Text

Enclosure B, Bechtel Report No. 25593-000-G83-GEG-00016-000, Effect of Laminar Cracks on Splice Capacity of No. 11 Bars Based on Testing Conducted at Purdue University and University of Kansas for Davis-Besse Shield Building. Part 4 of 7
	ML15299A148
Person / Time
Site:	Davis Besse
Issue date:	07/30/2012
From:	Liano R, Munshi J, Reilly R; Bechtel Power Corp
To:	; Office of Nuclear Reactor Regulation
Shared Package
ML15299A142	List: L-15-328, Enclosure B, Bechtel Report No. 25593-000-G83-GEG-00016-000, Effect of Laminar Cracks on Splice Capacity of No. 11 Bars Based on Testing Conducted at Purdue University and University of Kansas for Davis-Besse Shield Building. Part 7 of 7; ML15299A143; ML15299A144; ML15299A146; ML15299A147; ML15299A148; ML15299A149; ML15299A150;
References
	L-15-328 25593-000-G83-GEG-00016-000
	Download: ML15299A148 (129)
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{{#Wiki_filter:bbiL-UUU-U83-U.5"U.-UUU1bt-UUU I-'age bb or "1"114ApedX:Apoedls oedeAppendtx Approved Iest Procedure 25539-O00-VIS-SY01-00001-003 Page I of 26BECHTEL POWER CORPORATION SUPPUER DOCUMENT REVIEWTests to Determine the Behavior CL.ASSIFICAT.ION & STATUSof #11 Bars with Lap Splices ...Bowen Laboratory ¶ El [] Purdue University El[ ,d ' El wodmsSpring 2012 2-" *Test Procedure ., , == =1.1 Formwork -,(iThe formwork shall be made using non-absorbent plywood. Itsinterior shall be caulked to prevent water leakage and it shall be covered with a thinlayer of oil before casting. The dimensions of the formwork shall be checked andrecorded using Form 1.1.2 Reinforcement CagesThe steel reinforcement cages shall be built following the drawings attached. Reinforcing bars shall be supported by steel chairs placed away from lap splices. Toensure alignment, the bars shall be tied to chairs and to one another using gage-16steel wire. The location of the reinforcement shall be recorded using Form 1. Thelocations of wire ties and rebar markings shall be recorded using Form 2.Tolerances (within the test region) are:3/16" for horizontal cover and horizontal spacing measured to the surface of the bar(excluding ribs)1/4" for vertical distances shown in Form 11.3 CastingFresh concrete properties to be measured include:Unit WeightSlumpAir ContentThese measurements shall be made following the Specifications and recorded usingForm 3.Revision 218-1REDACTED VERSION boYJ-uUU-UdJ-ULUc-Uuu3 b-UUU r'age tbtU 011 114 Appendix 8: Approved lest Procedure 2bbJiY-UUU-ViS-:SYU1-UUUU1-UUit rage z oT Slump shall be measured before any other activity related to casting takes place tomake sure that the delivered mix has ,satisfactory workability. The mixing truckshall deliver a ticket with the batched mix weights. These weights shall be examinedto corroborate that the delivered mix has the specified proportions. Concrete shallnot be accepted if it arrives more than 45 min. after leaving the batching plant. Nowater shall be added to the mix after the truck leaves the plant.Specimens and cylinders shall be cast and vibrated in two lifts following theSpecifications. The vibrators to be used shall have the following cross-sectional dimensions: For cylinders: 3/4" -7/8"For Larger Specimens: 1-3/4"Their frequencies shall be between 50 and 200 Hz.Excess concrete shall be removed off the formwork. The exposed surfaces of thespecimens shall be finished using cast magnesium floats. Lifting inserts shall beinserted in the fresh concrete as soon as the finishing is completed. Each test beam shall be cast using concrete from a single mixing truck. A completeset of concrete samples (cylinders) shall be obtained from each truck. Test beamsand samples shall be marked with a number referring to the truck from which theywere cast and the date of casting. In each casting day, trucks shall be numberedsequentially starting at 1. The number assigned to a truck shall be written clearlyon the mix ticket describing the mix proportions for the batch. Test beams shall becast and tested oriented in the North-South axis of the laboratory. During finishing, the north end of each beam shall be marked with the letter N.These activities shall be documented using Form 31.4 C:uringAs soon as casting is completed all specimens shall be covered with impermeable sheets. When the concrete surface sets, wet burlap shall be inserted between thesesheets and the exposed concrete. All formwork and molds shall be struck no laterthan three days after the cast.All exposed concrete surfaces shall be covered by wet burlap and impermeable sheets for a total of at least seven days after casting.Burlap shall be doused with water at least every other day during the curing period.Curing activities shall be logged using Form 4.Revision2 25-2REDACTED VERSION

inage bU1 0? 11I 14 A~ppendix s: Approved lest Procedure 2bW3-UUU-V'15-bSYU'1-UUUU'1-UUtS frage it or 2uTest cylinders shall be stored and cured next to the test specimens and undersimilar conditions of temperature and humidity. The variation of concrete strength with time shall be monitored as specified in theSpecifications. The results of cylinder tests shall be recorded using Form 5.2. Calibration Three types of measurements will be made: displacement, force, air content.The apparatuses to be used to calibrate sensors to measure these quantities are:Displacement Sensors: INSTRON Universal Testing Machine (S.N.:)Load Sensors: INSTRON Universal Testing Machine (S.N.:)Air Content: Calibrated Cylinder (S.N.)Load and displacement sensors will be calibrated following steps listed below:1) Connect the sensor to the data-acquisition system that is going to be used inthe test2) Set and record the excitation voltage to the maximum possible value (notexceeding the maxima specified for the data-acquisition system and thesensor)3) Set the data-acquisition equipment to record voltage4) Set the gain of the data-acquisition system to the first available level lowerthan the ratio of the maximum range of the system to the maximum expectedoutput from the sensor.5) Mount the sensor on the universal testing machine6) Apply a series of known displacement or force increments to the sensorranging between 10% and 90% of the rated capacity of the sensor7) Record the voltage read on the data-acquisition system at each knowndisplacement or force increment

8) Create a plot of change in output voltage vs. change in force or displacement

9) Fit a line to the plot from 7) using "least squares"10) Record the slope of the line from 8) (sensor sensitivity)

11) Label the cable used in the calibration with the serial number of the sensorSensors shall be calibrated before the first test and after the final test.The apparatus used to measure air content of the fresh concrete shall be calibrated following the procedure described in ASTM standard 231. Form 6B shall be used todocument the calibration.

Revision2 38-3REDACTED VERSION bbg:i-UUU-LUdi-ULUL-UUU1 b-UUU i-'age bb2 01"1114. Appendix 8: Approved lest Procedure 2bbtJY-UUU-V1 -UUUU1 -UUi wage 4 07tLtiAll calibrations shall be performed by at least two persons: one leading each stepand the other checking the work of the first independently. A log of each calibration shall be made using Form 6 and it shall include an estimate of the accuracy of thesensor.Sensors for which the sensitivity obtained in 9) above deviates by more than 10%from the nominal sensitivity (as reported by the manufacturer) shall not be used inany of the tests.3. SetupEach test beam shall be placed on two roller supports as described in theattached proposal. The final location of the supports shall be measured (to thenearest 1/16 in.j with maximum deviation of in and reported using Form 7. As-built external dimensions of each test beam shall be recorded using the same form.The maximum deviation from nominal dimensions in the test region shall be 1/4/ in.The test beam shall be placed with the reinforcement facing up as shown in theattached proposal. The shear spans shall be reinforced with external stirrups (pairs of 5/8-in threadedrods) installed at a spacing not exceeding 12 in. The locations of the stirrups shall bemeasured. The measurements shall be recorded using Form 7.The loading rigs (consisting of a loading tube, two hydraulic rams, two threadedrods, plates and nuts, and one load cell per rig) shall be placed on the test specimenand connected to "the strong floor" of the laboratory (without applying load to thespecimen other than the weight of the rigs) as described in the attached proposal. The rams in each rig shall be connected to a single manifold and pump using 10,000-psi hydraulic hoses. All hoses and other hydraulic hardware shall be inspected visually and replaced -if defective-before testing.4. Instrumentation Displacement sensors shall be installed at midspan, at each support, and at eachload point. They shall be secured to the strong floor of the laboratory directly belowthe point where displacement is to be measured. All sensors (displacement and force) shall be connected to the data acquisition system using the same cables used during calibration. The excitation voltage andgain shall also be set to the value used in calibration. The data acquisition systemshall be set to record voltage changes caused by loading. Before applying load withthe hydraulic rams, all sensors shall be set to read a voltage value between 10% and90% of the voltage output of the sensor at its rated capacity. These voltages shall bereferred to as the "zero offsets" of the sensors. If a sensor is set to have an initialRevision2 48-4REDACTED VERSION

Hage o011114 Appendix 8: Approved lest Procedure 2bb68-UUU-Vl:5-bYU1-UUUU1-UUi Page b ot Zbvoltage exceeding 20% of its output at rated capacity, the sign of the initial "zerooffset" shall be opposite to the sign of the expected change in its signal.Set the data acquisition System to scan all sensors and save at least one record persensor every 1 sec.Record a file of "zero offsets" capturing at least 10 min. of data before any load isapplied with the hydraulic system.Means of initial voltages for all sensors (mean "zero offsets"), sensor serial numbers,the most recent sensitivity constants, excitation

voltages, and the channels of thedata-acquisition system used for each sensor shall be recorded using Form 8. Thepairing of channels and sensors shall be checked by a second person workingindependently from the person making the initial connections.

Infrared targets to be used to measure displacements as described in the attachedproposal shall be glued to one face of the test beam using epoxy adhesive. Thenumbering sequence of these targets shall be recorded using Form 9.Video cameras (one for long-time lapse video and one for high-speed video) will bepositioned to capture the response of the mid third of each specimen. To the extentpossible, the location of the cameras shall be the same in all tests.5. TestingThe following actions shall take place during each test:At the end of each loading increment: Mark Cracks: all visible cracks shall be marked using black permanent markers. Cracks shall be marked by drawing lines parallel tothem and with an offset of approximately 0.25 in.Measure Crack Widths: Crack widths shall be measured using crackcomparators or graduated handheld microscopes. Measure coordinates of infrared coordinates: A set of coordinates shall beobtained using an OptoTrack System 600 Pro. A set of fourtargets shall be attached to the strong floor. They shall belocated at approximately the same distance to the OptoTrack cameras as targets attached to the test beam. Coordinates forthese reference targets shall be obtained at each loadingincrement. They are to be used to monitor the stability of theOptotrack system by computing the variation in the distances between reference targets.Revision2 58-5REDACTED VERSION

M'age bi40ot 1114 Appendix Approved lest Procedure l-'age 0 ot ZbIn-Test Data Backup: At every loading increment the data being produced bythe data-acquisition system shall be copied to an external harddrive.Photographs: a set of high-resolution photographs shall be obtained aftercracks are marked at each loading increment. The photographs shall includes views of both elevations of the test beam and thetop concrete surface above lap splices.The following data shall be recorded throughout each test:Sensor readings: to be recorded on a hard drive in volts. Conversion toengineering units shall be done after the test as follows:-Subtract zero offsets-Divide the result by the sensitivity obtained in the most recentcalibration Lapse video photographs: to be obtained every 5 min.Actions to be taken at failureTrigger high-speed camera to record breaking away of the concrete coverand relative movement of the bars.Actions to be taken after testGenerate a record of sensors that may have malfunctioned or beenaccidentally moved during the testRemove from all files recordings from sensors for which the results of theafter-test calibration differ by more than 5% from the before-test calibration.

6. Reporting and BackupProduce all the captured data in two ways:By uploading data, photos, and video to a private project at nees.org.

By recording all data, photos, and video on a magnetic hard driveReports shall be produced as described in the Specifications. Revision2 68-6REDACTED VERSION Form 1I23 "SOUTHINORTHI ..,-654.Section A-A2 Spa. @3,3'FAAKBKLcK DKEKF*For section B-Bthrough F-Fsee Sheet 3of 3Series ADrawing: Series A Formwork As-builts Sheet: 1 of 3BOWEN OWN, JLB YProject: Experimental Investigation of Drawn by: BPR Checked by: SPPURDUE UNIVERSITYCaatofLpSlcsfNo 11 Reinforcing Bars Date: 04/04/2012 8-7R Form 1II -~2-I--31SOUTHNORTH654 _Section A-A2 Spa. @33,FAAK BLCKDKEKF*For section B-Bthrough F-Fsee Sheet 3of 3Series BSeries B Formwork As-builts Sheet: 2 of 3Experimental Investigation of Drawn by: BPR Checked by: SPCapacity of Lap Splices of No.11 Reinforcing Bars Date: 04/04/2012 8-8R E D IO0N Form 1I" ~8I" ~8 -64 52 '764- 571--31--3Section C-C, D-D, & E-E*Facing NorthSection B-B & F-F*Facing North-- BOWENPURDUE UNIVERSITY Formwork As-built Sections Sheet: 3 of 3Experimental Investigation of Drawn by: BPR Checked by: SPCapacity of Lap Splices of No.11 Reinforcing Bars Date: 04/04/2012 8-9RE N Form 1Project: Tests to Determine theBehavior of Spliced #11 BarsAs-built Dimensions v.1(Rev. 04/04/2012) Specimen: Sheet ilof 2Formwork As-built Dimensions Section1 2 3 4 5 6 7 8A-AB-BC-cD-DE-EF-FRecorded by: Signature Date TimeChecked by: Signature Date TimeChecked by: Signature Date TimeComments:

See formwork as-built drawings for dimension locations 8 -10R IO0N Form IAs-built Dimensions v.1(Rev. 04/04/20 12)Project:

Tests to Determine theBehavior of Spliced #11 BarsSpecimen: Sheet 2 of 2Formwork As-built Dimensions Key -Series ASection1 2 3 4 5 6 7 8A-A 14'-6" 10'-0" 14'-6" 14'-6" 10'-0" 14'-6" N/A N/AB-B 4-3/8" 6" 4-3/8" 23-5/8" 23-5/8" 30" 30" 17-5/8"c-C 3" 6" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8"D-D 3" 6" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8"E-E 3" 6" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8"F-F 3" 8-3/4" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8"Formwork As-built Dimensions Key -Series BSection1 2 3 4 5 6 7 8A-A 13 -10.5" 6'-7" 13 -10.5" 13'-10.5" 6'-7" 13 -10.5" N/A N/AB-B 4-3/8" 6" 4-3/8" 23-5/8" 23-5/8" 30" 30" 17-5/8"C-C 3" 6" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8"D-D 3" 6" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8"E-E 3" 6" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8"F-F 3" 8-3/4" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8"8-11R E IO N Form 2ieWire TiesNORTHBar MarksNORTHOWENSpecimen: _ _B dTO YProject: Behavior of Lap Splices of No. Drawn by: Checked by:PUgR DU E UN I VE R SI TY 11 Reinforcing BarsDaeRe~isi~n 2REDACTED VERSION btUj-UuU-Ud-ULi3LP-UUU1U-UUU i-age h(1 ot 1114Project: Tests to Determine theBehavior of Spliced #11 BarsAppendix 8: AI P'rocedure Casting Documentation v.1(Rev. 03/30/2012) Mage 1i ot zbSpecimen:_____________ Sheet 1 of 1General Information Date Disp Ticket Num Truck No. JTime on Ticket Time of Arrival Temp. in LabMeasurements made upon arrival of concreteSlump (ASTM C143 -l0a) Air Content (ASTM C231 -10)Time1 Result1 Time1 Result1 S/N of Air MeterTime2 Result2 Time2 Result2 S/N of ScaleUnit Weight (ASTM C138 -l0b)Time1 Wt. of Cont.1 Total Wt. 1 Wt. of Conc.1 Result1 = Wt. of Conc./Vol. of Cont.Time2 Wt. of Cont.2 Total Wt. 2 Wt. of Conc.2 Result2 = Wt. of Conc./Vol. of Cont.Times of actions during and after castingLae lcd Layer 1 vibration Layer 2 vibration Top surface struck Truck Departing complete Lae lcd complete off LabLifting Inserts Covered with Patcrmvd Covered with Burlap doused Covered withPlaced plastic burlap with water plasticRecorded by Signature Date TimeChecked by Signature Date TimeChecked by Signature Date TimeComments:

The following ASTM standards and specifications will be followed during casting:

C172-10, C192-07, C470-098-13R EDAI~~~nLSI ON bbU3-UUU-Ud;J-UIUL-UUUl b-UUU -~age at 1114.Project: Tests to Determine theBehavior of Spliced #11 BarsAppendllx 8: Al1ymd4est Procedure Curing Documentation v.1'(Rev. 03/30/2012) Yb3-UUU-V15-:SYU1-UUUU1-UUj I-age 14 01" 2bPurdue University -Bowen Laboratory Sheet 1 of 1General Information Specimen(s) Date Specimen AgeTime Beginning Time EndingTemperature inside Lab (deg. F)Description of Work Performed Recorded by Signature Date TimeChecked by Signature Date TimeChecked by Signature Date TimeComments:

Test specimens and associated cylinders are to be cured under wet burlap for seven days8-14R E I O N Form 5Project:

Tests to Determine theBehavior of Spliced #11 BarsCylinder Compression Tests Documentation v.2(Rev. 04/01/2012) Specimen:* Sheet i of 2Diameter [nearest 0.01 in.] Length [nearest 0.05 in.] Fracture TypeSpecimen Date Time of Test Wet/Dry Pmax [Ibf]1 2 1 2 3(1-6)1~23456S/N of Testing Machine: Recorded by: Signature Date TimeChecked by: Signature Date TimeChecked by: Signature Date TimeComments:

Cylinders to be test per ASTM C-39-22 and C-1231-20a with a loading rate of 60,0001bf/min at concrete ages of 3, 7, 14, 28 days, and on same day that test ofcorrespondingspecimen is conducted.

Specimens and caps free of defects unless otherwise noted in comments. Average cylinder diameter and area and unitcompressive stress (f'c) calculated on sheet 2 of 2.8-15R IO N Form 5Project: Tests to Determine theBehavior of Spliced #11 BarsCylinder Compression Tests Documentation v.2(Rev. 04/01/2012) Specimen: Sheet 2 of 2Average Cross-Specimen Date Age Time of Test Wet/Dry Measured sectional Area Prnax [Ibf] f' [psi] FrcueTpDia. [in.] [in2](1 )2 0-Jan 12:00 AM 0 #DIV/0! #DIV/0! 0 #DIV/0! 02_____ 0-Jan 12:00 AM 0 #DIV/0! #DIV/0! 0 #DIV/0! 0456S/N of Testing Machine:d.Recorded by:Signature DateTi me0 0 0Checked by: Signature Date Time0 Sintr0________________ 0_________ Checked by: Signature_________ Date______Time ___Comments:

Cylinders to be test per ASTM C-39-12 and C-1231-10a with a loading rate of 60,0001bf/min at concrete ages of 3, 7, 14, 28 days, and on same day that test ofcorresponding specimen is conducted.

Specimens and caps free of defects unless otherwise noted in comments. Recorded data is shown on sheet 1 of 2.8-16R EDAljii(E:S IO N

I-age bib oT 1114Project: Tests to Determine theBehavior of Spliced #11 BarsAppendix 85: est -'rocedure Calibration Documentation v.1(Rev. 04/02/2012) Iage 1 ( ot ZbBowen Lab -Purdue University Sheet 1 of 1Calibration Instrument Name and S.N.:Data Acquisition System:Gain:Excitation Voltage:Channel:Sensor:Sensor S.N.:Measurand Voltage Measurand Voltage Measurand VoltageOperator Signature Date TimeChecked by Signature Date TimeChecked by Signature Date TimeSensitivity AccuracyResultsNotes:Re~is~n 2REDACTED VERSION

I-sage fbf ot 1114Project: Tests to Determine theBehavior of Spliced #11 BarsAppendix 8: f~~l~ 6EtProcedure Calibration Documentation v.1(Rev. 04/06/2012) I-'age id oT 2tiBowen Lab -Purdue University Sheet 1 of 1Meter S.N.+Tve fMee.4-Meter Brand NameTarget Air Content Measured Air ContentOperatorSignature DateTimeI + 4Checked by Signature Date TimeChecked by Signature Date TimeNotes:Re~is~n 2REDACTED VERSION Form 7111+/- 111111I I I I I I I I I II I I I I I I I I I IYII III I I I I I III INORTHILLLLLLLLLI__-LLLLLLLLLL ______________________________________________I I I I I I I I I I II I I I I I I I I IF q................................. fT111111111 I111111111 I~8 NORTH1 1 1 1. ..1 1 £ I---*-j4~~~~~*a-I PURDUE UNIVERSITY Behavior of Lap Splices of No. 11Reinforcing Bars8-19R EDgAl~i~icnESI ON Form 7ISOUTHSOUTHIi-, ~2Top Plan2 Spa. @3' '-60" Ea. =' 3'KB Ko L LEL FProfile*For section B-B through F-F see Sheet 3 of 3I" 3 "NORTHNORTHF-_I4Bottom Plan.. SOWEND- LABORA TORYP U RD UE U-NI-VERS IT-YSeries A Concrete As-builts Sheet: 2 of 4Experimental Investigation of Drawn by: BPR Checked by: SPCapacity of Lap Splices of No.11 Reinforcing Bars Date: 04/04/2012 8 -20R E IO0N Form 7ISOUTHSOUTHINORTH2 1Top Plan2 Spa. @3' ----39.5" Ea.--- 3'Profile*For section B-B through F-F see Sheet 3 of 3V" 3 "NORTHI ,,I4Bottom PlanSeries B Concrete As-builts Sheet: 3 of 4Experimental Investigation of Drawn by: BPR Checked by: SPCapacity of Lap Splices of No.11 Reinforcing Bars Date: 04/04/2012 8 -21R I0 Form 7I" ~142-~3 -Section B-B, C-C, D-D, E-E & F-F*Facjng North__________ jr B W NDrawing: Concrete As-built Sections Sheet: 4 of 4___ __BO Experimental Investigation of Drawn by: BPR Checked by: SPP UR D.UE U NIVERS ITY Capacity of Lap Splices of No.11 Reinforcing Bars Date: 04/04/2012 8 -22R E gAl~l~LS IO N Form 7Project: Tests to Determine theBehavior of Spliced #11 BarsSetup and As-built Dimensions v.1(Rev. 04/04/2012) Specimen: Sheet Ilof 2Concrete As-built Dimensions Section1 234 5 678PlanB-BC-CD-DE-EF-FRecorded by: Signature Date TimeChecked by: Signature Date TimeChecked by: Signature Date TimeComments:

See concrete as-built drawings for dimension locations 8 -23R Form 7Setup and As-built Dimensions v.1(Rev. 04/04/2012)

Project: Tests to Determine theBehavior of Spliced #11 BarsSpecimen: Sheet 2 of 2Concrete As-built Dimensions Key -Series ASection1 2 3 4 5 6 7 8Plan 39'-0" 39'-0" 39'-0" 39'-0" N/A N/A N/A N/AB-B 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/AC-C 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/AD-D 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/AE-E 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/AF-F 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/AConcrete As-built Dimensions Key -Series BSection1 2 3 4 5 6 7 8Plan 34'-4" 34'-4" 34'-4" 34'-4" N/A N/A N/A N/AB-B 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/AC-C 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/AD-D 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/AE-E 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/AF-F 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A8 -24R I ON Form 8Project: Tests to Determine theBehavior of Spliced #11 BarsInstrumentation Documentation v.1(Rev. 04/01/2012) Specimen: Sheet __ __of____Data Acquisition System:Channel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location CommentsOperator Signature Date TimeChecked by Signature Date TimeChecked by Signature Date TimeNotes:Re~isi~n 2REDACTED VERSION Form 9Jj...111...1111jt ' -4 111111111 FI I [ ] IIITh NORTHI I I I4; 4" ,. , , ,-BOWENflLABORA TORYPURDUE UNVRSITSpecimenBehavior of Lap Splices of No. 11Reinforcing BarsRe~isi~n 2REDACTED VERSION Purdue University Specimen: A-IDate: 4/LI/1Average Joad North South North Splice Md (i) South Splice LVDT North LVDT South North Load Cell South Load Cell DG North DG South Tm(I- Overhang (in) Overhang (in) End (in) Mdpan (i) End (in) Support Support "J ." J! J" Overhang (in) Overhang (in) Time_____ 6 Q.-O."~ o.1S 0.o:7 0.o-i o.0 " .oQoo .-o.ooo 6 & O. i'l6 A_____, c?.c2 " 0. , o! c,0 0 ,If o.o" -O .oo0 -0,00 j"L- 7. O. 6H 0 .qO : "'ASI o.,9o Q. 4 .Q.It~ -c).ooo ooo !' !' 0.0060 0. /,O"/ 6 "tO 1.7. 1.L7 o.-I~ o.V. -0.Qoo -0.oo( -'o -'o- I./' VL.66 Io:ooA6 tl.< tG -Ge4- O.gov "oQ o, oo ,.~.6AO i' .o0' "toS Q,?I oA&6 o.=1 -0ol.oo -o.oo' "V 6 L.38 IQ',.A" ' 1. 3.. ____ ______ _____ -oo,_-oo_ ___ ,!_.__ 0 q13 1-.." I,0 , '[ 0. cj. L", O." 0,.1 -o.oo6' -o~o <?.'. q.o;F15 iQ , "2.-I" ".-62 o.4" o .* c.4'i q -o.oog 1"1-..o I',O"IZ.16 3.?"'f 0.9;1. 0.70 0 .c G -.oo" -o.oo-f "A..Q. 2A.0. 12i":7P" O7 q q. .0:1O (\.o! o1$'7 -..c." ..o, LIL.\ Ho.o 20 __, ___ __.___ L.LI, 1 t. 1.Li( 1.15 -.oio -. 0 '.litH , __ __ __ __ _ _______9-IREDACTED VERSION I' ..0UPurdue University Specimen: Date: Average Load North South North Splice Md ()South Splice LVDT North LVDT South North Load Cell South Load Cell 06 North D6 Sauth Tm(lbf) Overhang (in) Overhang (in) End (in) Misa i) End (in) Support Support *(Ibf) (]bf) Overhang (in) Overhang (in) Time____1 ~ .0 0 -0.0!l 0 -0.01 -0.001 -0.ool0. 0.2.. 0.7 .O~0 .!,-1 O.AI 0.0I .01 -0.00oo -0.00l S, G Q.W]L l1I" 0,-H'- O.-f-i 0.06 0.10 o~o 6 -.0.oo -0.001 V"L 11. 0.G3' Q.6?"t $'?5A, "1.qi16 .1"/ Q.!"1 O,"1,6 7.I1 0...0oo -0.00' %" ,IA t55~ ,.6"7 , .6 I.Q .2tz ;.3- 0.'Vl" -O.oO"t -0.0O1 30 t7Ol."e~ I.I'zQ T:J;A, _____ ..21 o..i-' o."z. -o.oo-. .-o.,:oo" ____ ____ 1.VI'/'- !.1t' 10 :3.,-- "z,"' "j,-' 0.33= -0.001 -o.o000o __ ___jj~ " 1o:S'JA11 1O.g ";,6o; Q,q O."t'. o,.' -v.oo-i.- -o.ool 10,.6 "-II .. i:]"A13'141618"209-2REDACTED VERSION 0Purdue University Specimen: A-35 /~O/l2Date:Averacejoad North South North Splice Midsa (In) South Splice LVDT North LVDT South North Load Cell South Load Cell DG North 06 South lm(fI<Overhang (in) Overhang (in) End (in) spn End (in) Support Support (1 Overhang (in) Overhang (in) Tm1 Q.(6 0.00 0.00 0.00 Q.QQ Q.oO -Q.o0"L -o.0o'L 0.Lt ,0. 0 .1 o.(t402 ,' o(t Q.Iq o.o'z. Q0 0.0 1 .o. .-O.ooL -0.0o02 6 6.-i:. o.L g. ?Li." 0.q-H o.-I1 O,01 0.1! o.o-l .o.o'-L _o.OOi t1.. tiL.. Q.C'1 g:w;_____ 08 o.gO .' 0.-1.- Q.1- -oQo3 0.ooo ____ Q,9? -o:;1A2 1.V; 1.1-9 oI'z, 0,-1 *-o.oo,0 o.'oi- 20I I-tl , 1.',1[,b O.L O. q' .? 0.i.9 O.ooq L6'1$ t.S tO : f101112131417ISi19o9-3REDACTED VERSION 0Purdue University Specimen: Date:4,/3/12Average Load North South " North Splice Misa i) South Splice LVOT*10rth LVDT south North Load Cell South Load Cell DG North DG South,, (Ibf) Overhang (in) Overhang (in) End (in) lsan(n End (in) Support Support __ I_____If) Overhang (in) Overhang (in)} Timeo,01 -o~oj -0.0 I -o.oQ -Q~oQ 0.00 -0.oo[ -0.00o O[ Q. 0.000 0.00 2 3..i. c atk ______3 6.0 0.11 0IGO1 0.0. 0.0'1 0.0"? -o.oo( -0.001 6.o 6-O 0.11 6 lL.1-O-I) O. CISoo Q.i.'l 0.0S -o.iool -o.oo0. 2:.I.O 'Li.I I.7lJ~ OI4~ To-IA' 3-J.S 1.-T? 0.1-c Q.-G -o-ooo -9.oo1 "i.'.9 L-1-fQ 1-iQE 9"1-IAN*,,~c VG __ __ ___ _ .oc'0 O.oO~10 N+" DG .- o.000 o-Qoo,, "o.O ?.x' 7-ISo, O.61 Q.6G 0.c6 -o.oo? 0.-I"l O.'3" ,¢.,jj0 Is O.-SI 0.66Q O.c; o~o(- tO".",.. 03 __i___'zC ,, -1,Q o.',5 0.660,c.*I -0.0oo' 000o 7A.1 Ul:5JA16 '.-: 7A.9 o.S9J Q.< Q.-&-f 0.o0Q3 ?6.o ___ .o_ VL:IbF9-4REDACTED VERSION UUUPurdue University / ll2Specimen: Date:Average Load North South North Splice South Splice LVDT North LVDT South North Load Cell South Load Cell i DG North DG South rm(lbf) Overhang (in) Overhang (In) End (In) Mldspan (in) End (In) Support Support (lbf) (Ibf} Overhang (in) Overhang (In) Ti_____e _1 0.01 0.00 -O.oot. -o.oc-i. 01. o.ooo o.Qoo "]:3gAVL,.Q 0.11~ 0,0-j o.1 o.0, -.oO).o -a.0" VI.'t (i.Q Q-16= ' 0.86 o.9j -o0,0L -o.ooi I-Q I.Q 0.860 Q!~1'I g:-[s'A, ta~c) -o .oc~t o~ooo "IA.O .o +0. 1.1.;! __l__7_ : t' ?0,0 U,,I L.,5b 0.31 0,L-J -o.ooi o.ooI 30.0 Qo.O i.G2.? b&1,69 S-W'A, DC, ,.-, __'_"Q.ooo Q.OOQ, 6.o .o"1..O1 '),4Q o..4i -o.ooo o.oo1 ?6.0 36.0 Q.-f4;o~ o.'If fQ:o64ii 'yc/qit -L.M1I Q2. 5' -o.o00 .O.ool ?1.7 '1 .q; O.e?" Q to':-A,N14S" PG v-oQ4.- 'z.ooo 0.oQQ13 3/4- 0.63 Q?.q 0.66 -Q.ooo -o.o0 o 2.0fo $.-]o iQ:ssA1-9 -lo,1 '-1.6-i. ,0."i Q.'" o.o0o -0.001 '-!o.6 i~,-I-f P9-5REDACTED VERSION Purdue University Specimen: A-C,Date:Average oad North South NorthSplice Md n) South Splice .VDT North LVDT South North Loa.Cel South Load Cel DG North 06 South T--(6 Overhang (in) Overhang (in) End (in) M span [I) End (in) Support Support Overhang (in) Overhang (in) TmO."V. 0.00 0.o0 0.00 -0.00 o.o0 -.0.0o0 -o~ooc' 0.? O... 0oo .000 F'Q- ot' 0.0'7, Q.o=; o.0ot -o.ooo 6.0 bQ O.i1!. oQ-i;i , ~z oA o Q,-o.+ 0,0-i ocoj 0.01 o.oo~ 0t.000 1'2..o ti..A I o .,913 I:'oP, o~g6 Q.%G 0.13 o.I9 v.007 -.001o {i~O 6 Vo ..67 I.61, 0."}.- O .'L6 o."js QOQ0 -0001" -2'fQ .0 Ao.. l. 6."3 L.6'1 "t.-{fP8 12c ,voi4" 0.000 aQvQQ "1;bF'15 vo ,L -3,oo 3.1' 0 .i'- O*e6 osq-I 0.o00' -o.007 1.oQ.I "Lo.3 0.?3? O.q(;6 P16 Q.tl," I.8 6 "i.. "..o Q,'j O.-jo 03.5 -o.0o7 O,1". O,"__-.0 _16 "1,'- 1 ."0 0 .Q O.&" -o..Oo" "_..__ .0_ ____ ___'9 '4..07 Q.(:,Q Q.g? 0.66 0.oo')J -0oo 3G .Q ?.o S-t- FP20 t(Q,3 iJ?". -j.-i0 Q0.'0 Q0e..7 9.7 q.oo -c'.oo'9 4,Q,-7 _,__,_ _______9-6'REDACTED VERSION

.rPurdue University Specimen:

Date:_6.g.2Average Load North South North Splice Midspan (in) South Splice LVDT North LVDT South North Load Cell South Load Cell DG North DG South Time(lbf) Overhang (In). Overhang (In) End (in)} ______ End (in) Support Support (lbf) (lbf) Overhang (in] Overhang (in) ______" -!. L.-0 L ,!-408; tt; .~ o o~t II H*.'. , F232426272829,3331,3233343617439-7REDACTED VERSION Purdue University ©IiSpecimen

DQ -_Date: -l0i:71 ~T rAverage North Overhang (in) South Overhang (in)North Splice End(in)Mldspan (in)South Splice End(in)LVDT North Support ILVDT South Support INorth Load Cell (lbf) ISouth Load Cell (Ibf)S o.'z -0.01 0 0 0 -o.00 -o.ooo o0S .o5 .o o.oj o o 0 3.5 3. -6 0 ..o .5 o. 045- _ _ _ _ _ _S G 0.~ Io.14 O. oZ- 0.o'?_ O.oZ o.ooi 0.001 ___ __6 I o.j o 0.o5 d.oe o.0oo3 o.oo01 I11 I0-o.- o.+/- 0.I _____o.I o..oo4r i13 2-4 I.I I.o-+ o.15 O-Is o. 1j o.oo2 1, 1e .Po 1. 1 o.I_5 O.31 0.12 0.00 o.oo3 ______1920ZMvo3 ~3A~4149-8REDACTED VERSION 0i ..Purdue University C)SSpecimen:

Date:Average Load North South North Splice Misa i) South Splice LVDT North LVDT South North Load Cell South Load Cell DG North DG South TnOverhang (in) Overhang (in) End (in) Misa I) End (in) ,- Support-Support ..a//,/ 't Overhang (in) Overhang (in) Time____1 o~. 0 o.oj 0 0 -Oofo -0.oo5 o.ool 0,3 0,L f-.0 0..o0Olo ?.:57-A___________ ______ O1 .0¢ 0 .O 0.'01 -0.005 0.001 0236 O~4 " 5oS 18 o.81 0. 8 0.1.1 0.13 O. Io -~o..oo____ ____ 0.__0_-__

1, 0 14 o.2 0.2. .00~ I.s~ra bo~ooA-P.ELA'TJVE 10 If o.s, o.i.5 ol' o.11- o.OOS, I, Ig -O. 32o I1:1o A12 19- I.% 1.9 o.j8 o.1- -ooo

.17;9-9REDACTED VERSION ...(0Purdue University Specimen: Date: /_/iAverage Load North South North Splice Mdan()South Splice LVDT North LVDT South North Load Cell South Load Cell DG North DG South lm4Jf. ! Overhang (in) Overhang (in) End (in) __dspan___n) End (in) Support Support J4 Overhang (in) Overhang (in) Time____1 o .% o o o -0.o -o.oo' o 0 '-S G.2. 0.14 oXlf o.o'L 0.o2 ,-o.oal -coa.oo 6.z 6.g. o.j14 o.Ij, 2,io.A" 0.4. 0.40 0.05 0.0-4 0.05 -...ooo -o.oo~Z. )Z oQAo7 ,35A,S 8 oJ .0-jo. 0 o.3 o-JO -o.o04 -o..oo? 18 lB o.-?4-- 9):o{-6 z 4 1.o09 I.of- 0. 14 o049 0.15 .--o.0of .-0.002 4,, L. .057- (. o6o ¢/' 30 I.43 1.41 j.1 0.25 o2. -0.ood/ -cooo 30 zo I., " ." .'25 03.3 o."5 -o 0,.0o0oo 3C, o J.aao !o'zB4,q0-o. Q44 o4 o.0? o.0J -o.oo~f o.,, oZ. o.,,/ (/;o5..41o 0% O 8G .1 O-Jk o.15 Oi12 -o.oo,0 -ooz 12.1 O.Saeto I1"1" 4141617'19209-10REDACTED VERSION Purdue University Specimen:, rh-HDate:_Averag Ove Nrthan (I) overhagin ENdr (pi) Mldspan (In) South Splice LVDT North LVDT South North Load Cell South Load C:ell DG North DG South(Ibf)_Overhan (in)____ Overhang__ ____n) __End _____in)_ End (In) Support Support (lbf) (Ibf) Overhang (in) Overhang (In) Time____.* o.o¢ 0 0 o0 o.ool 0. .. o. 4:jq/:' 04" 0 o o o o o ogp0 o. o.,'2 o. ,2o2 o.,loZ It z2426282728293031,32333436373839409-11REDACTED VERSION Purdue University Specimen

Iz:-Date: -'Average Load North South North Splice Mlsa i) South Splice LVDT North LVOT South North Load Cell South Load Cell DG North DG South Tm(Ibf) Overhang (In) Overhang (in) End (in) Mldspan__in)

End {in) Support Support (Ibf) (Ibf) Overhang (in) Overhang (in) imS 0 oo000 -o.ooyZ -o.0o1 _.___o. o._o..__._,_I-- 0 .. 0.o5 0 0 0 -o.ooi o __.__ 5.Z o.z45 oif_65 ______ 0.1 0z~.. 005 0o 0.00l ____ ii.__ 0.5V(L 0.s'5 1_58____o. __ O.___ o._oo-I 0.08 0.00-3 o__o___ _____ __.__I o______ ____, L-> 'ST .S1Ll CI-, .Ac v. __ __ _ __ _ __ ____ _'24[ 0.c5 o. o.0o G.I5 O.0o-J g0 iAi~i' 1.i41' 3'3-, _ _ _ _. _ _r _ _. _- _ 0-I -o 2. l 0.W. o , o( o .oo 4 .I.Y /U :I.:9::/ I.:& 0. 0.2..,4 .___ .____ ___ -__ 41213141516171814209-12REDACTED VERSION UPurdue University Specimen

_________

Date: Average Load North South North Splice Mi i) South Splice LVDT North LVDT South North Load Cell South Load Cell DG North DG South Tm(Ibf) Overhang (in) Overhang (in) End (in) ___span_____ End (in) Support Support ..II L-- Ia Overhang (in) Overhang (in) Tm0.4 0 o 0 0 o 0 O _____ O~. o ' 0.2_ 0 0 0) 0 0 o-ool o.i_ o,-2 0 0.-900 _____ O.oO 0.c~ aOo2 0.0i o. oo'2. o.0oo1.. 6 0. I =P6 ____ o,' 0.04 0.01 0.09 o. 04 o. ooZ ' ~ .oGO8 l4011P1V 5 o.l. o5.9,5 o.o2. o-II oC4' 0c4 2e 15A -o.l o.92,5 2z'78'M* 1.oi 0.30 O.l9 o.17 o.I:7 0.05 20 30i 1-0.? I. 3:16W' z E ID & S ; _ _ _ _ ._ _ _ .o 00 ( J O)__ __o._ o.z8 o.Zf. o.00s o,0o/-osL L.5,Z.' 3:4411'"1 o o.59 0.39 0.05 0.o0 o.o5 o..oo3 o.oo'2 o ______ 12I 9.JG o.14 o~o 0.jI -o.Io .04 o.o0z __ __ _ .4_____o._______-_ 1.2l& .Q0 o0 I o.I .02 00o ___________. 14 3'._ 1.54 I. ¢ -_-___._ _ooo___ _____ --- -s ..o ?'M15161819209-13REDACTED VERSION U00Date: S ,.5 Purdue University Specimen" Average Lgad North South North Splice Mda(n) South Splice LVDT North LVDT South North Load Cell South Load Cell DG North DG South re-]1 Overhang (in) Overhang (in) End (In) Midspan___n) End (In) Support Support 4J.f I c Overhang (in) Overhang (in) Tmo.1_ .O__ O.0', 0 0 0 -0.0b06 0. O.10O 2 k.: .c,_ __ _ __ _ _ _ __ _ __ _ __ _S6 04i o~ 0.01 0.01 -oo 0.005Ooo .6 o.105 'Z-9A12 IO1.t 0.39 0.05 0.o0, 0.0ot -.xo~o, 12 V,2Z 1 8 0.:/5 0.1 0.0,9 o.ll 0.08 18 18 o.=jl %ob,4__________ .o__.$ O.l' o.oo,/ I.o3,L j4l~f _______.__-- i.0. ! oOZ ..1 -o.001 o.oob ffijZ- v.'S 1O-1i,10 _____ L, [,'& O.i~l 0,1 -OOOI 0.005 ?,5 1.16ft 1.2.56 " o o.o~t 0.05 -oo o.oo. o.z o.ApL o.So5 I0oA.o12 0.81 0.9,o o.11 0.13 0-!0 oR.o, 1l Z O.'Bo5 0.85 t2-IIo(,A 171.99-14REDACTED VERSION bbY;5-UUU-Ut$;5-U1:U-UUUlth-UUU I-'age oT 1114ApedxU:alrtoneticas Appendix 1U: (JertlTicates TAKING ACCURATE THERMAOMETER READINGSCOMMON TYPES OF THERMOMETERS AND FACTORS AFFECTING THEIR USETOTAL IMMERSION thermometers are designed with scales calibrated to indicate the true temperature when the bulb and the portion of thethermometer that contains the mercury column are exposed to the temperature to be measured (practically,, less than an inch is permitted to extendabove the surface,.o permit the reading to be made). Most total immersion thermometers can also be used in a condition of complete immersion, inwhich case the entire thermometer is exposed to the temperature being measured, such as in a freezer.PARTIAL IMMERSION thermometers are designed with scales calibrated to indicate the true temperature when the thermometers are immersed tospecified depths. The portion that should be immersed is indicated on the back of each thermometer. COMPUTATION OF EMERGENT STEM CORRECTION When total immersion thermometers are used only partially

immersed, a stem correction may he calculated and applied to the reading for precision results.

To compute an emergent stem correction, the following variables must be defined:T = the reading of the thermometer in situ.N = the number of degrees on the thermometer scale between the liquid surface and the top of the mercury column.A = the average temperature of the emergent mercury column. To find value A, suspend alongside the subject thermometer a secondary or auxiliary thermometer with its bulb centered between the liquid level and the temperature indicated on the subject. thermometer. The temperature indicated on this auxiliary thermometer will he value A.Find the stem correction (SC) by computation from the following formula:SC = 0.00016 x (N x (T-A)) for Celsius temperatures, orSC = 0.00009 x (N x (T-A)) for Fahrenheit temperatures. Example: A thermometer graduated from -1° to 101°C., immersed to 20°C on its scale, reading 90°C. The auxiliary thermometer reads 42C. Hence,T=90, N=70 (90.20). A---42Working the formula, SC =.00016 x (70 x (90 -42)) yields a value for SC of +.537. This value must he added to the observed indication of the subjectthermometer to determine the true temperature of the liquid. Hence, the true temperature of the liquid is 90° + .54° (rounded result) = 90. 540GENERAL CONSIDERATIONS FOR MAKING AN ACCURATE READ)INGThe error due to parlla may be eliminated by taking care that the reflection of the scale can be seen in the mercury thread, and by adjusting theline of sight so that the graduation of the scale nearest the meniscus exactly hides its own image: the line of sight will then be normal to the stem atthat point. In reading thermometers, account must be taken of the fact that the lines are of appreciable width. The best practice is to consider theposition of the lines as defined by their middle parts."PERFORMING A CALIBRATION AT THE ICE POINT (0 DEGREES CELSIUS OR 32 DEGREES FAHRENHEIT) Select clear pieces of ice, preferably made from relatively pure water. Discard any cloudy or unsound portions. Rinse the ice with distilled water andshave or crush into sm~all pieces, avoiding direct contact with the hands or any chemically unclean objects. Fill a Dewar or other insulated vesselwith the crushed ice and add sufficient distilled (and preferably precooled) water to form a slush, but not enough to float the ice. Insert the*thermometer, packing the ice gentiy about the stem, to a depth sufficient to cover the 0°C (32°F) graduation. As the ice melts, drain off some of thewater and add more crushed ice.Raise the thermometer a few millimeters after at least 3 minutes have elapsed, tap the stem gently and observe the reading. Successive readingstaken at least one minute apart should agree within one tenth of one graduation. APPLYING THE CORRECTION AT ICE POINTRecord readings and compare with previous readings. If the readings are found to be higher or lower than the reading corresponding tO a previouscalibration, readings at all other temperatures will he correspondingly increased or decreased. Reproduced in part from ASTM E77.KESSLER THERMOMETER CORP.Precision and ReliabilitY... from aname you can trust.REDACTED VERSION lbu)i-UUU-U.5IJ-U.1--U-UUU1Ii-UUU l-'age Ijuu ot 1114ApeixU:airtonetlcte Appendix 1U: L;allbratlon Cerl:lrlcates CALSER CORPORATION 302 N. BELT EAST SWANSEA, IL 62226(618)277-0329 TESTING MACHINE CERTIFICATE OF CALIBRATION Owner : Purdue University Report #:Location

1040 South River Rd. -Bowen LabWest Lafayette, IN 47907 Page :Machine : Fomey 600,0001bf Model F-600-DFM/1 Serial No. : 99058 -§ liaef wI Fomey DFM/1 Digital R/O #9902182wI/Dynisco P/T #02-23-990747 This is to certify that the testing machine listed above has been calibrated by Calser Corporation personnel.

The method Of verification and listed data are in accordance with ASTM E 4-09.Accuracy of all calibration devices is traceable to the National Institute of Standards and Testing (NIST)*and all calculations have been corrected for temperature where applicable. VN# 65602 of 20616111, Capacity RangeRun 1600,000lbf RangeRun 2600,0001bf RangeRun 3600,0001bf RangeLoading Range5,000 -600,0005,000 -600,0005,000 -600,000Max. Error1.20 %0.10 %0.08 %Verification Equipment Used:(400,000 Load Cell Set)Admet Gage Buster Digital Readout, Serial # GB-991 1092,and Load Cell(s) Listed Below.Serial # Ranne Calib. Date901 120B 716.99 -10,000 lbf 08/19/2009 090716C (LO) 5,572.38 -100,000 lbf 08/10/2010 0907160 (HI) 39,281.95 -400,000 lbf 08/10/201 0Uncertainty 1.792 16f13.931 lbf98.205 IbfThis cerlilicate is Issued as a statement of the fact that on the above date the listed testing machine has an accuracy as Indicated. It should notbe construed or regarded as a Guarantee or Warra~nty of any kInd (In favor of the client, the client's customers, or the public at large) that the testngmachine Will continue to retain the same percentage (%) of accuracy or efficiency as determined on the date when the calibration, and adjustments if required, was performed and reported by 'Calser Corqrration' since the calibrator has absolutely no control over the future operation, damage.maintenance,

repairs, and overa~l condition of the testing machine and hereby expressly disclaims any and aDlliaLbility for damage or loss sustained by all parties adslng or resulting from th deterioration, obsolescence, malfunction or substandard perfonnance of said testing machine; wtrlch*shall remain the sole responsribiliy of the machine's regula custodian.

owner. andlor user. This certilicate shall not be reporoduced except in full,without the written approval of Calser Corporation. CALSER CORPORATION Quality Control DirectorForm # 104-01-Rev 3REDACTED VERSION bbi-UUU-LUb3-Utz-U-UUUId-UUU l-'age bU1 OT 1114ApeixU:alrtonertcas Appendix 1U: Calibration CertlTicates A.CALSER CORPORATION 302 N. Belt East, Swansea, IL 62226 (618) 277-0329TESTING MACHINE CALIBRATION DATA AND REPORT,-.Customer Purdue University _ Location 1040 South River Rd. -Bowen Lab' West Lafayette, IN 47907-1Report #: VN# 6560Page 1 of 2Date of Service 06/06111Cost order No. VerbalOrder Date 06102/111 Temp. 74" FDate Done 05119110MachineSerial No.Auxilay Equiprnent: ,Fomey 600,0001bf Model F-600-DFMI1 99058w/ Fomey DFMfl Digital RIO #9902182I _____________w/D nisco P/T #02-23-990747 -_____AoppledForc __ _Ind'l cted Forel : rE, z I j)I " n l' et Frce r~ .E .I " 1 Idicted orc ErsIo"Run #1 _ Run #1 "As Formd" Co~rrdon __ Run #2 "As Left" Conclion Run #3 ."As Left" Condition 600,0001bf Range *__ l01bf/I DIV

00 60 0 0 0.00 60 0 0 0.00 6C 0 0 0.0015.000 60 4,940 -60 1.20 60 5,000 0 0.00 60 5,000 0 0.0010.000 7 9.880 -120 1.20 7 9.990 -10 0.10 7 10.000 0 0.0020,,000 7 19.790 -2.10 1.05 7 19,990 -10 0.05 7 ,19,990 -10 0.0540,000 8 39.530 -470 1.18 ,8 40.000 0 0.00 8 .40.000 0] 0.0060.000 8 59,340 -660 1.10 8 60.010 10 0.02, 8 " 60.000 0 0.0080.000! 8 79.1 50 -850 1.06 8 80.050 50; 0.06 8 80.030 30 0.04..00...00.............0..

.,8...........98940 ....0,05t1 -1.065 ... --.8 .... ...- 00 60*...........66(.....6 .6, -.80-.0........00.70 .100...070 .70 ...... 0.07007125.000 8 123.600 -1,400 1.12 8 90 0.07; 8 125.100 100 0.08150.0001 8 148.330 -1,670; 1.11. 8 150,150 150 0.10 8 150,120 120 0.08200.000 8 197,650 -2,350 1.18 8 199,980 -20 0.0,1. 8 200,010 10 0.01300,000 8 296,650 -3j30 1.12 8 300§6 60 0.02 8 300.040 40 0.01400.000 8 395.880 -4.120 1.03 8 400.120 120 0.03 8 400,090 90 0.02500,000! 8 495.110 -4.890! 0.98 8 500,260 260 0.05 8 500.210 210 0.04600,000 8 593,770 -620 1.04 8 600.310 310 0.051 8 600,290 290 0.050 8 0 20 0.00 8 0 -100O.00i8 0 -30 0.00Notes:D- Calibration in accordance with ASTM E4-09,! and Calser Corporation Procedure

1-01, Rev 1.ACCURACY SUMMARY ..capacity Rane Loadin Range Max. ErrorRun I1_____________

600,0001bf Range 5,000 -600,000 1.2.0 %Run 2 ______fl00,O001bf Range 5,000 -600.000 0.10 %Run3 3__________ 600,000!bf Range 5,000 -600,000 0.08 %*CAMBRATI.ON EQUIPMENT All verification equrlpmerf-Incuding dead weights, provin rings, load cells. etc., Iscalibrated and traceable to the latest procedu'es $tipulated by the National Ins titute ofStandards and Test~ng (NIST) and ASTM E74-06. All equipment is tr'aceable under9ukleeines set forth In ISO/IEC 17025. Alt instrument readings have been corrected fortemperature whiere necessary. _______ VERIFICATION EQUIPMENT _ _ _ _ _ _ _& Sertali ____ nd_ ncertalty(L.BF) & DateStrainsense 60 716.99 -10.000 Ibf Morehouse 901120B 1.792 lbf 08/19/09Strainsense 7 5,572.38-100,O0001bf Morehouse 0907160 (10) 13.931 Ibt" 08/10/10Strainsense 8 39,281.95 -400,000 lbf Morehouse 0907160 (HI) 98.205 Ibf 08110110This report shall not be copied except in its entiretywithout express written approval of Calser Corp.Formi# 103-01-Rev 3Calibraton Tedcnican Jerry ParkerI)REDACTED VERSION bbW~-UUU-Ud~-UbU"UUU~~-UUU wags Uu~ ot VI14 Appendix W: uslieritian Lertilicitis CERTIFICATE OF CALIBRATION ISSUED BY: INSTRON CALIBRATION LABORATORY DATE OF ISSUE: 30-Jan-12 CERTIFICATE NUMBER: 340013012113643 Lab code: 200301-0~instron825 University AvenueNSTRON~Norwood, MA 02052-2643 II C a" Teephone: (800) 473-7838Fax: (781) 575-5750Email: servicejreq uests~instran.cam Type of Calibration: Relevant Standard: ASTM E83-10Page 1 of 3 pagesAPPROVED SIGNATORY Richard-Digh ineo d b ihrfDNcn=Rlchard Binford,:c=US, l=Norwaod, st=MA,---v -- -5'00'Date of Calibration: 30-Jan-I12 Name: PURDUE UNIVERSITY Address:550 STADIUM MALL DR.WEST LAFAYETITEJ N 47907KBROWER@PURDUE.EDU KEVIN BROWERPRO.Contract No.:Contact:Manufacturer. BALDWIN Manufacturer. INSTRONSerial Number. 120BTEC502040 Transducer ID: 2630-115/590 System ID:.Range Type:120BTEC502040 SingleExtensometer Type:Travel (Tension): Travel (Compression): Gauge Length:Mode:Type Ilin0.1 in2inStatic (Tension/Compression) -At,-&r A'~?? z&L.The following indicators of the extensometer system were verified and classed:Indicator TypeIndicator Range Full ScaleUnits (%)SystemClassDescription

1. Digital Readoutstrain100B-IAll indicators listed above were verified on-site at customer location by Instron in accordance with ASTM E83.The verification and equipment used conform to a controlled Quality Assurance program which meets the specifications outlined in ANSIJNCSL Z540-I, 150 10012, ISO 900 1:2008 and ISO/lEO 17025:2005.

The testing machine was verified in the 'as found' condition. Instron Calpro Version 3.23The results indicted on this certificate and the following report relate only to the items verifed. If there aremethods or data included that arc not covered bythe NVLAP accreditation it wilt he identfifed in the comments. Any limitations of u.e as a result of this verification will be indicated in the comments. Thisreport must nrot be used to chins product endorsement by NVLAP or the United States government. This report shalt not be reproduced, except in lull, withoutthe approval of te issuing laboratory. REDACTED VERSION bb~6.UUUU~S-UbW-UUUlW-UUU rage wu~t or VI 14 Appendix iu: Lalibration Lartiticatma CERTIFICATE OF CALIBRATION NVLAP ACCREDITED CALIBRATION LABORATORY No. 200301-0CERTIFICATE NUMBER:340013012113643 Page 3 of 3 pagesIndicator

1. -Digital Readout (strain)RangeRun 1Indicated (strai)Applied(in) IRunZ2Indicated (st-ain)Applied(in)100% Range (Full Scale:l1.00016 in)Rim Temperature:

70.0 °F40 J 0.19991 0.400580701 0.34995 0.700010100J 0.49985 1.000162Run Temperature: 70.1 0F0.1995 0.4000130.349987 0.7000230.49899 1.000050Verification Equipment: SerialCalibration Measurement Make/Model Number Description Agency Range Cal Date Cal DueExtech 445580 1003552 temp. indicator Tektronix NA 12-Feb-il 12-Feb-13 Epsilon 3590VH1R A5010 disp. indicator Instron Ltd 2.00 in 14-Feb-I11 14-Feb-12 (ASTM)* Instron US Gauge Bar 1902 gauge bar £4 Jansson NA 11l-May-10 1 1-May-12* HBM ML38 90630412 force indicator Instron NA 21-Jan-li 21-Jan-13

Epsilon 3590 VHR AS010 (Note: Also used for displacement measurements and listed above.)(ASTM)* Equipment used for gauge length measurements.

Verification Equipment Usage:Measurement Serial RangeType Number (% Full Scale) Percent(s) of RangeDisplacement A5010 (ASTM) 100 0/10120140/70/100 Instron standards are traceable to NIST and/or other National standards. Verified by: Rich BinfordField Service EngineerNOTE: Clause 9 of ASTM E-83 states; It is recommended that extensometer systems be verified annually or more frequently ifrequired. In no case shall the time interval between verifications exceed 18 months (unless an extensometer is being used in along-time test running beyond the 18 month period). An extensometer system shall not be used after an adjustment or repairthat could affect its accuracy without first veritying its accuracy utilizing the procedure described in this practice. instron Caipro Version 3.23REDACTED VERSION

h~age tbU40oT 11 14Apeix1:ajrtonettcte Appenalx 3.U: Calibration (Jertltlcates INSTR:O:3N .CEAST/ Dynatup I Wilson / WOI.PE1RT itnstron-Service

825 University, Avenue .3-Norwood, MA 02062-2643 Tel" m

Fax: +1-78'1-575-5755 www.lnstron.com Field'Seivice Repor,Company:Address:*Contact;.

Service Order#:Field Engineer. Service Notes: '-550 Stadium Mail DriveCivi RoomG151*West Lafayette,'IN 47907.USA=Brower Kevin-.SV1201120017@§1 TCredit.Card 'Richard Binford :Reference

Contract Total Amount:.$2330.

Verified force,displcement~and~the extensometer. Keep aregular check on the pressure transducer oil~capsule

gap regulatly to' insure the .030" gap for accurate force readings.

Labor Activities-01130/2012-120BTEC502040 =0.02 S1400-003-A Zone 3 For Tensile Service01.121 .120BTEC502040 .1.00 -1460-011-A Crosshead.Displacement Verification 0113012012 1208TECS02040 2.00 S1481-017-C-A ..Force Verification. 68K Ib-300K lb_______ __________ _________ _______ __________Compression ,,01130/2012 2630-11'5/590 -120BTEC502040 .1.00 .$1490-003-A Strain Verification,. Static Ext or"__________________________ ______ _________Detfectometer Materialsi I I II .0113012012

Technical Support:

Service_Support@Instron.com Email: Serylcereq uests@lnstron.com Page I oiltREDACTED VERSION bbMI-UUU-.5-LdMI-Ub-JUU1U1-UUU 11196 iUb 0? 1114Apnax1:clirtnumrcts Appenalx 1U: Calibration Certificates CERTIFICATE OF CALIBRATION ISSUED BY :INSTRON CALIBRATION LABORATORY DATE OF ISSUE : 30-.Tan-2012 CERTIFICATE NUMBER: 340013012110833 Lab code: 200301-0Page 1 of 3INSTRON~Instron825 University AvenueNorwood, MA 02062-2643 Telephone: (800) 473- 7838Fax: (781) 575 -5755Email: serviceqrequests~instron.com APPROVED SIGNATORY Richard , icarBi" " i=Narwc°cd, st-MA, au=OVRB Vno rdCustomer Requested Due Date: 30-Jan-2013 Type of Calibration: 3D Relevant Standard: astm e2309Date of Calibration: 30-Jan-2012 9us1m&4Lt,. PURDUE UN~IVERSITY 550 STADIUM MALL DR.WEST LAFAYETITE, IN 47907I :~.ccw~gE~ 4'- .~ A..Serial No :Make :Model :C502040BALDWIN12OBTEP.O. Number :Contact :HARRY TIDRICK1. Digital Readout (in)This certifies that the displacements verified with machine indicator 1 (listed above) were venifled byr Instron inaccordance with ASTM E2309-05 (Follow-the-Displacement Method) and Instron work instruction ICA-8-07. The testing machine was verified on-site at customer location. Adjustments are noted in the comments section of thisreport with a reference to the "As Found" data.The verification and equipment used conform to a controlled Quality Assurance program which meets thespecifications outlined in ANSI/NCSL Z540-1, ISO 10012, 1SO 9001:2000, and ISO/fEC 17025:2005. The Instronmeasurement equipment used for verification is traceable to NIST.Indicator 1- Digital Readout (in)Verified Range(in)Max Error Max Error(in) (%)Max RepeatError(in)Max RepeatError(36)ASTMSystem Resolution Resolution Lower LimitClass* (in) Class (in)0.2 0.00268 -0.355 0.001 12 0.257 B .001 B 0.2*Sys tern Class is derived from assessment of the following: error, repeatability, resolution, and standard device classification. The results indicated on this certificate and report relate only to the items verified. If there are methods or data included that are notcovered by the NYLAP accreditation it will be identified in the comments. Any limitations of use as a result of this verification willbe indicated in the comments. This report must not be used to claim product endorsement by NYLAP or the United Statesgovernment. This report shall not be reproduced, except in full, without the approval of Irnstron. CalproSDS version 3.3REDACTED VERSION

b-UUU P'age dUb5 07"1114ApndxU:airtoneticae Appendix 1U: Calibration Certlllcates CERTIFICATE OF CALIBRATION ISSUED BY :INSTRON CALIBRATION LABORATORY DATE OF ISSUE : 30-Jan-2012 CERTIFICATE NUMBER: 340013012110833 I IPage 2of 3Direction of Displacement

Ascending Suggested Run I Runi1 Run 2 Run 2 Run 3 Run 3 RepeatValue IError Error Error Error Error Error Error Uncertainty Coverage(in) I(in) (%) (in) (%) (in) (%) (in) (in)* Factor = k0.2 0.00007 0.035 -0.00045

-0.222 -0.00026 -0.129 0.00052 0.00081 2.260.4 -0.00110 -0.276 -0.00086 -0.213 -0.00091 -0.227 0.00024 0.00070 2.260.6 -0.00105 -0.153 -0.00214 -0.355 -0.00176 -0.292 0.00109 0.00150 2.780.8 -0.00268 -0.331 -0.00156 -0.189 -0.00162 -0.203 0.00112 0.00165 2.781 -0.00168 -0.164 -0.00142 -0.142 -0.00198 -0.196 0.00056 0.00086 2.26*ThW reported expanded uncertainty of measurement is based on a combined uncertainty multipied by a coverage factor k toprovide a level of confidence of approximately 95 %.Runs 1 and 2 are performed to comply with the requirements of ASTM E2309, run 3 is performed to calculate the uncertainty ofmeasurement. Temperature at start of verification

67.9 0FRun 1Run 2Run 3Suggested ErrorValue Applied Indicated Class Applied Indicated 0.2 0.19993 0.200 A 0.20245 0.2020.4 0.39810 0.397 A 0.40286 0.4020.6 0.68605 0.685 A 0.60314 0.6010.8 0.80968 0.807 A 0.82356 0.8221 1.02568 1.024 A 1.00142 1.000For runs 1 and2.' the worst Resolution Class is B and the worst Repeatability Class isATemperature at end of verification

70 0FErrorClassAppliedIndicated AAAAA0.201260.400910.601760.799621.007980.2010.4000.6000.7981.006Starting Point of crosshead

0 inUncertainty ofMake/Model Serial No. Description Cal Agency Calibration Resolution Cal Date Due DateInstron LDS-10 06105014 Linear Gage AA .IANSSONEXTECH 445580 1003552 Thermometer TEKTRONIX The standards used for this verification are traceable to NIST..000013 in1 °F.00001 in 3-Aug-10 3-Aug-12.I°F 12-Feb-Il 12-Feb-13 CalproSDS version 3.3REDACTED VERSION YiU-uuu-LUb-i-L-UU-uu1 d-UUU Page bUt oT 1114 Appendix 1U: Calibration certiticates CETIIATE OF CALIBRATION ISSUED BY : INSTRON CALIBRATION LABORATORY DATE OF ISSUE : 30-Jan-2012 CERTTFICATE NUMBER: 340013012110833 Page 3 of 3Verified By:RICHARD BINFORDSNR.SERV.ENGR, CalproSDS version 3.3REDALTED VERSION

~bbU-UUU-yU3-UbU--UUUltU-UUU Huge 01"1114 Apni U mirto ettcuAppendix 1U: Calibration CeFtltlCates CERTIFICATE OF CALIBRATION ISSUED BY: INSTRON CALIBRATION LABORATORY DATE OF ISSUE: 30-Jan-12 CERTIFICATE NUMBER: 340013012095410 IINF[ tIL_4jInstronLab code: 200301-0825 University Avenue Page 1 of 4 pagesID "'R O N Norwood, MA 02082-2643 APPROVED SIGNATORY I T R~Telephone: (800) 473-7838 "Digitally signed by RichardEalFax: (781) 575-5750 sevc euss~nto~o ichoa rd ' BinfordEmai: sevlceequets~istra~comU~ItI.C ON: cn=Rlchard Binford,Sc=US, I=Norwood, st=MA,Type of Calibration: @ V Date: 2012.01.30 11:08:19o -05'00'Relevant Standard: ASTM E4-1 0Date of Calibration: Customer Requested Due Date: 30-Jan-13 Name: PURDUE UNIVERSITY Address: 550 STADIUM MALL DR.WEST LAFAYETrE,IN 47907KBROWER@PURDUE.EDU P.Ol/Contract No.:Contact: KEVIN BROWERManufacturer: BALDWIN Manufacturer. BALDWINSerial Number, 120BTEC502040 Transducer ID: 120BTEC502040 System ID: 120BTEC502040 Capacity: 120000 lbfRange Type: Single Type: Compression

1. Digital Readout -PASSEDThis certifies that the forces verified with machine indicator(s)

(listed above) that passed are WITHIN +t 1 % accuracy, 1 %repeatability, and zero return tolerance. All machine indicators were verified on-site at customer location by Instron in accordance with ASTM £4.The certification is based on runs 1 and 2 only. A third run is taken to satisfy uncertainty requirements according to ISO 17025specifications. The verification and equipment used conform to a controlled Quality Assurance program which meets the specifications outlined in ANSIINCSL Z540-1, ISO 10012, ISO 9001:2008 and ISO/IEC 17025:2005. The testing machine was verified in the 'as found' condition with no adjustments carded out.Instroa CalproCR Version 3.23The results indicated on this certificate and the following report relate only to the items verified. If there are methods or data included that are not covered by the NVLAPaccreditation it will be identified in the comments. Any limitations of use as a result of this verification will be indicated in the comments. This report must not be usedto claim product endorsement by NVLAP or the United Staten government. Thin report shall not be reproduced, except in fisil, without the approval of the issuinglaboratory, REDACTED VERSION b~W5-UUU-I~iWj-tjbU-UUU~I~.UUU wage ~UU 0? VI14 Appendix w: Lalrnration Certaticates I CCIDTEIIP/ATE: ('Al IDDATIfiklI UI U vf I !, %f U VIrlLi.,U~lfall U fI 'I,11 CERTFIFCATE NUMBER:340013012096410 NVL.AP ACCREDITED CALIBRATION LABORATORY No. 200301-0Pg o aeTemperature at start of verification: 67.00 0F.Indicator

1. -Digital Readout (ibf)Range ASTM E4 ASTM E4 ASThI E4Full Scale Tested Force Range Max Max Repeat Zero Resolution Lower Limit(%) (lbf) Mode Error (%) Error (%) Return (lbf) (IbI100 -1194.4 to -119044.9 C 0.88 0.1I1 Pass 1 200Temperature at end of verification:

67.80 0F.-'s A 4'~ .... .... ". ... ...... ....... .' 2', g ' .&; "-COMPRESSION Run 1 Run 2 Run 3 ASTM E4 Relative Uncertainty ofError Error Error Repeat Error U~ncertainty* Measurement* % of Range (%) (%) (%) (%) (%) (+/- lbf)100% Range (Full Scale: -119044.9 INf)1 0.47 0.43 0.43 0.04 0.14 1.6612 O.41 0.48 0.49 0.07 0.14 3.3214 0.42 0.46 0.45 0.04 0.13. 6.2137 0.77 0.76 0.77 0.01 0.14 11.25410 0.82 0.75 0.76 0.07 0.14 16.90820 0.88 0.77 0.78 0.11 0.15 36.18740 0.81 0.81 0.80 0.00 0.14 64.28370 0.81 0.80 0.81 0.01 0.14 112.494100 0.80 0.81 0.81 0.01 0.14 160.702* The reported expanded uncertainty is based on a standard uncertairny multiplied by a coverage factor I = 2. providing a level ofconfidence of approxhnately 95%.COMPRESSION Indicated Applied Indicated Applied Indicated Applied% of Range (lbf) (b) (INb) (ibI (Ibi) (Ib)100% Range (Full Scale: -119044.9 Ibt)0OReturn 1 0 1200 -1194.4 -1200 -1194.9 -1200 -1194.852 -2400 -2390.3 -2400 -2388.5 -2400 -2388.24 -4800 -4780.1 -4800 -4777.95 -4800 -4778.57 -8400 -8335.52 -8400 -8336.7 -8400 -8336.1110 -12000 -11902.07 -12000 -1191023 -12000 -11909.74 20 -24000 -23789.98 -24000 -23815.94 -24000 -23815.35 40 -48000 -47615.95 -48000 -47615.36 -48000 -47618.970 -84000 -83326.29: -84000 -83333.37 .-84000 -83327.47 100 -120000 -119044.89 -120000 -119034.86 -120000 -119034.86 Instran CalproCR Version 3.23REDACTED VERSION ~bWs-UUU-UU~-U~U-UUU1U-UUU i~age wiU 0? VFI4 Appendix iu: Lallbratlan LartItacates f'lC r'AI IDDATrIflL ',lglx II U[1 Jfl/ I En %I flfl/ I IVI CERTIFICATE NUMBER:340013012095410 NVLAP ACCREDITED CALIBRATION LABORATORY No. 200301-0Page 3 of 4 pagesThe Return to Zero tolerance Is the indicator resolution, 0.1] % of the maximum force verified in the range, or 1 % of the low ast forcever f/led in the range, whichever is greater.100% Range1.2 Compression 0.8 3 S,, 0.4 N-t- Runi10 -0_____________________ -Run 2-1.00%*IU -0.4 ______________________________ -1.00%**tASTM E4 Error Tolerance -0.8-1.2o o o 0 0 .1 7 "Percent of RangeSerial Calibration Make/Model Number Description Agency Capacity Cal Date Cal DueExtech 445580 1003552 temp. indicator Tektronix NA 12-Feb-l 1 12-Feb-13 HBM ML38 90630412 force indicator lnstron NA 21-Jan-il 21-Jan-13 Strainsense 050530 050530 load cell Instron 120000 lbf 10-Dec-10 10-Dec-12 HBM IOKFRR 688077 load cell Instron 12000 1Wf 24-Apr-10 24-Apr-12 Range Lower Limit fbrFull Scale Standard Standard Class(%) Serial Number Mode Percent(s) of Range A / Al (lb,1100 050530 C 7/10/20/40/701100 5000 /5000100 688077 C 1/2/4 200 /200Instron standards are traceable to NIST.The standard Class A lower limit is used for systems with on accuracy of +/- 1.0% and the standard Closs A1 lower limit is used forsystems with on accuracy of +1- 0.5%Standard forces have been temperature compensated as necessary. Instron CalproCR Version 3.23REDACTED VERSION

-'age b1i 0i" 1114ApedxU:airaonertcte AppeFidlX 1U: Calibration Certlllcates CERTIFICATE OF CALIBRATION ISSUED BY: INSTRON CALIBRATION LABORATORY DATE OF ISSUE: 12-Apr-12 CERTIFICATE NUMBER: 516041212091759 Lab code: 200301-0INS---RON 5Type of Calibration: Relevant Standard: Date of Calibration: Instron825 University AvenueNorwood, MA 02062-2643 Telephone: (800) 473-7838Fax: (781) 575-5750Email: service requests@instron.com StrainASTM E83-1012-Apr-12 Page 1 of 3 pagesAPPROVED SIGNATORY Jimm\ Digitally signed by Jimmy Warnerg II I II I I UI N: cn=Jimmy Warner, c=US,/ \l=Norwood, st=MA, ou=OVR?¢ Reason: I attest to the accuracyA I e I and in~tegnty. of this documentVd -[11 [Date: Customer Requested Due Date: 23-Mar-13 [Customer 'Name:Address:P.0./Contract No.:Contact:Purdue University 550 Stadium Mall DriveCivil Room G151West Lafayette IN 47907sarahh@purdue.edu Kevin Brower1MachineTransducer , .Manufacturer: Serial Number:System ID:Range Type:BALDWIN120BTEC502040 120BTEC502040 SingleManufacturer: Transducer ID:Extensometer Type:Travel (Tension): Gauge Length:Mode:EPSILON3543-0800-200T-ST/E89895 Type 12 in8 inStatic (Tension) Clsification ,-The following indicators of the extensometer system were verified and classed:Indicator Indicator Range Full Scale SystemType Description Units (%) ClassI. Digital Readout strain 100 B-iCertification Statement All indicators listed above were verified on-site at customer location by Instron in accordance with ASTM E83.S .,4tThe verificationi and equipment used conform to a controlled Quality Assurance program which meets the specifications outlined in ANSI/NCSL Z540-l, ISO 10012, ISO 9001:2008 and ISO/IEC 17025:2005. The testing machine was verified in the 'as found' condition. Instron Calpro Version 3.23The results indicated on this certificate and the following report relate only to the items verified. If there are methods or data included that are not covered bythe NVLAP accreditation it will be identified in the comments. Any limitations of use as a result of this verification will he indicated in the comments. Thisreport must not be used to claim product endorsement by NVLAP or the United States government. This report shall not be reproduced, except in full, withoutthe approval of the issuing laboratory. REDACTED VERSION

r-age b512 or 1114 Apni U a~ainCriiae AppencllX 1U: Calibration Certltlcates PI::DTICIP^Ti: t"tl: PAl mL-I I I I r' I I. VI i i!.ii CERTIFICATE NUMBER:516041212091759 NVLAP ACCREDITED CALIBRATION LABORATORY No. 200301-0Page 2 of 3 pages[Summary of ResultsIndicator

1. -Digital Readout (strain)Range ASTM E83Full Scale Tested Range System Resolution Resolution Lower Limit(%) (in) Mode Class* (strain)

Class (in)100 0.2 to 2 Tension B-i 0.00000 1 A 0.0008* System Class for a range is the worst of the following classes: gauge length class, resolution class, individual point errorclass, repeatability class and is also based on the measurement capability of the laboratory. [Gauge Length Measurement and Classification] Nominal Actual Error in ASTM E83 Uncertainty ofGauge Length Gauge Length Measurement Gauge Length Gauge Length Measuremnent* (in) (in) Type (%) Class (in)8 7.9897 Direct -0.13 B-i 0.0062* The reported expanded uncertainty is based on a standard uncertainty multiplied by a coverage factor k = 2, providing alevel of confidence of approximately 95%.[Data Summary and Classification] Indicator

1. -Digital Readout (strain)Run 1 Error Run 2 Error RepeatI Uncertainty of% of Fixed Relative Fixed Relative Error[ Worst Measurement*

Range (strain) (% of strain) (strain) (% of strain) (strain) j Class (strain)100% Range (Full Scale: 2 in)10 0o00000 0o1 -0o0001 -0037 0.00001 A 0.00002520 -0.00003 -0.0541 0.00000 -0.0041 0.000031 A 0.00004240 0.00003 0.0281 0.00003 0.0341 0.000001 A 0.00007970 0.00001 0.005 0.00005 0.028 0.00004 A 0.000137100 -0.00016 -0.064 -0.00019 -0.074 0.00003 A 0.000195* The reported expanded uncertainty is based on a standard uncertainty multiplied by a coverage factor k = 2, providing alevel of confidence of approximately 95%.[DataIndicator

1. -Digital Readout (strain)Runi 1j Run 2% fIndicated AppliedI Indicated AppliedRange (strain)

(in) (strain) (in)100% Range (Full Scale: 2 in)Run Temperature: 73.0 0F Run Temperature: 73.3 0F0 0.00000o1 0.000000 0.000006 0.0000001 0 0.025004 0.200000 0.024998 0.20001020 0.049975 0.4000 10 0.050004 0.400000Instron Calpro Version 3.23REDACTED VERSION bbU;-UUU-Udi3-~LS~--UUU1b-UUU I-'age b1i o1T 1114ApedxU:alrtoneriits Appenalx 1U: L:allDratlon Certltlcates tIEDTIEIIPATI= flE fPAl II:DATIfltM mum--I I I I -1" I I. !.I l.lllIllU I CERTIFICATE NUMBER:516041212091759 NVLAP ACCREDITED CALIBRATION LABORATORY No. 200301-0Pae3o3pgs [DataIndicator

1. -Digital Readout (strain)% fRuni 1 Apie Run 2%ojIndicated ApidIndicated AppliedRange (strain)

(in) j(strain) (in)100% Range (Full Scale: 2 in)Run Temperature: 73.0 °F Run Temperature: 73.3 0F401 0.100030 0.800010 0.100040 0.800000701 0.175010 1.400000 0.175060 1.400040100 0.249840 2.000000 0.249820 2.000000Verification Equipment adUsageVerification Equipment: Serial Calibration Measurement Make/Model Number Description Agency Range Cal Date Cal DueExtech 445580 984437 temp. indicator Tektronix NA 28-Dec-il 28-Dec-13 Boeckeler Micrometer 20641 disp. indicator A.A. Jansson 2.00 in 07-Oct-il 07-Oct-12 1398 (ASTM)* Fowler Economy SH9J2879982 disp. indicator AA Jansson NA 20-Apr-10 20-Apr-12 Electronic

Equipment used for gauge length measurements.

Verification Equipment Usage:Measurement Serial RangeType Number (% Full Scale) Percent(s) of RangeDisplacement 20641 (ASTM) 100 0/10/20/40/70/100 Instron standards are traceable to NIST and/or other National standards. [Comments] noneVerified by: James WarnerField Service EngineerNOTE: Clause 9 of ASTM E-83 states; It is recommended that extensometer systems be verified annually or more frequently ifrequired. In no case shall the time interval between verifications exceed 18 months (unless an extensometer is being used in along-time test running beyond the 18 month period). An extensometer system shall not be used after an adjustment or repairthat could affect its accuracy without first verify'ing its accuracy utilizing the procedure described in this practice. Instron Calpro Version 3.23REDACTED VERSION bYi-UUU-Ubi3-UW(,-UUU1b-UUU h-'age til 4 o011114ApeixU:airaonettcts Appendix "IU: Calibration Cerl:lllcates CALIBRATION CERTIFICATE Address86 Seabro AvenueAniltyville, NY 11701Websitewww.kessslerusa.com KESSLER THERMOMETER CORPORATION Telephone 631-841-5500 Facsimile 631-841-5553 E-mailKesslerUSA@aol~com CALIBRATION REPORT FOR THERMOMETER THIS REPORT OF CALIBRATION SHALL DOCUMENT THAT ThE INSTRUMENT DESCRIBED HEREIN WAS EXAMINED AND TESTED INKESSLER'S CALIBRATION LABORATORY AGAINST NIST TRACEABLE REFERENCE STANDARDS, IN ACCORDANCE TO KESSLER'S PROCEDURE T-2008, WHICH IS BASED ON ASTM E-77-98 (2003) AND NIST PIBLICATION 250-23. THIS CALIBRATION MEETS THEREQUIREMENTS OF ISOIIEC 17025, ANSI/NCLS Z2540-1 -1 994 AND THE ISO 9000 AND QS 9000 SERIES OF QUALITY STANDARDS. CUSTOMER INFORMATION: GILSON COMPANY, INC..Purchase Order Number: P000096475 Date Calibrated: September 20, 2011INSTRUMENT DESCRIPTION: Next Recommended Due Date: October 20, 2012Serial No.: 689373Scale Range: 30/124°FMarked: KESSLER USADivisions: 0.2°FCatalog No.: 6340-FCImmersion: 3"RESULTS OF PHYSICAL EXAMINATION: ......This instrument was examined under a polarized lens and strains in the glass, if any, were juidged to be minimal and of no detriment tothe function of the instrument. The capillary was examined under magnification and no irregularities or foreign material was.discovered. It was determined that this instruent was suitable for calibration. RESULTS OF CALIBRATION: TEST TEMP32.0060.0080.00100.00120.00READING32.0460.0080.20100.20120.20CORRECTION -0.040.00-0.20-0.20-0.20UNCERTAINTY +/-0.06+/-0.06+/-0.06+/-0.06+/-0.06* The above readings were made under magnification and resolved to one tenth of one scale division.

The indications of this instrument cannot be adjusted or modified by ordinary means: accordingly, the readings given in thetable above should be considered, in effect to be both "As Found" and "As Left" rfeadings
Laboratory Environment Conditions:

Temperature: 25°C +/-+ 50C / Relative Humidity: Between 40% and 60%* All temperatures given in this report are based on the International Scale of 1990 (ITS-90)TRACEABILITY INFORMATION: NIST Primary Standard: Rosemount Model 162CE Serial No. 5058Transfer Standard: Hart Scientific 1502A Serial No. A 14422 / 547027Approved By: John LewisCalibration Performed By: Barbara PlazaCalibration Report Prepared By: RPReport No.: 092011-03 1REDACTED VERSION

i-'age bib ot 1114ApeixU:alraonettcte Appendix 1U: Calibration (.:ertlllcates CALIBRATION REPORTPI TAPE[Report Number: I02221223040412 Date Issued:] Apr-04-12 Pi Tape Corporation Serial Number: 02221223Tape Size: 2" -12" 0.0.Actual Findings and Procedure NumbersTape Reads 4.9000 Over 4.9000" IProcedure 1Remarks: New GageCalibration Equipment UsedS Gage I Serial Number I Test Date I Due Date I NIST Traceable Report Number4.9" 102098 *May-12-I1 May-12-12 86903-1This tape has been checked at one or more points over a calibrated measuring standard. Calibration performed in accordance with ANSI/NCSL Z540-1-1 994, ISO/IEC 17025 and the former MIL-STD 45662A.All standards are traceable to the National Institute of Standards and Technology Jerry Mathis, Quality Assurance ManagerThis calibration report shall not be reproduced, except in full, without the written approval of the issuing laboratory. Results listed relate only to the item beIng calibrated. Pi Tape Corporation 344 N. Vinewood St. Escondido, CA 92029 USAPhone (760) 746-9830 Fax (760) 746-9196www.pitape.com Page 1 of 1REDACTED VERSION

Jl-'age btl 0? A114CERTIFICA T D'ETALONNAGE KALIBRIER-ZERTIFIKA TCALIBRATION CERTIFICATE ~\ 2N026594DateDatumDate13.10.2009 ObjetGegenstand ObjectTypeTypModelNum6ro de s~rieSerien-Nummer Serial numberInstrument verticalVertikal-Messgerait Vertical instrument V1004+10473 /ADate d'dmission du certificat Ausgabedatum des Zertifikates Certificate issue date13.10.2009 Ddclaration de confirmit6 L'instrument de mesureauquel se r~f~re ce certificat a et6 conformdment aux donnees techniques deTRIMOS contenues dansles documents de vente(prospectus, manuelsd'utilisation). Ko nformititserkliirung Das Messgerat;,auf weiches sich diesesZertifikat

bezieht, wurdeentsprechend den vonTRIMOS in den Verkaufs-unterlagen (Prospekte, Gebrauchsanleitung) angegebenen technischen Daten hergestellt.

Conformity declaration The measuring instrument to which this certificate refers to has beenmanufactured inacordance with the givenTRIMOS specifications stated in sale documents (leaflets, instructions foruse).Responsable departement qualit6:Leiter der Qualitatsabteilung: Manager of quality department: Gilbert VillardContr61eur: Pn~ifer:Inspector: Philippe DespondsLa publication ou Ia reproduction de ce document n'est autorls~e que dans sa forme Der Inhalt dieses Dakumentes darf nur in voltstindiger Form ver~ffentlicht oder weitergegeben werden.This document may not be published or forwarded other than in its entire form.PageSeitePage118I TRIMOS SAS++41 21 633 01 01Av. de Longema lie 5 CH-1 020 Ren ensS++41 21 633 01 Switzerland htto://www.trimos.ch mtitiUUU-ubJ-u._i-UUU1 b-UUU l-h'age till ot )l 14 ICERTIFICA T D'ETALONNAGE KALIBRIER-ZERTIFIKA TCALIBRATION CERTIFICATE RMO~IN 26594DateDatumDate13.10.2009 Caract6ristique do r'objet mesur6Merkmale des Gegenstander der Kalibrierung Features of the calibrated objectNornbre d'axes de mesuresAnzahl der Messachsen Number of measuring axis1Etendue de mesureMessbereich Measuring range0 -990 mm0- ?~ci7~A(Coefficient de dilatation lin~aireLinearer Ausdehnu ngskoeffizient Linear expansion coefficient Etalonnage Kalibrierung Calibration Accessoire(s) utilis6(s) Verwendete ZubehoreUsed accessories Pas de mesureMessstufen Measuring stepsNombre de serie de mesuresAnzahl von Messreihen Number of measurement series11.5 V-120 mm t '-3Principe de mesureMessprinzip Principle of measurement Condition de Referenzbedingungen Reference conditions En montantAntastung aufw~rtsUpwards direction Temperatures / Temperatur / Temperature Humiditd relative / Relative Luftfeuchtigkeit / Relativ humidityPression d'air / Luftdruck / Air pressureLa publication ou la reproduction de co document n'est autoris~e que dans sa forina int6grale. Der Inhalt dieses Dokumentes daif nut in volistindiger Form ver(Tffeantliclht oder weitergageben wardenl.This document may not be published or forwarded other than in its entire form.20°C +/- 0.5°C50% +/- 5%722 mm HgPageSeitePage2/8I TRIMOS SAS++41 21 6330101OAv. de Longemalle 5 CH-1 020 RenensS++41 21 633 01 Switzerland! httD:llwww.trimos.ch Iti~-U-G~-U~5UURt-UU4M-'g bt iCERTIFICA T D'ETALONNAGE KALIBRIER-ZERTIFIKA TCALIBRATION CERTIFICATE N° 26594DateDatumDate13.10.2009 Etalon do rMf~rence et traa~bilit6 Bezugsnormal und R(Jckverfolgbarkeit Reference standard and tracability Los r~sultats de mesure contenus dans ce certificat se r~fdrent, par unetra~abilit6 documentf~e, aux dtalons reconnus sur le plan national et dont Ia conformit6 avecle syst~me international d'unit6 (SI) est ddmontrde. L'4talon do rf6frence est composd desdl~ments suivants:* Die in diesem Kalibrierzertifikat erhaltenen Ergebnisse von Messungen sind Bezugs-normale bsw. Einrichtungen auf national Normale rickverfolgbar. Deren Uboreinstimmung ist durch das Internationale Einheitensystem (SI) nachgew~iesen. Das Bezugsnormal bestehtaus folgenden Elementen: All measurement results contained in this calibration certificat~e maintain a link, of tracability recognized by national standards. -Teir accordarl( with the international system (SI) isproved. The referonce standard is composed~of the fo/llowing cmp~nents: !Etalon do reference Bezugsnormal Reference standardN° des~reSerien-Nr. Serial no.N" du certi6fiat Zertifikat-Nr. Certificate no.Etalonn6 parKalibriert durchCalibrated byChock-Master 800002 81228 Fabricant Equerre 215-904 E310Z106 Kunz SCSMarbre 2000x1800 1644 R402B028 Kunz SCS* Mdtrologie et accre.ditation suisseLa publication ou la reproduction de co document n'est quo dans sa forme int~grale. Der Inhalt dieses Dokumentes dart nut in vonlstindiger Form ver~ffentlicht odor weitergegeben werden.This document may not be published or forwarded other than in its entire form.PageSeitePage3/8I TRIMOS SAS++41 21 633 01 01Av. de Longemalle 5 CH-1 020 Renenstt++4! 21 g33 01 0 Switzerland httD://www~trimns.ch ~1-UUU-U-ti~¶i-UUUTh-UUU ~ age tilti O]114R MOSCER TIFICA T D'ETAL ONNA GEKALIBRIER-ZERTIFIKA TCALIBRA TION CERTIFICATE N026594DateDatumDate13.10. 2009JustesseRichtigkeit Freedom from bias* S~iel* S&1e2AS&Srie3IValeur reelleWahrer WertTrue valuemm0.00009.999930.000350.000470.000790.0007110.001130.0009150.0009170.0009190.0009S6rle 1Serie ISeries 1mm0.00010.00030.00050.00070.00090.001110.001130.001150.000170.000189.999S6rie 2 S6rie 3Serie 2 Sele 3Series 2 Series 3mm mmMoyenne Ecart moyenMittenwert Mittenabweichung Average Average deviation mm n0.00010.00030.00049.99970.00090,001110.001130,001150.000170.000189.9990.00010.00030.00049.99970.00090.000110.001130.001150.000170.000189.9990.00010,00030. 00049.99970.00090,001110.001130.001150.000170.000189.9990.00.1-0.3-1.1-0.70.00.00.1-0.9-0.9-1.9La publication ou la reproduction de ce document n~est autodts~e que cdans sa forme int~grale. Der' Inhalt dieses Dokumentes dadt nur in vollstindiger Form Vert~ffentlicht oder weltergegeben werden.This document may not be published or forwarded other than in its entire form.PageSeitePage418I TRIMOS SA Av.de Longemalle 5 EATD CH-1020 Renens+ +41 21 633 01 01 -+-41 21 633 01 @trimosD hSwitzerland htto;//www.trimos.ch

b-UUU tZU at 1 14CERTIFICA T D'ETALONNAGE KALIBRIER-ZERTIFIKA TCALIBRATION CERTIFICATE N° 26594DateDatumDate13.10.2009 Valeur vraieWahrer WertTrue valuemm210.0009230.001250.001270.001290.0009310.0009330.0007350.0006370.0006390.0006410.0006430.0006450.0004470.0006490.0003510.0004530.0002550.0002570.0001590.0001610630650670.0001689.9999709.9999729.9997749.9997769.9998789.9998809.9997829.9998849.9997869.9996889.9996909.9998929.9997949.9996969.9995989.9996S6rle 1Serie 1Series 1mm209.999230,000249.999269.998289. 998309.999329.999349.998369.998389.999409.99842.9988449.998469.998489.998509.998529.997549.998589.998609.997629.998649.997669.998689.997709.998729.997749.998769.997789.997809.997829.997849.997869.998889.997909.997929.997949.997969.997989.997S6rle 2Serie 2Series 2mm209.999230.000249.999269.998289.998309.999329.998349.998369.998389.999 429.998.449.998 S469.998S489.998 529.997 .569.997-589.998 629.998649.997669.998689.997709.998729.997749.998769.997789.997809.997829.997849.997869.998889.997909. 997929.997949.997969.997989.997S6rie 3 Moyenne Ecart moyenSerie 3 Mittenwert Mlttenabweichung Series 3 Average Average deviation mm mm p209.999230.000249.999269.998289.998309.998329. 998349.998369.998389.998409.998429.998-449.998469.998!489.998S52 9.998S549.998569.997589.998.609.997629.998649.997669.998689.997709.998729.997749.998769.997789.997809.997829.997849.997869.998889.997909.997929.997949.996969.997989.996209.999230.000249.999269.998289.998309.999329.998349. 998369.998389.999i409.998429.998'469.998S489.9981 509.99829.997997, 5!89.998629.998649,997669.998689.997709.998729.997749.998769. 997789.997809.997829.997849.997869.998889.997909.997929.997949.997969.997989.997PageSeitePage-1.90-1.00-2.00-3.00-2.90-2.23-2.37-2.60-2.60-1.93-2.60-2.60-2.40-2.60-2.30-2.40-2.87-2.20-3.10-2.10-3.00-2.00-3.00-2.10-2.90-1.90-2.70-1.70-2.80-2.80-2.70-2.80-2.70-1.60-2.60-2.80-2.70-2.93-2.50-2.935/8La publication ou la reproduction de ce document n'est que dlans sa forme int~grale. Der Inhalt dieses Dowumentes dadf nur in vollstindiger Form ver6ffentlicht oder weitergegeben werden.This document may nat be published or forwarded other than in its entire form.I TRIMOS SA Av. de Longemalle 5 CH-1 020 RenensS++41 21 633 01 01 ++41 21 633 01 oFEDACTED VElf~Itrimos,¢h Switzerland httD://www.trimos.ch )agebLz]ot 1114CERTIFICA T D'ETALONNAGE KALIBRIER-ZER TIFIKA TCAL.IBRATION CERTIFICA TEfRtMOSN° 26594DateDatumDate13.10.2.009 R6sultas do mesureMessergebnlsse Measurement resultsErreur maximale autorisee Max. Fehlergrenze Maximum permissible errorErreur maximale Gr~sste gemessene Abweichung Maximum error measured5.8 ptm3.2 p.rmFid~IiteWiederholpraizision Repeatability +/- 2s <2 jiIncertitude do mesure ',. Messunsicherheit

i ..Uncertainty of measurement L'iceritue d meure"U"indiqu~e pouir la determination erreurs de mesures englobe:l'objet r'~talon de r&f&ence, l'0tendue de mesure et les conditions de r~f~rence.

Die nachstehend angegebene Messunsicherheit "U" fi~ir die Ermittlung der Messabweichungen umfasstfolgende Komponente: das kalibrierte Objekt, das Bezugsnormal, den Messbereich unddie Referenzbedingungen. The uncertainty of measurement "U" for the determination of the errors of measurement given hereafter includes the calibrated object, the reference

standard, the measuring range and the reference conditions.

le niveau de confiance est de 95%Das Vertrauensniveau betr~igt 95%Confidence probability is 95%Incertitude de mesureMessunsicherheit Uncertainty of measurement K =2U 95 = 2.5 jm + (L(mm) / 300 )La publication ou la reproduction do co document n'est autodis~e quo dans so fornme int~grale. Der Inholt dieses Dokumentes dadt nur in volistindiger Form verbffentllcht odor weitergegeben worden.This document may not be published or forwarded other than in its entire form.PageSeitePage6/8I TRIMOS SAS++41 21 6330101OAv. de Longemalle 5 CH-1 020 Renens& ++41 21 6330 OlO[EDACTED VEfl~~trimos.ch Switzerland htto:I/www.trimos.ch

b-UUU t-'age t>LZ ot 114CERTIFICA T D'ETALONNAGE KALIBRIER-ZERTIFIKA TCALIBRA TiON CERTIFICATE R!IN026594DateDatumDate13.10.2009 C6ntrole de la perpendicularite ( direction de mesure )Kontrolle der Rechtwinkligkeit ( Messrichtung )Checking of the squareness ( measuring direction )10.0 I I t I-2 ~Q~04Q~__600 700 800 90010-10HauteurHoheHeightmm050100150200250300350400450500EcartAbweichung Deviation 0.0-1.0-2.0-2.0-2.0-2.0-3.0-3.0-2.0-2.0-4.0La publication ou Ia reproduction de ce document n'est autorisie que dans sa forme Der Inhalt dieses Dokumentes dalrf flur in vo~llstindiger Form ver~ffentlicht oder weitergegeben werden.This document may not be published or forwarded other thian in its entire form.PageSeitePage7/8I TRIMOS SAS++41 21 63301 01Av. de Longemalle 5 CH-1 020 RenensS++41 21 633 01 0 VE~!tI!;rimos~ch Switzerland http://www.trimos.ch I-age tiuj or CER TIFICA T D 'ETAL ONNA GEKALIBRIER-ZERTIFIKA TCALIBRATION CERTIFICA TEN026594DateDatumDate13.10.2009 HauteurHoheHeightmm5506006507007508008509009501000EcartAbweichung Deviation -4.0-4.0-4.0-6.0-6.0-6.0-8.0-8.0-8.0-8.0Resultats du contr~le do la perpsndicularit6 ( dane s !direton de mes.* ) :Ergebnisse der Rechtwinkllgkeltprflfung (in MessuiChtun~g)

Resulits of squareness In

....Erreur maximale autoris~e

-Max. angegebene Fehlergrenze

Maximum permissible error -Erreur de la perpendicularit6 mesur~eGemessene Rechtwinkl igkeitsa bweichung Squareness error measured12.0 j!tm8.0 j~mLa publication ou la reproduction de ce document n'est autoris~e que dans sa forrme int~graie.

Der inhalt dieses Dokumentes darf nur in volistindiger Form verbffentlicht oder weitergegeben werden.This document may not be published or forwarded other than in its entire form.PageSeitePage818I TRIMOS SAS++41 21 633 01 01Av. de Longemalle 5 CH-1 020 RenensS++41 21 6;33 01 Switzerland htto://www.trimos.chI -tM UU(b3- -UUU I-age b24 Or 1114 AppendllX 1U: Calloratlon Lertmtcates TROEMNERHenry Troemner LLCC libration Certificate 201 Wolf Drive o P.O. Box 870 T"horofare, NJ 08086-0087 oPhone: 856-686-160Q o F~x: 856-686-1601 o www.troemner.com o e-mail: troemner@troemner.com Page 1 of 7 PagesWeightSECTION 1: NAME AND ADDRESS OF CUSTOMEREnd userPurdue University 1040 S. River RoadBowen Laboratory West Lafayette IN 47907SECTION 2: APPROVED SIGNATORY ManagerSECTION 3: PERSON PERFORMING WORKDaniel FoglioSECTION 4: CERTIFICATE INFORMATION Certificate Number 663 364-1Date of Calibration 30-APR-2012 ClientPrecision Weighing Balances30 South Cross RoadBradford MA 01835-8232 Description of Masses: Grip Handle,Accuracy Class

NIST 105-1 Class F Date ReceivedOrder Number : 100001369

"'Date of Calibration Construction

Two Piece N, Date of IssueMaterial
Cast Iron N5 'Weight RangeSECTION 5: ENVIRONMENTAL CONDI'TIONS TEST: 30-APR-20 12: 30-APR-2012
30-APR-20 12: 1001bTemperature:

21 .840CPressure: 769.06 mm Pig--,Relative Humidity: 48%SECTION 6: PERTINENT INFORMATION The Weights listed on this .calibration report have been compared to reference mass standards that aredirectly traceable to the National Institute of Standards and Technology under Test No. 822-275872-il. Reference standards and balances used to perform the calibration are listed in Section 10.* The weights calibrated for this report have been calibrated in accordance with Troemner's ca~libration process. The calibration performed meets Level III criteria as described in theNIST/NVLAP Technical Guide 150-2.This calibration also meets specifications as outlined in ISO 9001, iSO/IEC 17025,ANSI/NCSL Z540-1-1994, NRC Document 10CFR50 Appendix B, and applicable documents. This certificate of calibration shall not be reproduced except in full, without the written approval of Troemner, LLC. This certificate of'calibration must not be used by the customer to claim product endorsement by NIST, NVLAP or any agency of the U.S. government. " ."-,REDACTED VERSION -. u cjL b-uuu -age ot 11 14 Appendix 1U: Lalibratlon (ertificates LKROEMNER Henry Troemner LLCCalibratdon Certific te201 Wolf Drive =P.O. Box 87

Thorofare, NJ 08086-0087 o Phone: 856-686-1600 oFax: 856-686-1601 o www.troemner.com o e-mail: troemner@troemner.com Page 2 of 7 PagesWeight*NAME AND ADDRESS OF CUSTOMEREnd userPurdue University 1040 S. River RoadBowen Laboratory West Lafayette

[N 47907Certificate Number 663364-1Date of Calibration 30-APR-20 12ClientPrecision Weighing Balances30 South Cross RoadBradford MA 01835-8232 SECTION 7: TRUE MASS (MASS IN VACUUM) CALIBRATION DATANominalMass Value.SerialNumberDensity'of WeightUncertainty (+ or-)True Mass100 ib45362.709 g7.2000 g/cm3450 mgyNI Density is assumed unless otherwise statedREDACTED VERSION UU (, -bIUUUllb-uuu Page bJ~b ot 1114 Appendix 1u: Calibratlon LSertmcates TROEMNERHenry Troemner LLCCalibration Certificate 201 Wolf Drive °P.O. Box 870o Thorofare, NJ 08086-0087 o Phone: 856-686-1600 o Fax: 856-686-1601,o www.troemner.com o e-mail: troemner@troemner.com Page 3 of 7 PagesWeightNAME AND ADDRESS OF CUSTOMEREnd userPurdue University 1040 S. River RoadBowen Laboratory West Lafayette IN 47907Certificate Number 663364-1Date of Calibration 30-APR.2012 ClientPrecision Weighing Balances30 South Cross RoadBradford MA 01835-8232 SECTION 8: MASS IN AIR CALIBRATION VALUE VS, REFERENCE DENSITY 8000 kg m-NominalMass ValueSerialNumberConventional Mass Value45361. 953 gUncertainty (+or-)Tolerance (+ or-)4. 5000 g100 lb450 mg\REDACTED VERSION -J L-L-UUUllb-UUU I-'age or 1114 Appendix 1U: CSalibration C:ertitcates LKROEMNER Henry Troemner LLCCalibration Certificate 201 Wolf Drive oP.O. Box 87 oThorofare, NJ 08086-0087 oPhone: 856-686-1600

Fax: 856-686-1601.

www.troemner.com o e-mail: troemner@troemner.com Page 4 of 7 PagesWeightNAME AND ADDRESS OF CUSTOMEREnd userPurdue University 1040 S. River RoadBowen Laboratory West Lafayette IN 47907Certificate Number 663364-1Date of Calibration 30-APR-2012 ClientPrecision Weighing Balances30 South Cross RoadBradford MA 01835-8232 SECTION 9: MASS IN AIR CALIBRATION DATA VS. REFERENCE DENSITY 8000 kg m-NominalMass ValueSerialNumberConventional MassCorrection Uncertainty (+ or-)450 mgTolerance (+ or-)4. 5000 gi00 lb2716 mgNAdREDACTED VERSION Y -UUU -. I-'age b2z5 Ot 11 14 Appendix 1U: (Jalibration C~ertmtcates IROEMNERHenry, Troemner LLCCalibratdon Certiflcate 201 Wolf Drive o P.O. Box 870o Thorofare, NJ 08086-00870o Phone: 856-686-1600 o Fax: 866-686-1601 ° www.troemner.como e-mail: troemner@troemner.com Page 5 of 7 PagesWeightNAME AND ADDRESS OF CUSTOMEREnd userPurdue University 1040 S. River RoadBowen Laboratory West Lafayette IN 47907Certificate Number 6633 64-1Date of Calibration 30-APR-20 12ClientPrecision Weighing Balances30 South Cross RoadBradford MA 01835-8232 SECTION 10: CALIBRATION PROCEDURE DATANominalMass ValueSerialNumberStandard CalSet No. DueBalanceUsedCalDueProcedure Used100 lbSl104 05/31/12 XP64003L-A01 11/30/12 Multi A-BA1 .'1REDACTED VERSION

I-'age rdZ90t q 114Appendix 1U: Calibration Certltlcates L<TROEMNER Henry Troemner LLC CalibratinCriia e~lboOO3201 Wolf Drive

P.O Box 870 Thorafare, NJ 08086-0087
Phone: 856-686-1600 o Fax: 856-686-1601
wvww.troernne~corn o e-nail: troemner@troernner cornPage 6 of 7 PagesWeightCertificate Number 663364-1NAME AND ADDRESS OF CUSTOMER Date Of Calibration 30-APR-2012 End user ClientPurdue University Precision Weighing Balances1040 S. River Road 30 South Cross RoadBowen Laboratory Bradford MA 01835-8232 West Lafayette IN 47907SECTION 11: GENERAL INFORMATION This calibration was performed in Troemner's High Precision Level I Mass Metrology Laboratory at201 Wolf Drive, Thorofare, New Jersey 08086 unless otherwise noted on page one. The internal procedures used are CAL-CLASSI and NIST HB 145.SECTION 12: DEFINITIONS AND TERMSMASS IN A VACUUM -The mass of a weight as if it were measured in a vacuum. Also known as True Mass.MASS IN AIR -The conventional value of the result of weighing in air, in accordance to International Recommendation OIML D 28. For a weight taken at 200 C, the conventional mass is the mass ofa reference weight of a density of 8003 kg~m"3 which it balances in air of a density of 1.2 kg~m-3.

AS FOUND MASS IN A VACUUM -The ~easured value of the mass(es) as they were receivdbrrenr AS LEFT MASS In A VACUUM -The value of the mass(es) after-they were adjusted,:repaird- .or replaced when necessary. The As Found\"Mass in a Vacuum willequal the As Left Mass in a ,--;::,;, if the mass(es) did not require adjustm.ent, or replacement. -.:. .--.NOMINAL MASS -The mass value-isg marked on the w ight."...'....." CORRECTION -The difference between the mass value of a we~ight..and its nominal value. A positive correction indicates that the mass value is greater than the nominal value by the amount of the correction. AS FOUND CONVENTIONAL MASS CORRECTION -The conventional correction of the result, as it received by Troemner, of weighing in air in accordance to International Recommendation D 28. ForI a weight taken at 20° C, the conventional mass is the mass of a reference weight of density 8000 kg.m3*. which it balances in air density of 1.2 kg'm -3 If the customer requires cleaning prior to clibration,; the after cleaning correction would be reported. AS LEFT CONVENTIONAL MASS CORRECTION -The conventional correction of the result, after moent repair, or replacement of weighing in air in accordance to International RecommendationiD 28.g a weight taken at 200 C, the conventional mass is the mass of a reference weight of density 8000 3which it balances in air density of 1.2 kg~m3.The As Found will equal the As Left Conventional MassCorrection if the mass(es) did not require adjustment, repair or replacement. (continued on next page)REDACTED VERSION Y-UUU ci-Uuu UUl -'U age ot 1114 Appencdlx 1u: Calibration Certitcates TROEMNER 7Henry Troemner LLC I;201 Wolf Drive oP.O. Box 87 o Thorofare, NJ 08086-0087 ° Phone: 856-686-1600,a Fax: 856-686-1601

www.troemner.com, e-mail: troemner@troemner.com Page 7 of 7 PagesWeightCertificate Number 663364-1NAME AND ADDRESS OF CUSTOMER Date of Calibration 30-APR-2012 End user ClientPurdue University Precision Weighing Balances1040 S. River Road 30 South Cross RoadBowen Laboratory Bradford MA 01835-8232 West Lafayette IN 47907SECTION 12: DEFINITIONS AND TERMS (continued)

UNCERTAINTIY -The standard deviation associated with the result of the measurement that characterizes thedispersion of the values that could reasonably be attributed to the measurand. The uncertainty is calculated inaccordance with NIST TechNote 1297 / UKAS M3003 using a coverage factor of k = 2 (k= 2 defines aninterval having a level of confidence of approximately 95 percent). The uncertainty does not include possibleeffects of magnetism. -Defines the limits in which the correction value and the uncertainty must fall to meet thetolerance specification for the given Class.AS FOUND CONVENTIONAL MASS VALUE -The measured value of the mass(es) as they were receivedby Troemner, of weighing in air in acc¢ordance to International Recommendation OIML D 28. For a weight takenat 200 C, the conventional mass is the \'nqass of a reference weight of density 8000 kg~m"3 which it balancesin air density of 1.2 kg~m-3.If the requires cleaning prior to calibration, the after cleaning valuewould be reported. F denotes Out of Tolerance Weight.AS LEFT CONVENTIONAL MASS VALUE -measured value of the mass(es) after they were adjusted, repaired or replaced when necessaVy-sf air in accordance to International Recommendation OIML D 28. For a weight taken at* the Conv~nftio~nal Mass is the mass of a reference weight of density8000 kg.m'3 which it balances in air density of 1.2 kgrmn The As Found will equal the As LeftConventional Mass Value if the mass(es) did not require adjt~stmnent, repair or replacement. ASTM E617-97 -Weights meet the tolerance specification for ASTM E617-97. Weights 2kg -I gscreened for magnetism using a Gaussmeter. REDACTED VERSION

l-age t531 0! 1114Project: Tests to Determine theBehavior of Spliced #11 BarsAppendix LU: Calibration (Jertificates Calibration Documentation v.1(Rev. 04/02/2012) Bowen Lab -Purdue University Sheet Ilof 2Calibration Instrument Name and S.N.: Instron 1044172Data Acquisition System: OptroTrack Pro Series 600Gain: NAExcitation Voltage: NAChannel: NASensor: OptroTrack pro Series 600Sensor S.N.: _________OptroTrack Pro Series 600Input [in.] Output [in.] Input [in.] Output [in.]0 0 6.5 6.5070 0 6.5 6.5071 1.001 _____ __ 4 3.999________ 1 1.001 _____ __ 4 3.999________ 4 3.998 _________1.5 1.4994 3.997 ________1.5 1.4986.5 6.502 _________ _ _ _ _ _ _ _ _ __ _ _ _ _ _ _ _ ____ ____6.5 6.502 ________ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ____ ____9 9.007 __ _ _ _ _ _ _ __ _ _ _ _ _ _ __ _ _ _ _ _ _ __ _ _ _ _ _ _9 9.007 ____ ___Operator Sig nature Date TimeChce y intreDt ime~Checked by Signature Date TimeSensitivity Accuracy1euls0.007 in.REDACTED VERSION bbEJ-UUU-U~tl4-UWI:-UUUIU-UUU P'age b;.t2 oT 1"114Project: Tests to Determine theBehavior of Spliced #11 BarsAppendix 1U: CaliDration Lertlricates Calibration Documentation v.1(Rev. 04/02/2012) Bowen Lab -Purdue Sheet 2 of~Notes: The accuracy of the INSTRON sensor is 0.003 in.REDACTED VERSION Page bi at 1114Project: Tests to Determine theBehavior of Spliced #11 BarsAppendix 1U: Calibration Certitcates Calibration Documentation v.1(Rev. 04/02/2012) Bowen Lab -Purdue University Sheet I of i.Calibration Instrument Name and SN'.: Data Acquisition System: /\31." t ?CJ 02.3Gain: IExcitation Voltage: Channel: MVQ "Sensor: PA HJ1G- D-L3MSensor S.N.: 3IJ100 0Measurand Voltage Measurand Voltage Measurand Voltage,4oZU 0.03 ____2____ 4,553 0°&75 ___________ Operator Si nature Date TimeChecked by Signat ure Date TimeChecked by Signature Date TimeSensitivity AccuracyResults__ _ _ _ __ _ _ __ _ _o.1 %Notes:REDACTED VERSION

l-UUU I-age ot 1114Project: Tests to Determine theBehavior of Spliced #11 BarsAppendix LU: Calibration Certificates Calibration Documentation v.1(Rev. 04/02/2012) Bowen Lab -Purdue University Sheet Ilof ICalibration Instrument Name and S.N.: 1044-172-Data Acquisition System: -(1 tOQO ?"'I Gain:__________________________ ExcitationVoltage: ___________________________ Channel: l i"Sensor: ?A"2Ot" iJC" Sensor S.N.: _______ 37i~910_______ ______Measurand Voltage Measurand Voltage Measurand Voltage__,____ 1.35 _ _ _ _4. 0/A IOperator 'ignature Date TimeChecked by Sig ur Date TimeChecked by Signature Date TimeSensitivity AccuracyResults 6,

o. °I%Notes:REDACTED VERSION

I-age oT 11 14Project: Tests to Determine theBehavior of Spliced #11 BarsAppendilx 1u: Lalidration Lertlticates Calibration Documentation v.1(Rev. 04/02/2012) Bowen Lab -Purdue University Sheet i of 1Calibration Instrument Name and S.N.: 1044 I72,Data Acquisition System: I -1000 P&i :) 2$Gain: IExcitation Voltage: -3333Channel: Hv I -2Sensor: BA -10 2L°___________ Sensor S.N.: 40 0k8 _______________ Measurand Voltage Measurand Voltage Measurand Voltage6.447 __ _. ____ __ _40,,o0 ______Operator Signature Date TimeChecked by SgaueDate TimeChecked by Signature Date TimeSensitivity AccuracyResulIts__,___ ______ 3°/-Notes:REDACTED VERSION

-'age bil ot 1114Project: Tests to Determine theBehavior of Spliced U11 BarsAppendix iU: C~alo~ratlon L~ertitlcates Calibration Documentation v.1(Rev. 04/02/2012) Bowen Lab -Purdue University SheetlIof 1C)Calibration Instrument Name and S.N.: 1-/i'T1 /,O 4 1Z 04 !4 12-Data Acquisition System: MIJ PC. I 6'2 Gain: "IExcitation Voltage:

3. 3:3Channel:

M J-o"3Sensor: P)A- IC-___ ___ Sensor S. N.: _ _ __ 400oI09&5_ _ _ __ _ _ _Measurand Voltage Measurand Voltage Measurand Voltage ____ ____~4 O2.5 Operator ii~gnature Date Tim es-.p. -zChecked by Signature Date TimeChecked by Signature Date TimeSensitivity Accuracy"ResultsNotes:REDACTED VERSION

I-'Uage ot 1114Project: Tests to Determine theBehavior of Spliced #11 BarsAppendix 1U: Lalibration Lertiticates Calibration Documentation v.1(Rev. 04/02/2012) Bowen Lab -Purdue University Sheet l of 1i Calibration Instrument Name and S.N.: IIJSTO/') 044172Data Acquisition System: $ [X 11O00 P;CI Gain: __________________________ Excitation Voltage: 3), 355Channel: 2Sensor: RA -__________ Sensor S.N.: ______ 4o010 l 77 ______Measurand Voltage Measurand Voltage Measurand Voltageg4.20_ 2~.5qo____ 4.bo7 !o33t _ __ _Operator Si nature Date Timesip,.Checked by Signa lre Date TimeChecked by Signature Date TimeSensitivity AccuracyResults3, Notes:frjZ-oREDACTED VERSION

I-age bad oT 1114Project: Tests to Determine theBehavior of Spliced #11 BarsAppendix 1U: Lailibration C~ertlTicates Calibration Documentation v.1(Rev. 04/02/2012) Bowen Lab -Purdue University Sheet 1 of 10©Calibration Instrument Name and S.N.: '" l0 e..-j H V?':.. -Data Acquisition System: t'JQ-- -S C 4T -1000 ['C-T Gain: .00Excitation Voltage: !. " .Channel:/" -0Sensor SN: _ _ _ _ _ _ _ _ _ _ _ _ _Measurand Voltage Measurand Voltage Measurand Voltage.0.02o153B -0,00600:25.3 -o0,00____0 30.LI -0,0I~~ _____________ Operator S gnature Date TimeChecked by igaueDate TimeChecked by Signature Date TimeSensitivity AccuracyResults__ _ _ _ _ _ --K// O. 1%Notes:REDACTED VERSION

P'age biU oT "11 14Project: Tests to Determine theBehavior of Spliced #11 BarsAppendix iU: C.alibration C~ertitcates Calibration Documentation v.1(Rev. 04/02/2012) Bowen Lab -Purdue University Sheet Ilof 1Calibration Instrument Name and S.N.: --0!~ /42t Data Acquisition System: PC--,"* Gain: /00Excitation Voltage: I 0Channel: --Sensor: ________ Sensor S.N.: H- Measurand Voltage Measurand Voltage Measurand Voltage0* 0 _ _i5.5 -0~o~bot5 ____ __ _____1Q.5 -0.00605-0-.5 uO, o _ __ __ __ __Operator Sign~tu~re -Date TimeChecked by Signature Date TimeChecked by Signature Date TimeSensitivity Accu racyResults -2%53K/v O. t%Notes:REDACTED VERSION

I-sage 4Uu oT 1114Project: Tests to Determine theBehavior of Spliced #11 BarsAppendix 1U: CaIlibration Lertitlcates Calibration Documentation v.1(Rev. 04/02/ 2012)Bowen Lab -Purdue University Sheet l of iCalibration Instrument Name and S.N.: 10441 72.Data Acquisition System: ?CI GZS9Gain:Excitation Voltage: ,Channel: M3OSensor: .LUCAS -2Oo____ ___ ___ Sensor S.N.: __ _ _ __ _ 7250 _______ __ _ _ _ _Measurand Voltage Measurand Voltage Measurand VoltageI.35 -4.272 _________

1. 500 -______.oo -o.25 ____ ____ ____2.t533_ ___0, 2-.5 __.__ ___ __Operator ignature Date TimeChckd ._ _ _ _atreDae

_mChecked by Signature Date TimeSensitivity AccuracyResultsNotes:REDACTED VERSION

I-age b41 ot 1114Project: Tests to Determine theBehavior of Spliced #11 BarsAppendix 1U: Calidration Ldertilicates Calibration Documentation v.1(Rev. 04/02/ 2012)Bowen Lab -Purdue University Sheet 1 of 1Calibration Instrument Name and S.N.: 1W04i 72.Data Acquisition System: H" -100O0 Gain: IExcitation Voltage: 3Channel: frI.3 1Sensor: LUCA 2o000____________ Sensor S.N.: ________ 7251 _______Measurand Voltage Measurand Voltage Measurand Voltage0.12Z5 4.1,..0 _ _ _ _ _ _ _ _ _ _ _ _ _ _0.5q7 __ __._ __ _ _ __ _ __ _ _o.}1f o.ozo_____ L.5o0 -2,4.14_____ ________, __ -4..02A5 _ _ _ _ _ _ _ _ _ _ _Operator Signature Date TimeChcedbPDt TmChecked by Signatu re DaeTimeSensitivity Accuracy*ResultsNotes:REDACTED VERSION

b-UUU I-age b4z or 1114Project: Tests to Determine theBehavior of Spliced #11 BarsAppendix 1U: C:alidration Lertitcates Calibration Documentation v.1(Rev. 04/02/2012) Bowen Lab -Purdue Universit' Sheet l of :Calibration Instrument Name and S.N.: ?U! D 10g!4I4'2. Data Acquisition System: MN, Scd.%-I 1000 I1 B Gain: IExcitation Voltage:

5. VChannel:

Mt-0(Sensor: 'PA _ _ _ _ _ Sensor S.N.: __ _ _ _ _ _ _ _ _________0 Measurand ,Voltage Measurand Voltage Measurand Voltage0.5/f o.95 __ _ __ __ __ _ __ _ _ _ _ _ _ I. i _ __-_ __ _ _ _ __ _ _._ _ _ _ _ _ _ _ _Operator Signature Date TimeChecked by Signlature Date TimeCekdb .... -Signature Date TimeSensitivity AccuracyResultsNotes: ~ u e.o' 4+ .% /D~ vi ~ 4iw j2-emx- r s 3 //REDACTED VERSION

b-UUU r-age ot 1114Project: Tests to Determine theBehavior of Spliced #11 Bars.Appendix 1U: (Caliaration Lertiticates Calibration Documentation v.1(Rev. 04/02/2012) Bowen Lab -Purdue Sheet i of 1Calibration Instrument Name and S.N.: I N.ST 6-c N 109 4 I Data Acquisition System: KNh $C')(1 1000 ,SN IlI Gain:Excitation Voltage: 3 *3 53 \Sensor: _______ Sensor S.N.: _________ T00L' _______Measurand Voltage Measurand Voltage Measurand Voltage4.5 ___._ __ __0.5 _____ _____ ____Operator Signature Date TimeChecked by Signature Date TimeSensitivity Accu racyResultsNotes: ,,4o -o.,°IREDACTED VERSION bbU3-UUU-ULi-(,U-UUU1 b-UUU Page OT 1114Project: Tests to Determine theBehavior of Spliced #11 BarsAppendlx iu: Callbration (Certltlcates Calibration Documentation v.1(Rev. 04/02/2012) Bowen Lab -Purdue Universit'3 Sheet 1 of~Calibration Instrument Name and S.N.: I NJ N 1 0441 ',2_Data Acquisition System: NI[ S-C.) 1 1O0O 0Gain:Excitation Voltage: Channel: M l- 2.Sensor: P,________ Sensor S.N.: ___0______ 0tMeasurand Voltage Measurand Voltage Measurand Voltage2 .5 (.2IOZ. G______-, I.8? __ _ _ __ _ _ __ _ _-_ _ _(o.5 2. .t__ __ ____ __Operator Signature Date TimeCheckd by ignatre Dae TimChecked by Signature Date TimeSensitivity AccuracyResulItsNotes: Devickova." 0.2-%REDACTED VERSION bU-UUU-UbJ-UIU-UUU1Ii-UUU l-age b4b ot 1114Project: Tests to Determine theBehavior of Spliced #11 BarsAppendix 1U: Calibration Certlticates Calibration Documentation v.1(Rev. 04/02/2012) Bowen Lab -Purdue Universit% Sheet 1 of :1Calibration Instrument Name and S.N.: I \ , I A41 " TZData Acquisition System: 1000 11S86O0]Gain:Excitation Voltage: VChannel: __ _ __ _ __ _ __ _ __ _ __ _ __ _ __ _Sensor: PA -10_____ ____ SensorS.N.: __ __ _ __ _ __ _ __ __ _ __ _ __ _ __ _Measurand Voltage Measurand Voltage Measurand Voltage'I8 _. _4.5 1.8~5 _ _ _ _ __ _ __ _ _ _ _Operator Signature Date TimeCheke by SignatueDatefTim Checked by Signature 'Date TimeSensitivity AccuracyResults_____________ .o?3. \JJ,/V\ 0.o3 %.'Notes:REDACTED VERSION

Irage b4g Ot 1114Project: Tests to Determine theBehavior of Spliced #11 BarsAppendix 2U: Calibration Certllticates Calibration Documentation v.1(Rev. 04/02/2012) Bowen Lab -Purdue Sheet 1lof ICalibration Instrument Name and S.N.: _____ -______________0 __41 __________- Data Acquisition System: -C,)( c000 (IS 6(01Gain: ___________________________ Excitation Voltage:

3. ; NChannel:

t'A2- 0Sensor: _______ Sensor S.N.: ____OO___O__ 4oo-Measurand Voltage Measurand Voltage Measurand. Voltagec3..54 ___._.__4.5" ' .841_ _ _ _ _S ." __ __Operator Signature Date TimeCheced y6SgnaureDat Time__Checked by Signature Date .TimeSensitivity Accu racyResults__ __ __ _ __ __ _o.. o.____ I_ ___ _Notes:REDACTED VERSION bbY3-UUU-L.i-L5-L(-UUUlh-UUU l-'age b4( ot 1114Project: Tests to Determine theBehavior of Spliced #11 BarsAppendlx 1Ui: Calibration Certiticates Calibration Documentation v.1(Rev. 04/02/2012) Bowen Lab -Purdue University Sheet l of ICalibration Instrument Name and S.N.: I ~\ .STE-o N 1044 [? 'ZData Acquisition System: .SC X-I I00 t6 Gain: O00Excitation Voltage: I OVChannel: Sensor: 44 3'_______ Sensor S.N.: 44 ______ ______Measurand Voltage Measurand Voltage Measurand Voltage-04-.1~o=0 0sk -j-o, -0.002.1i Iok+-t-o4 -o.oo4,o _____I4-.6k--o., -o oo5s _____I9.04+o.1t -o.oo'8- _____ _____a4.ik+/- 04 -o.ooo~sg4 -o.Olla ____ ____ ___Operator Signature Date TimeChecked by SDate TimeChecked by Signature Date TimeSensitivity Accu racyResults_____________ -I. 5Thv iV/V @FSV o_______Io__ Notes: b'I~o r/ "a 5//aREDACTED VERSION bIUj-UUU-ULSJ-UIU-UUUIh-UUU H'age tbq. 071114Project: Tests to Determine theBehavior of Spliced #11 BarsAppendix 1U: Calibration Lertinlcates Calibration Documentation v.1(Rev. 04/02/2012) Bowen Lab -Purdue Universit% Sheet 1 of ICalibration Instrument Name and S.N.: I N STZ-O A 104 41 ? 2..Data Acquisition System: .Scx 1000 GO7"Gain: 1O00Excitation Voltage: 1 0 V/Channel: -Sensor: 4~4Z.__ _ _ _ _ _ Sensor S.N.:Measurand Voltage Measurand Voltage Measurand Voltage-o.,4+/-o.4k o~ooool ____ ____ ____4.J05 -jo'I-oR __ __ __ __ _ _ __ _ _ __ _ __ _ _1%.1k +o.4 -o.oo~ ______ _____04 -oom o_Operator Signature Date TimeChecked_____by __ Signa____ure613Dae Time__Checked by Signature Date Time.Sensitivity AccuracyResulItsNotes: LDev-v, 0,,. .2REDACTED VERSION Project: Tests to Determine theBehavior of Spliced #11 BarsAppendilX LU: Calioration Certlrlcates Calibration Documentation v.1(Rev. 04/02/2012) Bowen Lab -Purdue Universit3 Sheet I of ICalibration .Instrument Name and S.N.: ) NJ ST NJ 104 4 1 : 'Data Acquisition System: NI ,SC)I 1000 Gain: IExcitation Voltage: 3 0 V/Channel: F -Sensor: LUCAS DODT -+-Z.."__ __ _ __ _ Sensor S.N.: JgZ O __ _ __ _ __ _ ___0_ _Measurand Voltage Measurand Voltage Measurand Voltage1.5 ' -_ .__- _-1 ,,"_ __1 .o o .1 1 2 ._ _ _ _ __-_ _ _0.51 2. 4'_ __ _ _ _ _ __ _ _Operator Signature Date TimeChecked_____by _Signature____ Date; '5TimeChecked by Signature Date TimeSensitivity AccuracyResultsNotes: Dvoiv.j2w /I' 4REDACTED VERSION

IibU ot 1114Project: Tests to Determine theBehavior of Spliced #11 BarsAppendilx 1u: Lalibration C=ertli"lcates Calibration Documentation v.1(Rev. 04/02/2012) Bowen Lab -Purdue Universit% Sheet l of 1Calibration Instrument Name and S.N.: INilS-T 1044[ Data Acquisition System: N I SX{ 1 I000 II SS 60 l"Gain: IExcitation Voltage: Channel: 1\11-- ISensor: LUCA.-& bCJT ____ ___ ___ Sensor S.N.: ,__ __-___ ,. .25j __ _ _ _ _ _ _ _ _ _ _ _Measurand Voltage Measurand Voltage Measurand Voltage0. 4A- . ______1.0" 0,1410Operator Signature Date TimeChecked by Signature Date Time.Checked by Signature Date TimeSensitivity ..AccuracyResultsNotes: D v~ i' -REDACTED VERSION bbi-UUU-Ud::J-U.5"U-UUUIIh-UUU t-'age 1bl 1" o 1114ApeixU:alrtonettcte AppencllX 1u: Lallbratlorl Lertltlcates ! :~T I--t I r-r I F F- -- .-5 --REDACTED VERSION FIRST LOADINGREDACTED VERSION FIRST LOADINGREDACTED VERSION FIRST LOADINGGIRDER A6-40 kipREDACTED VERSION RELOADING REDACTED VERSION RELOADING NoIRDEloAd GIRDERA3(iIKUEK A4 -41 KIpREDACTED VERSION RELOADING GIRDER A5 -42 kipREDACTED VERSION FIRST LOADINGREDACTED VERSION FIRST LOADINGREDACTED VERSION FIRST LOADINGREDACTED VERSION RELOADING No reloadI::Z -Loaa = ib Kip.REDACTED VERSION RELOADING 1C~IRLThK 133- Load = 3b kipNoIReload4 GIRDER B4REDACTED VERSION RELOADING GIRDER B5 -24 kio.REDACTED VERSION

Project:

Tests to Determine theBehavior of Spliced #11 BarsInstrumentation Documentation v.1(Rev. 04/01/2012) Specimen: A -ISheet __ __of IData Acquisition System:Channel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location CommentsC) /11-o ( 3.3g3 OA-p-o -.': -Vt:2-zr Mj.o,-L 2.?-z5I MI-I I " " 3Thoo't~ -6. I7- -l1=.o2 S. " .,S2 I ', A-IO '-oolc5'r6, 3.'~l-5 !,% N5lc- 0,3l:t-.,2 3 hI-3 I " " 4oioioii 3.i6'=t 'f " b 2--0. I ____1__5 ",:-3! J 0..23,5 100 i0 '-,P1O 43 -______ o0,2D'C1 J, -., /t1 1 oO 10 ___-- __ _.-_-___.__!l< s -_______m r-'v-o 3o 2_0 ooos -0o(30 "I 2'2-1O. o OOO So ." o., oooOOperator Signature Date TimeChecked ___by__Signature_ 6 Date Time~'Checked by Signature Date TimeNotes:12-1REDACTED VERSION v$*0p~o~1 ~243~4*5I.-id, .-- I-4 -I 4-U.- ;.---- ; --4----1;----I~--U- ... --U- --I~ -m -U -4NothIII* qF *f 12 13 1 ! 15'IIF qFI-I '4II- II l --I -I I, I l- U I. --lI 44-2@10--20 A @520_ r410Q10:100 r41 4E_1 _4 5=20_ 1 '21=-0 1I--!I-.Back 4Front45qm Wv .... J,4ISpecimen A -ILAORTRYBehavior of Lap Splices of No. 11Reinforcing Bars12-2REDACTED VERSION Project: Tests to Determine theBehavior of Spliced #11 BarsInstrumentation Documentation v.1(Rev. 04/01/2012) Specimen: Sheet I of _____Data Acquisition System:-,.T vChannel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location Comments0 11I-O 1 3.333 'A-.20 3=,IOo~o -6.197-r -l::.oft ______- _ __ __ _ __ _, _ __ __ _ 3TlOOq -6,16=7- -jI-, I , " ;2 hlI-2 ____ "___ PA-Io ,9OOIOc 3.R-S i.2zr tJ.5Yv4 0.3B%3 14I-3 I r,"'40tolo~'=I O .4&O_____-_ I " ot~f' 3.17-3 O.qIi O,3!!9 frl2-; [6O JO L_.it,.soK ____-__5 0.3DeI -o.ooo'oo 4 10-0Lo 10 _____ L.-t2 -0.L[wJ s. =7- 113-0 ( 3o Lw'c.c 2. -J7-:2SO 0.0OO1 0,013ht13-I I 30 "___ T+2Sz1 ,.209 -o,0oof $. "-o.5OprtrSgaueDate TimeChecked by ~SignatureDaeTm Checked by Signature Date TimeNotes:12-3KEILAL I FU VLIOIbUI'J i i f I f , I6.1, Ii9A6* qr *

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Sensitivity Zero Offset Location Comments0 fl-c " "~3 .-,)s " .(vef ,:O2//;2pt-z I " Ai-IO 5 /11I-3 I "I 0 +/-,01:L/ 3 /o"WS OQ.LAo 053 /I &ov 2 'o,.oo pJ, s.1,,- -0oo2'3 t3-1I 30""-0-2 2 o..;o1 -FO.:o % 0, r0)OIOperator Signature Date Times .l? UJOL_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Checked by Signature Date TimeChecked by Signature Date Time~Noes ~ ~bj~12 -2.1-REDACTED VERSION 439 40 414243"44 --m -mF ---t[ I -.- -.S. F534..L....-I----4 I -4 I -U -4 I -I I- U -II -'-4 I -I I-~ U ---~ I m m m m m-4= -m m mlb j~p jgj9j~5152!v v v v v v47 4849 5051 62North34Cl= = U. .=1-I 55 568 7"65960 61 8212@Io=2o 37 ;,--36,351- Front =: ,I=6Q10=60 _,2@10 -204@4.75=19 404.75=19 12ft71In. Specimen ~, -5LABORATORY Behavior of Lap Splices of No.11 Drawn by~ 1@~P~. Checked by: Vy~PURDUE UNIVERSITY ReinforclngBars Date: ~/J6/U~.12 -22REDACTED VERSION UJ00Specimen: Sheet 1 of 1-Project: Tests to Determine theBehavior of Spliced #11 BarsInstrumentation Documentation v.1(Rev. 04/01/2012) Data Acquisition System:[>JChannel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location CommentsI. /141-1 I " " B -F?,___ S, k 2 t- MI- I " !A- 10 9/OoOlCIf 3, 1:-5 O,.% 0,27--¥:3 14I-3 I "' " C010c11 "3,Aif _,5___,___po ______q/ I1)-O I ____ " -tooIO~ o -B,7.-3 IS 15 5 s\w _.______5 /12-2 100 boy _o____3 _____ O.Jo_ Ki -______so ti- oo Io'J "I L/.I2 0.255 .O,2 CKJ <,___-o ___7- 113-b ! 3ov T 0 0.0oo 0.oooI{ P13-1 30\I " -s .9o0o~o2 &. Operator Signature Date TimeChecked by Signature Date TimeChecked by Signature Date TimeNotes:12 -23REDACTED VERSION Norlh 3,_ .Front _4@4.75=194(.. 12 ft7 In.I "Specimen g --LABRAOR Behavior of Lap Splices of No. 1:1P URDUIE VER:S~ITY Reinforcing Bars12 -24REDACTED VERSION bbiL-UUU-U83-U.5"U.-UUU1bt-UUU I-'age bb or "1"114ApedX:Apoedls oedeAppendtx Approved Iest Procedure 25539-O00-VIS-SY01-00001-003 Page I of 26BECHTEL POWER CORPORATION SUPPUER DOCUMENT REVIEWTests to Determine the Behavior CL.ASSIFICAT.ION & STATUSof #11 Bars with Lap Splices ...Bowen Laboratory ¶ El [] Purdue University El[ ,d ' El wodmsSpring 2012 2-" *Test Procedure ., , == =1.1 Formwork -,(iThe formwork shall be made using non-absorbent plywood. Itsinterior shall be caulked to prevent water leakage and it shall be covered with a thinlayer of oil before casting. The dimensions of the formwork shall be checked andrecorded using Form 1.1.2 Reinforcement CagesThe steel reinforcement cages shall be built following the drawings attached. Reinforcing bars shall be supported by steel chairs placed away from lap splices. Toensure alignment, the bars shall be tied to chairs and to one another using gage-16steel wire. The location of the reinforcement shall be recorded using Form 1. Thelocations of wire ties and rebar markings shall be recorded using Form 2.Tolerances (within the test region) are:3/16" for horizontal cover and horizontal spacing measured to the surface of the bar(excluding ribs)1/4" for vertical distances shown in Form 11.3 CastingFresh concrete properties to be measured include:Unit WeightSlumpAir ContentThese measurements shall be made following the Specifications and recorded usingForm 3.Revision 218-1REDACTED VERSION boYJ-uUU-UdJ-ULUc-Uuu3 b-UUU r'age tbtU 011 114 Appendix 8: Approved lest Procedure 2bbJiY-UUU-ViS-:SYU1-UUUU1-UUit rage z oT Slump shall be measured before any other activity related to casting takes place tomake sure that the delivered mix has ,satisfactory workability. The mixing truckshall deliver a ticket with the batched mix weights. These weights shall be examinedto corroborate that the delivered mix has the specified proportions. Concrete shallnot be accepted if it arrives more than 45 min. after leaving the batching plant. Nowater shall be added to the mix after the truck leaves the plant.Specimens and cylinders shall be cast and vibrated in two lifts following theSpecifications. The vibrators to be used shall have the following cross-sectional dimensions: For cylinders: 3/4" -7/8"For Larger Specimens: 1-3/4"Their frequencies shall be between 50 and 200 Hz.Excess concrete shall be removed off the formwork. The exposed surfaces of thespecimens shall be finished using cast magnesium floats. Lifting inserts shall beinserted in the fresh concrete as soon as the finishing is completed. Each test beam shall be cast using concrete from a single mixing truck. A completeset of concrete samples (cylinders) shall be obtained from each truck. Test beamsand samples shall be marked with a number referring to the truck from which theywere cast and the date of casting. In each casting day, trucks shall be numberedsequentially starting at 1. The number assigned to a truck shall be written clearlyon the mix ticket describing the mix proportions for the batch. Test beams shall becast and tested oriented in the North-South axis of the laboratory. During finishing, the north end of each beam shall be marked with the letter N.These activities shall be documented using Form 31.4 C:uringAs soon as casting is completed all specimens shall be covered with impermeable sheets. When the concrete surface sets, wet burlap shall be inserted between thesesheets and the exposed concrete. All formwork and molds shall be struck no laterthan three days after the cast.All exposed concrete surfaces shall be covered by wet burlap and impermeable sheets for a total of at least seven days after casting.Burlap shall be doused with water at least every other day during the curing period.Curing activities shall be logged using Form 4.Revision2 25-2REDACTED VERSION