-15-T-E-Q-00 (160-16616-16),

L08-12-16-T-R-S-00 (160-16616-17), L08-12-17-T-E-S-00 (160-16616-18), L08-12-18-T-E-B-00 (160-16616-19), (LCS 160-242185/2-A),

(MB 160-242185/1-A) and (160-16616-A-1-G DU)

Preparation Batch 160-242185:

The following sample, analyzed by gamma spectroscopy, did not meet the thorium-234 detection goal; L08-12-10-T-E-S-00 (160-16616-10). The samples final activity was above the MDC. The samples are reported with the MDC achieved.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

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,Procedure l:IDP-PR-QA-006, Chain of Custody Page l of!

Hematite Decommissioning Project !Revision: 4 I

I Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to l:IDP.

Chain of Cutodr ID No. I F-031816-01 Pae:e Project Name:

Westinghouse Electric Company Contact Person:

Clark Evers Phone Number:

314-810-3336 Sampler Name Kyle Weldon Sample ID Date Time L08-l2-01-T-E-S-00 3/18/2016 8:40 L08-12-02-T-E-S-OO 3/18/2016 8:42 L08-12-03-T-E-S-OO 3/18/2016 8:48 L08-12-04-T-R-S-OO 3/18/2016 9:00 L08-12-05-T-E-S-OO 3/18/2016 9:05 L08-12-06-T-E-S-OO 3/18/2016 9:14 L08-12-07-T-R-S-OO 3/18/2016 9:20 L08-12-08-T-E-S-OO 3/18/2016 9:22 L08-l 2-09-T-R-S-OO 3/18/2016 9:25 L08-l 2-1 O-T-E-S-00 3/18/2016 9:27 L08-12-l l-T-E-S-OO 3/18/2016 9:35 L08-12-12-T-R-S-00 3/18/2016 9:37 Reli.oouished by: ~ Date/rime CLvt ~,t--1

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708-870-8453 Rush LSA 08-12 LSA 08-12 LSA08-12 LSA 08-12 Tum Around Time (7 days)

Remarks 1 LSA08-12 1 LSA 08-12 1 LSA08-12 1 LSA08-1.2 rm 111 II 1II Ill II I Ill I 160-16616 Chain of Custody 1 LSA 08-12 1 LSA 08-12 1 LSA 08-12 LSA 08-12 Cooler Temperature:

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10 11 12 Procedure HDP-PR-QA-006, Chain of Custody Page 1 ofl Hematite Decommissioning Project jRevision: 4 I

I Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User mlist verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain ofCutody ID No. I F-031816-01 Page 2 of2 Project Name:

Westinghouse Electric Company Contact Person:

Clark Evers Phone Number:

314-8.10-3336 Sampler Name Kyle Weldon Sample ID L08-12-13-T-E-S-OO 108-12-14-T-R-S-OO L08-12-15-T-E-S-OO L08-12-15-T-E-Q-OO L08-12-l 6-T-R-S-OO L08-12-l 7-T-E-S-OO L08-12-l 8-T-E-B-OO Relinquished by:

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Date Time 3/18/2016 9:40 3/18/2016 9:46 3/18/2016 9:50 3/18/2016 9:50 3/18/2016 9:55 3/18/2016 9:57 3/18/2016 10:02 Date/Time 3/d'~/lv OC\\t,0 Date/Time Date/Tirp,e

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Cooler ID: !Shipper and Number:

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Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-16616-1 Login Number: 16616 Question Answer Comment Creator: Dedner, Connie L List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.

True The cooler's custody seal, if present, is intact.

N/A Sample custody seals, if present, are intact.

True The cooler or samples do not appear to have been compromised or tampered with.

N/A Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the containers received and the COC.

True Samples are received within Holding Time (excluding tests with immediate HTs)

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified.

True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

N/A Residual Chlorine Checked.

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Definitions/Glossary TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Qualifiers Metals Qualifier Description J

Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Qualifier F1 MS and/or MSD Recovery is outside acceptance limits.

Rad Qualifier Description U

Result is less than the sample detection limit.

Qualifier F1 MS and/or MSD Recovery is outside acceptance limits.

Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation

%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)

NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method Summary TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL DOE GA-01-R Cesium-137 & Other Gamma Emitters (GS)

TAL SL Protocol

References:

DOE = U.S. Department of Energy EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 9 of 37 1

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Sample Summary TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID Client Sample ID Received Collected Matrix 160-16616-1 L08-12-01-T-E-S-00 Solid 03/18/16 08:40 03/22/16 10:45 160-16616-2 L08-12-02-T-E-S-00 Solid 03/18/16 08:42 03/22/16 10:45 160-16616-3 L08-12-03-T-E-S-00 Solid 03/18/16 08:48 03/22/16 10:45 160-16616-4 L08-12-04-T-R-S-00 Solid 03/18/16 09:00 03/22/16 10:45 160-16616-5 L08-12-05-T-E-S-00 Solid 03/18/16 09:05 03/22/16 10:45 160-16616-6 L08-12-06-T-E-S-00 Solid 03/18/16 09:14 03/22/16 10:45 160-16616-7 L08-12-07-T-R-S-00 Solid 03/18/16 09:20 03/22/16 10:45 160-16616-8 L08-12-08-T-E-S-00 Solid 03/18/16 09:22 03/22/16 10:45 160-16616-9 L08-12-09-T-R-S-00 Solid 03/18/16 09:25 03/22/16 10:45 160-16616-10 L08-12-10-T-E-S-00 Solid 03/18/16 09:27 03/22/16 10:45 160-16616-11 L08-12-11-T-E-S-00 Solid 03/18/16 09:35 03/22/16 10:45 160-16616-12 L08-12-12-T-R-S-00 Solid 03/18/16 09:37 03/22/16 10:45 160-16616-13 L08-12-13-T-E-S-00 Solid 03/18/16 09:40 03/22/16 10:45 160-16616-14 L08-12-14-T-R-S-00 Solid 03/18/16 09:46 03/22/16 10:45 160-16616-15 L08-12-15-T-E-S-00 Solid 03/18/16 09:50 03/22/16 10:45 160-16616-16 L08-12-15-T-E-Q-00 Solid 03/18/16 09:50 03/22/16 10:45 160-16616-17 L08-12-16-T-R-S-00 Solid 03/18/16 09:55 03/22/16 10:45 160-16616-18 L08-12-17-T-E-S-00 Solid 03/18/16 09:57 03/22/16 10:45 160-16616-19 L08-12-18-T-E-B-00 Solid 03/18/16 10:02 03/22/16 10:45 TestAmerica St. Louis Page 10 of 37 1

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Client Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16616-1 Client Sample ID: L08-12-01-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 08:40 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.12 (2+/-)

0.176 (2+/-)

1 03/26/16 19:47 03/25/16 10:09 pCi/g 0.0790 RL MDC 0.135 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 19:47 1

0.105 0.0623 0.0623 U

0.00470 Americium 241 pCi/g 03/25/16 10:09 03/26/16 19:47 1

0.530 0.381 0.371 0.822 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 19:47 1

0.0734 0.145 0.108 0.920 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 19:47 1

0.0751 0.170 0.0878 1.12 Lead 212 pCi/g 03/25/16 10:09 03/26/16 19:47 1

0.0741 0.135 0.0860 1.00 Lead 214 pCi/g 03/25/16 10:09 03/26/16 19:47 1

0.256 2.34 1.25 19.4 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 19:47 1

1.09 0.326 0.318 U

0.658 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 19:47 1

0.0734 1.00 0.145 0.108 0.920 Radium 226 pCi/g 03/25/16 10:09 03/26/16 19:47 1

0.860 1.00 0.351 0.327 1.21 Thorium 234 pCi/g 03/25/16 10:09 03/26/16 19:47 1

0.231 0.186 0.181 0.434 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 19:47 1

5.52 3.35 3.34 U

2.54 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 19:47 1

0.0790 0.176 0.135 1.12 Thorium 232 Pb-210 1.82 0.613 0.649 0.769 pCi/g 03/25/16 10:09 03/26/16 19:47 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.366 0.0510 0.0636 0.0392 pCi/g 03/25/16 10:09 03/26/16 19:47 1

Lab Sample ID: 160-16616-1 Client Sample ID: L08-12-01-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 08:40 Percent Solids: 87.1 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00019 0.000064 0.000019 mg/Kg

03/23/16 08:23 03/24/16 09:16 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 3.34 (2+/-)

0.383 (2+/-)

1 03/24/16 09:16 03/23/16 08:23 pCi/g 0.220 1.28 RL MDC 0.228 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:23 03/24/16 09:16 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 88 Lab Sample ID: 160-16616-2 Client Sample ID: L08-12-02-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 08:42 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.28 (2+/-)

0.195 (2+/-)

1 03/26/16 21:02 03/25/16 10:09 pCi/g 0.0995 RL MDC 0.147 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.105 0.122 0.122 U

-0.0245 Americium 241 pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.423 0.507 0.483 1.50 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.0692 0.160 0.105 1.17 Bismuth 214 TestAmerica St. Louis Page 11 of 37 1

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Client Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16616-2 Client Sample ID: L08-12-02-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 08:42 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 212 1.15 (2+/-)

0.169 (2+/-)

1 03/26/16 21:02 03/25/16 10:09 pCi/g 0.0683 RL MDC 0.0796 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.0670 0.150 0.0808 1.22 Lead 214 pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.287 2.45 1.09 21.8 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 21:02 1

1.14 0.283 0.274 U

0.652 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.0692 1.00 0.160 0.105 1.17 Radium 226 pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.757 1.00 0.575 0.512 2.50 Thorium 234 pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.193 0.129 0.121 0.450 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 21:02 1

5.22 3.31 3.23 7.49 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.0995 0.195 0.147 1.28 Thorium 232 Tl-208 0.419 0.0517 0.0673 0.0376 pCi/g 03/25/16 10:09 03/26/16 21:02 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16616-2 Client Sample ID: L08-12-02-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 08:42 Percent Solids: 84.5 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00020 0.000066 0.000020 mg/Kg

03/23/16 08:23 03/24/16 09:28 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 3.36 (2+/-)

0.317 (2+/-)

1 03/24/16 09:28 03/23/16 08:23 pCi/g 0.226 1.32 RL MDC 0.0727 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:23 03/24/16 09:28 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 89 Lab Sample ID: 160-16616-3 Client Sample ID: L08-12-03-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 08:48 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.993 (2+/-)

0.168 (2+/-)

1 03/26/16 19:48 03/25/16 10:09 pCi/g 0.0753 RL MDC 0.133 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 19:48 1

0.0917 0.0544 0.0544 U

-0.00179 Americium 241 pCi/g 03/25/16 10:09 03/26/16 19:48 1

0.261 0.360 0.327 1.45 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 19:48 1

0.0574 0.128 0.0883 0.888 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 19:48 1

0.0501 0.156 0.0687 1.09 Lead 212 pCi/g 03/25/16 10:09 03/26/16 19:48 1

0.0610 0.131 0.0853 0.961 Lead 214 pCi/g 03/25/16 10:09 03/26/16 19:48 1

0.303 2.16 1.05 18.5 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 19:48 1

1.05 0.647 0.644 U

-0.600 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 19:48 1

0.0574 1.00 0.128 0.0883 0.888 Radium 226 TestAmerica St. Louis Page 12 of 37 1

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Client Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16616-3 Client Sample ID: L08-12-03-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 08:48 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 234 1.49 (2+/-)

0.322 (2+/-)

1 03/26/16 19:48 03/25/16 10:09 pCi/g 0.752 1.00 RL MDC 0.282 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 19:48 1

0.200 0.153 0.148 0.404 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 19:48 1

4.67 2.72 2.72 U

0.950 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 19:48 1

0.0753 0.168 0.133 0.993 Thorium 232 Tl-208 0.327 0.0401 0.0525 0.0283 pCi/g 03/25/16 10:09 03/26/16 19:48 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16616-3 Client Sample ID: L08-12-03-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 08:48 Percent Solids: 84.6 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00031 0.000066 0.000020 mg/Kg

03/23/16 08:23 03/24/16 09:43 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 5.28 (2+/-)

0.616 (2+/-)

1 03/24/16 09:43 03/23/16 08:23 pCi/g 0.225 1.32 RL MDC 0.378 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:23 03/24/16 09:43 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 89 Lab Sample ID: 160-16616-4 Client Sample ID: L08-12-04-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:00 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.18 (2+/-)

0.205 (2+/-)

1 03/26/16 20:22 03/25/16 10:09 pCi/g 0.144 RL MDC 0.166 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.126 0.0756 0.0755 U

-0.0300 Americium 241 pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.833 0.478 0.478 U

0.0397 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.0860 0.163 0.127 0.979 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.0897 0.178 0.102 1.13 Lead 212 pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.0916 0.148 0.0983 1.06 Lead 214 pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.255 2.48 1.41 19.9 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 20:22 1

1.22 0.450 0.446 U

0.518 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.0860 1.00 0.163 0.127 0.979 Radium 226 pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.853 1.00 0.581 0.556 1.61 Thorium 234 pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.297 0.163 0.160 U

0.256 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 20:22 1

8.34 4.85 4.84 U

1.98 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.144 0.205 0.166 1.18 Thorium 232 TestAmerica St. Louis Page 13 of 37 1

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Client Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16616-4 Client Sample ID: L08-12-04-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:00 Date Received: 03/22/16 10:45 Tl-208 0.405 0.0667 0.0789 0.0483 pCi/g 03/25/16 10:09 03/26/16 20:22 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16616-4 Client Sample ID: L08-12-04-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:00 Percent Solids: 78.4 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000087 0.000069 0.000021 mg/Kg

03/23/16 08:23 03/24/16 09:47 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.50 (2+/-)

0.488 (2+/-)

1 03/24/16 09:47 03/23/16 08:23 pCi/g 0.238 1.39 RL MDC 0.468 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:23 03/24/16 09:47 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 90 Lab Sample ID: 160-16616-5 Client Sample ID: L08-12-05-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:05 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.09 (2+/-)

0.158 (2+/-)

1 03/26/16 20:22 03/25/16 10:09 pCi/g 0.0848 RL MDC 0.111 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.103 0.0621 0.0621 U

-0.0311 Americium 241 pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.451 0.310 0.303 0.632 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.0540 0.139 0.0909 1.01 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.0572 0.162 0.0728 1.12 Lead 212 pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.0654 0.132 0.0779 1.02 Lead 214 pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.338 2.14 1.04 18.3 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 20:22 1

1.02 0.178 0.174 U

0.324 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.0540 1.00 0.139 0.0909 1.01 Radium 226 pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.746 1.00 0.287 0.264 1.08 Thorium 234 pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.228 0.140 0.139 U

0.110 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 20:22 1

4.60 2.71 2.71 U

1.56 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 20:22 1

0.0848 0.158 0.111 1.09 Thorium 232 Tl-208 0.363 0.0424 0.0567 0.0285 pCi/g 03/25/16 10:09 03/26/16 20:22 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

TestAmerica St. Louis Page 14 of 37 1

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Client Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16616-5 Client Sample ID: L08-12-05-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:05 Percent Solids: 77.5 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000082 0.000070 0.000021 mg/Kg

03/23/16 08:23 03/24/16 09:51 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.40 (2+/-)

0.172 (2+/-)

1 03/24/16 09:51 03/23/16 08:23 pCi/g 0.241 1.41 RL MDC 0.114 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:23 03/24/16 09:51 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 92 Lab Sample ID: 160-16616-6 Client Sample ID: L08-12-06-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:14 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.11 (2+/-)

0.200 (2+/-)

1 03/26/16 20:23 03/25/16 10:09 pCi/g 0.122 RL MDC 0.165 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 20:23 1

0.0939 0.0560 0.0560 U

-0.0155 Americium 241 pCi/g 03/25/16 10:09 03/26/16 20:23 1

0.530 0.588 0.572 1.33 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 20:23 1

0.0723 0.141 0.105 0.896 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 20:23 1

0.0675 0.157 0.0804 1.04 Lead 212 pCi/g 03/25/16 10:09 03/26/16 20:23 1

0.0731 0.138 0.0972 0.940 Lead 214 pCi/g 03/25/16 10:09 03/26/16 20:23 1

0.238 2.20 1.17 18.3 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 20:23 1

1.10 0.236 0.232 U

0.424 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 20:23 1

0.0723 1.00 0.141 0.105 0.896 Radium 226 pCi/g 03/25/16 10:09 03/26/16 20:23 1

0.828 1.00 0.544 0.527 1.31 Thorium 234 pCi/g 03/25/16 10:09 03/26/16 20:23 1

0.187 0.136 0.135 U

0.140 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 20:23 1

6.09 3.10 3.08 U

3.65 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 20:23 1

0.122 0.200 0.165 1.11 Thorium 232 Tl-208 0.397 0.0562 0.0697 0.0425 pCi/g 03/25/16 10:09 03/26/16 20:23 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16616-6 Client Sample ID: L08-12-06-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:14 Percent Solids: 73.0 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00013 0.000075 0.000023 mg/Kg

03/23/16 08:23 03/24/16 09:55 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 2.26 (2+/-)

0.300 (2+/-)

1 03/24/16 09:55 03/23/16 08:23 pCi/g 0.258 1.51 RL MDC 0.216 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

TestAmerica St. Louis Page 15 of 37 1

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Client Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16616-6 Client Sample ID: L08-12-06-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:14 Percent Solids: 73.0 Date Received: 03/22/16 10:45 Re 30 - 110 Carrier 03/23/16 08:23 03/24/16 09:55 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 90 Lab Sample ID: 160-16616-7 Client Sample ID: L08-12-07-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:20 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.09 (2+/-)

0.195 (2+/-)

1 03/26/16 21:00 03/25/16 10:09 pCi/g 0.127 RL MDC 0.160 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 21:00 1

0.123 0.0731 0.0731 U

0.00541 Americium 241 pCi/g 03/25/16 10:09 03/26/16 21:00 1

0.534 0.618 0.600 1.41 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 21:00 1

0.0945 0.166 0.132 0.977 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 21:00 1

0.0728 0.165 0.0831 1.11 Lead 212 pCi/g 03/25/16 10:09 03/26/16 21:00 1

0.0682 0.163 0.109 1.17 Lead 214 pCi/g 03/25/16 10:09 03/26/16 21:00 1

0.243 2.25 1.31 17.9 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 21:00 1

1.39 0.847 0.844 U

-0.633 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 21:00 1

0.0945 1.00 0.166 0.132 0.977 Radium 226 pCi/g 03/25/16 10:09 03/26/16 21:00 1

0.996 1.00 0.674 0.644 1.92 Thorium 234 pCi/g 03/25/16 10:09 03/26/16 21:00 1

0.236 0.195 0.192 0.356 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 21:00 1

4.39 4.44 4.32 10.2 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 21:00 1

0.127 0.195 0.160 1.09 Thorium 232 Tl-208 0.404 0.0645 0.0769 0.0474 pCi/g 03/25/16 10:09 03/26/16 21:00 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16616-7 Client Sample ID: L08-12-07-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:20 Percent Solids: 80.2 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00011 0.000068 0.000020 mg/Kg

03/23/16 08:23 03/24/16 09:59 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.92 (2+/-)

0.198 (2+/-)

1 03/24/16 09:59 03/23/16 08:23 pCi/g 0.233 1.36 RL MDC 0.0885 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:23 03/24/16 09:59 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 90 TestAmerica St. Louis Page 16 of 37 1

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Client Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16616-8 Client Sample ID: L08-12-08-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:22 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.08 (2+/-)

0.186 (2+/-)

1 03/26/16 21:02 03/25/16 10:09 pCi/g 0.174 RL MDC 0.150 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.109 0.0650 0.0650 U

0.0148 Americium 241 pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.362 0.460 0.435 1.44 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.0796 0.166 0.121 1.09 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.0739 0.172 0.0903 1.13 Lead 212 pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.0798 0.165 0.101 1.25 Lead 214 pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.376 2.35 1.33 19.0 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 21:02 1

1.22 0.360 0.353 U

0.639 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.0796 1.00 0.166 0.121 1.09 Radium 226 pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.970 1.00 0.362 0.351 U

0.835 Thorium 234 pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.243 0.148 0.148 U

0.115 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 21:02 1

5.69 3.47 3.46 U

2.80 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 21:02 1

0.174 0.186 0.150 1.08 Thorium 232 Tl-208 0.392 0.0626 0.0747 0.0472 pCi/g 03/25/16 10:09 03/26/16 21:02 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16616-8 Client Sample ID: L08-12-08-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:22 Percent Solids: 81.1 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00020 0.000068 0.000020 mg/Kg

03/23/16 08:23 03/24/16 10:03 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 3.44 (2+/-)

0.339 (2+/-)

1 03/24/16 10:03 03/23/16 08:23 pCi/g 0.234 1.37 RL MDC 0.123 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:23 03/24/16 10:03 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 89 Lab Sample ID: 160-16616-9 Client Sample ID: L08-12-09-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:25 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.08 (2+/-)

0.164 (2+/-)

1 03/26/16 21:03 03/25/16 10:09 pCi/g 0.0924 RL MDC 0.121 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 21:03 1

0.0824 0.0489 0.0489 U

0.00594 Americium 241 pCi/g 03/25/16 10:09 03/26/16 21:03 1

0.403 0.332 0.313 1.06 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 21:03 1

0.0598 0.131 0.0912 0.904 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 21:03 1

0.0563 0.169 0.0748 1.17 Lead 212 TestAmerica St. Louis Page 17 of 37 1

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Client Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16616-9 Client Sample ID: L08-12-09-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:25 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 214 1.05 (2+/-)

0.141 (2+/-)

1 03/26/16 21:03 03/25/16 10:09 pCi/g 0.0626 RL MDC 0.0895 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 21:03 1

0.266 2.26 1.07 19.4 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 21:03 1

1.08 0.662 0.659 U

-0.610 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 21:03 1

0.0598 1.00 0.131 0.0912 0.904 Radium 226 pCi/g 03/25/16 10:09 03/26/16 21:03 1

0.758 1.00 0.504 0.484 1.34 Thorium 234 pCi/g 03/25/16 10:09 03/26/16 21:03 1

0.183 0.140 0.137 0.272 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 21:03 1

4.45 2.98 2.90 6.75 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 21:03 1

0.0924 0.164 0.121 1.08 Thorium 232 Pb-210 1.43 0.541 0.567 0.713 pCi/g 03/25/16 10:09 03/26/16 21:03 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.377 0.0432 0.0583 0.0295 pCi/g 03/25/16 10:09 03/26/16 21:03 1

Lab Sample ID: 160-16616-9 Client Sample ID: L08-12-09-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:25 Percent Solids: 92.1 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00015 0.000060 0.000018 mg/Kg

03/23/16 08:23 03/24/16 10:07 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 2.58 (2+/-)

0.245 (2+/-)

1 03/24/16 10:07 03/23/16 08:23 pCi/g 0.204 1.19 RL MDC 0.0610 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:23 03/24/16 10:07 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 91 Lab Sample ID: 160-16616-10 Client Sample ID: L08-12-10-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:27 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.22 (2+/-)

0.207 (2+/-)

1 03/26/16 21:37 03/25/16 10:09 pCi/g 0.159 RL MDC 0.165 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.122 0.0729 0.0729 U

0.0169 Americium 241 pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.438 0.599 0.560 2.03 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.105 0.185 0.146 1.09 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.0999 0.192 0.115 1.19 Lead 212 pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.0840 0.152 0.101 1.10 Lead 214 pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.406 2.55 1.47 20.3 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 21:37 1

1.28 0.307 0.301 U

0.576 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.105 1.00 0.185 0.146 1.09 Radium 226 TestAmerica St. Louis Page 18 of 37 1

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Client Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16616-10 Client Sample ID: L08-12-10-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:27 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 234 1.18 (2+/-)

0.362 (2+/-)

1 03/26/16 21:37 03/25/16 10:09 pCi/g 1.01 1.00 RL MDC 0.340 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.211 0.156 0.155 0.228 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 21:37 1

6.48 2.27 2.26 U

2.38 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.159 0.207 0.165 1.22 Thorium 232 Tl-208 0.419 0.0624 0.0761 0.0465 pCi/g 03/25/16 10:09 03/26/16 21:37 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16616-10 Client Sample ID: L08-12-10-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:27 Percent Solids: 82.1 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00013 0.000071 0.000021 mg/Kg

03/23/16 08:23 03/24/16 10:10 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 2.23 (2+/-)

0.366 (2+/-)

1 03/24/16 10:10 03/23/16 08:23 pCi/g 0.243 1.42 RL MDC 0.303 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:23 03/24/16 10:10 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 84 Lab Sample ID: 160-16616-11 Client Sample ID: L08-12-11-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:35 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.31 (2+/-)

0.218 (2+/-)

1 03/26/16 21:37 03/25/16 10:09 pCi/g 0.101 RL MDC 0.172 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.0949 0.0561 0.0561 U

0.00198 Americium 241 pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.337 0.441 0.410 1.57 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.0648 0.151 0.100 1.09 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.0759 0.171 0.0888 1.13 Lead 212 pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.0763 0.164 0.0972 1.27 Lead 214 pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.379 2.37 1.16 20.2 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 21:37 1

1.13 0.270 0.265 U

0.461 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.0648 1.00 0.151 0.100 1.09 Radium 226 pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.866 1.00 0.566 0.548 1.32 Thorium 234 pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.165 0.125 0.124 U

0.161 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 21:37 1

5.07 2.88 2.88 U

0.728 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 21:37 1

0.101 0.218 0.172 1.31 Thorium 232 TestAmerica St. Louis Page 19 of 37 1

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Client Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16616-11 Client Sample ID: L08-12-11-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:35 Date Received: 03/22/16 10:45 Pb-210 1.76 0.579 0.615 0.750 pCi/g 03/25/16 10:09 03/26/16 21:37 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.374 0.0460 0.0601 0.0329 pCi/g 03/25/16 10:09 03/26/16 21:37 1

Lab Sample ID: 160-16616-11 Client Sample ID: L08-12-11-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:35 Percent Solids: 82.3 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000043 J 0.000069 0.000021 mg/Kg

03/23/16 08:23 03/24/16 10:14 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.733 (2+/-)

0.112 (2+/-)

1 03/24/16 10:14 03/23/16 08:23 pCi/g 0.235 1.38 RL MDC 0.0895 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:23 03/24/16 10:14 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 88 Lab Sample ID: 160-16616-12 Client Sample ID: L08-12-12-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:37 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.26 (2+/-)

0.227 (2+/-)

1 03/26/16 21:38 03/25/16 10:09 pCi/g 0.110 RL MDC 0.187 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.114 0.0679 0.0679 U

0.0111 Americium 241 pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.462 0.532 0.508 1.52 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.0710 0.163 0.116 1.11 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.0810 0.183 0.0959 1.20 Lead 212 pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.0772 0.161 0.101 1.21 Lead 214 pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.290 2.46 1.35 20.0 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.829 0.504 0.493 0.966 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.0710 1.00 0.163 0.116 1.11 Radium 226 pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.956 1.00 0.350 0.342 U

0.706 Thorium 234 pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.194 0.146 0.145 U

0.159 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 21:38 1

6.14 3.90 3.86 U

5.27 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.110 0.227 0.187 1.26 Thorium 232 Tl-208 0.433 0.0553 0.0712 0.0375 pCi/g 03/25/16 10:09 03/26/16 21:38 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

TestAmerica St. Louis Page 20 of 37 1

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Client Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16616-12 Client Sample ID: L08-12-12-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:37 Percent Solids: 82.4 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000045 J 0.000067 0.000020 mg/Kg

03/23/16 08:23 03/24/16 10:18 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.762 (2+/-)

0.140 (2+/-)

1 03/24/16 10:18 03/23/16 08:23 pCi/g 0.229 1.34 RL MDC 0.121 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:23 03/24/16 10:18 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 90 Lab Sample ID: 160-16616-13 Client Sample ID: L08-12-13-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:40 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.16 (2+/-)

0.178 (2+/-)

1 03/26/16 21:38 03/25/16 10:09 pCi/g 0.131 RL MDC 0.135 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.107 0.0633 0.0633 U

0.0170 Americium 241 pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.438 0.503 0.482 1.40 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.0702 0.148 0.104 1.02 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.0720 0.164 0.0840 1.09 Lead 212 pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.0816 0.156 0.105 1.11 Lead 214 pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.407 2.80 1.32 24.6 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 21:38 1

1.28 0.246 0.239 U

0.554 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.0702 1.00 0.148 0.104 1.02 Radium 226 pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.917 1.00 0.613 0.587 1.69 Thorium 234 pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.257 0.171 0.170 U

0.179 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 21:38 1

5.76 3.32 3.32 U

0.783 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 21:38 1

0.131 0.178 0.135 1.16 Thorium 232 Tl-208 0.377 0.0493 0.0627 0.0378 pCi/g 03/25/16 10:09 03/26/16 21:38 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16616-13 Client Sample ID: L08-12-13-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:40 Percent Solids: 84.6 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00044 0.000065 0.000019 mg/Kg

03/23/16 08:23 03/24/16 10:34 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 7.60 (2+/-)

0.813 (2+/-)

1 03/24/16 10:34 03/23/16 08:23 pCi/g 0.222 1.30 RL MDC 0.414 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

TestAmerica St. Louis Page 21 of 37 1

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Client Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16616-13 Client Sample ID: L08-12-13-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:40 Percent Solids: 84.6 Date Received: 03/22/16 10:45 Re 30 - 110 Carrier 03/23/16 08:23 03/24/16 10:34 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 91 Lab Sample ID: 160-16616-14 Client Sample ID: L08-12-14-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:46 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.09 (2+/-)

0.157 (2+/-)

1 03/26/16 21:39 03/25/16 10:09 pCi/g 0.0822 RL MDC 0.111 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 21:39 1

0.0944 0.0564 0.0564 U

0.0161 Americium 241 pCi/g 03/25/16 10:09 03/26/16 21:39 1

0.402 0.476 0.451 1.48 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 21:39 1

0.0624 0.120 0.0818 0.846 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 21:39 1

0.0647 0.160 0.0783 1.08 Lead 212 pCi/g 03/25/16 10:09 03/26/16 21:39 1

0.0614 0.135 0.0795 1.05 Lead 214 pCi/g 03/25/16 10:09 03/26/16 21:39 1

0.320 2.43 1.14 20.9 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 21:39 1

1.01 0.276 0.267 U

0.651 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 21:39 1

0.0624 1.00 0.120 0.0818 0.846 Radium 226 pCi/g 03/25/16 10:09 03/26/16 21:39 1

0.772 1.00 0.567 0.519 2.20 Thorium 234 pCi/g 03/25/16 10:09 03/26/16 21:39 1

0.187 0.160 0.156 0.333 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 21:39 1

4.51 2.94 2.89 5.41 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 21:39 1

0.0822 0.157 0.111 1.09 Thorium 232 Tl-208 0.348 0.0476 0.0598 0.0370 pCi/g 03/25/16 10:09 03/26/16 21:39 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16616-14 Client Sample ID: L08-12-14-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:46 Percent Solids: 82.2 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00027 0.000070 0.000021 mg/Kg

03/23/16 08:23 03/24/16 10:38 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 4.69 (2+/-)

0.548 (2+/-)

1 03/24/16 10:38 03/23/16 08:23 pCi/g 0.239 1.40 RL MDC 0.337 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:23 03/24/16 10:38 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 90 TestAmerica St. Louis Page 22 of 37 1

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Client Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16616-15 Client Sample ID: L08-12-15-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:50 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.17 (2+/-)

0.193 (2+/-)

1 03/26/16 22:09 03/25/16 10:09 pCi/g 0.118 RL MDC 0.152 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.118 0.0698 0.0698 U

0.00256 Americium 241 pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.648 0.432 0.426 0.697 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.0865 0.172 0.129 1.09 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.0733 0.175 0.0920 1.15 Lead 212 pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.0838 0.155 0.102 1.13 Lead 214 pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.390 2.39 1.37 19.1 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 22:09 1

1.31 0.257 0.255 U

0.345 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.0865 1.00 0.172 0.129 1.09 Radium 226 pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.906 1.00 0.606 0.583 1.58 Thorium 234 pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.277 0.176 0.176 U

0.0705 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 22:09 1

6.59 3.95 3.94 U

2.91 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.118 0.193 0.152 1.17 Thorium 232 Tl-208 0.326 0.0524 0.0624 0.0400 pCi/g 03/25/16 10:09 03/26/16 22:09 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16616-15 Client Sample ID: L08-12-15-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:50 Percent Solids: 82.0 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00012 0.000068 0.000020 mg/Kg

03/23/16 08:23 03/24/16 10:41 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 2.11 (2+/-)

0.244 (2+/-)

1 03/24/16 10:41 03/23/16 08:23 pCi/g 0.234 1.36 RL MDC 0.149 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:23 03/24/16 10:41 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 90 Lab Sample ID: 160-16616-16 Client Sample ID: L08-12-15-T-E-Q-00 Matrix: Solid Date Collected: 03/18/16 09:50 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.03 (2+/-)

0.151 (2+/-)

1 03/26/16 22:09 03/25/16 10:09 pCi/g 0.0700 RL MDC 0.108 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.0705 0.0509 0.0507 U

0.0436 Americium 241 pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.379 0.423 0.406 1.16 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.0562 0.130 0.0857 0.942 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.0708 0.159 0.0825 1.05 Lead 212 TestAmerica St. Louis Page 23 of 37 1

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Client Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16616-16 Client Sample ID: L08-12-15-T-E-Q-00 Matrix: Solid Date Collected: 03/18/16 09:50 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 214 1.09 (2+/-)

0.144 (2+/-)

1 03/26/16 22:09 03/25/16 10:09 pCi/g 0.0622 RL MDC 0.0882 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.380 2.11 1.04 17.9 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 22:09 1

1.00 0.612 0.610 U

-0.495 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.0562 1.00 0.130 0.0857 0.942 Radium 226 pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.803 1.00 0.522 0.507 1.20 Thorium 234 pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.246 0.146 0.146 U

0.104 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 22:09 1

3.99 2.96 2.93 U

3.45 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 22:09 1

0.0700 0.151 0.108 1.03 Thorium 232 Tl-208 0.350 0.0448 0.0577 0.0324 pCi/g 03/25/16 10:09 03/26/16 22:09 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16616-16 Client Sample ID: L08-12-15-T-E-Q-00 Matrix: Solid Date Collected: 03/18/16 09:50 Percent Solids: 81.6 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000098 0.000068 0.000020 mg/Kg

03/23/16 08:23 03/24/16 10:45 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.68 (2+/-)

0.163 (2+/-)

1 03/24/16 10:45 03/23/16 08:23 pCi/g 0.233 1.36 RL MDC 0.0505 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:23 03/24/16 10:45 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 87 Lab Sample ID: 160-16616-17 Client Sample ID: L08-12-16-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:55 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.18 (2+/-)

0.171 (2+/-)

1 03/26/16 22:10 03/25/16 10:09 pCi/g 0.119 RL MDC 0.122 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 22:10 1

0.106 0.0631 0.0631 U

0.00515 Americium 241 pCi/g 03/25/16 10:09 03/26/16 22:10 1

0.391 0.485 0.458 1.55 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 22:10 1

0.0898 0.134 0.0985 0.877 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 22:10 1

0.0743 0.172 0.0884 1.14 Lead 212 pCi/g 03/25/16 10:09 03/26/16 22:10 1

0.0718 0.141 0.0926 1.02 Lead 214 pCi/g 03/25/16 10:09 03/26/16 22:10 1

0.253 2.40 1.26 19.9 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 22:10 1

1.19 0.308 0.304 U

0.420 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 22:10 1

0.0898 1.00 0.134 0.0985 0.877 Radium 226 pCi/g 03/25/16 10:09 03/26/16 22:10 1

0.919 1.00 0.588 0.575 1.18 Thorium 234 TestAmerica St. Louis Page 24 of 37 1

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Client Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16616-17 Client Sample ID: L08-12-16-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:55 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Uranium 235 0.211 U (2+/-)

0.148 (2+/-)

1 03/26/16 22:10 03/25/16 10:09 pCi/g 0.244 RL MDC 0.147 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 22:10 1

6.74 2.96 2.96 U

0.000 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 22:10 1

0.119 0.171 0.122 1.18 Thorium 232 Tl-208 0.411 0.0611 0.0745 0.0469 pCi/g 03/25/16 10:09 03/26/16 22:10 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16616-17 Client Sample ID: L08-12-16-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:55 Percent Solids: 81.4 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00013 0.000070 0.000021 mg/Kg

03/23/16 08:26 03/24/16 10:57 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 2.24 (2+/-)

0.213 (2+/-)

1 03/24/16 10:57 03/23/16 08:26 pCi/g 0.241 1.41 RL MDC 0.0536 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:26 03/24/16 10:57 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 88 Lab Sample ID: 160-16616-18 Client Sample ID: L08-12-17-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:57 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.23 (2+/-)

0.173 (2+/-)

1 03/26/16 22:11 03/25/16 10:09 pCi/g 0.127 RL MDC 0.120 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 22:11 1

0.105 0.185 0.185 U

-0.0177 Americium 241 pCi/g 03/25/16 10:09 03/26/16 22:11 1

0.300 0.380 0.345 1.55 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 22:11 1

0.0658 0.164 0.105 1.22 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 22:11 1

0.0853 0.194 0.0991 1.28 Lead 212 pCi/g 03/25/16 10:09 03/26/16 22:11 1

0.0770 0.161 0.0939 1.26 Lead 214 pCi/g 03/25/16 10:09 03/26/16 22:11 1

0.312 2.54 1.16 22.4 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 22:11 1

1.24 0.762 0.758 U

-0.781 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 22:11 1

0.0658 1.00 0.164 0.105 1.22 Radium 226 pCi/g 03/25/16 10:09 03/26/16 22:11 1

0.847 1.00 0.310 0.288 1.09 Thorium 234 pCi/g 03/25/16 10:09 03/26/16 22:11 1

0.253 0.155 0.155 U

0.0451 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 22:11 1

5.39 3.24 3.23 U

2.09 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 22:11 1

0.127 0.173 0.120 1.23 Thorium 232 TestAmerica St. Louis Page 25 of 37 1

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Client Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16616-18 Client Sample ID: L08-12-17-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:57 Date Received: 03/22/16 10:45 Pb-210 1.81 0.655 0.688 0.790 pCi/g 03/25/16 10:09 03/26/16 22:11 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.380 0.0515 0.0646 0.0411 pCi/g 03/25/16 10:09 03/26/16 22:11 1

Lab Sample ID: 160-16616-18 Client Sample ID: L08-12-17-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:57 Percent Solids: 81.5 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000062 J 0.000070 0.000021 mg/Kg

03/23/16 08:26 03/24/16 11:01 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.06 (2+/-)

0.186 (2+/-)

1 03/24/16 11:01 03/23/16 08:26 pCi/g 0.239 1.40 RL MDC 0.159 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:26 03/24/16 11:01 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 87 Lab Sample ID: 160-16616-19 Client Sample ID: L08-12-18-T-E-B-00 Matrix: Solid Date Collected: 03/18/16 10:02 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.35 (2+/-)

0.214 (2+/-)

1 03/26/16 22:12 03/25/16 10:09 pCi/g 0.145 RL MDC 0.164 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 22:12 1

0.115 0.0685 0.0685 U

-0.0221 Americium 241 pCi/g 03/25/16 10:09 03/26/16 22:12 1

0.376 0.450 0.422 1.51 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 22:12 1

0.0777 0.159 0.116 1.05 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 22:12 1

0.0701 0.179 0.0892 1.20 Lead 212 pCi/g 03/25/16 10:09 03/26/16 22:12 1

0.0803 0.153 0.101 1.11 Lead 214 pCi/g 03/25/16 10:09 03/26/16 22:12 1

0.463 2.38 1.29 19.5 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 22:12 1

1.12 0.687 0.684 U

-0.628 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 22:12 1

0.0777 1.00 0.159 0.116 1.05 Radium 226 pCi/g 03/25/16 10:09 03/26/16 22:12 1

0.837 1.00 0.333 0.314 1.06 Thorium 234 pCi/g 03/25/16 10:09 03/26/16 22:12 1

0.204 0.156 0.154 0.265 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 22:12 1

5.71 3.20 3.20 U

-0.278 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 22:12 1

0.145 0.214 0.164 1.35 Thorium 232 Tl-208 0.388 0.0511 0.0650 0.0369 pCi/g 03/25/16 10:09 03/26/16 22:12 1

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

TestAmerica St. Louis Page 26 of 37 1

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Client Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16616-19 Client Sample ID: L08-12-18-T-E-B-00 Matrix: Solid Date Collected: 03/18/16 10:02 Percent Solids: 81.1 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000078 0.000071 0.000021 mg/Kg

03/23/16 08:26 03/24/16 11:05 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.33 (2+/-)

0.195 (2+/-)

1 03/24/16 11:05 03/23/16 08:26 pCi/g 0.244 1.42 RL MDC 0.152 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:26 03/24/16 11:05 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 87 TestAmerica St. Louis Page 27 of 37 1

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QC Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-241767/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242133 Prep Batch: 241767 RL MDL Technetium 99 ND 0.000050 0.000015 mg/Kg 03/23/16 08:23 03/24/16 08:53 1

MB MB Analyte Dil Fac Analyzed Prepared D

Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-241767/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242133 Prep Batch: 241767 Technetium 99 0.00119 0.00120 mg/Kg 101 80 - 120 Analyte LCS LCS D

Unit Result Qualifier

%Rec Spike Added

%Rec.

Limits Client Sample ID: L08-12-01-T-E-S-00 Lab Sample ID: 160-16616-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 242133 Prep Batch: 241767 Technetium 99 0.00019 0.00137 0.00158 mg/Kg 101 75 - 125

Analyte MS MS D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Client Sample ID: L08-12-01-T-E-S-00 Lab Sample ID: 160-16616-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 242133 Prep Batch: 241767 Technetium 99 0.00019 0.00136 0.00160 mg/Kg 103 75 - 125 2

30

Analyte MSD MSD D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Limit RPD RPD Client Sample ID: Method Blank Lab Sample ID: MB 160-241768/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242133 Prep Batch: 241768 RL MDL Technetium 99 ND 0.000053 0.000016 mg/Kg 03/23/16 08:26 03/24/16 10:49 1

MB MB Analyte Dil Fac Analyzed Prepared D

Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-241768/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242133 Prep Batch: 241768 Technetium 99 0.00119 0.00125 mg/Kg 105 80 - 120 Analyte LCS LCS D

Unit Result Qualifier

%Rec Spike Added

%Rec.

Limits Client Sample ID: Matrix Spike Lab Sample ID: 160-16618-A-1-D MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 242133 Prep Batch: 241768 Technetium 99 0.0015 F1 0.00139 0.00186 F1 mg/Kg 23 75 - 125

Analyte MS MS D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Client Sample ID: Matrix Spike Duplicate Lab Sample ID: 160-16618-A-1-E MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 242133 Prep Batch: 241768 Technetium 99 0.0015 F1 0.00143 0.00201 F1 mg/Kg 34 75 - 125 8

30

Analyte MSD MSD D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Limit RPD RPD TestAmerica St. Louis Page 28 of 37 1

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QC Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-241767/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242134 Prep Batch: 241767 Technetium 99 Analyte U

1 03/24/16 08:53 03/23/16 08:23 pCi/g 0.172 MDC 1.01 RL 0.0671 0.0670 (2+/-)

(2+/-)

MB 0.05584 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Carrier Re 30 - 110 03/23/16 08:23 03/24/16 08:53 1

Dil Fac Prepared Analyzed Qualifier Limits

%Yield 99 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-241767/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242134 Prep Batch: 241767 Technetium 99 Analyte 120 80 101 20.59 20.4 1.96 1.02 0.174 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Re Carrier 30 - 110 LCS Qualifier Limits

%Yield 98 LCS Client Sample ID: L08-12-01-T-E-S-00 Lab Sample ID: 160-16616-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 242134 Prep Batch: 241767 Technetium 99 Analyte 125 75 101 26.96 23.4 3.34 2.63 1.29 0.220 RL MDC (2+/-)

MS MS pCi/g Unit Result Qual

%Rec Added Spike Result Sample Sample Qual Limits

%Rec.

Uncert.

Total Re Carrier 30 - 110 MS Qualifier Limits

%Yield 89 MS Client Sample ID: L08-12-01-T-E-S-00 Lab Sample ID: 160-16616-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 242134 Prep Batch: 241767 Technetium 99 Analyte 1

0.09 125 75 103 27.45 23.3 3.34 2.92 1.29 0.221 RL MDC (2+/-)

MSD MSD pCi/g Unit Result Qual

%Rec Limit Added Spike Result Sample Sample Qual Limits

%Rec.

Uncert.

Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits

%Yield 89 MSD Client Sample ID: Method Blank Lab Sample ID: MB 160-241768/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242134 Prep Batch: 241768 Technetium 99 Analyte U

1 03/24/16 10:49 03/23/16 08:26 pCi/g 0.183 MDC 1.07 RL 0.0587 0.0586 (2+/-)

(2+/-)

MB 0.04217 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total TestAmerica St. Louis Page 29 of 37 1

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QC Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)

Client Sample ID: Method Blank Lab Sample ID: MB 160-241768/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242134 Prep Batch: 241768 Carrier Re 30 - 110 03/23/16 08:26 03/24/16 10:49 1

Dil Fac Prepared Analyzed Qualifier Limits

%Yield 94 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-241768/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242134 Prep Batch: 241768 Technetium 99 Analyte 120 80 105 21.44 20.4 2.36 1.08 0.185 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Re Carrier 30 - 110 LCS Qualifier Limits

%Yield 93 LCS Client Sample ID: Matrix Spike Lab Sample ID: 160-16618-A-1-D MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 242134 Prep Batch: 241768 Technetium 99 Analyte 125 75 23 F1 31.83 23.8 26.2 3.18 1.34 0.229 RL MDC (2+/-)

MS MS pCi/g Unit Result Qual

%Rec Added Spike Result Sample Sample Qual Limits

%Rec.

Uncert.

Total Re Carrier 30 - 110 MS Qualifier Limits

%Yield 88 MS Client Sample ID: Matrix Spike Duplicate Lab Sample ID: 160-16618-A-1-E MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 242134 Prep Batch: 241768 Technetium 99 Analyte 1

0.41 125 75 34 F1 34.48 24.4 26.2 3.31 1.34 0.230 RL MDC (2+/-)

MSD MSD pCi/g Unit Result Qual

%Rec Limit Added Spike Result Sample Sample Qual Limits

%Rec.

Uncert.

Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits

%Yield 89 MSD Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-242185/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242406 Prep Batch: 242185 Actinium 228 Analyte U

1 03/26/16 19:45 03/25/16 10:09 pCi/g 0.0414 MDC RL 0.00948 0.00948 (2+/-)

(2+/-)

MB 0.001431 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.0144 0.00726 0.00726 U

0.0008751 Americium 241 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.200 0.0963 0.0963 U

0.009725 Bismuth 212 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.0642 0.0241 0.0241 U

-0.003331 Bismuth 214 TestAmerica St. Louis Page 30 of 37 1

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QC Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Client Sample ID: Method Blank Lab Sample ID: MB 160-242185/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242406 Prep Batch: 242185 Lead 212 Analyte U

1 03/26/16 19:45 03/25/16 10:09 pCi/g 0.0342 MDC RL 0.367 0.367 (2+/-)

(2+/-)

MB

-0.009185 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.0324 0.0144 0.0144 U

0.0001966 Lead 214 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.274 2.48 2.48 U

-0.06207 Potassium 40 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.265 0.0606 0.0606 U

0.0000 Protactinium 231 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.0642 1.00 0.0241 0.0241 U

-0.003331 Radium 226 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.275 1.00 0.136 0.136 U

0.05337 Thorium 234 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.0690 0.0719 0.0719 U

-0.004786 Uranium 235 1

03/26/16 19:45 03/25/16 10:09 pCi/g 1.90 15.2 15.2 U

-0.3801 Protactinium 234m 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.0414 0.00948 0.00948 U

0.001431 Thorium 232 Other Detected Radionuclide None MB (2+/-)

(2+/-)

MDC RL pCi/g 03/25/16 10:09 03/26/16 19:45 1

MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-242185/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242401 Prep Batch: 242185 Americium 241 Analyte 116 87 98 98.98 101 10.3 0.517 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 34.1 33.22 3.48 0.200 0.144 pCi/g 97 87 - 120 Cobalt 60 31.8 30.25 3.05 0.132 pCi/g 95 87 - 115 Client Sample ID: L08-12-01-T-E-S-00 Lab Sample ID: 160-16616-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 242398 Prep Batch: 242185 Actinium 228 Analyte 1

0.03 1.106 1.12 0.160 0.108 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Americium 241 0.00470 U 0.03218 U 0.0505 0.0749 pCi/g 0.24 1

Bismuth 212 0.822 0.9261 0.360 0.485 pCi/g 0.14 1

Bismuth 214 0.920 0.8284 0.127 0.0670 pCi/g 0.34 1

Lead 212 1.12 1.169 0.171 0.0616 pCi/g 0.13 1

Lead 214 1.00 1.058 0.138 0.0538 pCi/g 0.20 1

Potassium 40 19.4 19.92 2.37 0.483 pCi/g 0.12 1

Protactinium 231 0.658 U 0.4408 U 0.225 1.08 pCi/g 0.39 1

Radium 226 0.920 0.8284 0.127 1.00 0.0670 pCi/g 0.34 1

Thorium 234 1.21 1.933 0.556 1.00 0.708 pCi/g 0.80 1

Uranium 235 0.434 0.4480 0.188 0.194 pCi/g 0.04 1

Protactinium 234m 2.54 U 1.610 U 2.84 4.78 pCi/g 0.15 1

Thorium 232 1.12 1.106 0.160 0.108 pCi/g 0.03 1

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QC Sample Results TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Pb-210 1

0.74 0.9261 1.82 0.554 0.758 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

RER RER Total Other Detected Radionuclides Tl-208 0.366 0.3813 0.0649 0.0390 pCi/g 0.12 1

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QC Association Summary TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Metals Prep Batch: 241767 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-16616-1 L08-12-01-T-E-S-00 Total/NA Solid None 160-16616-1 MS L08-12-01-T-E-S-00 Total/NA Solid None 160-16616-1 MSD L08-12-01-T-E-S-00 Total/NA Solid None 160-16616-2 L08-12-02-T-E-S-00 Total/NA Solid None 160-16616-3 L08-12-03-T-E-S-00 Total/NA Solid None 160-16616-4 L08-12-04-T-R-S-00 Total/NA Solid None 160-16616-5 L08-12-05-T-E-S-00 Total/NA Solid None 160-16616-6 L08-12-06-T-E-S-00 Total/NA Solid None 160-16616-7 L08-12-07-T-R-S-00 Total/NA Solid None 160-16616-8 L08-12-08-T-E-S-00 Total/NA Solid None 160-16616-9 L08-12-09-T-R-S-00 Total/NA Solid None 160-16616-10 L08-12-10-T-E-S-00 Total/NA Solid None 160-16616-11 L08-12-11-T-E-S-00 Total/NA Solid None 160-16616-12 L08-12-12-T-R-S-00 Total/NA Solid None 160-16616-13 L08-12-13-T-E-S-00 Total/NA Solid None 160-16616-14 L08-12-14-T-R-S-00 Total/NA Solid None 160-16616-15 L08-12-15-T-E-S-00 Total/NA Solid None 160-16616-16 L08-12-15-T-E-Q-00 Total/NA Solid None LCS 160-241767/2-A Lab Control Sample Total/NA Solid None MB 160-241767/1-A Method Blank Total/NA Prep Batch: 241768 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-16616-17 L08-12-16-T-R-S-00 Total/NA Solid None 160-16616-18 L08-12-17-T-E-S-00 Total/NA Solid None 160-16616-19 L08-12-18-T-E-B-00 Total/NA Solid None 160-16618-A-1-D MS Matrix Spike Total/NA Solid None 160-16618-A-1-E MSD Matrix Spike Duplicate Total/NA Solid None LCS 160-241768/2-A Lab Control Sample Total/NA Solid None MB 160-241768/1-A Method Blank Total/NA Analysis Batch: 242133 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 241767 160-16616-1 L08-12-01-T-E-S-00 Total/NA Solid 6020A 241767 160-16616-1 MS L08-12-01-T-E-S-00 Total/NA Solid 6020A 241767 160-16616-1 MSD L08-12-01-T-E-S-00 Total/NA Solid 6020A 241767 160-16616-2 L08-12-02-T-E-S-00 Total/NA Solid 6020A 241767 160-16616-3 L08-12-03-T-E-S-00 Total/NA Solid 6020A 241767 160-16616-4 L08-12-04-T-R-S-00 Total/NA Solid 6020A 241767 160-16616-5 L08-12-05-T-E-S-00 Total/NA Solid 6020A 241767 160-16616-6 L08-12-06-T-E-S-00 Total/NA Solid 6020A 241767 160-16616-7 L08-12-07-T-R-S-00 Total/NA Solid 6020A 241767 160-16616-8 L08-12-08-T-E-S-00 Total/NA Solid 6020A 241767 160-16616-9 L08-12-09-T-R-S-00 Total/NA Solid 6020A 241767 160-16616-10 L08-12-10-T-E-S-00 Total/NA Solid 6020A 241767 160-16616-11 L08-12-11-T-E-S-00 Total/NA Solid 6020A 241767 160-16616-12 L08-12-12-T-R-S-00 Total/NA Solid 6020A 241767 160-16616-13 L08-12-13-T-E-S-00 Total/NA Solid 6020A 241767 160-16616-14 L08-12-14-T-R-S-00 Total/NA Solid 6020A 241767 160-16616-15 L08-12-15-T-E-S-00 Total/NA Solid 6020A 241767 160-16616-16 L08-12-15-T-E-Q-00 Total/NA TestAmerica St. Louis Page 33 of 37 1

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QC Association Summary TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Metals (Continued)

Analysis Batch: 242133 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 241768 160-16616-17 L08-12-16-T-R-S-00 Total/NA Solid 6020A 241768 160-16616-18 L08-12-17-T-E-S-00 Total/NA Solid 6020A 241768 160-16616-19 L08-12-18-T-E-B-00 Total/NA Solid 6020A 241768 160-16618-A-1-D MS Matrix Spike Total/NA Solid 6020A 241768 160-16618-A-1-E MSD Matrix Spike Duplicate Total/NA Solid 6020A 241767 LCS 160-241767/2-A Lab Control Sample Total/NA Solid 6020A 241768 LCS 160-241768/2-A Lab Control Sample Total/NA Solid 6020A 241767 MB 160-241767/1-A Method Blank Total/NA Solid 6020A 241768 MB 160-241768/1-A Method Blank Total/NA General Chemistry Analysis Batch: 241632 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-16616-1 L08-12-01-T-E-S-00 Total/NA Solid Moisture 160-16616-1 DU L08-12-01-T-E-S-00 Total/NA Solid Moisture 160-16616-2 L08-12-02-T-E-S-00 Total/NA Solid Moisture 160-16616-3 L08-12-03-T-E-S-00 Total/NA Solid Moisture 160-16616-4 L08-12-04-T-R-S-00 Total/NA Solid Moisture 160-16616-5 L08-12-05-T-E-S-00 Total/NA Solid Moisture 160-16616-6 L08-12-06-T-E-S-00 Total/NA Solid Moisture 160-16616-7 L08-12-07-T-R-S-00 Total/NA Solid Moisture 160-16616-8 L08-12-08-T-E-S-00 Total/NA Solid Moisture 160-16616-9 L08-12-09-T-R-S-00 Total/NA Solid Moisture 160-16616-10 L08-12-10-T-E-S-00 Total/NA Solid Moisture 160-16616-11 L08-12-11-T-E-S-00 Total/NA Solid Moisture 160-16616-12 L08-12-12-T-R-S-00 Total/NA Solid Moisture 160-16616-13 L08-12-13-T-E-S-00 Total/NA Solid Moisture 160-16616-14 L08-12-14-T-R-S-00 Total/NA Solid Moisture 160-16616-15 L08-12-15-T-E-S-00 Total/NA Solid Moisture 160-16616-16 L08-12-15-T-E-Q-00 Total/NA Solid Moisture 160-16616-17 L08-12-16-T-R-S-00 Total/NA Solid Moisture 160-16616-18 L08-12-17-T-E-S-00 Total/NA Solid Moisture 160-16616-19 L08-12-18-T-E-B-00 Total/NA Rad Leach Batch: 241584 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-16616-1 L08-12-01-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-1 DU L08-12-01-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-2 L08-12-02-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-3 L08-12-03-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-4 L08-12-04-T-R-S-00 Total/NA Solid Dry and Grind 160-16616-5 L08-12-05-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-6 L08-12-06-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-7 L08-12-07-T-R-S-00 Total/NA Solid Dry and Grind 160-16616-8 L08-12-08-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-9 L08-12-09-T-R-S-00 Total/NA Solid Dry and Grind 160-16616-10 L08-12-10-T-E-S-00 Total/NA TestAmerica St. Louis Page 34 of 37 1

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QC Association Summary TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Rad (Continued)

Leach Batch: 241584 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-16616-11 L08-12-11-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-12 L08-12-12-T-R-S-00 Total/NA Solid Dry and Grind 160-16616-13 L08-12-13-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-14 L08-12-14-T-R-S-00 Total/NA Solid Dry and Grind 160-16616-15 L08-12-15-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-16 L08-12-15-T-E-Q-00 Total/NA Solid Dry and Grind 160-16616-17 L08-12-16-T-R-S-00 Total/NA Solid Dry and Grind 160-16616-18 L08-12-17-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-19 L08-12-18-T-E-B-00 Total/NA Prep Batch: 241767 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-16616-1 L08-12-01-T-E-S-00 Total/NA Solid None 160-16616-1 MS L08-12-01-T-E-S-00 Total/NA Solid None 160-16616-1 MSD L08-12-01-T-E-S-00 Total/NA Solid None 160-16616-2 L08-12-02-T-E-S-00 Total/NA Solid None 160-16616-3 L08-12-03-T-E-S-00 Total/NA Solid None 160-16616-4 L08-12-04-T-R-S-00 Total/NA Solid None 160-16616-5 L08-12-05-T-E-S-00 Total/NA Solid None 160-16616-6 L08-12-06-T-E-S-00 Total/NA Solid None 160-16616-7 L08-12-07-T-R-S-00 Total/NA Solid None 160-16616-8 L08-12-08-T-E-S-00 Total/NA Solid None 160-16616-9 L08-12-09-T-R-S-00 Total/NA Solid None 160-16616-10 L08-12-10-T-E-S-00 Total/NA Solid None 160-16616-11 L08-12-11-T-E-S-00 Total/NA Solid None 160-16616-12 L08-12-12-T-R-S-00 Total/NA Solid None 160-16616-13 L08-12-13-T-E-S-00 Total/NA Solid None 160-16616-14 L08-12-14-T-R-S-00 Total/NA Solid None 160-16616-15 L08-12-15-T-E-S-00 Total/NA Solid None 160-16616-16 L08-12-15-T-E-Q-00 Total/NA Solid None LCS 160-241767/2-A Lab Control Sample Total/NA Solid None MB 160-241767/1-A Method Blank Total/NA Prep Batch: 241768 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-16616-17 L08-12-16-T-R-S-00 Total/NA Solid None 160-16616-18 L08-12-17-T-E-S-00 Total/NA Solid None 160-16616-19 L08-12-18-T-E-B-00 Total/NA Solid None 160-16618-A-1-D MS Matrix Spike Total/NA Solid None 160-16618-A-1-E MSD Matrix Spike Duplicate Total/NA Solid None LCS 160-241768/2-A Lab Control Sample Total/NA Solid None MB 160-241768/1-A Method Blank Total/NA Prep Batch: 242185 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 241584 160-16616-1 L08-12-01-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16616-1 DU L08-12-01-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16616-2 L08-12-02-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16616-3 L08-12-03-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16616-4 L08-12-04-T-R-S-00 Total/NA Solid Fill_Geo-0 241584 160-16616-5 L08-12-05-T-E-S-00 Total/NA TestAmerica St. Louis Page 35 of 37 1

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QC Association Summary TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Rad (Continued)

Prep Batch: 242185 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 241584 160-16616-6 L08-12-06-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16616-7 L08-12-07-T-R-S-00 Total/NA Solid Fill_Geo-0 241584 160-16616-8 L08-12-08-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16616-9 L08-12-09-T-R-S-00 Total/NA Solid Fill_Geo-0 241584 160-16616-10 L08-12-10-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16616-11 L08-12-11-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16616-12 L08-12-12-T-R-S-00 Total/NA Solid Fill_Geo-0 241584 160-16616-13 L08-12-13-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16616-14 L08-12-14-T-R-S-00 Total/NA Solid Fill_Geo-0 241584 160-16616-15 L08-12-15-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16616-16 L08-12-15-T-E-Q-00 Total/NA Solid Fill_Geo-0 241584 160-16616-17 L08-12-16-T-R-S-00 Total/NA Solid Fill_Geo-0 241584 160-16616-18 L08-12-17-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16616-19 L08-12-18-T-E-B-00 Total/NA Solid Fill_Geo-0 LCS 160-242185/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-242185/1-A Method Blank Total/NA TestAmerica St. Louis Page 36 of 37 1

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Tracer/Carrier Summary TestAmerica Job ID: 160-16616-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110)

Re 88 160-16616-1 Percent Yield (Acceptance Limits)

L08-12-01-T-E-S-00 89 160-16616-1 MS L08-12-01-T-E-S-00 89 160-16616-1 MSD L08-12-01-T-E-S-00 89 160-16616-2 L08-12-02-T-E-S-00 89 160-16616-3 L08-12-03-T-E-S-00 90 160-16616-4 L08-12-04-T-R-S-00 92 160-16616-5 L08-12-05-T-E-S-00 90 160-16616-6 L08-12-06-T-E-S-00 90 160-16616-7 L08-12-07-T-R-S-00 89 160-16616-8 L08-12-08-T-E-S-00 91 160-16616-9 L08-12-09-T-R-S-00 84 160-16616-10 L08-12-10-T-E-S-00 88 160-16616-11 L08-12-11-T-E-S-00 90 160-16616-12 L08-12-12-T-R-S-00 91 160-16616-13 L08-12-13-T-E-S-00 90 160-16616-14 L08-12-14-T-R-S-00 90 160-16616-15 L08-12-15-T-E-S-00 87 160-16616-16 L08-12-15-T-E-Q-00 88 160-16616-17 L08-12-16-T-R-S-00 87 160-16616-18 L08-12-17-T-E-S-00 87 160-16616-19 L08-12-18-T-E-B-00 88 160-16618-A-1-D MS Matrix Spike 89 160-16618-A-1-E MSD Matrix Spike Duplicate 98 LCS 160-241767/2-A Lab Control Sample 93 LCS 160-241768/2-A Lab Control Sample 99 MB 160-241767/1-A Method Blank 94 MB 160-241768/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 37 of 37 1

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Westinghouse Hematite Decommissioning Project - Final Status Survey Final Report Vol. 3, Chapter 21, Survey Area Release Record for Land Survey Area 08, Survey Units 09, 12 and 13, Rev. 1, J16616-1 Uds Level 2 Report Final Report
Person / Time
ML18075A008
Site:	07000036
Issue date:	03/29/2016
From:	TestAmerica Labs - St. Louis, Westinghouse
To:	Office of Nuclear Material Safety and Safeguards
Shared Package
ML18074A285	List: ML18074A217 ML18074A218 ML18074A219 ML18074A220 ML18074A221 ML18074A222 ML18074A223 ML18074A224 ML18074A225 ML18074A227 ML18074A292 ML18074A293 ML18074A295 ML18074A296 ML18074A297 ML18074A298 ML18074A299 ML18075A008 ML18075A009 ML18075A010 ML18075A011 ML18075A012 ML18075A013 ML18075A014 ML18075A015 ML18075A016 ML18075A017
References
HEM-18-6
Download: ML18075A008 (37)
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