IR 05000409/1986016

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Forwards Safety Insp Rept 50-409/86-16 on 861208-12,15 & 16. No Violations Noted
ML20207N281
Person / Time
Site: La Crosse File:Dairyland Power Cooperative icon.png
Issue date: 01/08/1987
From: Shafer W
NRC OFFICE OF INSPECTION & ENFORCEMENT (IE REGION III)
To: Taylor J
DAIRYLAND POWER COOPERATIVE
References
NUDOCS 8701140097
Download: ML20207N281 (2)


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JAN 8 1987 Docket No. 50-409 Dairyland Power Cooperative ATTN: Mr. J. W. Taylor General Manager 2615 East Avenue - South La Crosse, WI 54601 Gentlemen:

This refers to the routine safety inspection conducted by A. G. Januska of this office on December 8-12,15 and 16,1986 of activities at La Crosse Boiling Water Reactor (LACBWR) authorized by Nuclear Regulatory Commission Operating License No. DPR-45 and to the discussion of our findings with Mr. G. Boyd and others of your staff at the conclusion of the inspection.

'

The enclosed copy of our inspection report identifies areas examined during the inspection. Within these areas, the inspection consisted of a sulective examination of procedures and representative records, observations, and interviews with personnel.

In addition, our Mobile Laboratory was at the site (

during the inspection to perform independent measurements of radioactivity.

No violations of NRC requirements were identified during the course of this inspection.

In accordance with 10 CFR 2.790 of the Commission's regulations, a copy of this letter and the enclosed inspection report will be placed in the NRC Public Document Room.

We will gladly discuss any questions you have concerning this inspection.

Sincerely 3' Original ai;0d by U.D. Shafer2'

8701140097 870108 PDR ADDCK 05000409 O

PDR W. D. Shafer, Chief Emergency Preparedness and Radiological Protection Branch

Enclosure:

Inspection Report

No. 50-409/86016(DRSS)

See Attached Distribution

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Dairyland Power Cooperative

JAN

8 1987

Distribution

REGION III==

Report No. 50-409/86016(DRSS)

Docket No. 50-409

License No. DPR-45

Licensee: Dairyland Power Cooperative

2615 East Avenue - South

La Crosse, WI 54601

Facility Name:

Lacrosse Boiling Water Reactor (LACBWR)

Inspection At:

LACBWR, Genoa, Wisconsin

Inspection Conducted: December 8-16, 1986

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Inspector:

A.G.bnuska

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Date

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Approved By:

M. Schumacher, Chief

Radiological Effluents and

Date

Chemistry Section

Inspection Summary

Inspection on December 8-16, 1986 (Inspection Report No. 50-409/86016(DRSS))

Areas Inspected:

Routine unannounced inspection of (1) the confirmatory

measurements program including sample split and onsite analysis with the

Region III Mobile Laboratory, (2) the radiological environmental monitoring

program and (3) open items identified during previous inspections.

Results: No violations or deviations were identified.

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DETAILS

1.

Persons Contacted

  • G. Boyd, Operations Supervisor
  • L. Nelson, Health and Safety Supervisor
  • P. Shafer, Radiation Protection Engineer
  • R. Wery, Quality Assurance Supervisor

A. Hansen, Senior Health Physics Technician

J. Gaynor, Health Physics Technician

G. Roediger, Health Physics Technician

M. Land, Health Physics Technician

  • Denotes those present at the exit interview on December 12, 1986.

2.

Licensee Action on Previous Inspection Findings

a.

(Closed) Open Item (409/84015-05): Evaluate the effect of high

alpha efficiency on effluent data for 1984. The licensee prepared

an Am-241 standard and determined a new counter efficiency. An

appropriate correction factor was applied to the first and second

quarter 1984 effluent results which had already been submitted in

a semiannual report. The corrected values for the first and second

quarter, along with the third and fourth quarter results, were

published in the 1984 Radioactive Effluent Report,

b.

(Closed) Open Item (409/85021-01):

Continue efforts to solve

chloride analytical problem. The licensee has continued to

evaluate the chloride problem since the last inspection and has

revised both technique and procedure. More rigid routine probe

maintenance has been implemented to compensate for drift which was

thought to be a significant part of the problem. A 20 minute test

using laboratory demineralized water must result in less than

a 2mV drift before a standard check on a 20, 40, 80, 120, or

160 ppb standard can be run. Although no finite numerical

acceptance range has been determined corrective measures are taken

based on management review. The inspector examined results for

the first, second, and third quarters of 1986 for the analytical

chemistry cross check with DPC Central Lab on chloride measurements.

Results for the three quarters show an improvement over previous

tests.

c.

(0 pen) Open Item (409/85021-02):

Analyze split sample for beta,

gamma, H-3, Sr-89, and Sr-90 and report results to Region III.

Results of the sample comparisons are listed in Table 2; comparison

criteria are given in Attachment 1.

The lone disagreement, Sr-90,

was from the portion of the sample analyzed by the licensee's

environmental contractor.

In order to determine the validity of

the result the licensee purchased a spike and had it analyzed by

the contractor. Results of the analysis were not available at the

close of the inspection. This item will remain open until the

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results are submitted to Region III.

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3.

Confirmatory Measurements

Seven samples (air particulate, charcoal, retention tank, gas, reactor

coolant and two spike particulates) were analyzed for gamma emitting

isotopes by the licensee and in the Region III mobile laboratory onsite.

Results are listed in Table 1.

The licensee achieved 40 agreements out

of 41 comparisons.

A stack air particulate filter counted yielded only one nuclide, Co-60,

which was not used for comparison because of poor counting statistics.

To check this geometry, the licensee's calibration standard was counted

and analyzed as an unknown (F SPIKED LIC). The inspector relaxed the

test criteria because of the differences in the NRC and licensee's

calibration. Although this resulted in agreements, the NRC's spiked

air particulate was counted (F SPIKED NRC) because of an apparent

conservative bias which was also observed in a previous inspection. A

gas sample analyzed resulted in a disagreement for Xe-135. As no reason

could be found for the disagreement, the licensee agreed to (1) prepare a

new standard, analyze it as an unknown and examine the 249 and 608 kev

areas and (2) generate a new efficiency curve to be compared with the

current curve before the next off gas sample is collected (0 pen Item

409/86016-01).

In addition to the disagreement, the analysis also

indicated a conservative bias. Discussion with the licensee revealed

that these calibrations were performed using a liquid to simulate the

particulate filter and the gas.

Liquid calibrations did not exhibit this

bias. The licensee stated that the use of air particulate and gas

standards supplied by an independent manufacturer will be evaluated (0 pen

Item 409/86016-02) and purchased if determined to be advantageous. A

reactor coolant sample split with the licensee initially resulted in

eight disagreements in 19 comparisons. The results averaged 20%

nonconservative with only two comparisons being conservative. Multiple

liquid geometries were compared by both the licensee and the NRC on

portions of the sane initial sample.

It was finally determined that some

of the sample preferentially adhered to the NRC's plastic bottle and not

the licensee's glass vial for the short period between putting the sample

in the containers and adding dilution water. Another split, made adding

the sample to dilution water already in the respective containers, resulted

in all agreements.

The licensee agreed to analyze a portion of a retention tank sample

(L WASTE) for gross S, tritium, strontium-89 and strontium-90 and

submit the results to Region III (0 pen Item 409/86016-03).

4.

Quality Control of Measurements

The licensee participates in cross check programs for inplant

measurements with a commercial contractor and for environmental

measurements with the EPA. Results of the annual inplant analyses

for 1986 were examined and found to be in complete agreement.

Quality Assurance Audit Report 70-86-1, conducted August 11 through

September 29, 1986, was examined. No findings were noted in the

[

Analytical Chemistry section of the audit.

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5.

Radiolegical Environmental Monitoring Program

The inspector examined five environmental air sample stations in the

company of a licensee representative during a normal scheduled sample

change. All stations were operating and in good repair. The

representative appeared very knowledgeable about sample change

requirements.

The inspector reviewed the 1985 Radiological Environmental Monitoring

Report. The program is conducted as required by Technical Specifications.

The results do not indicate a significant effect due to the operation of

the plant. Although there were disagreements between the licensee and

the State of Wisconsin for tritium in water samples, the licensee's

values were less than the NRC LLD requirements in all but one instance.

The licensee changed gross counting equipment during the period which

resulted in closer agreement with the State.

6.

Open Items

Open items are matters which have been discussed with the licensee, which

will be reviewed further by the inspector, and which involve some action

on the part of the NRC or licensee or both. Open items identified during

the inspection are discussed in Section 3.

7.

Exit Interview

The inspector met with licensee representatives denotes in Section 1 on

December 12, 1986. The scope and findings were discussed. The licensee

acknowledged the need to resolve the bias in the air particulate and gas

geometries and agreed to count a portion of the retention tank sample and

report the results to Region III.

During the exit interview, the inspector discussed the likely

informational content of the inspection report with regard to documents

or processes reviewed by the inspector during the inspection.

Licensee

representatives did not identify any such documents or processes as

proprietary.

Attachments:

1.

Table 1, Confirmatory Measurements

Program Results, 4th Quarter 1986

2.

Table 2, Confirmatory Measurements

Program Results, 4th Quarter 1985

3.

Attachment 1, Criteria for Comparing

Analytical Measurements

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TABLE 1

U S NUCLEAR REGULATORY COMMISSION

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OFFICE'OF INSPECTION AND ENFORCEMENT

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CONFIRMATORY MEASUREMENTS. PROGRAM

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FACILITY: LACBWR

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FOR THE 4 QUARTER OF 1986

NRC-

--


LICENSEE----

---LICENSEE:NRC----

SAMPLE

ISOTOPE RESULT

ERROR'

RESULT

ERROR

RATIO

RES

T

L WASTE

NN-54

4.5E-05

6.9E-07

4.3E-05

4.OE-07

9.6E-01

6.5E 01

A

C O - 5 8 J-

1.8E-06

3.5E-07

1.6E-06

1.8E-07

8.9E-01

5.1E 00

A

CO-60

1.5E-04

1.OE-06

1.4E-04

7.2E-07

9.3E-01

1.5E O2

A

NP-239

5.8E-06

5.1E-07

6.3E-06

7.1E-07

1.1E 00

1.1E 01

A

SR-91

1.3E-05

2.2E-06

7.9E-06

8.8E-07

6.1E-01

5.9E 00

A

SR-92

1.5E-06

4.8E-07

2.OE-06

1.9E-07

1.3E 00

3.1E 00

A

CS-137

1.6E-05

5.OE-07

1.5E-05

2.9E-07

9.4E-01

3.2E 01

.A

LA-140

2.5E-06

2.1E-07

2.3E-06

1.4E-07

9.2E-01

1.2E 01

A

OFF GAS

KR-85M

4.6E-03

7.5E-05

5.OE-03

1.5E-05

1.1E 00

6.1E 01

A

KR-88

1.5E-02

1.OE-03

1.8E-02

8.9E-05

1.2E 00

1.5E 01

A

XE-133

2.2E-03

1.2E-05

2.6E-03

1.OE-05

1.2E 00

1.8E O2

A

XE-133M 1.5E-04

2.5E-05

1.8E-04

2.OE-05

1.2E 00

6.OE 00

A

XE-135

2.7E-02

5.1E-05

3.6E-02

2.5E-05

1.3E 00

5.3E O2

D.

C FILTER I-131

1.1E-11

2.3E-13

1.OE-11

1.2E-13

9.1E-01

4.8E 01

A

I-133

2.7E-11

3.SE-13

2.5E-11

1.8E-13

9.3E-01

7.1E 01

A

I-135

1.7E-11

1.2E-12

1.8E-11

4.7E-13

1.1E 00

1.4E 01

A

F SPIKED CO-57

1.OE-03

3.1E-05

1.4E-03

3.5E-05

1.4E 00

3.2E 01

A*

LIC

CO-60

6.1E-03

1.6E-04

7.1E-03

1.9E-03

1.2E 00

3.8E 01

A*

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Y-88

7.6E-03

1.8E-04

1.2E-02

2.SE-04

1.6E 00

4.2E 01

A*

CD-109

2.OE-02

6.7E-04

2.9E-02

8.OE-04

1.5E 00

3.OE 01

A*

SN-113

4.4E-03

1.OE-04

6.1E-03

1.3E-04

1.4E 00

4.4E 01

A*

CS-137

7.OE-03

1.6E-04

8.1E-03

1.6E-04

1.2E 00

4.4E 01

A*

CE-139

1.1E-03

3.5E-05

1.7E-03

4.5E-05

1.5E 00

3.1E 01

A+

PRIMARY

CR-51

6.3E-03

5.1E-04

7.2E-03

4.1E-04

1.1E 00

1.2E 01

A

MN-54

4.5E-03

1.2E-04

4.2E-03

1.1E-04

9.3E-01

3.7E 01

A

FE-59

2.6E-03

2.OE-04

2.8E-03

1.9E-04

1.1E 00

1.3E 01

A

CO-58

3.7E-03

1.4E-04

3.5E-03

1.1E-04

9.5E-01

2.6E 01

A

CO-60

1.6E-02

1.8E-04

  • 1.3E-02

2.1E-04

8.1E-01

8.9E 01

A

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T TEST RESULTS:

A= AGREEMENT

D= DISAGREEMENT

o= CRITERIA RELAXED

N=NO COMPARISON

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TABLE 1

U S NUCLEAR REGULATORY COMMISSION

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OFFICE'OF INSPECTION AND ENFORCEMENT

CONFIRMATORY MEASUREMENTS, PROGRAM

-

FACILITY: LACBWR

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FOR THE 4 QUARTER OF 1986


NRC-------


LICENSEE----

---LICENSEE:NRC----

SAMPLE _

ISOTOPE RESULT

ERROR

RESULT

ERROR

RATIO

RES

T

PRIMARY-W-187

8.5E-03

5.4E-04

7.1E-03

4.2E-04

8.4E-01

1.6E 01

A

NP-239

5.4E-03

1.9E-04

4.9E-03

3.7E-04

9.1E-01

2.8E 01

A

I-131

2.1E-04

5.4E-05

2.1E-04

4.3E-05

1.OE 00

3.9E 00

A

I-133

6.9E-04

1.6E-04

6.2E-04

1.2E-04

9.OE-01

4.3E 00

A

ZR-97

4.6E-04

1.2E-04

3.8E-04

1.1E-04

8.3E-01

3.8E 00

A

RU-103

8.5E-04

7.OE-05

6.2E-04

5.8E-05

7.3E-01

1.2E 01

A

BA-140

2.oE-03

2.OE-04

2.OE-03

2.7E-04

1.OE 00

1.OE 01

A

CE-141

3.6E-04

5.1E-05

3.3E-04

3.5E-05

9.2E-01

7.1E 00

A

CE-144

3.4E-03

3.3E-04

2.7E-03

2.OE-04

7.9E-01

1.OE 01

A

F SPIKED CO-57

2.OE-04

3.SE-05

2.4E-04

1.9E-05

1.2E 00 -5.3E 00

A

gge

CO-60

1.5E-02

3.6E-04

1.5E-02

2.6E-04

1.OE 00

4.2E 01

A

CD-109

3.9E-02

1.3E-03

4.7E-02

1.OE-03

1.2E 00

3.OE 01

A

CS-137

1.9E-02

3.5E-04

2.1E-02

2.3E-04

1.1E 00

5.4E 01

A

T TEST RESULTS:

A= AGREEMENT

D= DISAGREEMENT

o= CRITERIA RELAXED

'N=NO COMPARISON

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TABLE'2

U S NUCLEAR REGULATORY COMMISSION

_g n.g

OFFICE OF INSPECTION AND ENFORCEMENT

M k?

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CONFIRMATORY MEASUREMENTS PPOGRAM

-

FACILITY: LACBWR

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FOR THE 4 OUARTER OF 1985


NRC


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LICENSEE----

---LICENSEE:NRC

SAMPLE

ISOTOPE RESULT

ERROR

RESULT

ERROR

RATIO

RES

T

L VASTE

BETA

6.6E-05

2.0E-06

6.0E-05

1.1E-06

9.1E-01

3.3E 01

A

SR-90

5.3E-07

3. 0E- 09

3.5E-07

0.OE-0.1

6.6E-01

1.PE 01

D

CO-58-

3.?E-06

4.0E-07

2.5E-06

1.7E-07

7.7E-01

8.3E 00

A

CO-60

6.4E-05

1.2E-06

7.2E-05

5.4E-07

1.!E 00

5.4E 01

A

CS-137

1.4E-05

4.0E-07

1.5E-05

2.4E-07

1.1E 00

3.5E 01

A

MN-54-

8.1E-06

3. 0E- 07

9.1E-06

2.4E-07

1.1E 00

2.7E 01

A

T TEST RESULTS:

-AsAGREEMENT

D= DISAGREEMENT

  • sCR I TER I A. REL AYED

' NANO COMPARISON

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ATTACHMENT 1

CRITERIA FOR COMPARING ANALYTICAL MEASUREMENTS

This attachment provides criteria for comparing results of capability tests

and verification measurements.

The criteria are based on an empirical

relationship which combines prior experience and the accuracy needs of this

program.

In these criteria, the judgment limits are variable in relation to the comparison

of the NRC's value to its associated one sigma uncertainty.

As that ratio,

referred to in this program as " Resolution", increases, the acceptability of a

licensee's measurement should be more selective.

Conversely, poorer agreement

should be considered acceptable as the resolution decreases.

The values in the

ratio criteria may be rounded to fewer significant figures reported by the NRC

Reference Laboratory, unless such rounding will result in a narrowed category of

acceptance.

RESOLUTION

RATIO = LICENSEE VALUE/NRC REFERENCE VALUE

Agreement

<4

0.4 - 2.5

,

4-

0.5 - 2.0

8-

0.6 - 1.66

16 - 50

0.75 - 1.33

51 - 200

0.80 - 1.25

200 -

0.85 - 1.18

Some discrepancies may result from the use of different equipment, techniques,

and for some specific nuclides.

These may be factored into the acceptance

criteria and identified on the data sheet.

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