ML18075A010

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Westinghouse Hematite Decommissioning Project - Final Status Survey Final Report Vol. 3, Chapter 21, Survey Area Release Record for Land Survey Area 08, Survey Units 09, 12 and 13, Rev. 1, J16618-1 Uds Level 2 Report Final Report
ML18075A010
Person / Time
Site: 07000036
Issue date: 03/29/2016
From:
TestAmerica Labs - St. Louis, Westinghouse
To:
Office of Nuclear Material Safety and Safeguards
Shared Package
ML18074A285 List:
References
HEM-18-6
Download: ML18075A010 (32)
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Text

ANALYTICAL REPORT TestAmerica Laboratories, Inc.

TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-16618-1 Client Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

For:

Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Mr. Martin Swanson Authorized for release by:

3/29/2016 4:54:42 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

TestAmerica Job ID: 160-16618-1 Page 2 of 32 Cover Page..............................................

1 Table of Contents.........................................

2 Case Narrative...........................................

3 Chain of Custody..........................................

5 Receipt Checklists.........................................

9 Definitions/Glossary.......................................

10 Method Summary.........................................

11 Sample Summary.........................................

12 Client Sample Results......................................

13 QC Sample Results........................................

25 QC Association Summary...................................

29 Tracer Carrier Summary....................................

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16618-1 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Job ID: 160-16618-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: HDP RFP-CBA-022 (7 DAY TAT)

Report Number: 160-16618-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT The samples were received on 3/22/2016 10:45 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperatures of the 2 coolers at receipt time were 20.0º C and 20.0º C. The container label for sample 160-16618-13 did not match the information listed on the Chain-of-Custody (COC): F-031816-02 The container labels list L08-13-12-T-E-S-00 while the COC lists L08-13-11-T-E-S-00 @14:30. The client was contacted and a corrected CoC was forwarded to the lab. The correct sample ID of L08-13-12-T-E-S-00 was entered for reporting purposes.

TECHNETIUM-99 (ICPMS)

Samples L08-13-01-T-E-S-00 (160-16618-1), L08-13-02-T-E-S-00 (160-16618-2), L08-13-03-T-E-S-00 (160-16618-3),

L08-13-04-T-E-S-00 (160-16618-4), L08-13-05-T-E-S-00 (160-16618-5), L08-13-06-T-E-S-00 (160-16618-6), L08-13-07-T-E-S-00 (160-16618-7), L08-13-08-T-E-S-00 (160-16618-8), L08-13-09-T-R-S-00 (160-16618-9), L08-13-10-T-E-S-00 (160-16618-10),

L08-13-11-T-E-S-00 (160-16618-11), L08-13-11-T-E-Q-00 (160-16618-12) and L08-13-12-T-E-S-00 (160-16618-13) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 03/23/2016 and analyzed on 03/24/2016.

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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16618-1 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Job ID: 160-16618-1 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 160-241768 and analytical batch 160-242133 were outside control limits for technetium. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits. (160-16618-A-1-D MS) and (160-16618-A-1-E MSD)

The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 160-241768 and analytical batch 160-242134 were outside control limits for technetium. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits. (160-16618-A-1-D MS) and (160-16618-A-1-E MSD)

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

PERCENT SOLIDS Samples L08-13-01-T-E-S-00 (160-16618-1), L08-13-02-T-E-S-00 (160-16618-2), L08-13-03-T-E-S-00 (160-16618-3),

L08-13-04-T-E-S-00 (160-16618-4), L08-13-05-T-E-S-00 (160-16618-5), L08-13-06-T-E-S-00 (160-16618-6), L08-13-07-T-E-S-00 (160-16618-7), L08-13-08-T-E-S-00 (160-16618-8), L08-13-09-T-R-S-00 (160-16618-9), L08-13-10-T-E-S-00 (160-16618-10),

L08-13-11-T-E-S-00 (160-16618-11), L08-13-11-T-E-Q-00 (160-16618-12) and L08-13-12-T-E-S-00 (160-16618-13) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 03/23/2016.

No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

CESIUM-137 & OTHER GAMMA EMITTERS (GS)

Samples L08-13-01-T-E-S-00 (160-16618-1), L08-13-02-T-E-S-00 (160-16618-2), L08-13-03-T-E-S-00 (160-16618-3),

L08-13-04-T-E-S-00 (160-16618-4), L08-13-05-T-E-S-00 (160-16618-5), L08-13-06-T-E-S-00 (160-16618-6), L08-13-07-T-E-S-00 (160-16618-7), L08-13-08-T-E-S-00 (160-16618-8), L08-13-09-T-R-S-00 (160-16618-9), L08-13-10-T-E-S-00 (160-16618-10),

L08-13-11-T-E-S-00 (160-16618-11), L08-13-11-T-E-Q-00 (160-16618-12) and L08-13-12-T-E-S-00 (160-16618-13) were analyzed for Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 03/22/2016, prepared on 03/25/2016 and analyzed on 03/26/2016 and 03/27/2016.

Preparation Batch 160-242186:

Radium-226 is reported in these samples at the client's request. Radium-226 is reported from the 609.31 keV line of bismuth-214.

Because the samples have not had 21-days of ingrowth, the activity for radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between radium-226 and bismuth-214 by the loss of radon-222 during sample preparation. The samples are reported with the MDC achieved. L08-13-02-T-E-S-00 (160-16618-2), L08-13-03-T-E-S-00 (160-16618-3),

L08-13-04-T-E-S-00 (160-16618-4), L08-13-05-T-E-S-00 (160-16618-5), L08-13-06-T-E-S-00 (160-16618-6), L08-13-07-T-E-S-00 (160-16618-7), L08-13-08-T-E-S-00 (160-16618-8), L08-13-09-T-R-S-00 (160-16618-9), L08-13-10-T-E-S-00 (160-16618-10),

L08-13-11-T-E-S-00 (160-16618-11), L08-13-11-T-E-Q-00 (160-16618-12), L08-13-12-T-E-S-00 (160-16618-13), (LCS 160-242186/2-A),

(MB 160-242186/1-A) and (160-16618-A-2-E DU)

Preparation Batch 160-242185:

Radium-226 is reported in these samples at the client's request. Radium-226 is reported from the 609.31 keV line of bismuth-214.

Because the samples have not had 21-days of ingrowth, the activity for radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between radium-226 and bismuth-214 by the loss of radon-222 during sample preparation. The samples are reported with the MDC achieved. L08-13-01-T-E-S-00 (160-16618-1), (LCS 160-242185/2-A), (MB 160-242185/1-A), (160-16616-A-1-F) and (160-16616-A-1-G DU)

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

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10 11 12 Procedure HDP-PR-QA-006, Chain ofCustody Page 1 of!

Hematite Decommissioning Project JRevision: 4 L

J Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organi2ation, a person from each organi2ation should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.

Chain of Cutody ID No. I F-031816-0L_Page Project Name:

Westinghouse Electric Company Contact Person:

Clark Evers Phone Number:

314=810-3336 Sampler Name Kyle Weldon I of2

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Remarks L08-13-0 l-T-E-S-00 3/18/2016 13:50 L08-I3-02-T-E-S-OO 3/18/2016 13:52 L08-l 3-03-T-E-S-OO 3/18/2016 13:55 L08-l 3-04-T-E-S-OO 3/18/2016 14:00 L08-I3-05-T-E-S-OO 3/18/2016 14:10 L08-l 3-06-T-E-S-OO 3/1 8/2016 14:15 L08-13-07-T-E-S-OO 3/18/2016 14:18 L08-l 3-08-T-E-S-OO 3/18/2016 14:25 L08-13-09-T-R-S-OO 3/18/2016 15:30 L08-l3-10-T-E-S-00 3/18/2016 15:32 L08-l 3-l 1-T-E-S-OO 3/18/2016 14:35 L08-13-1 l-T-E-Q-OO 3/18/2016 14;35 Relinquished bv: Cf~vtA et,..,._7~

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10 11 12 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project Revision. 4 I

Page 1 of !

Westinghouse Non-Proprietary Class 3

, '--'" nur-r 1'.-\\,lA.*vvu - 1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed Coe to HDP.

Chain of Cutody ID No.

F-031816-02 Paee 2 of 2

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Laboratorv Name:

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Vania, Ivan From:

Swanson, Martin B. (SAIC) [swansomb@westinghouse.com]

Sent:

Tuesday, March 22, 2016 12:40 PM To:

Vania, Ivan Cc:

Gorski, Chad J

Subject:

RE: Samples Going Out This Morning Page 1 of 2 3/22/2016 The sample ID on page 2 of CoC F03181602 is incorrect. Please make the following correction: L081312TE S00. A corrected CoC will be sent along with the sample shipment on 3/23/16.

Regards, MartinSwanson Environmental Engineer Hematite Decommissioning Project Westinghouse Electric Company 3300 State Road P Festus, MO 63028 Phone: 3148103321 Fax: 3148103301 From: Vania, Ivan [1]

Sent: Tuesday, March 22, 2016 12:19 PM To: Swanson, Martin B. (SAIC)

Subject:

FW: Samples Going Out This Morning Good Afternoon Martin, The sample on page two of this CoC has a label ID of L08-13-12-T-E-S-00. Please advise if the label ID shouldbe used.

Regards, IvanHVania Project Manager II TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 13715 Rider Trail North Earth City, MO 63045 Tel 314.298.8566 l Fax 314.298.8757 www.testamericainc.com Weappreciateyourbusiness!

From: Swanson, Martin B. (SAIC) [2]

Sent: Tuesday, March 22, 2016 9:25 AM To: Vania, Ivan Cc: Dedner, Connie

Subject:

Samples Going Out This Morning Samples going out this morning from Westinghouse - Hematite are listed on the attached CoCs.

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Regards, MartinSwanson Environmental Engineer Hematite Decommissioning Project Westinghouse Electric Company 3300 State Road P Festus, MO 63028 Phone: 3148103321 Fax: 3148103301 This e-mail may contain proprietary information of the sending organization. Any unauthorized or improper disclosure, copying, distribution, or use of the contents of this e-mail and attached document(s) is prohibited. The information contained in this e-mail and attached document(s) is intended only for the personal and private use of the recipient(s) named above. If you have received this communication in error, please notify the sender immediately by email and delete the original e-mail and attached document(s).

This e-mail may contain proprietary information of the sending organization. Any unauthorized or improper disclosure, copying, distribution, or use of the contents of this e-mail and attached document(s) is prohibited. The information contained in this e-mail and attached document(s) is intended only for the personal and private use of the recipient(s) named above. If you have received this communication in error, please notify the sender immediately by email and delete the original e-mail and attached document(s).

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Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-16618-1 Login Number: 16618 Question Answer Comment Creator: Dedner, Connie L List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.

True The cooler's custody seal, if present, is intact.

N/A Sample custody seals, if present, are intact.

True The cooler or samples do not appear to have been compromised or tampered with.

N/A Samples were received on ice.

True Cooler Temperature is acceptable.

True Cooler Temperature is recorded.

True COC is present.

True COC is filled out in ink and legible.

True COC is filled out with all pertinent information.

True Is the Field Sampler's name present on COC?

True There are no discrepancies between the containers received and the COC.

True Samples are received within Holding Time (excluding tests with immediate HTs)

True Sample containers have legible labels.

True Containers are not broken or leaking.

True Sample collection date/times are provided.

True Appropriate sample containers are used.

True Sample bottles are completely filled.

True Sample Preservation Verified.

True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

True Multiphasic samples are not present.

True Samples do not require splitting or compositing.

N/A Residual Chlorine Checked.

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Definitions/Glossary TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Qualifiers Metals Qualifier Description F1 MS and/or MSD Recovery is outside acceptance limits.

Qualifier Rad Qualifier Description U

Result is less than the sample detection limit.

Qualifier F1 MS and/or MSD Recovery is outside acceptance limits.

Glossary These commonly used abbreviations may or may not be present in this report.

Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation

%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)

NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method Summary TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL DOE GA-01-R Cesium-137 & Other Gamma Emitters (GS)

TAL SL Protocol

References:

DOE = U.S. Department of Energy EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory

References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 11 of 32 1

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Sample Summary TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID Client Sample ID Received Collected Matrix 160-16618-1 L08-13-01-T-E-S-00 Solid 03/18/16 13:50 03/22/16 10:45 160-16618-2 L08-13-02-T-E-S-00 Solid 03/18/16 13:52 03/22/16 10:45 160-16618-3 L08-13-03-T-E-S-00 Solid 03/18/16 13:55 03/22/16 10:45 160-16618-4 L08-13-04-T-E-S-00 Solid 03/18/16 14:00 03/22/16 10:45 160-16618-5 L08-13-05-T-E-S-00 Solid 03/18/16 14:10 03/22/16 10:45 160-16618-6 L08-13-06-T-E-S-00 Solid 03/18/16 14:15 03/22/16 10:45 160-16618-7 L08-13-07-T-E-S-00 Solid 03/18/16 14:18 03/22/16 10:45 160-16618-8 L08-13-08-T-E-S-00 Solid 03/18/16 14:25 03/22/16 10:45 160-16618-9 L08-13-09-T-R-S-00 Solid 03/18/16 15:30 03/22/16 10:45 160-16618-10 L08-13-10-T-E-S-00 Solid 03/18/16 15:32 03/22/16 10:45 160-16618-11 L08-13-11-T-E-S-00 Solid 03/18/16 14:35 03/22/16 10:45 160-16618-12 L08-13-11-T-E-Q-00 Solid 03/18/16 14:35 03/22/16 10:45 160-16618-13 L08-13-12-T-E-S-00 Solid 03/18/16 14:30 03/22/16 10:45 TestAmerica St. Louis Page 12 of 32 1

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Client Sample Results TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-1 Client Sample ID: L08-13-01-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 13:50 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.17 (2+/-)

0.203 (2+/-)

1 03/26/16 22:41 03/25/16 10:09 pCi/g 0.120 RL MDC 0.164 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:09 03/26/16 22:41 1

0.125 0.0743 0.0743 U

-0.0214 Americium 241 pCi/g 03/25/16 10:09 03/26/16 22:41 1

0.426 0.534 0.508 1.60 Bismuth 212 pCi/g 03/25/16 10:09 03/26/16 22:41 1

0.0792 0.155 0.123 0.904 Bismuth 214 pCi/g 03/25/16 10:09 03/26/16 22:41 1

0.0865 0.173 0.100 1.09 Lead 212 pCi/g 03/25/16 10:09 03/26/16 22:41 1

0.0858 0.152 0.108 1.03 Lead 214 pCi/g 03/25/16 10:09 03/26/16 22:41 1

0.271 2.34 1.40 18.4 Potassium 40 pCi/g 03/25/16 10:09 03/26/16 22:41 1

1.23 0.308 0.305 U

0.392 Protactinium 231 pCi/g 03/25/16 10:09 03/26/16 22:41 1

0.0792 1.00 0.155 0.123 0.904 Radium 226 pCi/g 03/25/16 10:09 03/26/16 22:41 1

0.984 1.00 0.349 0.337 U

0.858 Thorium 234 pCi/g 03/25/16 10:09 03/26/16 22:41 1

0.277 0.167 0.167 U

0.112 Uranium 235 pCi/g 03/25/16 10:09 03/26/16 22:41 1

7.64 4.33 4.33 U

1.14 Protactinium 234m pCi/g 03/25/16 10:09 03/26/16 22:41 1

0.120 0.203 0.164 1.17 Thorium 232 Pb-210 2.03 0.720 0.758 0.880 pCi/g 03/25/16 10:09 03/26/16 22:41 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.425 0.0608 0.0752 0.0408 pCi/g 03/25/16 10:09 03/26/16 22:41 1

Lab Sample ID: 160-16618-1 Client Sample ID: L08-13-01-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 13:50 Percent Solids: 82.6 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.0015 F1 0.000069 0.000021 mg/Kg

03/23/16 08:26 03/24/16 11:08 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 26.2 (2+/-)

3.50 (2+/-)

1 03/24/16 11:08 03/23/16 08:26 pCi/g 0.235 1.37 RL MDC 2.54 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:26 03/24/16 11:08 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 87 Lab Sample ID: 160-16618-2 Client Sample ID: L08-13-02-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 13:52 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.14 (2+/-)

0.159 (2+/-)

1 03/26/16 22:43 03/25/16 10:17 pCi/g 0.103 RL MDC 0.111 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 03/26/16 22:43 1

0.0797 0.149 0.149 U

-0.00416 Americium 241 pCi/g 03/25/16 10:17 03/26/16 22:43 1

0.404 0.363 0.332 1.43 Bismuth 212 pCi/g 03/25/16 10:17 03/26/16 22:43 1

0.0620 0.137 0.0933 0.972 Bismuth 214 TestAmerica St. Louis Page 13 of 32 1

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Client Sample Results TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-2 Client Sample ID: L08-13-02-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 13:52 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 212 1.12 (2+/-)

0.163 (2+/-)

1 03/26/16 22:43 03/25/16 10:17 pCi/g 0.0594 RL MDC 0.0729 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 03/26/16 22:43 1

0.0591 0.131 0.0764 1.02 Lead 214 pCi/g 03/25/16 10:17 03/26/16 22:43 1

0.346 2.24 1.05 19.7 Potassium 40 pCi/g 03/25/16 10:17 03/26/16 22:43 1

1.11 0.678 0.675 U

-0.530 Protactinium 231 pCi/g 03/25/16 10:17 03/26/16 22:43 1

0.0620 1.00 0.137 0.0933 0.972 Radium 226 pCi/g 03/25/16 10:17 03/26/16 22:43 1

0.718 1.00 0.464 0.451 1.05 Thorium 234 pCi/g 03/25/16 10:17 03/26/16 22:43 1

0.229 0.147 0.146 U

0.0873 Uranium 235 pCi/g 03/25/16 10:17 03/26/16 22:43 1

4.69 2.55 2.54 U

2.63 Protactinium 234m pCi/g 03/25/16 10:17 03/26/16 22:43 1

0.103 0.159 0.111 1.14 Thorium 232 Pb-210 1.36 0.541 0.564 0.673 pCi/g 03/25/16 10:17 03/26/16 22:43 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.384 0.0450 0.0599 0.0322 pCi/g 03/25/16 10:17 03/26/16 22:43 1

Lab Sample ID: 160-16618-2 Client Sample ID: L08-13-02-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 13:52 Percent Solids: 88.1 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00043 0.000060 0.000018 mg/Kg

03/23/16 08:26 03/24/16 11:32 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 7.42 (2+/-)

0.852 (2+/-)

1 03/24/16 11:32 03/23/16 08:26 pCi/g 0.206 1.20 RL MDC 0.510 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:26 03/24/16 11:32 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 90 Lab Sample ID: 160-16618-3 Client Sample ID: L08-13-03-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 13:55 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.09 (2+/-)

0.158 (2+/-)

1 03/26/16 22:44 03/25/16 10:17 pCi/g 0.107 RL MDC 0.112 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 03/26/16 22:44 1

0.103 0.0620 0.0619 U

-0.0265 Americium 241 pCi/g 03/25/16 10:17 03/26/16 22:44 1

0.258 0.336 0.311 1.21 Bismuth 212 pCi/g 03/25/16 10:17 03/26/16 22:44 1

0.0752 0.136 0.104 0.841 Bismuth 214 pCi/g 03/25/16 10:17 03/26/16 22:44 1

0.0657 0.157 0.0807 1.04 Lead 212 pCi/g 03/25/16 10:17 03/26/16 22:44 1

0.0599 0.125 0.0785 0.938 Lead 214 pCi/g 03/25/16 10:17 03/26/16 22:44 1

0.402 2.26 1.18 18.8 Potassium 40 pCi/g 03/25/16 10:17 03/26/16 22:44 1

1.01 0.268 0.259 U

0.611 Protactinium 231 TestAmerica St. Louis Page 14 of 32 1

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Client Sample Results TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-3 Client Sample ID: L08-13-03-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 13:55 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Radium 226 0.841 (2+/-)

0.136 (2+/-)

1 03/26/16 22:44 03/25/16 10:17 pCi/g 0.0752 1.00 RL MDC 0.104 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 03/26/16 22:44 1

0.776 1.00 0.317 0.300 0.997 Thorium 234 pCi/g 03/25/16 10:17 03/26/16 22:44 1

0.184 0.0410 0.0410 U

0.0212 Uranium 235 pCi/g 03/25/16 10:17 03/26/16 22:44 1

5.36 3.24 3.24 U

0.806 Protactinium 234m pCi/g 03/25/16 10:17 03/26/16 22:44 1

0.107 0.158 0.112 1.09 Thorium 232 Pb-210 1.58 0.622 0.649 0.786 pCi/g 03/25/16 10:17 03/26/16 22:44 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.338 0.0461 0.0579 0.0334 pCi/g 03/25/16 10:17 03/26/16 22:44 1

Lab Sample ID: 160-16618-3 Client Sample ID: L08-13-03-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 13:55 Percent Solids: 83.2 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00058 0.000066 0.000020 mg/Kg

03/23/16 08:26 03/24/16 11:36 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 9.91 (2+/-)

1.20 (2+/-)

1 03/24/16 11:36 03/23/16 08:26 pCi/g 0.227 1.33 RL MDC 0.786 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:26 03/24/16 11:36 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 89 Lab Sample ID: 160-16618-4 Client Sample ID: L08-13-04-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:00 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.14 (2+/-)

0.165 (2+/-)

1 03/26/16 23:14 03/25/16 10:17 pCi/g 0.112 RL MDC 0.117 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 03/26/16 23:14 1

0.0701 0.0476 0.0474 U

0.0390 Americium 241 pCi/g 03/25/16 10:17 03/26/16 23:14 1

0.447 0.517 0.495 1.43 Bismuth 212 pCi/g 03/25/16 10:17 03/26/16 23:14 1

0.0633 0.133 0.0946 0.907 Bismuth 214 pCi/g 03/25/16 10:17 03/26/16 23:14 1

0.0659 0.153 0.0766 1.02 Lead 212 pCi/g 03/25/16 10:17 03/26/16 23:14 1

0.0693 0.135 0.0808 1.04 Lead 214 pCi/g 03/25/16 10:17 03/26/16 23:14 1

0.315 2.32 1.10 20.0 Potassium 40 pCi/g 03/25/16 10:17 03/26/16 23:14 1

1.08 0.666 0.662 U

-0.668 Protactinium 231 pCi/g 03/25/16 10:17 03/26/16 23:14 1

0.0633 1.00 0.133 0.0946 0.907 Radium 226 pCi/g 03/25/16 10:17 03/26/16 23:14 1

0.819 1.00 0.292 0.276 0.921 Thorium 234 pCi/g 03/25/16 10:17 03/26/16 23:14 1

0.241 0.146 0.145 U

0.103 Uranium 235 pCi/g 03/25/16 10:17 03/26/16 23:14 1

4.38 2.49 2.49 U

0.753 Protactinium 234m TestAmerica St. Louis Page 15 of 32 1

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Client Sample Results TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-4 Client Sample ID: L08-13-04-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:00 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Thorium 232 1.14 (2+/-)

0.165 (2+/-)

1 03/26/16 23:14 03/25/16 10:17 pCi/g 0.112 RL MDC 0.117 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Pb-210 1.82 0.611 0.648 0.758 pCi/g 03/25/16 10:17 03/26/16 23:14 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.361 0.0503 0.0627 0.0377 pCi/g 03/25/16 10:17 03/26/16 23:14 1

Lab Sample ID: 160-16618-4 Client Sample ID: L08-13-04-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:00 Percent Solids: 78.8 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00065 0.000073 0.000022 mg/Kg

03/23/16 08:26 03/24/16 11:39 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 11.1 (2+/-)

1.15 (2+/-)

1 03/24/16 11:39 03/23/16 08:26 pCi/g 0.251 1.47 RL MDC 0.524 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:26 03/24/16 11:39 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 88 Lab Sample ID: 160-16618-5 Client Sample ID: L08-13-05-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:10 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 0.822 (2+/-)

0.132 (2+/-)

1 03/26/16 23:15 03/25/16 10:17 pCi/g 0.0560 RL MDC 0.102 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 03/26/16 23:15 1

0.0891 0.0530 0.0530 U

0.0117 Americium 241 pCi/g 03/25/16 10:17 03/26/16 23:15 1

0.462 0.319 0.313 0.593 Bismuth 212 pCi/g 03/25/16 10:17 03/26/16 23:15 1

0.0590 0.113 0.0854 0.718 Bismuth 214 pCi/g 03/25/16 10:17 03/26/16 23:15 1

0.0596 0.120 0.0678 0.762 Lead 212 pCi/g 03/25/16 10:17 03/26/16 23:15 1

0.0656 0.116 0.0859 0.746 Lead 214 pCi/g 03/25/16 10:17 03/26/16 23:15 1

0.309 1.74 1.01 13.9 Potassium 40 pCi/g 03/25/16 10:17 03/26/16 23:15 1

0.884 0.233 0.229 U

0.382 Protactinium 231 pCi/g 03/25/16 10:17 03/26/16 23:15 1

0.0590 1.00 0.113 0.0854 0.718 Radium 226 pCi/g 03/25/16 10:17 03/26/16 23:15 1

0.781 1.00 0.348 0.303 1.65 Thorium 234 pCi/g 03/25/16 10:17 03/26/16 23:15 1

0.180 0.172 0.157 0.696 Uranium 235 pCi/g 03/25/16 10:17 03/26/16 23:15 1

4.61 2.61 2.58 U

3.73 Protactinium 234m pCi/g 03/25/16 10:17 03/26/16 23:15 1

0.0560 0.132 0.102 0.822 Thorium 232 TestAmerica St. Louis Page 16 of 32 1

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Client Sample Results TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-5 Client Sample ID: L08-13-05-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:10 Date Received: 03/22/16 10:45 Tl-208 0.268 0.0442 0.0522 0.0320 pCi/g 03/25/16 10:17 03/26/16 23:15 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16618-5 Client Sample ID: L08-13-05-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:10 Percent Solids: 87.5 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.0016 0.000067 0.000020 mg/Kg

03/23/16 08:26 03/24/16 11:43 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 27.6 (2+/-)

2.68 (2+/-)

1 03/24/16 11:43 03/23/16 08:26 pCi/g 0.228 1.33 RL MDC 0.865 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:26 03/24/16 11:43 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 86 Lab Sample ID: 160-16618-6 Client Sample ID: L08-13-06-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:15 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.15 (2+/-)

0.180 (2+/-)

1 03/26/16 23:17 03/25/16 10:17 pCi/g 0.117 RL MDC 0.138 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 03/26/16 23:17 1

0.0751 0.0461 0.0458 U

0.0507 Americium 241 pCi/g 03/25/16 10:17 03/26/16 23:17 1

0.468 0.541 0.517 1.53 Bismuth 212 pCi/g 03/25/16 10:17 03/26/16 23:17 1

0.0849 0.147 0.110 0.942 Bismuth 214 pCi/g 03/25/16 10:17 03/26/16 23:17 1

0.0730 0.170 0.0848 1.14 Lead 212 pCi/g 03/25/16 10:17 03/26/16 23:17 1

0.0751 0.153 0.101 1.10 Lead 214 pCi/g 03/25/16 10:17 03/26/16 23:17 1

0.355 2.55 1.23 22.2 Potassium 40 pCi/g 03/25/16 10:17 03/26/16 23:17 1

1.09 0.255 0.248 U

0.512 Protactinium 231 pCi/g 03/25/16 10:17 03/26/16 23:17 1

0.0849 1.00 0.147 0.110 0.942 Radium 226 pCi/g 03/25/16 10:17 03/26/16 23:17 1

0.801 1.00 0.524 0.507 1.26 Thorium 234 pCi/g 03/25/16 10:17 03/26/16 23:17 1

0.259 0.157 0.156 U

0.176 Uranium 235 pCi/g 03/25/16 10:17 03/26/16 23:17 1

5.02 2.93 2.92 U

1.19 Protactinium 234m pCi/g 03/25/16 10:17 03/26/16 23:17 1

0.117 0.180 0.138 1.15 Thorium 232 Tl-208 0.425 0.0503 0.0666 0.0378 pCi/g 03/25/16 10:17 03/26/16 23:17 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

TestAmerica St. Louis Page 17 of 32 1

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Client Sample Results TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-6 Client Sample ID: L08-13-06-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:15 Percent Solids: 82.6 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00034 0.000070 0.000021 mg/Kg

03/23/16 08:26 03/24/16 11:47 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 5.79 (2+/-)

0.955 (2+/-)

1 03/24/16 11:47 03/23/16 08:26 pCi/g 0.241 1.41 RL MDC 0.793 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:26 03/24/16 11:47 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 87 Lab Sample ID: 160-16618-7 Client Sample ID: L08-13-07-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:18 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.15 (2+/-)

0.163 (2+/-)

1 03/26/16 23:16 03/25/16 10:17 pCi/g 0.128 RL MDC 0.113 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 03/26/16 23:16 1

0.0692 0.0409 0.0409 U

0.00762 Americium 241 pCi/g 03/25/16 10:17 03/26/16 23:16 1

0.442 0.362 0.342 1.15 Bismuth 212 pCi/g 03/25/16 10:17 03/26/16 23:16 1

0.0479 0.126 0.0868 0.883 Bismuth 214 pCi/g 03/25/16 10:17 03/26/16 23:16 1

0.0590 0.161 0.0765 1.10 Lead 212 pCi/g 03/25/16 10:17 03/26/16 23:16 1

0.0559 0.134 0.0819 1.02 Lead 214 pCi/g 03/25/16 10:17 03/26/16 23:16 1

0.357 2.35 1.16 20.0 Potassium 40 pCi/g 03/25/16 10:17 03/26/16 23:16 1

1.10 0.177 0.174 U

0.302 Protactinium 231 pCi/g 03/25/16 10:17 03/26/16 23:16 1

0.0479 1.00 0.126 0.0868 0.883 Radium 226 pCi/g 03/25/16 10:17 03/26/16 23:16 1

0.737 1.00 0.507 0.481 1.54 Thorium 234 pCi/g 03/25/16 10:17 03/26/16 23:16 1

0.176 0.117 0.116 U

0.150 Uranium 235 pCi/g 03/25/16 10:17 03/26/16 23:16 1

4.45 2.66 2.66 U

1.68 Protactinium 234m pCi/g 03/25/16 10:17 03/26/16 23:16 1

0.128 0.163 0.113 1.15 Thorium 232 Pb-210 1.88 0.643 0.680 0.784 pCi/g 03/25/16 10:17 03/26/16 23:16 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.324 0.0423 0.0540 0.0299 pCi/g 03/25/16 10:17 03/26/16 23:16 1

Lab Sample ID: 160-16618-7 Client Sample ID: L08-13-07-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:18 Percent Solids: 85.8 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000078 0.000069 0.000021 mg/Kg

03/23/16 08:26 03/24/16 11:51 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier TestAmerica St. Louis Page 18 of 32 1

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Client Sample Results TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-7 Client Sample ID: L08-13-07-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:18 Percent Solids: 85.8 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.33 (2+/-)

0.363 (2+/-)

1 03/24/16 11:51 03/23/16 08:26 pCi/g 0.237 1.38 RL MDC 0.341 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:26 03/24/16 11:51 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 86 Lab Sample ID: 160-16618-8 Client Sample ID: L08-13-08-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:25 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.07 (2+/-)

0.159 (2+/-)

1 03/27/16 12:32 03/25/16 10:17 pCi/g 0.0787 RL MDC 0.116 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 03/27/16 12:32 1

0.0722 0.0428 0.0428 U

-0.00565 Americium 241 pCi/g 03/25/16 10:17 03/27/16 12:32 1

0.332 0.409 0.385 1.31 Bismuth 212 pCi/g 03/25/16 10:17 03/27/16 12:32 1

0.0467 0.108 0.0735 0.759 Bismuth 214 pCi/g 03/25/16 10:17 03/27/16 12:32 1

0.0559 0.144 0.0684 0.976 Lead 212 pCi/g 03/25/16 10:17 03/27/16 12:32 1

0.0593 0.114 0.0742 0.829 Lead 214 pCi/g 03/25/16 10:17 03/27/16 12:32 1

0.350 2.06 0.996 17.6 Potassium 40 pCi/g 03/25/16 10:17 03/27/16 12:32 1

0.698 0.378 0.373 U

0.589 Protactinium 231 pCi/g 03/25/16 10:17 03/27/16 12:32 1

0.0467 1.00 0.108 0.0735 0.759 Radium 226 pCi/g 03/25/16 10:17 03/27/16 12:32 1

0.730 1.00 0.598 0.582 1.33 Thorium 234 pCi/g 03/25/16 10:17 03/27/16 12:32 1

0.150 0.134 0.132 0.195 Uranium 235 pCi/g 03/25/16 10:17 03/27/16 12:32 1

4.19 2.45 2.45 U

1.25 Protactinium 234m pCi/g 03/25/16 10:17 03/27/16 12:32 1

0.0787 0.159 0.116 1.07 Thorium 232 Tl-208 0.349 0.0436 0.0567 0.0313 pCi/g 03/25/16 10:17 03/27/16 12:32 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16618-8 Client Sample ID: L08-13-08-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:25 Percent Solids: 85.2 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00039 0.000066 0.000020 mg/Kg

03/23/16 08:26 03/24/16 11:55 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 6.68 (2+/-)

0.617 (2+/-)

1 03/24/16 11:55 03/23/16 08:26 pCi/g 0.227 1.33 RL MDC 0.0588 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:26 03/24/16 11:55 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 88 TestAmerica St. Louis Page 19 of 32 1

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Client Sample Results TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-9 Client Sample ID: L08-13-09-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 15:30 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.04 (2+/-)

0.167 (2+/-)

1 03/27/16 12:33 03/25/16 10:17 pCi/g 0.103 RL MDC 0.129 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 03/27/16 12:33 1

0.0928 0.0560 0.0559 U

0.0343 Americium 241 pCi/g 03/25/16 10:17 03/27/16 12:33 1

0.361 0.372 0.359 0.926 Bismuth 212 pCi/g 03/25/16 10:17 03/27/16 12:33 1

0.0801 0.143 0.112 0.860 Bismuth 214 pCi/g 03/25/16 10:17 03/27/16 12:33 1

0.0659 0.141 0.0783 0.907 Lead 212 pCi/g 03/25/16 10:17 03/27/16 12:33 1

0.0772 0.120 0.0814 0.843 Lead 214 pCi/g 03/25/16 10:17 03/27/16 12:33 1

0.260 2.10 1.18 17.0 Potassium 40 pCi/g 03/25/16 10:17 03/27/16 12:33 1

0.819 0.347 0.341 U

0.596 Protactinium 231 pCi/g 03/25/16 10:17 03/27/16 12:33 1

0.0801 1.00 0.143 0.112 0.860 Radium 226 pCi/g 03/25/16 10:17 03/27/16 12:33 1

0.823 1.00 0.304 0.288 0.935 Thorium 234 pCi/g 03/25/16 10:17 03/27/16 12:33 1

0.200 0.173 0.172 U

0.189 Uranium 235 pCi/g 03/25/16 10:17 03/27/16 12:33 1

5.63 2.94 2.93 U

2.49 Protactinium 234m pCi/g 03/25/16 10:17 03/27/16 12:33 1

0.103 0.167 0.129 1.04 Thorium 232 Tl-208 0.334 0.0459 0.0575 0.0280 pCi/g 03/25/16 10:17 03/27/16 12:33 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16618-9 Client Sample ID: L08-13-09-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 15:30 Percent Solids: 84.1 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00091 0.000065 0.000020 mg/Kg

03/23/16 08:26 03/24/16 11:59 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 15.5 (2+/-)

1.53 (2+/-)

1 03/24/16 11:59 03/23/16 08:26 pCi/g 0.223 1.30 RL MDC 0.556 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:26 03/24/16 11:59 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 90 Lab Sample ID: 160-16618-10 Client Sample ID: L08-13-10-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 15:32 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.09 (2+/-)

0.155 (2+/-)

1 03/27/16 13:15 03/25/16 10:17 pCi/g 0.0818 RL MDC 0.108 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 03/27/16 13:15 1

0.0813 0.0605 0.0602 U

0.0527 Americium 241 pCi/g 03/25/16 10:17 03/27/16 13:15 1

0.355 0.416 0.388 1.45 Bismuth 212 pCi/g 03/25/16 10:17 03/27/16 13:15 1

0.0555 0.127 0.0871 0.894 Bismuth 214 pCi/g 03/25/16 10:17 03/27/16 13:15 1

0.0554 0.163 0.0736 1.12 Lead 212 TestAmerica St. Louis Page 20 of 32 1

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Client Sample Results TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-10 Client Sample ID: L08-13-10-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 15:32 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Lead 214 0.976 (2+/-)

0.129 (2+/-)

1 03/27/16 13:15 03/25/16 10:17 pCi/g 0.0708 RL MDC 0.0797 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 03/27/16 13:15 1

0.338 2.26 1.11 19.2 Potassium 40 pCi/g 03/25/16 10:17 03/27/16 13:15 1

1.07 0.654 0.652 U

-0.545 Protactinium 231 pCi/g 03/25/16 10:17 03/27/16 13:15 1

0.0555 1.00 0.127 0.0871 0.894 Radium 226 pCi/g 03/25/16 10:17 03/27/16 13:15 1

0.767 1.00 0.506 0.488 1.28 Thorium 234 pCi/g 03/25/16 10:17 03/27/16 13:15 1

0.223 0.135 0.134 U

0.0865 Uranium 235 pCi/g 03/25/16 10:17 03/27/16 13:15 1

5.89 1.55 1.55 U

0.124 Protactinium 234m pCi/g 03/25/16 10:17 03/27/16 13:15 1

0.0818 0.155 0.108 1.09 Thorium 232 Tl-208 0.361 0.0436 0.0575 0.0310 pCi/g 03/25/16 10:17 03/27/16 13:15 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16618-10 Client Sample ID: L08-13-10-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 15:32 Percent Solids: 81.1 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00021 0.000069 0.000021 mg/Kg

03/23/16 08:26 03/24/16 12:14 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 3.66 (2+/-)

0.446 (2+/-)

1 03/24/16 12:14 03/23/16 08:26 pCi/g 0.235 1.37 RL MDC 0.292 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:26 03/24/16 12:14 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 89 Lab Sample ID: 160-16618-11 Client Sample ID: L08-13-11-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:35 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.24 (2+/-)

0.170 (2+/-)

1 03/27/16 13:17 03/25/16 10:17 pCi/g 0.0821 RL MDC 0.114 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 03/27/16 13:17 1

0.0974 0.0587 0.0586 U

-0.0300 Americium 241 pCi/g 03/25/16 10:17 03/27/16 13:17 1

0.409 0.505 0.470 1.78 Bismuth 212 pCi/g 03/25/16 10:17 03/27/16 13:17 1

0.0705 0.144 0.102 0.982 Bismuth 214 pCi/g 03/25/16 10:17 03/27/16 13:17 1

0.0614 0.165 0.0777 1.13 Lead 212 pCi/g 03/25/16 10:17 03/27/16 13:17 1

0.0713 0.132 0.0841 0.981 Lead 214 pCi/g 03/25/16 10:17 03/27/16 13:17 1

0.283 2.39 1.12 20.6 Potassium 40 pCi/g 03/25/16 10:17 03/27/16 13:17 1

1.12 0.281 0.273 U

0.632 Protactinium 231 pCi/g 03/25/16 10:17 03/27/16 13:17 1

0.0705 1.00 0.144 0.102 0.982 Radium 226 pCi/g 03/25/16 10:17 03/27/16 13:17 1

0.766 1.00 0.307 0.277 1.26 Thorium 234 TestAmerica St. Louis Page 21 of 32 1

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Client Sample Results TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-11 Client Sample ID: L08-13-11-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:35 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte Uranium 235 0.199 U (2+/-)

0.170 (2+/-)

1 03/27/16 13:17 03/25/16 10:17 pCi/g 0.208 RL MDC 0.169 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 03/27/16 13:17 1

5.64 14.6 14.6 U

-0.365 Protactinium 234m pCi/g 03/25/16 10:17 03/27/16 13:17 1

0.0821 0.170 0.114 1.24 Thorium 232 Pb-210 1.52 0.561 0.589 0.736 pCi/g 03/25/16 10:17 03/27/16 13:17 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Tl-208 0.359 0.0445 0.0580 0.0336 pCi/g 03/25/16 10:17 03/27/16 13:17 1

Lab Sample ID: 160-16618-11 Client Sample ID: L08-13-11-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:35 Percent Solids: 80.7 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00011 0.000070 0.000021 mg/Kg

03/23/16 08:26 03/24/16 12:18 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.87 (2+/-)

0.263 (2+/-)

1 03/24/16 12:18 03/23/16 08:26 pCi/g 0.241 1.41 RL MDC 0.200 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:26 03/24/16 12:18 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 86 Lab Sample ID: 160-16618-12 Client Sample ID: L08-13-11-T-E-Q-00 Matrix: Solid Date Collected: 03/18/16 14:35 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.30 (2+/-)

0.246 (2+/-)

1 03/27/16 13:19 03/25/16 10:17 pCi/g 0.134 RL MDC 0.207 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 03/27/16 13:19 1

0.0888 0.0523 0.0523 U

-0.00328 Americium 241 pCi/g 03/25/16 10:17 03/27/16 13:19 1

0.396 0.486 0.459 1.54 Bismuth 212 pCi/g 03/25/16 10:17 03/27/16 13:19 1

0.0674 0.155 0.110 1.05 Bismuth 214 pCi/g 03/25/16 10:17 03/27/16 13:19 1

0.0719 0.173 0.0876 1.15 Lead 212 pCi/g 03/25/16 10:17 03/27/16 13:19 1

0.0871 0.148 0.0980 1.07 Lead 214 pCi/g 03/25/16 10:17 03/27/16 13:19 1

0.400 2.44 1.32 20.1 Potassium 40 pCi/g 03/25/16 10:17 03/27/16 13:19 1

1.14 0.693 0.691 U

-0.512 Protactinium 231 pCi/g 03/25/16 10:17 03/27/16 13:19 1

0.0674 1.00 0.155 0.110 1.05 Radium 226 pCi/g 03/25/16 10:17 03/27/16 13:19 1

0.822 1.00 0.535 0.521 1.18 Thorium 234 pCi/g 03/25/16 10:17 03/27/16 13:19 1

0.242 0.144 0.144 U

0.0567 Uranium 235 pCi/g 03/25/16 10:17 03/27/16 13:19 1

6.01 3.59 3.58 U

2.22 Protactinium 234m pCi/g 03/25/16 10:17 03/27/16 13:19 1

0.134 0.246 0.207 1.30 Thorium 232 TestAmerica St. Louis Page 22 of 32 1

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Client Sample Results TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-12 Client Sample ID: L08-13-11-T-E-Q-00 Matrix: Solid Date Collected: 03/18/16 14:35 Date Received: 03/22/16 10:45 Tl-208 0.374 0.0585 0.0702 0.0447 pCi/g 03/25/16 10:17 03/27/16 13:19 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

Lab Sample ID: 160-16618-12 Client Sample ID: L08-13-11-T-E-Q-00 Matrix: Solid Date Collected: 03/18/16 14:35 Percent Solids: 80.2 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000073 0.000069 0.000021 mg/Kg

03/23/16 08:26 03/24/16 12:22 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.25 (2+/-)

0.125 (2+/-)

1 03/24/16 12:22 03/23/16 08:26 pCi/g 0.236 1.38 RL MDC 0.0472 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:26 03/24/16 12:22 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 89 Lab Sample ID: 160-16618-13 Client Sample ID: L08-13-12-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:30 Date Received: 03/22/16 10:45 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte Actinium 228 1.05 (2+/-)

0.155 (2+/-)

1 03/27/16 13:51 03/25/16 10:17 pCi/g 0.0684 RL MDC 0.112 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

pCi/g 03/25/16 10:17 03/27/16 13:51 1

0.107 0.0637 0.0637 U

-0.00701 Americium 241 pCi/g 03/25/16 10:17 03/27/16 13:51 1

0.275 0.337 0.314 1.18 Bismuth 212 pCi/g 03/25/16 10:17 03/27/16 13:51 1

0.0667 0.127 0.0939 0.820 Bismuth 214 pCi/g 03/25/16 10:17 03/27/16 13:51 1

0.0603 0.145 0.0727 0.970 Lead 212 pCi/g 03/25/16 10:17 03/27/16 13:51 1

0.0706 0.142 0.0964 0.999 Lead 214 pCi/g 03/25/16 10:17 03/27/16 13:51 1

0.267 2.16 1.05 18.4 Potassium 40 pCi/g 03/25/16 10:17 03/27/16 13:51 1

1.09 0.153 0.152 U

0.193 Protactinium 231 pCi/g 03/25/16 10:17 03/27/16 13:51 1

0.0667 1.00 0.127 0.0939 0.820 Radium 226 pCi/g 03/25/16 10:17 03/27/16 13:51 1

0.814 1.00 0.295 0.280 0.878 Thorium 234 pCi/g 03/25/16 10:17 03/27/16 13:51 1

0.226 0.118 0.118 U

0.110 Uranium 235 pCi/g 03/25/16 10:17 03/27/16 13:51 1

4.53 1.79 1.78 U

0.854 Protactinium 234m pCi/g 03/25/16 10:17 03/27/16 13:51 1

0.0684 0.155 0.112 1.05 Thorium 232 Tl-208 0.345 0.0452 0.0577 0.0325 pCi/g 03/25/16 10:17 03/27/16 13:51 1

(2+/-)

(2+/-)

MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.

Uncert.

TestAmerica St. Louis Page 23 of 32 1

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Client Sample Results TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Lab Sample ID: 160-16618-13 Client Sample ID: L08-13-12-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 14:30 Percent Solids: 83.1 Date Received: 03/22/16 10:45 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00058 0.000068 0.000020 mg/Kg

03/23/16 08:26 03/24/16 12:26 1

Analyte Dil Fac Analyzed Prepared Unit D

Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 10.0 (2+/-)

1.07 (2+/-)

1 03/24/16 12:26 03/23/16 08:26 pCi/g 0.234 1.37 RL MDC 0.539 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.

Uncert.

Re 30 - 110 Carrier 03/23/16 08:26 03/24/16 12:26 1

Dil Fac Analyzed Prepared Qualifier Limits

%Yield 89 TestAmerica St. Louis Page 24 of 32 1

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QC Sample Results TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-241768/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242133 Prep Batch: 241768 RL MDL Technetium 99 ND 0.000053 0.000016 mg/Kg 03/23/16 08:26 03/24/16 10:49 1

MB MB Analyte Dil Fac Analyzed Prepared D

Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-241768/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242133 Prep Batch: 241768 Technetium 99 0.00119 0.00125 mg/Kg 105 80 - 120 Analyte LCS LCS D

Unit Result Qualifier

%Rec Spike Added

%Rec.

Limits Client Sample ID: L08-13-01-T-E-S-00 Lab Sample ID: 160-16618-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 242133 Prep Batch: 241768 Technetium 99 0.0015 F1 0.00139 0.00186 F1 mg/Kg 23 75 - 125

Analyte MS MS D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Client Sample ID: L08-13-01-T-E-S-00 Lab Sample ID: 160-16618-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 242133 Prep Batch: 241768 Technetium 99 0.0015 F1 0.00143 0.00201 F1 mg/Kg 34 75 - 125 8

30

Analyte MSD MSD D

Unit Result Qualifier

%Rec Spike Added Sample Result Sample Qualifier

%Rec.

Limits Limit RPD RPD Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-241768/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242134 Prep Batch: 241768 Technetium 99 Analyte U

1 03/24/16 10:49 03/23/16 08:26 pCi/g 0.183 MDC 1.07 RL 0.0587 0.0586 (2+/-)

(2+/-)

MB 0.04217 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Carrier Re 30 - 110 03/23/16 08:26 03/24/16 10:49 1

Dil Fac Prepared Analyzed Qualifier Limits

%Yield 94 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-241768/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242134 Prep Batch: 241768 Technetium 99 Analyte 120 80 105 21.44 20.4 2.36 1.08 0.185 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Re Carrier 30 - 110 LCS Qualifier Limits

%Yield 93 LCS TestAmerica St. Louis Page 25 of 32 1

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QC Sample Results TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)

Client Sample ID: L08-13-01-T-E-S-00 Lab Sample ID: 160-16618-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 242134 Prep Batch: 241768 Technetium 99 Analyte 125 75 23 F1 31.83 23.8 26.2 3.18 1.34 0.229 RL MDC (2+/-)

MS MS pCi/g Unit Result Qual

%Rec Added Spike Result Sample Sample Qual Limits

%Rec.

Uncert.

Total Re Carrier 30 - 110 MS Qualifier Limits

%Yield 88 MS Client Sample ID: L08-13-01-T-E-S-00 Lab Sample ID: 160-16618-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 242134 Prep Batch: 241768 Technetium 99 Analyte 1

0.41 125 75 34 F1 34.48 24.4 26.2 3.31 1.34 0.230 RL MDC (2+/-)

MSD MSD pCi/g Unit Result Qual

%Rec Limit Added Spike Result Sample Sample Qual Limits

%Rec.

Uncert.

Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits

%Yield 89 MSD Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Client Sample ID: Method Blank Lab Sample ID: MB 160-242185/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242406 Prep Batch: 242185 Actinium 228 Analyte U

1 03/26/16 19:45 03/25/16 10:09 pCi/g 0.0414 MDC RL 0.00948 0.00948 (2+/-)

(2+/-)

MB 0.001431 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.0144 0.00726 0.00726 U

0.0008751 Americium 241 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.200 0.0963 0.0963 U

0.009725 Bismuth 212 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.0642 0.0241 0.0241 U

-0.003331 Bismuth 214 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.0342 0.367 0.367 U

-0.009185 Lead 212 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.0324 0.0144 0.0144 U

0.0001966 Lead 214 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.274 2.48 2.48 U

-0.06207 Potassium 40 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.265 0.0606 0.0606 U

0.0000 Protactinium 231 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.0642 1.00 0.0241 0.0241 U

-0.003331 Radium 226 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.275 1.00 0.136 0.136 U

0.05337 Thorium 234 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.0690 0.0719 0.0719 U

-0.004786 Uranium 235 1

03/26/16 19:45 03/25/16 10:09 pCi/g 1.90 15.2 15.2 U

-0.3801 Protactinium 234m 1

03/26/16 19:45 03/25/16 10:09 pCi/g 0.0414 0.00948 0.00948 U

0.001431 Thorium 232 Other Detected Radionuclide None MB (2+/-)

(2+/-)

MDC RL pCi/g 03/25/16 10:09 03/26/16 19:45 1

MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Radionuclides Other Detected TestAmerica St. Louis Page 26 of 32 1

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QC Sample Results TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-242185/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242401 Prep Batch: 242185 Americium 241 Analyte 116 87 98 98.98 101 10.3 0.517 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 34.1 33.22 3.48 0.200 0.144 pCi/g 97 87 - 120 Cobalt 60 31.8 30.25 3.05 0.132 pCi/g 95 87 - 115 Client Sample ID: Duplicate Lab Sample ID: 160-16616-A-1-G DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 242398 Prep Batch: 242185 Actinium 228 Analyte 1

0.03 1.106 1.12 0.160 0.108 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Americium 241 0.00470 U 0.03218 U 0.0505 0.0749 pCi/g 0.24 1

Bismuth 212 0.822 0.9261 0.360 0.485 pCi/g 0.14 1

Bismuth 214 0.920 0.8284 0.127 0.0670 pCi/g 0.34 1

Lead 212 1.12 1.169 0.171 0.0616 pCi/g 0.13 1

Lead 214 1.00 1.058 0.138 0.0538 pCi/g 0.20 1

Potassium 40 19.4 19.92 2.37 0.483 pCi/g 0.12 1

Protactinium 231 0.658 U 0.4408 U 0.225 1.08 pCi/g 0.39 1

Radium 226 0.920 0.8284 0.127 1.00 0.0670 pCi/g 0.34 1

Thorium 234 1.21 1.933 0.556 1.00 0.708 pCi/g 0.80 1

Uranium 235 0.434 0.4480 0.188 0.194 pCi/g 0.04 1

Protactinium 234m 2.54 U 1.610 U 2.84 4.78 pCi/g 0.15 1

Thorium 232 1.12 1.106 0.160 0.108 pCi/g 0.03 1

Pb-210 1

0.74 0.9261 1.82 0.554 0.758 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

RER RER Total Other Detected Radionuclides Tl-208 0.366 0.3813 0.0649 0.0390 pCi/g 0.12 1

Client Sample ID: Method Blank Lab Sample ID: MB 160-242186/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242401 Prep Batch: 242186 Actinium 228 Analyte U

1 03/26/16 22:42 03/25/16 10:17 pCi/g 0.0431 MDC RL 0.0231 0.0230 (2+/-)

(2+/-)

MB 0.01796 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total 1

03/26/16 22:42 03/25/16 10:17 pCi/g 0.0283 0.00553 0.00553 U

0.0000 Americium 241 1

03/26/16 22:42 03/25/16 10:17 pCi/g 0.162 0.0855 0.0855 U

-0.01549 Bismuth 212 1

03/26/16 22:42 03/25/16 10:17 pCi/g 0.0333 0.000308 0.000307 U

-0.0001777 Bismuth 214 1

03/26/16 22:42 03/25/16 10:17 pCi/g 0.0214 0.192 0.192 U

-0.01085 Lead 212 1

03/26/16 22:42 03/25/16 10:17 pCi/g 0.0314 0.0140 0.0140 U

-0.002635 Lead 214 1

03/26/16 22:42 03/25/16 10:17 pCi/g 0.173 2.63 2.63 U

-0.06570 Potassium 40 1

03/26/16 22:42 03/25/16 10:17 pCi/g 0.321 0.176 0.176 U

-0.02543 Protactinium 231 1

03/26/16 22:42 03/25/16 10:17 pCi/g 0.0333 1.00 0.000308 0.000307 U

-0.0001777 Radium 226 1

03/26/16 22:42 03/25/16 10:17 pCi/g 0.236 1.00 0.134 0.134 U

-0.01194 Thorium 234 1

03/26/16 22:42 03/25/16 10:17 pCi/g 0.0533 0.573 0.573 U

-0.006775 Uranium 235 1

03/26/16 22:42 03/25/16 10:17 pCi/g 2.30 4.66 4.66 U

-0.5363 Protactinium 234m TestAmerica St. Louis Page 27 of 32 1

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QC Sample Results TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Client Sample ID: Method Blank Lab Sample ID: MB 160-242186/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242401 Prep Batch: 242186 Thorium 232 Analyte U

1 03/26/16 22:42 03/25/16 10:17 pCi/g 0.0431 MDC RL 0.0231 0.0230 (2+/-)

(2+/-)

MB 0.01796 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Other Detected Radionuclide None MB (2+/-)

(2+/-)

MDC RL pCi/g 03/25/16 10:17 03/26/16 22:42 1

MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.

Count Uncert.

Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-242186/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242404 Prep Batch: 242186 Americium 241 Analyte 116 87 101 101.7 101 10.6 0.499 RL MDC (2+/-)

LCS LCS pCi/g Unit Result Qual

%Rec Added Spike Limits

%Rec.

Uncert.

Total Cesium 137 34.1 33.92 3.55 0.200 0.175 pCi/g 100 87 - 120 Cobalt 60 31.8 31.15 3.15 0.111 pCi/g 98 87 - 115 Client Sample ID: L08-13-02-T-E-S-00 Lab Sample ID: 160-16618-2 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 242406 Prep Batch: 242186 Actinium 228 Analyte 1

0.01 1.145 1.14 0.193 0.113 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

Total RER RER Americium 241

-0.00416 U 0.03285 U 0.0665 0.111 pCi/g 0.17 1

Bismuth 212 1.43 1.045 0.432 0.424 pCi/g 0.49 1

Bismuth 214 0.972 0.9215 0.145 0.0673 pCi/g 0.18 1

Lead 212 1.12 1.073 0.162 0.0658 pCi/g 0.14 1

Lead 214 1.02 0.9782 0.138 0.0823 pCi/g 0.17 1

Potassium 40 19.7 18.30 2.29 0.363 pCi/g 0.30 1

Protactinium 231

-0.530 U 0.4918 U 0.303 1.34 pCi/g 1.04 1

Radium 226 0.972 0.9215 0.145 1.00 0.0673 pCi/g 0.18 1

Thorium 234 1.05 1.012 0.337 1.00 0.834 pCi/g 0.04 1

Uranium 235 0.0873 U 0.09470 U 0.152 0.256 pCi/g 0.02 1

Protactinium 234m 2.63 U 5.657 U 2.75 7.01 pCi/g 0.57 1

Thorium 232 1.14 1.145 0.193 0.113 pCi/g 0.01 1

Pb-210 1

0.32 0.9675 1.36 0.678 0.879 RL MDC (2+/-)

DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.

RER RER Total Other Detected Radionuclides Tl-208 0.384 0.3164 0.0601 0.0400 pCi/g 0.57 1

TestAmerica St. Louis Page 28 of 32 1

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QC Association Summary TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Metals Prep Batch: 241768 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-16618-1 L08-13-01-T-E-S-00 Total/NA Solid None 160-16618-1 MS L08-13-01-T-E-S-00 Total/NA Solid None 160-16618-1 MSD L08-13-01-T-E-S-00 Total/NA Solid None 160-16618-2 L08-13-02-T-E-S-00 Total/NA Solid None 160-16618-3 L08-13-03-T-E-S-00 Total/NA Solid None 160-16618-4 L08-13-04-T-E-S-00 Total/NA Solid None 160-16618-5 L08-13-05-T-E-S-00 Total/NA Solid None 160-16618-6 L08-13-06-T-E-S-00 Total/NA Solid None 160-16618-7 L08-13-07-T-E-S-00 Total/NA Solid None 160-16618-8 L08-13-08-T-E-S-00 Total/NA Solid None 160-16618-9 L08-13-09-T-R-S-00 Total/NA Solid None 160-16618-10 L08-13-10-T-E-S-00 Total/NA Solid None 160-16618-11 L08-13-11-T-E-S-00 Total/NA Solid None 160-16618-12 L08-13-11-T-E-Q-00 Total/NA Solid None 160-16618-13 L08-13-12-T-E-S-00 Total/NA Solid None LCS 160-241768/2-A Lab Control Sample Total/NA Solid None MB 160-241768/1-A Method Blank Total/NA Analysis Batch: 242133 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 241768 160-16618-1 L08-13-01-T-E-S-00 Total/NA Solid 6020A 241768 160-16618-1 MS L08-13-01-T-E-S-00 Total/NA Solid 6020A 241768 160-16618-1 MSD L08-13-01-T-E-S-00 Total/NA Solid 6020A 241768 160-16618-2 L08-13-02-T-E-S-00 Total/NA Solid 6020A 241768 160-16618-3 L08-13-03-T-E-S-00 Total/NA Solid 6020A 241768 160-16618-4 L08-13-04-T-E-S-00 Total/NA Solid 6020A 241768 160-16618-5 L08-13-05-T-E-S-00 Total/NA Solid 6020A 241768 160-16618-6 L08-13-06-T-E-S-00 Total/NA Solid 6020A 241768 160-16618-7 L08-13-07-T-E-S-00 Total/NA Solid 6020A 241768 160-16618-8 L08-13-08-T-E-S-00 Total/NA Solid 6020A 241768 160-16618-9 L08-13-09-T-R-S-00 Total/NA Solid 6020A 241768 160-16618-10 L08-13-10-T-E-S-00 Total/NA Solid 6020A 241768 160-16618-11 L08-13-11-T-E-S-00 Total/NA Solid 6020A 241768 160-16618-12 L08-13-11-T-E-Q-00 Total/NA Solid 6020A 241768 160-16618-13 L08-13-12-T-E-S-00 Total/NA Solid 6020A 241768 LCS 160-241768/2-A Lab Control Sample Total/NA Solid 6020A 241768 MB 160-241768/1-A Method Blank Total/NA General Chemistry Analysis Batch: 241632 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-16618-1 L08-13-01-T-E-S-00 Total/NA Solid Moisture 160-16618-2 L08-13-02-T-E-S-00 Total/NA Solid Moisture 160-16618-3 L08-13-03-T-E-S-00 Total/NA Solid Moisture 160-16618-4 L08-13-04-T-E-S-00 Total/NA Solid Moisture 160-16618-5 L08-13-05-T-E-S-00 Total/NA Solid Moisture 160-16618-6 L08-13-06-T-E-S-00 Total/NA Solid Moisture 160-16618-7 L08-13-07-T-E-S-00 Total/NA Solid Moisture 160-16618-8 L08-13-08-T-E-S-00 Total/NA TestAmerica St. Louis Page 29 of 32 1

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General Chemistry (Continued)

Analysis Batch: 241632 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-16618-9 L08-13-09-T-R-S-00 Total/NA Solid Moisture 160-16618-10 L08-13-10-T-E-S-00 Total/NA Solid Moisture 160-16618-11 L08-13-11-T-E-S-00 Total/NA Solid Moisture 160-16618-12 L08-13-11-T-E-Q-00 Total/NA Solid Moisture 160-16618-13 L08-13-12-T-E-S-00 Total/NA Solid Moisture 160-16618-13 DU L08-13-12-T-E-S-00 Total/NA Rad Leach Batch: 241584 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-16616-A-1-G DU Duplicate Total/NA Solid Dry and Grind 160-16618-1 L08-13-01-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-2 L08-13-02-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-2 DU L08-13-02-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-3 L08-13-03-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-4 L08-13-04-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-5 L08-13-05-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-6 L08-13-06-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-7 L08-13-07-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-8 L08-13-08-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-9 L08-13-09-T-R-S-00 Total/NA Solid Dry and Grind 160-16618-10 L08-13-10-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-11 L08-13-11-T-E-S-00 Total/NA Solid Dry and Grind 160-16618-12 L08-13-11-T-E-Q-00 Total/NA Solid Dry and Grind 160-16618-13 L08-13-12-T-E-S-00 Total/NA Prep Batch: 241768 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-16618-1 L08-13-01-T-E-S-00 Total/NA Solid None 160-16618-1 MS L08-13-01-T-E-S-00 Total/NA Solid None 160-16618-1 MSD L08-13-01-T-E-S-00 Total/NA Solid None 160-16618-2 L08-13-02-T-E-S-00 Total/NA Solid None 160-16618-3 L08-13-03-T-E-S-00 Total/NA Solid None 160-16618-4 L08-13-04-T-E-S-00 Total/NA Solid None 160-16618-5 L08-13-05-T-E-S-00 Total/NA Solid None 160-16618-6 L08-13-06-T-E-S-00 Total/NA Solid None 160-16618-7 L08-13-07-T-E-S-00 Total/NA Solid None 160-16618-8 L08-13-08-T-E-S-00 Total/NA Solid None 160-16618-9 L08-13-09-T-R-S-00 Total/NA Solid None 160-16618-10 L08-13-10-T-E-S-00 Total/NA Solid None 160-16618-11 L08-13-11-T-E-S-00 Total/NA Solid None 160-16618-12 L08-13-11-T-E-Q-00 Total/NA Solid None 160-16618-13 L08-13-12-T-E-S-00 Total/NA Solid None LCS 160-241768/2-A Lab Control Sample Total/NA Solid None MB 160-241768/1-A Method Blank Total/NA Prep Batch: 242185 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 241584 160-16616-A-1-G DU Duplicate Total/NA TestAmerica St. Louis Page 30 of 32 1

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QC Association Summary TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Rad (Continued)

Prep Batch: 242185 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 241584 160-16618-1 L08-13-01-T-E-S-00 Total/NA Solid Fill_Geo-0 LCS 160-242185/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-242185/1-A Method Blank Total/NA Prep Batch: 242186 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 241584 160-16618-2 L08-13-02-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16618-2 DU L08-13-02-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16618-3 L08-13-03-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16618-4 L08-13-04-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16618-5 L08-13-05-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16618-6 L08-13-06-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16618-7 L08-13-07-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16618-8 L08-13-08-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16618-9 L08-13-09-T-R-S-00 Total/NA Solid Fill_Geo-0 241584 160-16618-10 L08-13-10-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16618-11 L08-13-11-T-E-S-00 Total/NA Solid Fill_Geo-0 241584 160-16618-12 L08-13-11-T-E-Q-00 Total/NA Solid Fill_Geo-0 241584 160-16618-13 L08-13-12-T-E-S-00 Total/NA Solid Fill_Geo-0 LCS 160-242186/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-242186/1-A Method Blank Total/NA TestAmerica St. Louis Page 31 of 32 1

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Tracer/Carrier Summary TestAmerica Job ID: 160-16618-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110)

Re 87 160-16618-1 Percent Yield (Acceptance Limits)

L08-13-01-T-E-S-00 88 160-16618-1 MS L08-13-01-T-E-S-00 89 160-16618-1 MSD L08-13-01-T-E-S-00 90 160-16618-2 L08-13-02-T-E-S-00 89 160-16618-3 L08-13-03-T-E-S-00 88 160-16618-4 L08-13-04-T-E-S-00 86 160-16618-5 L08-13-05-T-E-S-00 87 160-16618-6 L08-13-06-T-E-S-00 86 160-16618-7 L08-13-07-T-E-S-00 88 160-16618-8 L08-13-08-T-E-S-00 90 160-16618-9 L08-13-09-T-R-S-00 89 160-16618-10 L08-13-10-T-E-S-00 86 160-16618-11 L08-13-11-T-E-S-00 89 160-16618-12 L08-13-11-T-E-Q-00 89 160-16618-13 L08-13-12-T-E-S-00 93 LCS 160-241768/2-A Lab Control Sample 94 MB 160-241768/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 32 of 32 1

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