ML15299A148

Enclosure B, Bechtel Report No. 25593-000-G83-GEG-00016-000, Effect of Laminar Cracks on Splice Capacity of No. 11 Bars Based on Testing Conducted at Purdue University and University of Kansas for Davis-Besse Shield Building. Part 4 of 7

ML15299A148
Person / Time
Site:	Davis Besse
Issue date:	07/30/2012
From:	Liano R, Munshi J, Reilly R Bechtel Power Corp
To:	Office of Nuclear Reactor Regulation
Shared Package
ML15299A142	List: L-15-328, Enclosure B, Bechtel Report No. 25593-000-G83-GEG-00016-000, Effect of Laminar Cracks on Splice Capacity of No. 11 Bars Based on Testing Conducted at Purdue University and University of Kansas for Davis-Besse Shield Building. Part 7 of 7 ML15299A143 ML15299A144 ML15299A146 ML15299A147 ML15299A148 ML15299A149 ML15299A150
References
L-15-328 25593-000-G83-GEG-00016-000
Download: ML15299A148 (129)

Text

{{#Wiki_filter:bbiL-UUU-U83-U.5"U.-UUU1bt-UUU I-'age bb or "1"114ApedX:Apoedls oede Appendtx Approved Iest Procedure 25539-O00-VIS-SY01-00001-003 Page I of 26 BECHTEL POWER CORPORATION SUPPUER DOCUMENT REVIEW Tests to Determine the Behavior CL.ASSIFICAT.ION & STATUS of #11 Bars with Lap Splices ...Bowen Laboratory ¶ El [] Purdue University El[ ,d ' El wodms Spring 2012 2-" *Test Procedure ., , == =1.1 Formwork -,(i The formwork shall be made using non-absorbent plywood. Its interior shall be caulked to prevent water leakage and it shall be covered with a thin layer of oil before casting. The dimensions of the formwork shall be checked and recorded using Form 1.1.2 Reinforcement Cages The steel reinforcement cages shall be built following the drawings attached.Reinforcing bars shall be supported by steel chairs placed away from lap splices. To ensure alignment, the bars shall be tied to chairs and to one another using gage-16 steel wire. The location of the reinforcement shall be recorded using Form 1. The locations of wire ties and rebar markings shall be recorded using Form 2.Tolerances (within the test region) are: 3/16" for horizontal cover and horizontal spacing measured to the surface of the bar (excluding ribs)1/4" for vertical distances shown in Form 1 1.3 Casting Fresh concrete properties to be measured include: Unit Weight Slump Air Content These measurements shall be made following the Specifications and recorded using Form 3.Revision 21 8-1 REDACTED VERSION boYJ-uUU-UdJ-ULUc-Uuu3 b-UUU r'age tbtU 011 114 Appendix 8: Approved lest Procedure 2bbJiY-UUU-ViS-:SYU1-UUUU1-UUit rage z oT Slump shall be measured before any other activity related to casting takes place to make sure that the delivered mix has ,satisfactory workability. The mixing truck shall deliver a ticket with the batched mix weights. These weights shall be examined to corroborate that the delivered mix has the specified proportions. Concrete shall not be accepted if it arrives more than 45 min. after leaving the batching plant. No water shall be added to the mix after the truck leaves the plant.Specimens and cylinders shall be cast and vibrated in two lifts following the Specifications. The vibrators to be used shall have the following cross-sectional dimensions: For cylinders: 3/4" -7/8" For Larger Specimens: 1-3/4" Their frequencies shall be between 50 and 200 Hz.Excess concrete shall be removed off the formwork. The exposed surfaces of the specimens shall be finished using cast magnesium floats. Lifting inserts shall be inserted in the fresh concrete as soon as the finishing is completed. Each test beam shall be cast using concrete from a single mixing truck. A complete set of concrete samples (cylinders) shall be obtained from each truck. Test beams and samples shall be marked with a number referring to the truck from which they were cast and the date of casting. In each casting day, trucks shall be numbered sequentially starting at 1. The number assigned to a truck shall be written clearly on the mix ticket describing the mix proportions for the batch. Test beams shall be cast and tested oriented in the North-South axis of the laboratory. During finishing, the north end of each beam shall be marked with the letter N.These activities shall be documented using Form 3 1.4 C:uring As soon as casting is completed all specimens shall be covered with impermeable sheets. When the concrete surface sets, wet burlap shall be inserted between these sheets and the exposed concrete. All formwork and molds shall be struck no later than three days after the cast.All exposed concrete surfaces shall be covered by wet burlap and impermeable sheets for a total of at least seven days after casting.Burlap shall be doused with water at least every other day during the curing period.Curing activities shall be logged using Form 4.Revision2 2 5-2 REDACTED VERSION

inage bU1 0? 11I 14 A~ppendix s: Approved lest Procedure 2bW3-UUU-V'15-bSYU'1-UUUU'1-UUtS frage it or 2u Test cylinders shall be stored and cured next to the test specimens and under similar conditions of temperature and humidity.The variation of concrete strength with time shall be monitored as specified in the Specifications. The results of cylinder tests shall be recorded using Form 5.2. Calibration Three types of measurements will be made: displacement, force, air content.The apparatuses to be used to calibrate sensors to measure these quantities are: Displacement Sensors: INSTRON Universal Testing Machine (S.N.:)Load Sensors: INSTRON Universal Testing Machine (S.N.:)Air Content: Calibrated Cylinder (S.N.)Load and displacement sensors will be calibrated following steps listed below: 1) Connect the sensor to the data-acquisition system that is going to be used in the test 2) Set and record the excitation voltage to the maximum possible value (not exceeding the maxima specified for the data-acquisition system and the sensor)3) Set the data-acquisition equipment to record voltage 4) Set the gain of the data-acquisition system to the first available level lower than the ratio of the maximum range of the system to the maximum expected output from the sensor.5) Mount the sensor on the universal testing machine 6) Apply a series of known displacement or force increments to the sensor ranging between 10% and 90% of the rated capacity of the sensor 7) Record the voltage read on the data-acquisition system at each known displacement or force increment 8) Create a plot of change in output voltage vs. change in force or displacement

9) Fit a line to the plot from 7) using "least squares" 10) Record the slope of the line from 8) (sensor sensitivity)

11) Label the cable used in the calibration with the serial number of the sensor Sensors shall be calibrated before the first test and after the final test.The apparatus used to measure air content of the fresh concrete shall be calibrated following the procedure described in ASTM standard 231. Form 6B shall be used to document the calibration.

Revision2 3 8-3 REDACTED VERSION bbg:i-UUU-LUdi-ULUL-UUU1 b-UUU i-'age bb2 01"1114. Appendix 8: Approved lest Procedure 2bbtJY-UUU-V1 -UUUU1 -UUi wage 4 07tLti All calibrations shall be performed by at least two persons: one leading each step and the other checking the work of the first independently. A log of each calibration shall be made using Form 6 and it shall include an estimate of the accuracy of the sensor.Sensors for which the sensitivity obtained in 9) above deviates by more than 10%from the nominal sensitivity (as reported by the manufacturer) shall not be used in any of the tests.3. Setup Each test beam shall be placed on two roller supports as described in the attached proposal. The final location of the supports shall be measured (to the nearest 1/16 in.j with maximum deviation of in and reported using Form 7. As-built external dimensions of each test beam shall be recorded using the same form.The maximum deviation from nominal dimensions in the test region shall be 1/4/ in.The test beam shall be placed with the reinforcement facing up as shown in the attached proposal.The shear spans shall be reinforced with external stirrups (pairs of 5/8-in threaded rods) installed at a spacing not exceeding 12 in. The locations of the stirrups shall be measured. The measurements shall be recorded using Form 7.The loading rigs (consisting of a loading tube, two hydraulic rams, two threaded rods, plates and nuts, and one load cell per rig) shall be placed on the test specimen and connected to "the strong floor" of the laboratory (without applying load to the specimen other than the weight of the rigs) as described in the attached proposal.The rams in each rig shall be connected to a single manifold and pump using 10,000-psi hydraulic hoses. All hoses and other hydraulic hardware shall be inspected visually and replaced -if defective-before testing.4. Instrumentation Displacement sensors shall be installed at midspan, at each support, and at each load point. They shall be secured to the strong floor of the laboratory directly below the point where displacement is to be measured.All sensors (displacement and force) shall be connected to the data acquisition system using the same cables used during calibration. The excitation voltage and gain shall also be set to the value used in calibration. The data acquisition system shall be set to record voltage changes caused by loading. Before applying load with the hydraulic rams, all sensors shall be set to read a voltage value between 10% and 90% of the voltage output of the sensor at its rated capacity. These voltages shall be referred to as the "zero offsets" of the sensors. If a sensor is set to have an initial Revision2 4 8-4 REDACTED VERSION

Hage o011114 Appendix 8: Approved lest Procedure 2bb68-UUU-Vl:5-bYU1-UUUU1-UUi Page b ot Zb voltage exceeding 20% of its output at rated capacity, the sign of the initial "zero offset" shall be opposite to the sign of the expected change in its signal.Set the data acquisition System to scan all sensors and save at least one record per sensor every 1 sec.Record a file of "zero offsets" capturing at least 10 min. of data before any load is applied with the hydraulic system.Means of initial voltages for all sensors (mean "zero offsets"), sensor serial numbers, the most recent sensitivity constants, excitation voltages, and the channels of the data-acquisition system used for each sensor shall be recorded using Form 8. The pairing of channels and sensors shall be checked by a second person working independently from the person making the initial connections. Infrared targets to be used to measure displacements as described in the attached proposal shall be glued to one face of the test beam using epoxy adhesive. The numbering sequence of these targets shall be recorded using Form 9.Video cameras (one for long-time lapse video and one for high-speed video) will be positioned to capture the response of the mid third of each specimen. To the extent possible, the location of the cameras shall be the same in all tests.5. Testing The following actions shall take place during each test: At the end of each loading increment: Mark Cracks: all visible cracks shall be marked using black permanent markers. Cracks shall be marked by drawing lines parallel to them and with an offset of approximately 0.25 in.Measure Crack Widths: Crack widths shall be measured using crack comparators or graduated handheld microscopes. Measure coordinates of infrared coordinates: A set of coordinates shall be obtained using an OptoTrack System 600 Pro. A set of four targets shall be attached to the strong floor. They shall be located at approximately the same distance to the OptoTrack cameras as targets attached to the test beam. Coordinates for these reference targets shall be obtained at each loading increment. They are to be used to monitor the stability of the Optotrack system by computing the variation in the distances between reference targets.Revision2 5 8-5 REDACTED VERSION

M'age bi40ot 1114 Appendix Approved lest Procedure l-'age 0 ot Zb In-Test Data Backup: At every loading increment the data being produced by the data-acquisition system shall be copied to an external hard drive.Photographs: a set of high-resolution photographs shall be obtained after cracks are marked at each loading increment. The photographs shall includes views of both elevations of the test beam and the top concrete surface above lap splices.The following data shall be recorded throughout each test: Sensor readings: to be recorded on a hard drive in volts. Conversion to engineering units shall be done after the test as follows:-Subtract zero offsets-Divide the result by the sensitivity obtained in the most recent calibration Lapse video photographs: to be obtained every 5 min.Actions to be taken at failure Trigger high-speed camera to record breaking away of the concrete cover and relative movement of the bars.Actions to be taken after test Generate a record of sensors that may have malfunctioned or been accidentally moved during the test Remove from all files recordings from sensors for which the results of the after-test calibration differ by more than 5% from the before-test calibration.

6. Reporting and Backup Produce all the captured data in two ways: By uploading data, photos, and video to a private project at nees.org.By recording all data, photos, and video on a magnetic hard drive Reports shall be produced as described in the Specifications.

Revision2 6 8-6 REDACTED VERSION Form 1 I 2 3 " SOUTH I NORTH I ..,-6 5 4.Section A-A 2 Spa. @3, 3'F A A KBKLc K D K EKF*For section B-Bthrough F-Fsee Sheet 3of 3 Series A Drawing: Series A Formwork As-builts Sheet: 1 of 3 BOWEN OWN , JLB YProject: Experimental Investigation of Drawn by: BPR Checked by: SP PURDUE UNIVERSITYCaatofLpSlcsfNo 11 Reinforcing Bars Date: 04/04/2012 8-7 R Form 1 I I -~2-I--31 SOUTH NORTH6 5 4 _Section A-A 2 Spa. @3 3 ,F A A K B LC KDKEKF*For section B-Bthrough F-Fsee Sheet 3of 3 Series B Series B Formwork As-builts Sheet: 2 of 3 Experimental Investigation of Drawn by: BPR Checked by: SP Capacity of Lap Splices of No.11 Reinforcing Bars Date: 04/04/2012 8-8 R E D IO0N Form 1 I" ~8 I" ~8 -6 4 5 2 '7 6 4- 5 7 1--3 1--3 Section C-C, D-D, & E-E*Facing North Section B-B & F-F*Facing North-- BOWEN PURDUE UNIVERSITY Formwork As-built Sections Sheet: 3 of 3 Experimental Investigation of Drawn by: BPR Checked by: SP Capacity of Lap Splices of No.11 Reinforcing Bars Date: 04/04/2012 8-9 RE N Form 1 Project: Tests to Determine the Behavior of Spliced #11 Bars As-built Dimensions v.1 (Rev. 04/04/2012) Specimen: Sheet ilof 2 Formwork As-built Dimensions Section 1 2 3 4 5 6 7 8 A-A B-B C-c D-D E-E F-F Recorded by: Signature Date Time Checked by: Signature Date Time Checked by: Signature Date Time Comments:*See formwork as-built drawings for dimension locations 8 -10 R IO0N Form I As-built Dimensions v.1 (Rev. 04/04/20 12)Project: Tests to Determine the Behavior of Spliced #11 Bars Specimen: Sheet 2 of 2 Formwork As-built Dimensions Key -Series A Section 1 2 3 4 5 6 7 8 A-A 14'-6" 10'-0" 14'-6" 14'-6" 10'-0" 14'-6" N/A N/A B-B 4-3/8" 6" 4-3/8" 23-5/8" 23-5/8" 30" 30" 17-5/8" c-C 3" 6" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8" D-D 3" 6" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8" E-E 3" 6" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8" F-F 3" 8-3/4" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8" Formwork As-built Dimensions Key -Series B Section 1 2 3 4 5 6 7 8 A-A 13 -10.5" 6'-7" 13 -10.5" 13'-10.5" 6'-7" 13 -10.5" N/A N/A B-B 4-3/8" 6" 4-3/8" 23-5/8" 23-5/8" 30" 30" 17-5/8" C-C 3" 6" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8" D-D 3" 6" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8" E-E 3" 6" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8" F-F 3" 8-3/4" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8" 8-11 R E IO N Form 2ie Wire Ties NORTH Bar Marks NORTHOWENSpecimen: _ _B dTO YProject: Behavior of Lap Splices of No. Drawn by: Checked by: PUgR DU E UN I VE R SI TY 11 Reinforcing BarsDae Re~isi~n 2 REDACTED VERSION btUj-UuU-Ud-ULi3LP-UUU1U-UUU i-age h(1 ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 8: AI P'rocedure Casting Documentation v.1 (Rev. 03/30/2012) Mage 1i ot zb Specimen:_____________ Sheet 1 of 1 General Information Date Disp Ticket Num Truck No. JTime on Ticket Time of Arrival Temp. in Lab Measurements made upon arrival of concrete Slump (ASTM C143 -l0a) Air Content (ASTM C231 -10)Time 1 Result 1 Time 1 Result 1 S/N of Air Meter Time 2 Result 2 Time 2 Result 2 S/N of Scale Unit Weight (ASTM C138 -l0b)Time 1 Wt. of Cont.1 Total Wt. 1 Wt. of Conc.1 Result 1 = Wt. of Conc./Vol. of Cont.Time 2 Wt. of Cont.2 Total Wt. 2 Wt. of Conc.2 Result2 = Wt. of Conc./Vol. of Cont.Times of actions during and after casting Lae lcd Layer 1 vibration Layer 2 vibration Top surface struck Truck Departing complete Lae lcd complete off Lab Lifting Inserts Covered with Patcrmvd Covered with Burlap doused Covered with Placed plastic burlap with water plastic Recorded by Signature Date Time Checked by Signature Date Time Checked by Signature Date Time Comments:*The following ASTM standards and specifications will be followed during casting: C172-10, C192-07, C470-09 8-13 R EDAI~~~nLSI ON bbU3-UUU-Ud;J-UIUL-UUUl b-UUU -~age at 1114.Project: Tests to Determine the Behavior of Spliced #11 Bars Appendllx 8: Al 1 ymd4est Procedure Curing Documentation v.1'(Rev. 03/30/2012) Yb3-UUU-V15-:SYU1-UUUU1-UUj I-age 14 01" 2b Purdue University -Bowen Laboratory Sheet 1 of 1 General Information Specimen(s) Date Specimen Age Time Beginning Time Ending Temperature inside Lab (deg. F)Description of Work Performed Recorded by Signature Date Time Checked by Signature Date Time Checked by Signature Date Time Comments:*Test specimens and associated cylinders are to be cured under wet burlap for seven days 8-14 R E I O N Form 5 Project: Tests to Determine the Behavior of Spliced #11 Bars Cylinder Compression Tests Documentation v.2 (Rev. 04/01/2012) Specimen:* Sheet i of 2 Diameter [nearest 0.01 in.] Length [nearest 0.05 in.] Fracture Type Specimen Date Time of Test Wet/Dry Pmax [Ibf]1 2 1 2 3(1-6)1~2 3 4 5 6 S/N of Testing Machine: Recorded by: Signature Date Time Checked by: Signature Date Time Checked by: Signature Date Time Comments:*Cylinders to be test per ASTM C-39-22 and C-1231-20a with a loading rate of 60,0001bf/min at concrete ages of 3, 7, 14, 28 days, and on same day that test of correspondingspecimen is conducted. Specimens and caps free of defects unless otherwise noted in comments. Average cylinder diameter and area and unit compressive stress (f'c) calculated on sheet 2 of 2.8-15 R IO N Form 5 Project: Tests to Determine the Behavior of Spliced #11 Bars Cylinder Compression Tests Documentation v.2 (Rev. 04/01/2012) Specimen: Sheet 2 of 2 Average Cross-Specimen Date Age Time of Test Wet/Dry Measured sectional Area Prnax [Ibf] f' [psi] FrcueTp Dia. [in.] [in2](1 )2 0-Jan 12:00 AM 0 #DIV/0! #DIV/0! 0 #DIV/0! 0 2_____ 0-Jan 12:00 AM 0 #DIV/0! #DIV/0! 0 #DIV/0! 0 4 5 6 S/N of Testing Machine: d.Recorded by: Signature Date Ti me 0 0 0 Checked by: Signature Date Time 0 Sintr0________________ 0_________ Checked by: Signature_________ Date______Time ___Comments:*Cylinders to be test per ASTM C-39-12 and C-1231-10a with a loading rate of 60,0001bf/min at concrete ages of 3, 7, 14, 28 days, and on same day that test of corresponding specimen is conducted. Specimens and caps free of defects unless otherwise noted in comments. Recorded data is shown on sheet 1 of 2.8-16 R EDAljii(E:S IO N

I-age bib oT 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 85: est -'rocedure Calibration Documentation v.1 (Rev. 04/02/2012) Iage 1 ( ot Zb Bowen Lab -Purdue University Sheet 1 of 1 Calibration Instrument Name and S.N.: Data Acquisition System: Gain: Excitation Voltage: Channel: Sensor: Sensor S.N.: Measurand Voltage Measurand Voltage Measurand Voltage Operator Signature Date Time Checked by Signature Date Time Checked by Signature Date Time Sensitivity Accuracy Results Notes: Re~is~n 2 REDACTED VERSION

I-sage fbf ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 8: f~~l~ 6EtProcedure Calibration Documentation v.1 (Rev. 04/06/2012) I-'age id oT 2ti Bowen Lab -Purdue University Sheet 1 of 1 Meter S.N.+Tve fMee.4-Meter Brand Name Target Air Content Measured Air Content Operator Signature Date Time I + 4 Checked by Signature Date Time Checked by Signature Date Time Notes: Re~is~n 2 REDACTED VERSION Form 7 111+/- 111111 I I I I I I I I I I I I I I I I I I I I I Y II II I I I I I I III INORTH ILLLLLLLLLI__-LLLLLLLLLL ______________________________________________I I I I I I I I I I I I I I I I I I I I I F q................................. fT 111111111 I 111111111 I~8 NORTH 1 1 1 1. ..1 1 £ I---*-j 4~~~~~*a-I PURDUE UNIVERSITY Behavior of Lap Splices of No. 11 Reinforcing Bars 8-19 R EDgAl~i~icnESI ON Form 7 I SOUTH SOUTH I i-, ~2 Top Plan 2 Spa. @3' '-60" Ea. =' 3'KB Ko L LEL F Profile*For section B-B through F-F see Sheet 3 of 3 I" 3 " NORTH NORTH F-_I 4 Bottom Plan.. SOWEN D- LABORA TORY P U RD UE U-NI-VERS IT-Y Series A Concrete As-builts Sheet: 2 of 4 Experimental Investigation of Drawn by: BPR Checked by: SP Capacity of Lap Splices of No.11 Reinforcing Bars Date: 04/04/2012 8 -20 R E IO0N Form 7 I SOUTH SOUTH I NORTH 2 1 Top Plan 2 Spa. @3' ----39.5" Ea.--- 3'Profile*For section B-B through F-F see Sheet 3 of 3 V" 3 " NORTH I ,,I 4 Bottom Plan Series B Concrete As-builts Sheet: 3 of 4 Experimental Investigation of Drawn by: BPR Checked by: SP Capacity of Lap Splices of No.11 Reinforcing Bars Date: 04/04/2012 8 -21 R I0 Form 7 I" ~1 4 2-~3 -Section B-B, C-C, D-D, E-E & F-F*Facjng North__________ jr B W NDrawing: Concrete As-built Sections Sheet: 4 of 4___ __BO Experimental Investigation of Drawn by: BPR Checked by: SP P UR D.UE U NIVERS ITY Capacity of Lap Splices of No.11 Reinforcing Bars Date: 04/04/2012 8 -22 R E gAl~l~LS IO N Form 7 Project: Tests to Determine the Behavior of Spliced #11 Bars Setup and As-built Dimensions v.1 (Rev. 04/04/2012) Specimen: Sheet Ilof 2 Concrete As-built Dimensions Section 1 234 5 678 Plan B-B C-C D-D E-E F-F Recorded by: Signature Date Time Checked by: Signature Date Time Checked by: Signature Date Time Comments:*See concrete as-built drawings for dimension locations 8 -23 R Form 7 Setup and As-built Dimensions v.1 (Rev. 04/04/2012) Project: Tests to Determine the Behavior of Spliced #11 Bars Specimen: Sheet 2 of 2 Concrete As-built Dimensions Key -Series A Section 1 2 3 4 5 6 7 8 Plan 39'-0" 39'-0" 39'-0" 39'-0" N/A N/A N/A N/A B-B 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A C-C 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A D-D 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A E-E 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A F-F 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A Concrete As-built Dimensions Key -Series B Section 1 2 3 4 5 6 7 8 Plan 34'-4" 34'-4" 34'-4" 34'-4" N/A N/A N/A N/A B-B 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A C-C 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A D-D 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A E-E 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A F-F 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A 8 -24 R I ON Form 8 Project: Tests to Determine the Behavior of Spliced #11 Bars Instrumentation Documentation v.1 (Rev. 04/01/2012) Specimen: Sheet __ __of____Data Acquisition System: Channel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location Comments Operator Signature Date Time Checked by Signature Date Time Checked by Signature Date Time Notes: Re~isi~n 2 REDACTED VERSION Form 9 Jj...1 1 1...1 1 1 1 jt ' -4 111111111 F I I [ ] I I I Th NORTH I I I I 4; 4" ,. , , ,-BOWEN flLABORA TORY PURDUE UNVRSIT Specimen Behavior of Lap Splices of No. 11 Reinforcing Bars Re~isi~n 2 REDACTED VERSION Purdue University Specimen: A-I Date: 4/LI/1 Average Joad North South North Splice Md (i) South Splice LVDT North LVDT South North Load Cell South Load Cell DG North DG South Tm (I- Overhang (in) Overhang (in) End (in) Mdpan (i) End (in) Support Support "J ." J! J" Overhang (in) Overhang (in) Time_____6 Q.-O."~ o.1S 0.o:7 0.o-i o.0 " .oQoo .-o.ooo 6 & O. i'l6 A_____, c?.c2 " 0. , o! c,0 0 ,If o.o" -O .oo0 -0,00 j"L- 7. O. 6H 0 .qO : "'A SI o.,9o Q. 4 .Q.It~ -c).ooo ooo !' !' 0.0060 0. /,O"/ 6 "tO 1.7. 1.L7 o.-I~ o.V. -0.Qoo -0.oo( -'o -'o- I./' VL.66 Io:ooA 6 tl.< tG -Ge4- O.gov "oQ o, oo ,.~.6A O i' .o0' "toS Q,?I oA&6 o.=1 -0ol.oo -o.oo' "V 6 L.38 IQ',.A" ' 1. 3.. ____ ______ _____ -oo,_-oo_ ___ ,!_.__ 0 q 13 1-.." I,0 , '[ 0. cj. L", O." 0,.1 -o.oo6' -o~o <?.'. q.o;F 15 iQ , "2.-I" ".-62 o.4" o .* c.4'i q -o.oog 1"1-..o I',O"IZ.16 3.?"'f 0.9;1. 0.70 0 .c G -.oo" -o.oo-f "A..Q. 2A.0. 12i":7P" O7 q q. .0:1O (\.o! o1$'7 -..c." ..o, LIL.\ Ho.o 20 __, ___ __.___ L.LI, 1 t. 1.Li( 1.15 -.oio -. 0 '.litH , __ __ __ __ _ _______9-I REDACTED VERSION I' ..0 U Purdue University Specimen: Date: Average Load North South North Splice Md ()South Splice LVDT North LVDT South North Load Cell South Load Cell 06 North D6 Sauth Tm (lbf) Overhang (in) Overhang (in) End (in) Misa i) End (in) Support Support *(Ibf) (]bf) Overhang (in) Overhang (in) Time____1 ~ .0 0 -0.0!l 0 -0.01 -0.001 -0.ool0. 0.2.. 0.7 .O~0 .!,-1 O.AI 0.0I .01 -0.00oo -0.00l S, G Q.W]L l1I" 0,-H'- O.-f-i 0.06 0.10 o~o 6 -.0.oo -0.001 V"L 11. 0.G3' Q.6?"t $'?5A , "1.qi16 .1"/ Q.!"1 O,"1,6 7.I1 0...0oo -0.00' %" ,IA t55~ ,.6"7 , .6 I.Q .2tz ;.3- 0.'Vl" -O.oO"t -0.0O1 30 t7Ol."e~ I.I'zQ T:J;A , _____ ..21 o..i-' o."z. -o.oo-. .-o.,:oo" ____ ____ 1.VI'/'- !.1t' 10 :3.,-- "z,"' "j,-' 0.33= -0.001 -o.o000o __ ___jj~ " 1o:S'JA 11 1O.g ";,6o; Q,q O."t'. o,.' -v.oo-i.- -o.ool 10,.6 "-II .. i:]"A 13'14 16 18"20 9-2 REDACTED VERSION 0 Purdue University Specimen: A-3 5 /~O/l2 Date: Averacejoad North South North Splice Midsa (In) South Splice LVDT North LVDT South North Load Cell South Load Cell DG North 06 South lm (fI<Overhang (in) Overhang (in) End (in) spn End (in) Support Support (1 Overhang (in) Overhang (in) Tm 1 Q.(6 0.00 0.00 0.00 Q.QQ Q.oO -Q.o0"L -o.0o'L 0.Lt ,0. 0 .1 o.(t40 2 ,' o(t Q.Iq o.o'z. Q0 0.0 1 .o. .-O.ooL -0.0o02 6 6.-i:. o.L g. ?Li." 0.q-H o.-I1 O,01 0.1! o.o-l .o.o'-L _o.OOi t1.. tiL.. Q.C'1 g:w;_____ 08 o.gO .' 0.-1.- Q.1- -oQo3 0.ooo ____ Q,9? -o:;1A2 1.V; 1.1-9 oI'z, 0,-1 *-o.oo,0 o.'oi- 20I I-tl , 1.',1[,b O.L O. q' .? 0.i.9 O.ooq L6'1$ t.S tO : f 10 11 12 13 14 17 ISi 19o 9-3 REDACTED VERSION 0 Purdue University Specimen: Date: 4,/3/12 Average Load North South " North Splice Misa i) South Splice LVOT*10rth LVDT south North Load Cell South Load Cell DG North DG South ,, (Ibf) Overhang (in) Overhang (in) End (in) lsan(n End (in) Support Support __ I_____If) Overhang (in) Overhang (in)} Time o,01 -o~oj -0.0 I -o.oQ -Q~oQ 0.00 -0.oo[ -0.00o O[ Q. 0.000 0.00 2 3..i. c atk ______3 6.0 0.11 0IGO1 0.0. 0.0'1 0.0"? -o.oo( -0.001 6.o 6-O 0.11 6 lL.1-O-I) O. CISoo Q.i.'l 0.0S -o.iool -o.oo0. 2:.I.O 'Li.I I.7lJ~ OI4~ To-IA' 3-J.S 1.-T? 0.1-c Q.-G -o-ooo -9.oo1 "i.'.9 L-1-fQ 1-iQE 9"1-IA N*,,~c VG __ __ ___ _ .oc'0 O.oO~10 N+" DG .- o.000 o-Qoo ,, "o.O ?.x' 7-ISo, O.61 Q.6G 0.c6 -o.oo? 0.-I"l O.'3" ,¢.,jj0 Is O.-SI 0.66Q O.c; o~o(- tO".",.. 03 __i___'zC ,, -1,Q o.',5 0.660,c.*I -0.0oo' 000o 7A.1 Ul:5JA 16 '.-: 7A.9 o.S9J Q.< Q.-&-f 0.o0Q3 ?6.o ___ .o_ VL:IbF 9-4 REDACTED VERSION U U U Purdue University / ll2 Specimen: Date: Average Load North South North Splice South Splice LVDT North LVDT South North Load Cell South Load Cell i DG North DG South rm (lbf) Overhang (in) Overhang (In) End (In) Mldspan (in) End (In) Support Support (lbf) (Ibf} Overhang (in) Overhang (In) Ti_____e _1 0.01 0.00 -O.oot. -o.oc-i. 01. o.ooo o.Qoo "]:3gA VL,.Q 0.11~ 0,0-j o.1 o.0, -.oO).o -a.0" VI.'t (i.Q Q-16= ' 0.86 o.9j -o0,0L -o.ooi I-Q I.Q 0.860 Q!~1'I g:-[s'A , ta~c) -o .oc~t o~ooo "IA.O .o +0. 1.1.;! __l__7_ : t' ?0,0 U,,I L.,5b 0.31 0,L-J -o.ooi o.ooI 30.0 Qo.O i.G2.? b&1,69 S-W'A , DC, ,.-, __'_"Q.ooo Q.OOQ , 6.o .o"1..O1 '),4Q o..4i -o.ooo o.oo1 ?6.0 36.0 Q.-f4;o~ o.'If fQ:o64 ii 'yc/qit -L.M1I Q2. 5' -o.o00 .O.ool ?1.7 '1 .q; O.e?" Q to':-A ,N14S" PG v-oQ4.- 'z.ooo 0.oQQ 13 3/4- 0.63 Q?.q 0.66 -Q.ooo -o.o0 o 2.0fo $.-]o iQ:ssA 1-9 -lo,1 '-1.6-i. ,0."i Q.'" o.o0o -0.001 '-!o.6 i~,-I-f P 9-5 REDACTED VERSION Purdue University Specimen: A-C, Date: Average oad North South NorthSplice Md n) South Splice .VDT North LVDT South North Loa.Cel South Load Cel DG North 06 South T--(6 Overhang (in) Overhang (in) End (in) M span [I) End (in) Support Support Overhang (in) Overhang (in) Tm O."V. 0.00 0.o0 0.00 -0.00 o.o0 -.0.0o0 -o~ooc' 0.? O... 0oo .000 F'Q- ot' 0.0'7, Q.o=; o.0ot -o.ooo 6.0 bQ O.i1!. oQ-i;i , ~z oA o Q,-o.+ 0,0-i ocoj 0.01 o.oo~ 0t.000 1'2..o ti..A I o .,913 I:'oP , o~g6 Q.%G 0.13 o.I9 v.007 -.001o {i~O 6 Vo ..67 I.61, 0."}.- O .'L6 o."js QOQ0 -0001" -2'fQ .0 Ao.. l. 6."3 L.6'1 "t.-{fP 8 12c ,voi4" 0.000 aQvQQ "1;bF'15 vo ,L -3,oo 3.1' 0 .i'- O*e6 osq-I 0.o00' -o.007 1.oQ.I "Lo.3 0.?3? O.q(;6 P 16 Q.tl," I.8 6 "i.. "..o Q,'j O.-jo 03.5 -o.0o7 O,1". O,"__-.0 _16 "1,'- 1 ."0 0 .Q O.&" -o..Oo" "_..__ .0_ ____ ___'9 '4..07 Q.(:,Q Q.g? 0.66 0.oo')J -0oo 3G .Q ?.o S-t- FP 20 t(Q,3 iJ?". -j.-i0 Q0.'0 Q0e..7 9.7 q.oo -c'.oo'9 4,Q,-7 _,__,_ _______9-6'REDACTED VERSION

• .r Purdue University Specimen: Date:_6.g.2 Average Load North South North Splice Midspan (in) South Splice LVDT North LVDT South North Load Cell South Load Cell DG North DG South Time (lbf) Overhang (In). Overhang (In) End (in)} ______ End (in) Support Support (lbf) (lbf) Overhang (in] Overhang (in) ______" -!. L.-0 L ,!-408; tt; .~ o o~t II H*.'. , F 23 24 26 27 28 29, 33 31, 32 33 34 36 17 43 9-7 REDACTED VERSION Purdue University

©Ii Specimen : DQ -_Date: -l0i: 71 ~T r Average North Overhang (in) South Overhang (in)North Splice End (in)Mldspan (in)South Splice End (in)LVDT North Support ILVDT South Support INorth Load Cell (lbf) ISouth Load Cell (Ibf)S o.'z -0.01 0 0 0 -o.00 -o.ooo o0 S .o5 .o o.oj o o 0 3.5 3. -6 0 ..o .5 o. 045- _ _ _ _ _ _S G 0.~ Io.14 O. oZ- 0.o'?_ O.oZ o.ooi 0.001 ___ __6 I o.j o 0.o5 d.oe o.0oo3 o.oo01 I 11 I0-o.- o.+/- 0.I _____o.I o..oo4r i 13 2-4 I.I I.o-+ o.15 O-Is o. 1j o.oo2 1, 1e .Po 1. 1 o.I_5 O.31 0.12 0.00 o.oo3 ______19 20 ZM vo 3 ~3A~414 9-8 REDACTED VERSION 0i ..Purdue University C)S Specimen: Date: Average Load North South North Splice Misa i) South Splice LVDT North LVDT South North Load Cell South Load Cell DG North DG South TnOverhang (in) Overhang (in) End (in) Misa I) End (in) ,- Support- Support ..a//,/ 't Overhang (in) Overhang (in) Time____1 o~. 0 o.oj 0 0 -Oofo -0.oo5 o.ool 0,3 0,L f-.0 0..o0Olo ?.:57-A___________ ______ O1 .0¢ 0 .O 0.'01 -0.005 0.001 0236 O~4 " 5o S 18 o.81 0. 8 0.1.1 0.13 O. Io -~o..oo____ ____ 0.__0_-__

1 , 0 14 o.2 0.2. .00~ I.s~ra bo~ooA-P.ELA'TJVE 10 If o.s, o.i.5 ol' o.11- o.OOS, I, Ig -O. 32o I1:1o A 12 19- I.% 1.9 o.j8 o.1- -ooo .17;9-9 REDACTED VERSION

...(0 Purdue University Specimen: Date: /_/i Average Load North South North Splice Mdan()South Splice LVDT North LVDT South North Load Cell South Load Cell DG North DG South lm 4Jf. ! Overhang (in) Overhang (in) End (in) __dspan___n) End (in) Support Support J4 Overhang (in) Overhang (in) Time____1 o .% o o o -0.o -o.oo' o 0 '-S G.2. 0.14 oXlf o.o'L 0.o2 ,-o.oal -coa.oo 6.z 6.g. o.j14 o.Ij, 2,io.A" 0.4. 0.40 0.05 0.0-4 0.05 -...ooo -o.oo~Z. )Z oQAo7 ,35A, S 8 oJ .0-jo. 0 o.3 o-JO -o.o04 -o..oo? 18 lB o.-?4-- 9):o{-6 z 4 1.o09 I.of- 0. 14 o049 0.15 .--o.0of .-0.002 4,, L. .057- (. o6o ¢/' 30 I.43 1.41 j.1 0.25 o2. -0.ood/ -cooo 30 zo I., " ." .'25 03.3 o."5 -o 0,.0o0oo 3C, o J.aao !o'zB4,q 0-o. Q44 o4 o.0? o.0J -o.oo~f o.,, oZ. o.,,/ (/;o5..4 1o 0% O 8G .1 O-Jk o.15 Oi12 -o.oo,0 -ooz 12.1 O.Saeto I1"1" 4 14 16 17'19 20 9-10 REDACTED VERSION Purdue University Specimen:, rh-H Date:_Averag Ove Nrthan (I) overhagin ENdr (pi) Mldspan (In) South Splice LVDT North LVDT South North Load Cell South Load C:ell DG North DG South (Ibf)_Overhan (in)____ Overhang__ ____n) __End _____in)_ End (In) Support Support (lbf) (Ibf) Overhang (in) Overhang (In) Time____.* o.o¢ 0 0 o0 o.ool 0. .. o. 4:jq/:' 04" 0 o o o o o ogp0 o. o.,'2 o. ,2o2 o.,loZ It z 24 26 28 27 28 29 30 31, 32 33 34 36 37 38 39 40 9-11 REDACTED VERSION Purdue University Specimen : Iz:-Date: -'Average Load North South North Splice Mlsa i) South Splice LVDT North LVOT South North Load Cell South Load Cell DG North DG South Tm (Ibf) Overhang (In) Overhang (in) End (in) Mldspan__in) End {in) Support Support (Ibf) (Ibf) Overhang (in) Overhang (in) im S 0 oo000 -o.ooyZ -o.0o1 _.___o. o._o..__._,_I-- 0 .. 0.o5 0 0 0 -o.ooi o __.__ 5.Z o.z45 oif_65 ______ 0.1 0z~.. 005 0o 0.00l ____ ii.__ 0.5 V(L 0.s'5 1_58____o. __ O.___ o._oo-I 0.08 0.00-3 o__o___ _____ __.__I o______ ____, L-> 'ST .S1Ll CI-, .Ac v. __ __ _ __ _ __ ____ _'24[ 0.c5 o. o.0o G.I5 O.0o-J g0 iAi~i' 1.i41' 3'3-, _ _ _ _. _ _r _ _. _- _ 0-I -o 2. l 0.W. o , o( o .oo 4 .I.Y /U :I.:9::/ I.:& 0. 0.2..,4 .___ .____ ___ -__ 4 12 13 14 15 16 17 18 14 20 9-12 REDACTED VERSION U Purdue University Specimen :_________ Date: Average Load North South North Splice Mi i) South Splice LVDT North LVDT South North Load Cell South Load Cell DG North DG South Tm (Ibf) Overhang (in) Overhang (in) End (in) ___span_____ End (in) Support Support ..II L-- Ia Overhang (in) Overhang (in) Tm 0.4 0 o 0 0 o 0 O _____ O~. o ' 0.2_ 0 0 0) 0 0 o-ool o.i_ o,-2 0 0.-900 _____ O.oO 0.c~ aOo2 0.0i o. oo'2. o.0oo1.. 6 0. I =P 6 ____ o,' 0.04 0.01 0.09 o. 04 o. ooZ ' ~ .oGO8 l4011P1 V 5 o.l. o5.9,5 o.o2. o-II oC4' 0c4 2e 15A -o.l o.92,5 2z'78'M* 1.oi 0.30 O.l9 o.17 o.I:7 0.05 20 30i 1-0.? I. 3:16W' z E ID & S ; _ _ _ _ ._ _ _ .o 00 ( J O)__ __o._ o.z8 o.Zf. o.00s o,0o/-osL L.5,Z.' 3:4411'"1 o o.59 0.39 0.05 0.o0 o.o5 o..oo3 o.oo'2 o ______ 12I 9.JG o.14 o~o 0.jI -o.Io .04 o.o0z __ __ _ .4_____o._______-_ 1.2l& .Q0 o0 I o.I .02 00o ___________. 14 3'._ 1.54 I. ¢ -_-___._ _ooo___ _____ --- -s ..o ?'M 15 16 18 19 20 9-13 REDACTED VERSION U 0 0 Date: S ,.5 Purdue University Specimen" Average Lgad North South North Splice Mda(n) South Splice LVDT North LVDT South North Load Cell South Load Cell DG North DG South re-]1 Overhang (in) Overhang (in) End (In) Midspan___n) End (In) Support Support 4J.f I c Overhang (in) Overhang (in) Tm o.1_ .O__ O.0', 0 0 0 -0.0b06 0. O.10O 2 k.: .c,_ __ _ __ _ _ _ __ _ __ _ __ _S6 04i o~ 0.01 0.01 -oo 0.005Ooo .6 o.105 'Z-9A 12 IO1.t 0.39 0.05 0.o0, 0.0ot -.xo~o, 12 V,2Z 1 8 0.:/5 0.1 0.0,9 o.ll 0.08 18 18 o.=jl %ob,4__________ .o__.$ O.l' o.oo,/ I.o3,L j4l~f _______.__-- i.0. ! oOZ ..1 -o.001 o.oob ffijZ- v.'S 1O-1i, 10 _____ L, [,'& O.i~l 0,1 -OOOI 0.005 ?,5 1.16ft 1.2.56 " o o.o~t 0.05 -oo o.oo. o.z o.ApL o.So5 I0oA.o 12 0.81 0.9,o o.11 0.13 0-!0 oR.o, 1l Z O.'Bo5 0.85 t2-IIo(,A 17 1.9 9-14 REDACTED VERSION bbY;5-UUU-Ut$;5-U1:U-UUUlth-UUU I-'age oT 1114ApedxU:alrtoneticas Appendix 1U: (JertlTicates TAKING ACCURATE THERMAOMETER READINGS COMMON TYPES OF THERMOMETERS AND FACTORS AFFECTING THEIR USE TOTAL IMMERSION thermometers are designed with scales calibrated to indicate the true temperature when the bulb and the portion of the thermometer that contains the mercury column are exposed to the temperature to be measured (practically,, less than an inch is permitted to extend above the surface,.o permit the reading to be made). Most total immersion thermometers can also be used in a condition of complete immersion, in which case the entire thermometer is exposed to the temperature being measured, such as in a freezer.PARTIAL IMMERSION thermometers are designed with scales calibrated to indicate the true temperature when the thermometers are immersed to specified depths. The portion that should be immersed is indicated on the back of each thermometer. COMPUTATION OF EMERGENT STEM CORRECTION When total immersion thermometers are used only partially immersed, a stem correction may he calculated and applied to the reading for precision results. To compute an emergent stem correction, the following variables must be defined: T = the reading of the thermometer in situ.N = the number of degrees on the thermometer scale between the liquid surface and the top of the mercury column.A = the average temperature of the emergent mercury column. To find value A, suspend alongside the subject thermometer a secondary or auxiliary thermometer with its bulb centered between the liquid level and the temperature indicated on the subject. thermometer. The temperature indicated on this auxiliary thermometer will he value A.Find the stem correction (SC) by computation from the following formula: SC = 0.00016 x (N x (T-A)) for Celsius temperatures, or SC = 0.00009 x (N x (T-A)) for Fahrenheit temperatures. Example: A thermometer graduated from -1° to 101°C., immersed to 20°C on its scale, reading 90°C. The auxiliary thermometer reads 42C. Hence, T=90, N=70 (90.20). A---42 Working the formula, SC =.00016 x (70 x (90 -42)) yields a value for SC of +.537. This value must he added to the observed indication of the subject thermometer to determine the true temperature of the liquid. Hence, the true temperature of the liquid is 90° + .54° (rounded result) = 90. 540 GENERAL CONSIDERATIONS FOR MAKING AN ACCURATE READ)ING The error due to parlla may be eliminated by taking care that the reflection of the scale can be seen in the mercury thread, and by adjusting the line of sight so that the graduation of the scale nearest the meniscus exactly hides its own image: the line of sight will then be normal to the stem at that point. In reading thermometers, account must be taken of the fact that the lines are of appreciable width. The best practice is to consider the position of the lines as defined by their middle parts." PERFORMING A CALIBRATION AT THE ICE POINT (0 DEGREES CELSIUS OR 32 DEGREES FAHRENHEIT) Select clear pieces of ice, preferably made from relatively pure water. Discard any cloudy or unsound portions. Rinse the ice with distilled water and shave or crush into sm~all pieces, avoiding direct contact with the hands or any chemically unclean objects. Fill a Dewar or other insulated vessel with the crushed ice and add sufficient distilled (and preferably precooled) water to form a slush, but not enough to float the ice. Insert the*thermometer, packing the ice gentiy about the stem, to a depth sufficient to cover the 0°C (32°F) graduation. As the ice melts, drain off some of the water and add more crushed ice.Raise the thermometer a few millimeters after at least 3 minutes have elapsed, tap the stem gently and observe the reading. Successive readings taken at least one minute apart should agree within one tenth of one graduation. APPLYING THE CORRECTION AT ICE POINT Record readings and compare with previous readings. If the readings are found to be higher or lower than the reading corresponding tO a previous calibration, readings at all other temperatures will he correspondingly increased or decreased. Reproduced in part from ASTM E77.KESSLER THERMOMETER CORP.Precision and ReliabilitY... from aname you can trust.REDACTED VERSION lbu)i-UUU-U.5IJ-U.1--U-UUU1Ii-UUU l-'age Ijuu ot 1114ApeixU:airtonetlcte Appendix 1U: L;allbratlon Cerl:lrlcates CALSER CORPORATION 302 N. BELT EAST SWANSEA, IL 62226 (618)277-0329 TESTING MACHINE CERTIFICATE OF CALIBRATION Owner : Purdue University Report #: Location : 1040 South River Rd. -Bowen Lab West Lafayette, IN 47907 Page : Machine : Fomey 600,0001bf Model F-600-DFM/1 Serial No. : 99058 -§ liaef wI Fomey DFM/1 Digital R/O #9902182 wI/Dynisco P/T #02-23-990747 This is to certify that the testing machine listed above has been calibrated by Calser Corporation personnel. The method Of verification and listed data are in accordance with ASTM E 4-09.Accuracy of all calibration devices is traceable to the National Institute of Standards and Testing (NIST)*and all calculations have been corrected for temperature where applicable. VN# 6560 2 of 20616111, Capacity Range Run 1 600,000lbf Range Run 2 600,0001bf Range Run 3 600,0001bf Range Loading Range 5,000 -600,000 5,000 -600,000 5,000 -600,000 Max. Error 1.20 %0.10 %0.08 %Verification Equipment Used: (400,000 Load Cell Set)Admet Gage Buster Digital Readout, Serial # GB-991 1092, and Load Cell(s) Listed Below.Serial # Ranne Calib. Date 901 120B 716.99 -10,000 lbf 08/19/2009 090716C (LO) 5,572.38 -100,000 lbf 08/10/2010 0907160 (HI) 39,281.95 -400,000 lbf 08/10/201 0 Uncertainty 1.792 16f 13.931 lbf 98.205 Ibf This cerlilicate is Issued as a statement of the fact that on the above date the listed testing machine has an accuracy as Indicated. It should not be construed or regarded as a Guarantee or Warra~nty of any kInd (In favor of the client, the client's customers, or the public at large) that the testng machine Will continue to retain the same percentage (%) of accuracy or efficiency as determined on the date when the calibration, and adjustments if required, was performed and reported by 'Calser Corqrration' since the calibrator has absolutely no control over the future operation, damage.maintenance, repairs, and overa~l condition of the testing machine and hereby expressly disclaims any and aDlliaLbility for damage or loss sustained by all parties adslng or resulting from th deterioration, obsolescence, malfunction or substandard perfonnance of said testing machine; wtrlch*shall remain the sole responsribiliy of the machine's regula custodian. owner. andlor user. This certilicate shall not be reporoduced except in full, without the written approval of Calser Corporation. CALSER CORPORATION Quality Control Director Form # 104-01-Rev 3 REDACTED VERSION bbi-UUU-LUb3-Utz-U-UUUId-UUU l-'age bU1 OT 1114ApeixU:alrtonertcas Appendix 1U: Calibration CertlTicates A.CALSER CORPORATION 302 N. Belt East, Swansea, IL 62226 (618) 277-0329 TESTING MACHINE CALIBRATION DATA AND REPORT ,-.Customer Purdue University _ Location 1040 South River Rd. -Bowen Lab' West Lafayette, IN 47907-1 Report #: VN# 6560 Page 1 of 2 Date of Service 06/06111 Cost order No. Verbal Order Date 06102/111 Temp. 74" F Date Done 05119110 Machine Serial No.Auxilay Equiprnent: ,Fomey 600,0001bf Model F-600-DFMI1 99058 w/ Fomey DFMfl Digital RIO #9902182I_____________w/D nisco P/T #02-23-990747 -_____AoppledForc __ _Ind'l cted Forel : rE, z I j)I " n l' et Frce r~ .E .I " 1 Idicted orc ErsIo" Run #1 _ Run #1 "As Formd" Co~rrdon __ Run #2 "As Left" Conclion Run #3 ."As Left" Condition 600,0001bf Range *__ l01bf/I DIV

• 0 0 60 0 0 0.00 60 0 0 0.00 6C 0 0 0.001 5.000 60 4,940 -60 1.20 60 5,000 0 0.00 60 5,000 0 0.00 10.000 7 9.880 -120 1.20 7 9.990 -10 0.10 7 10.000 0 0.00 20,,000 7 19.790 -2.10 1.05 7 19,990 -10 0.05 7 ,19,990 -10 0.05 40,000 8 39.530 -470 1.18 ,8 40.000 0 0.00 8 .40.000 0] 0.00 60.000 8 59,340 -660 1.10 8 60.010 10 0.02, 8 " 60.000 0 0.00 80.000! 8 79.1 50 -850 1.06 8 80.050 50; 0.06 8 80.030 30 0.04..00...00.............0..

.,8...........98940 ....0,05t1 -1.065 ... --.8 .... ...- 00 60*...........66(.....6 .6, -.80-.0........00.70 .100...070 .70 ...... 0.07007 125.000 8 123.600 -1,400 1.12 8 90 0.07; 8 125.100 100 0.08 150.0001 8 148.330 -1,670; 1.11. 8 150,150 150 0.10 8 150,120 120 0.08 200.000 8 197,650 -2,350 1.18 8 199,980 -20 0.0,1. 8 200,010 10 0.01 300,000 8 296,650 -3j30 1.12 8 300§6 60 0.02 8 300.040 40 0.01 400.000 8 395.880 -4.120 1.03 8 400.120 120 0.03 8 400,090 90 0.02 500,000! 8 495.110 -4.890! 0.98 8 500,260 260 0.05 8 500.210 210 0.04 600,000 8 593,770 -620 1.04 8 600.310 310 0.051 8 600,290 290 0.05 0 8 0 20 0.00 8 0 -100O.00i8 0 -30 0.00 Notes: D- Calibration in accordance with ASTM E4-09,! and Calser Corporation Procedure

1. 1-01, Rev 1.ACCURACY

SUMMARY

..capacity Rane Loadin Range Max. Error Run I1_____________

600,0001bf Range 5,000 -600,000 1.2.0 %Run 2 ______fl00,O001bf Range 5,000 -600.000 0.10 %Run3 3__________ 600,000!bf Range 5,000 -600,000 0.08 %*CAMBRATI.ON EQUIPMENT All verification equrlpmerf-Incuding dead weights, provin rings, load cells. etc., Is calibrated and traceable to the latest procedu'es $tipulated by the National Ins titute of Standards and Test~ng (NIST) and ASTM E74-06. All equipment is tr'aceable under 9ukleeines set forth In ISO/IEC 17025. Alt instrument readings have been corrected for temperature whiere necessary. _______ VERIFICATION EQUIPMENT _ _ _ _ _ _ _& Sertali ____ nd_ ncertalty(L.BF) & Date Strainsense 60 716.99 -10.000 Ibf Morehouse 901120B 1.792 lbf 08/19/09 Strainsense 7 5,572.38-100,O0001bf Morehouse 0907160 (10) 13.931 Ibt" 08/10/10 Strainsense 8 39,281.95 -400,000 lbf Morehouse 0907160 (HI) 98.205 Ibf 08110110 This report shall not be copied except in its entirety without express written approval of Calser Corp.Formi# 103-01-Rev 3 Calibraton Tedcnican Jerry Parker I)REDACTED VERSION bbW~-UUU-Ud~-UbU"UUU~~-UUU wags Uu~ ot VI14 Appendix W: uslieritian Lertilicitis CERTIFICATE OF CALIBRATION ISSUED BY: INSTRON CALIBRATION LABORATORY DATE OF ISSUE: 30-Jan-12 CERTIFICATE NUMBER: 340013012113643 Lab code: 200301-0~instron 825 University Avenue NSTRON~Norwood, MA 02052-2643 II C a" Teephone: (800) 473-7838 Fax: (781) 575-5750 Email: servicejreq uests~instran.cam Type of Calibration: Relevant Standard: ASTM E83-10 Page 1 of 3 pages APPROVED SIGNATORY Richard- Digh ineo d b ihr fDNcn=Rlchard Binford,:c=US, l=Norwaod, st=MA,---v -- -5'00'Date of Calibration: 30-Jan-I12 Name: PURDUE UNIVERSITY Address: 550 STADIUM MALL DR.WEST LAFAYETITEJ N 47907 KBROWER@PURDUE.EDU KEVIN BROWER PRO.Contract No.: Contact: Manufacturer. BALDWIN Manufacturer. INSTRON Serial Number. 120BTEC502040 Transducer ID: 2630-115/590 System ID:.Range Type: 120BTEC502040 Single Extensometer Type: Travel (Tension): Travel (Compression): Gauge Length: Mode: Type I lin 0.1 in 2in Static (Tension/Compression)-At,-&r A'~?? z&L.The following indicators of the extensometer system were verified and classed: Indicator Type Indicator Range Full Scale Units (%)System Class Description

1. Digital Readout strain 100 B-I All indicators listed above were verified on-site at customer location by Instron in accordance with ASTM E83.The verification and equipment used conform to a controlled Quality Assurance program which meets the specifications outlined in ANSIJNCSL Z540-I, 150 10012, ISO 900 1:2008 and ISO/lEO 17025:2005.

The testing machine was verified in the 'as found' condition. Instron Calpro Version 3.23 The results indicted on this certificate and the following report relate only to the items verifed. If there aremethods or data included that arc not covered by the NVLAP accreditation it wilt he identfifed in the comments. Any limitations of u.e as a result of this verification will be indicated in the comments. This report must nrot be used to chins product endorsement by NVLAP or the United States government. This report shalt not be reproduced, except in lull, without the approval of te issuing laboratory. REDACTED VERSION bb~6.UUUU~S-UbW-UUUlW-UUU rage wu~t or VI 14 Appendix iu: Lalibration Lartiticatma CERTIFICATE OF CALIBRATION NVLAP ACCREDITED CALIBRATION LABORATORY No. 200301-0 CERTIFICATE NUMBER: 340013012113643 Page 3 of 3 pages Indicator

1. -Digital Readout (strain)Range Run 1 Indicated (strai)Applied (in) I RunZ2 Indicated (st-ain)Applied (in)100% Range (Full Scale:l1.00016 in)Rim Temperature:

70.0 °F 40 J 0.19991 0.400580 701 0.34995 0.700010 100J 0.49985 1.000162 Run Temperature: 70.1 0 F 0.1995 0.400013 0.349987 0.700023 0.49899 1.000050 Verification Equipment: Serial Calibration Measurement Make/Model Number Description Agency Range Cal Date Cal Due Extech 445580 1003552 temp. indicator Tektronix NA 12-Feb-il 12-Feb-13 Epsilon 3590VH1R A5010 disp. indicator Instron Ltd 2.00 in 14-Feb-I11 14-Feb-12 (ASTM)* Instron US Gauge Bar 1902 gauge bar £4 Jansson NA 11l-May-10 1 1-May-12* HBM ML38 90630412 force indicator Instron NA 21-Jan-li 21-Jan-13* Epsilon 3590 VHR AS010 (Note: Also used for displacement measurements and listed above.)(ASTM)* Equipment used for gauge length measurements. Verification Equipment Usage: Measurement Serial Range Type Number (% Full Scale) Percent(s) of Range Displacement A5010 (ASTM) 100 0/10120140/70/100 Instron standards are traceable to NIST and/or other National standards. Verified by: Rich Binford Field Service Engineer NOTE: Clause 9 of ASTM E-83 states; It is recommended that extensometer systems be verified annually or more frequently if required. In no case shall the time interval between verifications exceed 18 months (unless an extensometer is being used in a long-time test running beyond the 18 month period). An extensometer system shall not be used after an adjustment or repair that could affect its accuracy without first veritying its accuracy utilizing the procedure described in this practice.instron Caipro Version 3.23 REDACTED VERSION

h~age tbU40oT 11 14Apeix1:ajrtonettcte Appenalx 3.U: Calibration (Jertltlcates INSTR:O:3N.CEAST/ Dynatup I Wilson / WOI.PE1RT itnstron-Service

825 University, Avenue .3-Norwood, MA 02062-2643 Tel" m

Fax

+1-78'1-575-5755 www.lnstron.com Field'Seivice Repor, Company: Address:*Contact;.

Service Order#: Field Engineer.Service Notes: '-550 Stadium Mail Drive Civi RoomG151*West Lafayette,'IN 47907.USA=Brower Kevin-.SV1201120017@§1 TCredit.Card 'Richard Binford :Reference

1. Contract Total Amount:.$2330.

Verified force,displcement~and~the extensometer. Keep aregular check on the pressure transducer oil~capsule

• gap regulatly to' insure the .030" gap for accurate force readings.Labor Activities-01130/2012-120BTEC502040

=0.02 S1400-003-A Zone 3 For Tensile Service 01.121 .120BTEC502040 .1.00 -1460-011-A Crosshead.Displacement Verification 0113012012 1208TECS02040 2.00 S1481-017-C-A ..Force Verification. 68K Ib-300K lb_______ __________ _________ _______ __________Compression ,, 01130/2012 2630-11'5/590 -120BTEC502040 .1.00 .$1490-003-A Strain Verification,. Static Ext or"__________________________ ______ _________Detfectometer Materialsi I I II .0113012012

• Technical Support: Service_Support@Instron.com Email: Serylcereq uests@lnstron.com Page I oilt REDACTED VERSION bbMI-UUU-.5-LdMI-Ub-JUU1U1-UUU 11196 iUb 0? 1114Apnax1:clirtnumrcts Appenalx 1U: Calibration Certificates CERTIFICATE OF CALIBRATION ISSUED BY :INSTRON CALIBRATION LABORATORY DATE OF ISSUE : 30-.Tan-2012 CERTIFICATE NUMBER: 340013012110833 Lab code: 200301-0 Page 1 of 3 INSTRON~Instron 825 University Avenue Norwood, MA 02062-2643 Telephone:

(800) 473- 7838 Fax: (781) 575 -5755 Email: serviceqrequests~instron.com APPROVED SIGNATORY Richard , icar Bi" " i=Narwc°cd, st-MA, au=OVR B Vno rd Customer Requested Due Date: 30-Jan-2013 Type of Calibration: 3D Relevant Standard: astm e2309 Date of Calibration: 30-Jan-2012 9us1m&4Lt,. PURDUE UN~IVERSITY 550 STADIUM MALL DR.WEST LAFAYETITE, IN 47907 I :~.ccw~gE~ 4'- .~ A..Serial No : Make : Model : C502040 BALDWIN 12OBTE P.O. Number : Contact : HARRY TIDRICK 1. Digital Readout (in)This certifies that the displacements verified with machine indicator 1 (listed above) were venifled byr Instron in accordance with ASTM E2309-05 (Follow-the-Displacement Method) and Instron work instruction ICA-8-07.The testing machine was verified on-site at customer location. Adjustments are noted in the comments section of this report with a reference to the "As Found" data.The verification and equipment used conform to a controlled Quality Assurance program which meets the specifications outlined in ANSI/NCSL Z540-1, ISO 10012, 1SO 9001:2000, and ISO/fEC 17025:2005. The Instron measurement equipment used for verification is traceable to NIST.Indicator 1- Digital Readout (in)Verified Range (in)Max Error Max Error (in) (%)Max Repeat Error (in)Max Repeat Error (36)ASTM System Resolution Resolution Lower Limit Class* (in) Class (in)0.2 0.00268 -0.355 0.001 12 0.257 B .001 B 0.2*Sys tern Class is derived from assessment of the following: error, repeatability, resolution, and standard device classification. The results indicated on this certificate and report relate only to the items verified. If there are methods or data included that are not covered by the NYLAP accreditation it will be identified in the comments. Any limitations of use as a result of this verification will be indicated in the comments. This report must not be used to claim product endorsement by NYLAP or the United States government. This report shall not be reproduced, except in full, without the approval of Irnstron.CalproSDS version 3.3 REDACTED VERSION

b-UUU P'age dUb5 07"1114ApndxU:airtoneticae Appendix 1U: Calibration Certlllcates CERTIFICATE OF CALIBRATION ISSUED BY :INSTRON CALIBRATION LABORATORY DATE OF ISSUE : 30-Jan-2012 CERTIFICATE NUMBER: 340013012110833 I IPage 2of 3 Direction of Displacement

Ascending Suggested Run I Runi1 Run 2 Run 2 Run 3 Run 3 Repeat Value IError Error Error Error Error Error Error Uncertainty Coverage (in) I(in) (%) (in) (%) (in) (%) (in) (in)* Factor = k 0.2 0.00007 0.035 -0.00045 -0.222 -0.00026 -0.129 0.00052 0.00081 2.26 0.4 -0.00110 -0.276 -0.00086 -0.213 -0.00091 -0.227 0.00024 0.00070 2.26 0.6 -0.00105 -0.153 -0.00214 -0.355 -0.00176 -0.292 0.00109 0.00150 2.78 0.8 -0.00268 -0.331 -0.00156 -0.189 -0.00162 -0.203 0.00112 0.00165 2.78 1 -0.00168 -0.164 -0.00142 -0.142 -0.00198 -0.196 0.00056 0.00086 2.26*ThW reported expanded uncertainty of measurement is based on a combined uncertainty multipied by a coverage factor k to provide a level of confidence of approximately 95 %.Runs 1 and 2 are performed to comply with the requirements of ASTM E2309, run 3 is performed to calculate the uncertainty of measurement.

Temperature at start of verification

67.9 0 F Run 1 Run 2 Run 3 Suggested Error Value Applied Indicated Class Applied Indicated 0.2 0.19993 0.200 A 0.20245 0.202 0.4 0.39810 0.397 A 0.40286 0.402 0.6 0.68605 0.685 A 0.60314 0.601 0.8 0.80968 0.807 A 0.82356 0.822 1 1.02568 1.024 A 1.00142 1.000 For runs 1 and2.' the worst Resolution Class is B and the worst Repeatability Class isA Temperature at end of verification

70 0 F Error Class Applied Indicated A A A A A 0.20126 0.40091 0.60176 0.79962 1.00798 0.201 0.400 0.600 0.798 1.006 Starting Point of crosshead

0 in Uncertainty of Make/Model Serial No. Description Cal Agency Calibration Resolution Cal Date Due Date Instron LDS-10 06105014 Linear Gage AA .IANSSON EXTECH 445580 1003552 Thermometer TEKTRONIX The standards used for this verification are traceable to NIST..000013 in 1 °F.00001 in 3-Aug-10 3-Aug-12.I°F 12-Feb-Il 12-Feb-13 CalproSDS version 3.3 REDACTED VERSION YiU-uuu-LUb-i-L-UU-uu1 d-UUU Page bUt oT 1114 Appendix 1U: Calibration certiticates CETIIATE OF CALIBRATION ISSUED BY : INSTRON CALIBRATION LABORATORY DATE OF ISSUE : 30-Jan-2012 CERTTFICATE NUMBER: 340013012110833 Page 3 of 3 Verified By: RICHARD BINFORD SNR.SERV.ENGR, CalproSDS version 3.3 REDALTED VERSION

~bbU-UUU-yU3-UbU--UUUltU-UUU Huge 01"1114 Apni U mirto ettcu Appendix 1U: Calibration CeFtltlCates CERTIFICATE OF CALIBRATION ISSUED BY: INSTRON CALIBRATION LABORATORY DATE OF ISSUE: 30-Jan-12 CERTIFICATE NUMBER: 340013012095410 IINF[ tIL_4j InstronLab code: 200301-0 825 University Avenue Page 1 of 4 pages ID "'R O N Norwood, MA 02082-2643 APPROVED SIGNATORY I T R~Telephone: (800) 473-7838 "Digitally signed by Richard EalFax: (781) 575-5750 sevc euss~nto~o ichoa rd ' Binford Emai: sevlceequets~istra~comU~ItI.C ON: cn=Rlchard Binford, Sc=US, I=Norwood, st=MA, Type of Calibration: @ V Date: 2012.01.30 11:08:19 o -05'00'Relevant Standard: ASTM E4-1 0 Date of Calibration: Customer Requested Due Date: 30-Jan-13 Name: PURDUE UNIVERSITY Address: 550 STADIUM MALL DR.WEST LAFAYETrE,IN 47907 KBROWER@PURDUE.EDU P.Ol/Contract No.: Contact: KEVIN BROWER Manufacturer: BALDWIN Manufacturer. BALDWIN Serial Number, 120BTEC502040 Transducer ID: 120BTEC502040 System ID: 120BTEC502040 Capacity: 120000 lbf Range Type: Single Type: Compression

1. Digital Readout -PASSED This certifies that the forces verified with machine indicator(s) (listed above) that passed are WITHIN +t 1 % accuracy, 1 %repeatability, and zero return tolerance.

All machine indicators were verified on-site at customer location by Instron in accordance with ASTM £4.The certification is based on runs 1 and 2 only. A third run is taken to satisfy uncertainty requirements according to ISO 17025 specifications. The verification and equipment used conform to a controlled Quality Assurance program which meets the specifications outlined in ANSIINCSL Z540-1, ISO 10012, ISO 9001:2008 and ISO/IEC 17025:2005. The testing machine was verified in the 'as found' condition with no adjustments carded out.Instroa CalproCR Version 3.23 The results indicated on this certificate and the following report relate only to the items verified. If there are methods or data included that are not covered by the NVLAP accreditation it will be identified in the comments. Any limitations of use as a result of this verification will be indicated in the comments. This report must not be used to claim product endorsement by NVLAP or the United Staten government. Thin report shall not be reproduced, except in fisil, without the approval of the issuing laboratory, REDACTED VERSION b~W5-UUU-I~iWj-tjbU-UUU~I~.UUU wage ~UU 0? VI14 Appendix w: Lalrnration Certaticates I CCIDTEIIP/ATE: ('Al IDDATIfiklI UI U vf I !, %f U VIrlLi.,U~lfall U fI 'I,11 CERTFIFCATE NUMBER: 340013012096410 NVL.AP ACCREDITED CALIBRATION LABORATORY No. 200301-0Pg o ae Temperature at start of verification: 67.00 0 F.Indicator

1. -Digital Readout (ibf)Range ASTM E4 ASTM E4 ASThI E4 Full Scale Tested Force Range Max Max Repeat Zero Resolution Lower Limit (%) (lbf) Mode Error (%) Error (%) Return (lbf) (IbI 100 -1194.4 to -119044.9 C 0.88 0.1I1 Pass 1 200 Temperature at end of verification:

67.80 0 F.-'s A 4'~ .... .... ". ... ...... ....... .' 2', g ' .&; "-COMPRESSION Run 1 Run 2 Run 3 ASTM E4 Relative Uncertainty of Error Error Error Repeat Error U~ncertainty* Measurement* % of Range (%) (%) (%) (%) (%) (+/- lbf)100% Range (Full Scale: -119044.9 INf)1 0.47 0.43 0.43 0.04 0.14 1.661 2 O.41 0.48 0.49 0.07 0.14 3.321 4 0.42 0.46 0.45 0.04 0.13. 6.213 7 0.77 0.76 0.77 0.01 0.14 11.254 10 0.82 0.75 0.76 0.07 0.14 16.908 20 0.88 0.77 0.78 0.11 0.15 36.187 40 0.81 0.81 0.80 0.00 0.14 64.283 70 0.81 0.80 0.81 0.01 0.14 112.494 100 0.80 0.81 0.81 0.01 0.14 160.702* The reported expanded uncertainty is based on a standard uncertairny multiplied by a coverage factor I = 2. providing a level of confidence of approxhnately 95%.COMPRESSION Indicated Applied Indicated Applied Indicated Applied% of Range (lbf) (b) (INb) (ibI (Ibi) (Ib)100% Range (Full Scale: -119044.9 Ibt)0OReturn 1 0 -1 1 -1200 -1194.4 -1200 -1194.9 -1200 -1194.85 2 -2400 -2390.3 -2400 -2388.5 -2400 -2388.2 4 -4800 -4780.1 -4800 -4777.95 -4800 -4778.5 7 -8400 -8335.52 -8400 -8336.7 -8400 -8336.11 10 -12000 -11902.07 -12000 -1191023 -12000 -11909.74 20 -24000 -23789.98 -24000 -23815.94 -24000 -23815.35 40 -48000 -47615.95 -48000 -47615.36 -48000 -47618.9 70 -84000 -83326.29: -84000 -83333.37 .-84000 -83327.47 100 -120000 -119044.89 -120000 -119034.86 -120000 -119034.86 Instran CalproCR Version 3.23 REDACTED VERSION ~bWs-UUU-UU~-U~U-UUU1U-UUU i~age wiU 0? VFI4 Appendix iu: Lallbratlan LartItacates f'lC r'AI IDDATrIflL ',lglx II U[1 Jfl/ I En %I flfl/ I IVI CERTIFICATE NUMBER: 340013012095410 NVLAP ACCREDITED CALIBRATION LABORATORY No. 200301-0 Page 3 of 4 pages The Return to Zero tolerance Is the indicator resolution, 0.1] % of the maximum force verified in the range, or 1 % of the low ast force ver f/led in the range, whichever is greater.100% Range 1.2 Compression 0.8 3 S ,, 0.4 N-t- Runi1 0 -0_____________________ -Run 2-1.00%*IU -0.4 ______________________________ -1.00%**t ASTM E4 Error Tolerance-0.8-1.2 o o o 0 0 .1 7 " Percent of Range Serial Calibration Make/Model Number Description Agency Capacity Cal Date Cal Due Extech 445580 1003552 temp. indicator Tektronix NA 12-Feb-l 1 12-Feb-13 HBM ML38 90630412 force indicator lnstron NA 21-Jan-il 21-Jan-13 Strainsense 050530 050530 load cell Instron 120000 lbf 10-Dec-10 10-Dec-12 HBM IOKFRR 688077 load cell Instron 12000 1Wf 24-Apr-10 24-Apr-12 Range Lower Limit fbr Full Scale Standard Standard Class (%) Serial Number Mode Percent(s) of Range A / Al (lb,1 100 050530 C 7/10/20/40/701100 5000 /5000 100 688077 C 1/2/4 200 /200 Instron standards are traceable to NIST.The standard Class A lower limit is used for systems with on accuracy of +/- 1.0% and the standard Closs A1 lower limit is used for systems with on accuracy of +1- 0.5%Standard forces have been temperature compensated as necessary. Instron CalproCR Version 3.23 REDACTED VERSION

-'age b1i 0i" 1114ApedxU:airaonertcte AppeFidlX 1U: Calibration Certlllcates CERTIFICATE OF CALIBRATION ISSUED BY: INSTRON CALIBRATION LABORATORY DATE OF ISSUE: 12-Apr-12 CERTIFICATE NUMBER: 516041212091759 Lab code: 200301-0 INS---RON 5 Type of Calibration: Relevant Standard: Date of Calibration: Instron 825 University Avenue Norwood, MA 02062-2643 Telephone: (800) 473-7838 Fax: (781) 575-5750 Email: service requests@instron.com Strain ASTM E83-10 12-Apr-12 Page 1 of 3 pages APPROVED SIGNATORY Jimm\ Digitally signed by Jimmy Warner g II I II I I UI N: cn=Jimmy Warner, c=US,/ \l=Norwood, st=MA, ou=OVR?¢ Reason: I attest to the accuracy A I e I and in~tegnty. of this document Vd -[11 [Date: Customer Requested Due Date: 23-Mar-13[Customer 'Name: Address: P.0./Contract No.: Contact: Purdue University 550 Stadium Mall Drive Civil Room G151 West Lafayette IN 47907 sarahh@purdue.edu Kevin Brower 1 Machine Transducer , .Manufacturer: Serial Number: System ID: Range Type: BALDWIN 120BTEC502040 120BTEC502040 Single Manufacturer: Transducer ID: Extensometer Type: Travel (Tension): Gauge Length: Mode: EPSILON 3543-0800-200T-ST/E89895 Type 1 2 in 8 in Static (Tension)Clsification ,-The following indicators of the extensometer system were verified and classed: Indicator Indicator Range Full Scale System Type Description Units (%) Class I. Digital Readout strain 100 B-i Certification Statement All indicators listed above were verified on-site at customer location by Instron in accordance with ASTM E83.S .,4t The verificationi and equipment used conform to a controlled Quality Assurance program which meets the specifications outlined in ANSI/NCSL Z540-l, ISO 10012, ISO 9001:2008 and ISO/IEC 17025:2005. The testing machine was verified in the 'as found' condition. Instron Calpro Version 3.23 The results indicated on this certificate and the following report relate only to the items verified. If there are methods or data included that are not covered by the NVLAP accreditation it will be identified in the comments. Any limitations of use as a result of this verification will he indicated in the comments. This report must not be used to claim product endorsement by NVLAP or the United States government. This report shall not be reproduced, except in full, without the approval of the issuing laboratory. REDACTED VERSION

r-age b512 or 1114 Apni U a~ainCriiae AppencllX 1U: Calibration Certltlcates PI::DTICIP^Ti: t"tl: PAl mL-I I I I r' I I. VI i i!.ii CERTIFICATE NUMBER: 516041212091759 NVLAP ACCREDITED CALIBRATION LABORATORY No. 200301-0 Page 2 of 3 pages[Summary of Results Indicator

1. -Digital Readout (strain)Range ASTM E83 Full Scale Tested Range System Resolution Resolution Lower Limit (%) (in) Mode Class* (strain) Class (in)100 0.2 to 2 Tension B-i 0.00000 1 A 0.0008* System Class for a range is the worst of the following classes: gauge length class, resolution class, individual point error class, repeatability class and is also based on the measurement capability of the laboratory.

[Gauge Length Measurement and Classification] Nominal Actual Error in ASTM E83 Uncertainty of Gauge Length Gauge Length Measurement Gauge Length Gauge Length Measuremnent*(in) (in) Type (%) Class (in)8 7.9897 Direct -0.13 B-i 0.0062* The reported expanded uncertainty is based on a standard uncertainty multiplied by a coverage factor k = 2, providing a level of confidence of approximately 95%.[Data Summary and Classification] Indicator

1. -Digital Readout (strain)Run 1 Error Run 2 Error RepeatI Uncertainty of% of Fixed Relative Fixed Relative Error[ Worst Measurement*

Range (strain) (% of strain) (strain) (% of strain) (strain) j Class (strain)100% Range (Full Scale: 2 in)10 0o00000 0o1 -0o0001 -0037 0.00001 A 0.000025 20 -0.00003 -0.0541 0.00000 -0.0041 0.000031 A 0.000042 40 0.00003 0.0281 0.00003 0.0341 0.000001 A 0.000079 70 0.00001 0.005 0.00005 0.028 0.00004 A 0.000137 100 -0.00016 -0.064 -0.00019 -0.074 0.00003 A 0.000195* The reported expanded uncertainty is based on a standard uncertainty multiplied by a coverage factor k = 2, providing a level of confidence of approximately 95%.[Data Indicator

1. -Digital Readout (strain)Runi 1j Run 2% fIndicated AppliedI Indicated Applied Range (strain) (in) (strain) (in)100% Range (Full Scale: 2 in)Run Temperature:

73.0 0 F Run Temperature: 73.3 0 F 0 0.00000o1 0.000000 0.000006 0.000000 1 0 0.025004 0.200000 0.024998 0.200010 20 0.049975 0.4000 10 0.050004 0.400000 Instron Calpro Version 3.23 REDACTED VERSION bbU;-UUU-Udi3-~LS~--UUU1b-UUU I-'age b1i o1T 1114ApedxU:alrtoneriits Appenalx 1U: L:allDratlon Certltlcates tIEDTIEIIPATI= flE fPAl II:DATIfltM mum--I I I I -1" I I. !.I l.lllIllU I CERTIFICATE NUMBER: 516041212091759 NVLAP ACCREDITED CALIBRATION LABORATORY No. 200301-0Pae3o3pgs [Data Indicator

1. -Digital Readout (strain)% fRuni 1 Apie Run 2%ojIndicated ApidIndicated Applied Range (strain) (in) j(strain) (in)100% Range (Full Scale: 2 in)Run Temperature:

73.0 °F Run Temperature: 73.3 0 F 401 0.100030 0.800010 0.100040 0.800000 701 0.175010 1.400000 0.175060 1.400040 100 0.249840 2.000000 0.249820 2.000000 Verification Equipment adUsage Verification Equipment: Serial Calibration Measurement Make/Model Number Description Agency Range Cal Date Cal Due Extech 445580 984437 temp. indicator Tektronix NA 28-Dec-il 28-Dec-13 Boeckeler Micrometer 20641 disp. indicator A.A. Jansson 2.00 in 07-Oct-il 07-Oct-12 1398 (ASTM)* Fowler Economy SH9J2879982 disp. indicator AA Jansson NA 20-Apr-10 20-Apr-12 Electronic

• Equipment used for gauge length measurements.

Verification Equipment Usage: Measurement Serial Range Type Number (% Full Scale) Percent(s) of Range Displacement 20641 (ASTM) 100 0/10/20/40/70/100 Instron standards are traceable to NIST and/or other National standards. [Comments] none Verified by: James Warner Field Service Engineer NOTE: Clause 9 of ASTM E-83 states; It is recommended that extensometer systems be verified annually or more frequently if required. In no case shall the time interval between verifications exceed 18 months (unless an extensometer is being used in a long-time test running beyond the 18 month period). An extensometer system shall not be used after an adjustment or repair that could affect its accuracy without first verify'ing its accuracy utilizing the procedure described in this practice.Instron Calpro Version 3.23 REDACTED VERSION bYi-UUU-Ubi3-UW(,-UUU1b-UUU h-'age til 4 o011114ApeixU:airaonettcts Appendix "IU: Calibration Cerl:lllcates CALIBRATION CERTIFICATE Address 86 Seabro Avenue Aniltyville, NY 11701 Website www.kessslerusa.com KESSLER THERMOMETER CORPORATION Telephone 631-841-5500 Facsimile 631-841-5553 E-mail KesslerUSA@aol~com CALIBRATION REPORT FOR THERMOMETER THIS REPORT OF CALIBRATION SHALL DOCUMENT THAT ThE INSTRUMENT DESCRIBED HEREIN WAS EXAMINED AND TESTED IN KESSLER'S CALIBRATION LABORATORY AGAINST NIST TRACEABLE REFERENCE STANDARDS, IN ACCORDANCE TO KESSLER'S PROCEDURE T-2008, WHICH IS BASED ON ASTM E-77-98 (2003) AND NIST PIBLICATION 250-23. THIS CALIBRATION MEETS THE REQUIREMENTS OF ISOIIEC 17025, ANSI/NCLS Z2540-1 -1 994 AND THE ISO 9000 AND QS 9000 SERIES OF QUALITY STANDARDS. CUSTOMER INFORMATION: GILSON COMPANY, INC..Purchase Order Number: P000096475 Date Calibrated: September 20, 2011 INSTRUMENT DESCRIPTION: Next Recommended Due Date: October 20, 2012 Serial No.: 689373 Scale Range: 30/124°F Marked: KESSLER USA Divisions: 0.2°F Catalog No.: 6340-FC Immersion: 3" RESULTS OF PHYSICAL EXAMINATION: ......This instrument was examined under a polarized lens and strains in the glass, if any, were juidged to be minimal and of no detriment to the function of the instrument. The capillary was examined under magnification and no irregularities or foreign material was.discovered. It was determined that this instruent was suitable for calibration. RESULTS OF CALIBRATION: TEST TEMP 32.00 60.00 80.00 100.00 120.00 READING 32.04 60.00 80.20 100.20 120.20 CORRECTION -0.04 0.00-0.20-0.20-0.20 UNCERTAINTY +/-0.06+/-0.06+/-0.06+/-0.06+/-0.06* The above readings were made under magnification and resolved to one tenth of one scale division.* The indications of this instrument cannot be adjusted or modified by ordinary means: accordingly, the readings given in the table above should be considered, in effect to be both "As Found" and "As Left" rfeadings* Laboratory Environment Conditions: Temperature: 25°C +/-+ 5 0 C / Relative Humidity: Between 40% and 60%* All temperatures given in this report are based on the International Scale of 1990 (ITS-90)TRACEABILITY INFORMATION: NIST Primary Standard: Rosemount Model 162CE Serial No. 5058 Transfer Standard: Hart Scientific 1502A Serial No. A 14422 / 547027 Approved By: John Lewis Calibration Performed By: Barbara Plaza Calibration Report Prepared By: RP Report No.: 092011-03 1 REDACTED VERSION

i-'age bib ot 1114ApeixU:alraonettcte Appendix 1U: Calibration (.:ertlllcates CALIBRATION REPORT PI TAPE[Report Number: I02221223040412 Date Issued:] Apr-04-12 Pi Tape Corporation Serial Number: 02221223 Tape Size: 2" -12" 0.0.Actual Findings and Procedure Numbers Tape Reads 4.9000 Over 4.9000" IProcedure 1 Remarks: New Gage Calibration Equipment Used S Gage I Serial Number I Test Date I Due Date I NIST Traceable Report Number 4.9" 102098 *May-12-I1 May-12-12 86903-1 This tape has been checked at one or more points over a calibrated measuring standard. Calibration performed in accordance with ANSI/NCSL Z540-1-1 994, ISO/IEC 17025 and the former MIL-STD 45662A.All standards are traceable to the National Institute of Standards and Technology Jerry Mathis, Quality Assurance Manager This calibration report shall not be reproduced, except in full, without the written approval of the issuing laboratory. Results listed relate only to the item beIng calibrated. Pi Tape Corporation 344 N. Vinewood St. Escondido, CA 92029 USA Phone (760) 746-9830 Fax (760) 746-9196 www.pitape.com Page 1 of 1 REDACTED VERSION

Jl-'age btl 0? A 1 1 4 CERTIFICA T D'ETALONNAGE KALIBRIER-ZERTIFIKA T CALIBRATION CERTIFICATE ~\ 2 N 0 26594 Date Datum Date 13.10.2009 Objet Gegenstand Object Type Typ Model Num6ro de s~rie Serien-Nummer Serial number Instrument vertical Vertikal-Messgerait Vertical instrument V1004+10473 /A Date d'dmission du certificat Ausgabedatum des Zertifikates Certificate issue date 13.10.2009 Ddclaration de confirmit6 L'instrument de mesure auquel se r~f~re ce certificat a et6 conformdment aux donnees techniques de TRIMOS contenues dans les documents de vente (prospectus, manuels d'utilisation). Ko nformititserkliirung Das Messgerat;,auf weiches sich dieses Zertifikat bezieht, wurde entsprechend den von TRIMOS in den Verkaufs-unterlagen (Prospekte, Gebrauchsanleitung) angegebenen technischen Daten hergestellt. Conformity declaration The measuring instrument to which this certificate refers to has been manufactured in acordance with the given TRIMOS specifications stated in sale documents (leaflets, instructions for use).Responsable departement qualit6: Leiter der Qualitatsabteilung: Manager of quality department: Gilbert Villard Contr61eur: Pn~ifer: Inspector: Philippe Desponds La publication ou Ia reproduction de ce document n'est autorls~e que dans sa forme Der Inhalt dieses Dakumentes darf nur in voltstindiger Form ver~ffentlicht oder weitergegeben werden.This document may not be published or forwarded other than in its entire form.Page Seite Page 118 I TRIMOS SA S++41 21 633 01 01 Av. de Longema lie 5 CH-1 020 Ren ens S++41 21 633 01 Switzerland htto://www.trimos.ch mtitiUUU-ubJ-u._i-UUU1 b-UUU l-h'age till ot )l 14 I CERTIFICA T D'ETALONNAGE KALIBRIER-ZERTIFIKA T CALIBRATION CERTIFICATE R MO~I N 26594 Date Datum Date 13.10.2009 Caract6ristique do r'objet mesur6 Merkmale des Gegenstander der Kalibrierung Features of the calibrated object Nornbre d'axes de mesures Anzahl der Messachsen Number of measuring axis 1 Etendue de mesure Messbereich Measuring range 0 -990 mm 0- ?~ci7~A(Coefficient de dilatation lin~aire Linearer Ausdehnu ngskoeffizient Linear expansion coefficient Etalonnage Kalibrierung Calibration Accessoire(s) utilis6(s) Verwendete Zubehore Used accessories Pas de mesure Messstufen Measuring steps Nombre de serie de mesures Anzahl von Messreihen Number of measurement series 11.5 V-1 20 mm t '-3 Principe de mesure Messprinzip Principle of measurement Condition de Referenzbedingungen Reference conditions En montant Antastung aufw~rts Upwards direction Temperatures / Temperatur / Temperature Humiditd relative / Relative Luftfeuchtigkeit / Relativ humidity Pression d'air / Luftdruck / Air pressure La publication ou la reproduction de co document n'est autoris~e que dans sa forina int6grale. Der Inhalt dieses Dokumentes daif nut in volistindiger Form ver(Tffeantliclht oder weitergageben wardenl.This document may not be published or forwarded other than in its entire form.20°C +/- 0.5°C 50% +/- 5%722 mm Hg Page Seite Page 2/8 I TRIMOS SA S++41 21 6330101O Av. de Longemalle 5 CH-1 020 Renens S++41 21 633 01 Switzerland! httD:llwww.trimos.ch I ti~-U-G~-U~5UURt-UU4M-'g bt i CERTIFICA T D'ETALONNAGE KALIBRIER-ZERTIFIKA T CALIBRATION CERTIFICATE N° 26594 Date Datum Date 13.10.2009 Etalon do rMf~rence et traa~bilit6 Bezugsnormal und R(Jckverfolgbarkeit Reference standard and tracability Los r~sultats de mesure contenus dans ce certificat se r~fdrent, par une tra~abilit6 documentf~e, aux dtalons reconnus sur le plan national et dont Ia conformit6 avec le syst~me international d'unit6 (SI) est ddmontrde. L'4talon do rf6frence est composd des dl~ments suivants:* Die in diesem Kalibrierzertifikat erhaltenen Ergebnisse von Messungen sind Bezugs-normale bsw. Einrichtungen auf national Normale rickverfolgbar. Deren Uboreinstimmung ist durch das Internationale Einheitensystem (SI) nachgew~iesen. Das Bezugsnormal besteht aus folgenden Elementen: All measurement results contained in this calibration certificat~e maintain a link, of tracability recognized by national standards. -Teir accordarl( with the international system (SI) is proved. The referonce standard is composed~of the fo/llowing cmp~nents: !Etalon do reference Bezugsnormal Reference standard N° des~re Serien-Nr. Serial no.N" du certi6fiat Zertifikat-Nr. Certificate no.Etalonn6 par Kalibriert durch Calibrated by Chock-Master 800002 81228 Fabricant Equerre 215-904 E310Z106 Kunz SCS Marbre 2000x1800 1644 R402B028 Kunz SCS* Mdtrologie et accre.ditation suisse La publication ou la reproduction de co document n'est quo dans sa forme int~grale. Der Inhalt dieses Dokumentes dart nut in vonlstindiger Form ver~ffentlicht odor weitergegeben werden.This document may not be published or forwarded other than in its entire form.Page Seite Page 3/8 I TRIMOS SA S++41 21 633 01 01 Av. de Longemalle 5 CH-1 020 Renens tt++4! 21 g33 01 0 Switzerland httD://www~trimns.ch ~1-UUU-U-ti~¶i-UUUTh-UUU ~ age tilti O]114 R MOS CER TIFICA T D'ETAL ONNA GE KALIBRIER-ZERTIFIKA T CALIBRA TION CERTIFICATE N 0 26594 Date Datum Date 13.10. 2009 Justesse Richtigkeit Freedom from bias* S~iel* S&1e2 AS&Srie3 I Valeur reelle Wahrer Wert True value mm 0.0000 9.9999 30.0003 50.0004 70.0007 90.0007 110.001 130.0009 150.0009 170.0009 190.0009 S6rle 1 Serie I Series 1 mm 0.000 10.000 30.000 50.000 70.000 90.001 110.001 130.001 150.000 170.000 189.999 S6rie 2 S6rie 3 Serie 2 Sele 3 Series 2 Series 3 mm mm Moyenne Ecart moyen Mittenwert Mittenabweichung Average Average deviation mm n 0.000 10.000 30.000 49.999 70.000 90,001 110.001 130,001 150.000 170.000 189.999 0.000 10.000 30.000 49.999 70.000 90.000 110.001 130.001 150.000 170.000 189.999 0.000 10,000 30. 000 49.999 70.000 90,001 110.001 130.001 150.000 170.000 189.999 0.0 0.1-0.3-1.1-0.7 0.0 0.0 0.1-0.9-0.9-1.9 La publication ou la reproduction de ce document n~est autodts~e que cdans sa forme int~grale. Der' Inhalt dieses Dokumentes dadt nur in vollstindiger Form Vert~ffentlicht oder weltergegeben werden.This document may not be published or forwarded other than in its entire form.Page Seite Page 418 I TRIMOS SA Av.de Longemalle 5 EATD CH-1020 Renens+ +41 21 633 01 01 -+-41 21 633 01 @trimosD h Switzerland htto;//www.trimos.ch

b-UUU tZU at 1 14 CERTIFICA T D'ETALONNAGE KALIBRIER-ZERTIFIKA T CALIBRATION CERTIFICATE N° 26594 Date Datum Date 13.10.2009 Valeur vraie Wahrer Wert True value mm 210.0009 230.001 250.001 270.001 290.0009 310.0009 330.0007 350.0006 370.0006 390.0006 410.0006 430.0006 450.0004 470.0006 490.0003 510.0004 530.0002 550.0002 570.0001 590.0001 610 630 650 670.0001 689.9999 709.9999 729.9997 749.9997 769.9998 789.9998 809.9997 829.9998 849.9997 869.9996 889.9996 909.9998 929.9997 949.9996 969.9995 989.9996 S6rle 1 Serie 1 Series 1 mm 209.999 230,000 249.999 269.998 289. 998 309.999 329.999 349.998 369.998 389.999 409.998 42.9988 449.998 469.998 489.998 509.998 529.997 549.998 589.998 609.997 629.998 649.997 669.998 689.997 709.998 729.997 749.998 769.997 789.997 809.997 829.997 849.997 869.998 889.997 909.997 929.997 949.997 969.997 989.997 S6rle 2 Serie 2 Series 2 mm 209.999 230.000 249.999 269.998 289.998 309.999 329.998 349.998 369.998 389.999 429.998.449.998 S469.998 S489.998 529.997 .569.997-589.998629.998 649.997 669.998 689.997 709.998 729.997 749.998 769.997 789.997 809.997 829.997 849.997 869.998 889.997 909. 997 929.997 949.997 969.997 989.997 S6rie 3 Moyenne Ecart moyen Serie 3 Mittenwert Mlttenabweichung Series 3 Average Average deviation mm mm p 209.999 230.000 249.999 269.998 289.998 309.998 329. 998 349.998 369.998 389.998 409.998 429.998-449.998 469.998!489.998 S52 9.998 S549.998 569.997 589.998.609.997 629.998 649.997 669.998 689.997 709.998 729.997 749.998 769.997 789.997 809.997 829.997 849.997 869.998 889.997 909.997 929.997 949.996 969.997 989.996 209.999 230.000 249.999 269.998 289.998 309.999 329.998 349. 998 369.998 389.999 i409.998 429.998'469.998 S489.998 1 509.99829.997997 , 5!89.998 629.998 649,997 669.998 689.997 709.998 729.997 749.998 769. 997 789.997 809.997 829.997 849.997 869.998 889.997 909.997 929.997 949.997 969.997 989.997 Page Seite Page-1.90-1.00-2.00-3.00-2.90-2.23-2.37-2.60-2.60-1.93-2.60-2.60-2.40-2.60-2.30-2.40-2.87-2.20-3.10-2.10-3.00-2.00-3.00-2.10-2.90-1.90-2.70-1.70-2.80-2.80-2.70-2.80-2.70-1.60-2.60-2.80-2.70-2.93-2.50-2.93 5/8 La publication ou la reproduction de ce document n'est que dlans sa forme int~grale. Der Inhalt dieses Dowumentes dadf nur in vollstindiger Form ver6ffentlicht oder weitergegeben werden.This document may nat be published or forwarded other than in its entire form.I TRIMOS SA Av. de Longemalle 5 CH-1 020 Renens S++41 21 633 01 01 ++41 21 633 01 oFEDACTED VElf~Itrimos,¢h Switzerland httD://www.trimos.ch )agebLz]ot 1114 CERTIFICA T D'ETALONNAGE KALIBRIER-ZER TIFIKA T CAL.IBRATION CERTIFICA TE fRtMOS N° 26594 Date Datum Date 13.10.2.009 R6sultas do mesure Messergebnlsse Measurement results Erreur maximale autorisee Max. Fehlergrenze Maximum permissible error Erreur maximale Gr~sste gemessene Abweichung Maximum error measured 5.8 ptm 3.2 p.rm Fid~Iite Wiederholpraizision Repeatability +/- 2s <2 ji Incertitude do mesure ',. Messunsicherheit

• i ..Uncertainty of measurement L'iceritue d meure"U"indiqu~e pouir la determination erreurs de mesures englobe: l'objet r'~talon de r&f&ence, l'0tendue de mesure et les conditions de r~f~rence.

Die nachstehend angegebene Messunsicherheit "U" fi~ir die Ermittlung der Messabweichungen umfasst folgende Komponente: das kalibrierte Objekt, das Bezugsnormal, den Messbereich und die Referenzbedingungen. The uncertainty of measurement "U" for the determination of the errors of measurement given hereafter includes the calibrated object, the reference standard, the measuring range and the reference conditions. le niveau de confiance est de 95%Das Vertrauensniveau betr~igt 95%Confidence probability is 95%Incertitude de mesure Messunsicherheit Uncertainty of measurement K =2 U 95 = 2.5 jm + (L(mm) / 300 )La publication ou la reproduction do co document n'est autodis~e quo dans so fornme int~grale. Der Inholt dieses Dokumentes dadt nur in volistindiger Form verbffentllcht odor weitergegeben worden.This document may not be published or forwarded other than in its entire form.Page Seite Page 6/8 I TRIMOS SA S++41 21 6330101O Av. de Longemalle 5 CH-1 020 Renens& ++41 21 6330 OlO[EDACTED VEfl~~trimos.ch Switzerland htto:I/www.trimos.ch

b-UUU t-'age t>LZ ot 114 CERTIFICA T D'ETALONNAGE KALIBRIER-ZERTIFIKA T CALIBRA TiON CERTIFICATE R!I N 0 26594 Date Datum Date 13.10.2009 C6ntrole de la perpendicularite ( direction de mesure )Kontrolle der Rechtwinkligkeit ( Messrichtung )Checking of the squareness ( measuring direction )10.0 I I t I-2 ~Q~04Q~__600 700 800 90010-10 Hauteur Hohe Height mm 0 50 100 150 200 250 300 350 400 450 500 Ecart Abweichung Deviation 0.0-1.0-2.0-2.0-2.0-2.0-3.0-3.0-2.0-2.0-4.0 La publication ou Ia reproduction de ce document n'est autorisie que dans sa forme Der Inhalt dieses Dokumentes dalrf flur in vo~llstindiger Form ver~ffentlicht oder weitergegeben werden.This document may not be published or forwarded other thian in its entire form.Page Seite Page 7/8 I TRIMOS SA S++41 21 63301 01 Av. de Longemalle 5 CH-1 020 Renens S++41 21 633 01 0 VE~!tI!;rimos~ch Switzerland http://www.trimos.ch I-age tiuj or CER TIFICA T D 'ETAL ONNA GE KALIBRIER-ZERTIFIKA T CALIBRATION CERTIFICA TE N 0 26594 Date Datum Date 13.10.2009 Hauteur Hohe Height mm 550 600 650 700 750 800 850 900 950 1000 Ecart Abweichung Deviation-4.0-4.0-4.0-6.0-6.0-6.0-8.0-8.0-8.0-8.0 Resultats du contr~le do la perpsndicularit6 ( dane s !direton de mes.* ) : Ergebnisse der Rechtwinkllgkeltprflfung (in MessuiChtun~g)

Resulits of squareness In

....Erreur maximale autoris~e

-Max. angegebene Fehlergrenze

Maximum permissible error -Erreur de la perpendicularit6 mesur~e Gemessene Rechtwinkl igkeitsa bweichung Squareness error measured 12.0 j!tm 8.0 j~m La publication ou la reproduction de ce document n'est autoris~e que dans sa forrme int~graie.

Der inhalt dieses Dokumentes darf nur in volistindiger Form verbffentlicht oder weitergegeben werden.This document may not be published or forwarded other than in its entire form.Page Seite Page 818 I TRIMOS SA S++41 21 633 01 01 Av. de Longemalle 5 CH-1 020 Renens S++41 21 6;33 01 Switzerland htto://www.trimos.chI -tM UU(b3- -UUU I-age b24 Or 1114 AppendllX 1U: Calloratlon Lertmtcates TROEMNER Henry Troemner LLC C libration Certificate 201 Wolf Drive o P.O. Box 870 T"horofare, NJ 08086-0087 oPhone: 856-686-160Q o F~x: 856-686-1601 o www.troemner.com o e-mail: troemner@troemner.com Page 1 of 7 Pages Weight SECTION 1: NAME AND ADDRESS OF CUSTOMER End user Purdue University 1040 S. River Road Bowen Laboratory West Lafayette IN 47907 SECTION 2: APPROVED SIGNATORY Manager SECTION 3: PERSON PERFORMING WORK Daniel Foglio SECTION 4: CERTIFICATE INFORMATION Certificate Number 663 364-1 Date of Calibration 30-APR-2012 Client Precision Weighing Balances 30 South Cross Road Bradford MA 01835-8232 Description of Masses: Grip Handle, Accuracy Class

• NIST 105-1 Class F Date Received Order Number : 100001369

"'Date of Calibration Construction

• Two Piece N, Date of Issue Material
• Cast Iron N5 'Weight Range SECTION 5: ENVIRONMENTAL CONDI'TIONS TEST: 30-APR-20 12: 30-APR-2012
• 30-APR-20 12: 1001b Temperature:

21 .84 0 C Pressure: 769.06 mm Pig--, Relative Humidity: 48%SECTION 6: PERTINENT INFORMATION The Weights listed on this .calibration report have been compared to reference mass standards that are directly traceable to the National Institute of Standards and Technology under Test No. 822-275872-il. Reference standards and balances used to perform the calibration are listed in Section 10.* The weights calibrated for this report have been calibrated in accordance with Troemner's ca~libration process. The calibration performed meets Level III criteria as described in the NIST/NVLAP Technical Guide 150-2.This calibration also meets specifications as outlined in ISO 9001, iSO/IEC 17025, ANSI/NCSL Z540-1-1994, NRC Document 10CFR50 Appendix B, and applicable documents. This certificate of calibration shall not be reproduced except in full, without the written approval of Troemner, LLC. This certificate of'calibration must not be used by the customer to claim product endorsement by NIST, NVLAP or any agency of the U.S. government." ."-,REDACTED VERSION -. u cjL b-uuu -age ot 11 14 Appendix 1U: Lalibratlon (ertificates LKROEMNER Henry Troemner LLC Calibratdon Certific te 201 Wolf Drive =P.O. Box 87

• Thorofare, NJ 08086-0087 o Phone: 856-686-1600 oFax: 856-686-1601 o www.troemner.com o e-mail: troemner@troemner.com Page 2 of 7 Pages Weight*NAME AND ADDRESS OF CUSTOMER End user Purdue University 1040 S. River Road Bowen Laboratory West Lafayette

[N 47907 Certificate Number 663364-1 Date of Calibration 30-APR-20 12 Client Precision Weighing Balances 30 South Cross Road Bradford MA 01835-8232 SECTION 7: TRUE MASS (MASS IN VACUUM) CALIBRATION DATA Nominal Mass Value.Serial Number Density'of Weight Uncertainty (+ or-)True Mass 100 ib 45362.709 g 7.2000 g/cm 3 450 mg y N I Density is assumed unless otherwise stated REDACTED VERSION UU (, -bIUUUllb-uuu Page bJ~b ot 1114 Appendix 1u: Calibratlon LSertmcates TROEMNER Henry Troemner LLC Calibration Certificate 201 Wolf Drive °P.O. Box 870o Thorofare, NJ 08086-0087 o Phone: 856-686-1600 o Fax: 856-686-1601,o www.troemner.com o e-mail: troemner@troemner.com Page 3 of 7 Pages Weight NAME AND ADDRESS OF CUSTOMER End user Purdue University 1040 S. River Road Bowen Laboratory West Lafayette IN 47907 Certificate Number 663364-1 Date of Calibration 30-APR.2012 Client Precision Weighing Balances 30 South Cross Road Bradford MA 01835-8232 SECTION 8: MASS IN AIR CALIBRATION VALUE VS, REFERENCE DENSITY 8000 kg m-Nominal Mass Value Serial Number Conventional Mass Value 45361. 953 g Uncertainty (+or-)Tolerance (+ or-)4. 5000 g 100 lb 450 mg\REDACTED VERSION -J L-L-UUUllb-UUU I-'age or 1114 Appendix 1U: CSalibration C:ertitcates LKROEMNER Henry Troemner LLC Calibration Certificate 201 Wolf Drive oP.O. Box 87 oThorofare, NJ 08086-0087 oPhone: 856-686-1600

• Fax: 856-686-1601.

www.troemner.com o e-mail: troemner@troemner.com Page 4 of 7 Pages Weight NAME AND ADDRESS OF CUSTOMER End user Purdue University 1040 S. River Road Bowen Laboratory West Lafayette IN 47907 Certificate Number 663364-1 Date of Calibration 30-APR-2012 Client Precision Weighing Balances 30 South Cross Road Bradford MA 01835-8232 SECTION 9: MASS IN AIR CALIBRATION DATA VS. REFERENCE DENSITY 8000 kg m-Nominal Mass Value Serial Number Conventional Mass Correction Uncertainty (+ or-)450 mg Tolerance (+ or-)4. 5000 g i00 lb 2716 mg N Ad REDACTED VERSION Y -UUU -. I-'age b2z5 Ot 11 14 Appendix 1U: (Jalibration C~ertmtcates IROEMNER Henry, Troemner LLC Calibratdon Certiflcate 201 Wolf Drive o P.O. Box 870o Thorofare, NJ 08086-00870o Phone: 856-686-1600 o Fax: 866-686-1601 ° www.troemner.como e-mail: troemner@troemner.com Page 5 of 7 Pages Weight NAME AND ADDRESS OF CUSTOMER End user Purdue University 1040 S. River Road Bowen Laboratory West Lafayette IN 47907 Certificate Number 6633 64-1 Date of Calibration 30-APR-20 12 Client Precision Weighing Balances 30 South Cross Road Bradford MA 01835-8232 SECTION 10: CALIBRATION PROCEDURE DATA Nominal Mass Value Serial Number Standard Cal Set No. Due Balance Used Cal Due Procedure Used 100 lb Sl104 05/31/12 XP64003L-A01 11/30/12 Multi A-B A 1 .'1 REDACTED VERSION

I-'age rdZ90t q 114 Appendix 1U: Calibration Certltlcates L<TROEMNER Henry Troemner LLC CalibratinCriia e~lboOO3 201 Wolf Drive

• P.O Box 870 Thorafare, NJ 08086-0087
• Phone: 856-686-1600 o Fax: 856-686-1601
• wvww.troernne~corn o e-nail: troemner@troernner corn Page 6 of 7 Pages Weight Certificate Number 663364-1 NAME AND ADDRESS OF CUSTOMER Date Of Calibration 30-APR-2012 End user Client Purdue University Precision Weighing Balances 1040 S. River Road 30 South Cross Road Bowen Laboratory Bradford MA 01835-8232 West Lafayette IN 47907 SECTION 11: GENERAL INFORMATION This calibration was performed in Troemner's High Precision Level I Mass Metrology Laboratory at 201 Wolf Drive, Thorofare, New Jersey 08086 unless otherwise noted on page one. The internal procedures used are CAL-CLASSI and NIST HB 145.SECTION 12: DEFINITIONS AND TERMS MASS IN A VACUUM -The mass of a weight as if it were measured in a vacuum. Also known as True Mass.MASS IN AIR -The conventional value of the result of weighing in air, in accordance to International Recommendation OIML D 28. For a weight taken at 200 C, the conventional mass is the mass of a reference weight of a density of 8003 kg~m" 3 which it balances in air of a density of 1.2 kg~m-3.AS FOUND MASS IN A VACUUM -The ~easured value of the mass(es) as they were receivdbrrenr AS LEFT MASS In A VACUUM -The value of the mass(es) after-they were adjusted,:repaird-

.or replaced when necessary. The As Found\"Mass in a Vacuum willequal the As Left Mass in a ,--;::,;, if the mass(es) did not require adjustm.ent, or replacement. -.:. .--.NOMINAL MASS -The mass value-isg marked on the w ight."...'....." CORRECTION -The difference between the mass value of a we~ight..and its nominal value. A positive correction indicates that the mass value is greater than the nominal value by the amount of the correction. AS FOUND CONVENTIONAL MASS CORRECTION -The conventional correction of the result, as it received by Troemner, of weighing in air in accordance to International Recommendation D 28. ForI a weight taken at 20° C, the conventional mass is the mass of a reference weight of density 8000 kg.m 3*. which it balances in air density of 1.2 kg'm -3 If the customer requires cleaning prior to clibration,; the after cleaning correction would be reported. AS LEFT CONVENTIONAL MASS CORRECTION -The conventional correction of the result, after moent repair, or replacement of weighing in air in accordance to International RecommendationiD 28.g a weight taken at 200 C, the conventional mass is the mass of a reference weight of density 8000 3 which it balances in air density of 1.2 kg~m 3.The As Found will equal the As Left Conventional Mass Correction if the mass(es) did not require adjustment, repair or replacement.(continued on next page)REDACTED VERSION Y-UUU ci-Uuu UUl -'U age ot 1114 Appencdlx 1u: Calibration Certitcates TROEMNER 7 Henry Troemner LLC I;201 Wolf Drive oP.O. Box 87 o Thorofare, NJ 08086-0087 ° Phone: 856-686-1600,a Fax: 856-686-1601

• www.troemner.com, e-mail: troemner@troemner.com Page 7 of 7 Pages Weight Certificate Number 663364-1 NAME AND ADDRESS OF CUSTOMER Date of Calibration 30-APR-2012 End user Client Purdue University Precision Weighing Balances 1040 S. River Road 30 South Cross Road Bowen Laboratory Bradford MA 01835-8232 West Lafayette IN 47907 SECTION 12: DEFINITIONS AND TERMS (continued)

UNCERTAINTIY -The standard deviation associated with the result of the measurement that characterizes the dispersion of the values that could reasonably be attributed to the measurand. The uncertainty is calculated in accordance with NIST TechNote 1297 / UKAS M3003 using a coverage factor of k = 2 (k= 2 defines an interval having a level of confidence of approximately 95 percent). The uncertainty does not include possible effects of magnetism. -Defines the limits in which the correction value and the uncertainty must fall to meet the tolerance specification for the given Class.AS FOUND CONVENTIONAL MASS VALUE -The measured value of the mass(es) as they were received by Troemner, of weighing in air in acc¢ordance to International Recommendation OIML D 28. For a weight taken at 200 C, the conventional mass is the \'nqass of a reference weight of density 8000 kg~m" 3 which it balances in air density of 1.2 kg~m-3.If the requires cleaning prior to calibration, the after cleaning value would be reported. F denotes Out of Tolerance Weight.AS LEFT CONVENTIONAL MASS VALUE -measured value of the mass(es) after they were adjusted, repaired or replaced when necessaVy-sf air in accordance to International Recommendation OIML D 28. For a weight taken at* the Conv~nftio~nal Mass is the mass of a reference weight of density 8000 kg.m'3 which it balances in air density of 1.2 kgrmn The As Found will equal the As Left Conventional Mass Value if the mass(es) did not require adjt~stmnent, repair or replacement. ASTM E617-97 -Weights meet the tolerance specification for ASTM E617-97. Weights 2kg -I g screened for magnetism using a Gaussmeter. REDACTED VERSION

l-age t531 0! 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix LU: Calibration (Jertificates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue University Sheet Ilof 2 Calibration Instrument Name and S.N.: Instron 1044172 Data Acquisition System: OptroTrack Pro Series 600 Gain: NA Excitation Voltage: NA Channel: NA Sensor: OptroTrack pro Series 600 Sensor S.N.: _________OptroTrack Pro Series 600 Input [in.] Output [in.] Input [in.] Output [in.]0 0 6.5 6.507 0 0 6.5 6.507 1 1.001 _____ __ 4 3.999________ 1 1.001 _____ __ 4 3.999________ 4 3.998 _________1.5 1.499 4 3.997 ________1.5 1.498 6.5 6.502 _________ _ _ _ _ _ _ _ _ __ _ _ _ _ _ _ _ ____ ____6.5 6.502 ________ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ____ ____9 9.007 __ _ _ _ _ _ _ __ _ _ _ _ _ _ __ _ _ _ _ _ _ __ _ _ _ _ _ _9 9.007 ____ ___Operator Sig nature Date Time Chce y intreDt ime~Checked by Signature Date Time Sensitivity Accuracy 1euls0.007 in.REDACTED VERSION bbEJ-UUU-U~tl4-UWI:-UUUIU-UUU P'age b;.t2 oT 1"114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 1U: CaliDration Lertlricates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue Sheet 2 of~Notes: The accuracy of the INSTRON sensor is 0.003 in.REDACTED VERSION Page bi at 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 1U: Calibration Certitcates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue University Sheet I of i.Calibration Instrument Name and SN'.: Data Acquisition System: /\31." t ?CJ 02.3 Gain: I Excitation Voltage: Channel: MVQ " Sensor: PA HJ1G- D-L3M Sensor S.N.: 3IJ100 0 Measurand Voltage Measurand Voltage Measurand Voltage ,4oZU 0.03 ____2____4,553 0°&75 ___________ Operator Si nature Date Time Checked by Signat ure Date Time Checked by Signature Date Time Sensitivity Accuracy Results__ _ _ _ __ _ _ __ _ _o.1 %Notes: REDACTED VERSION

l-UUU I-age ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix LU: Calibration Certificates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue University Sheet Ilof I Calibration Instrument Name and S.N.: 1044-172-Data Acquisition System: -(1 tOQO ?"'I Gain:__________________________ ExcitationVoltage: ___________________________ Channel: l i" Sensor: ?A"2Ot" iJC" Sensor S.N.: _______ 37i~910_______ ______Measurand Voltage Measurand Voltage Measurand Voltage__,____ 1.35 _ _ _ _4. 0/A I Operator 'ignature Date Time Checked by Sig ur Date Time Checked by Signature Date Time Sensitivity Accuracy Results 6, o. °I%Notes: REDACTED VERSION

I-age oT 11 14 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendilx 1u: Lalidration Lertlticates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue University Sheet i of 1 Calibration Instrument Name and S.N.: 1044 I72, Data Acquisition System: I -1000 P&i :) 2$Gain: I Excitation Voltage: -3333 Channel: Hv I -2 Sensor: BA -10 2L°___________ Sensor S.N.: 40 0k8 _______________ Measurand Voltage Measurand Voltage Measurand Voltage6.447 __ _. ____ __ _40,,o0 ______Operator Signature Date Time Checked by SgaueDate Time Checked by Signature Date Time Sensitivity Accuracy ResulIts__,___ ______ 3°/-Notes: REDACTED VERSION

-'age bil ot 1114 Project: Tests to Determine the Behavior of Spliced U11 Bars Appendix iU: C~alo~ratlon L~ertitlcates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue University SheetlIof 1 C)Calibration Instrument Name and S.N.: 1-/i'T1 /,O 4 1Z 04 !4 12-Data Acquisition System: MIJ PC. I 6'2 Gain: "I Excitation Voltage: 3. 3:3 Channel: M J-o"3 Sensor: P)A- IC-___ ___ Sensor S. N.: _ _ __ 400oI09&5_ _ _ __ _ _ _Measurand Voltage Measurand Voltage Measurand Voltage____ ____~4 O2.5 Operator ii~gnature Date Tim e s-.p. -z Checked by Signature Date Time Checked by Signature Date Time Sensitivity Accuracy"Results Notes: REDACTED VERSION

I-'Uage ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 1U: Lalibration Lertiticates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue University Sheet l of 1 i Calibration Instrument Name and S.N.: IIJSTO/') 044172 Data Acquisition System: $ [X 11O00 P;CI Gain: __________________________ Excitation Voltage: 3), 355 Channel: 2 Sensor: RA -__________ Sensor S.N.: ______ 4o010 l 77 ______Measurand Voltage Measurand Voltage Measurand Voltage g4.2 0_ 2~.5qo____ 4.bo7 !o33t _ __ _Operator Si nature Date Time sip,.Checked by Signa lre Date Time Checked by Signature Date Time Sensitivity Accuracy Results 3, Notes: frjZ-o REDACTED VERSION

I-age bad oT 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 1U: Lailibration C~ertlTicates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue University Sheet 1 of 1 0©Calibration Instrument Name and S.N.: '" l0 e..-j H V?':.. -Data Acquisition System: t'JQ-- -S C 4T -1000 ['C-T Gain: .00 Excitation Voltage: !. " .Channel:/" -0 Sensor SN: _ _ _ _ _ _ _ _ _ _ _ _ _Measurand Voltage Measurand Voltage Measurand Voltage.0.02o 153B -0,00600:25.3 -o0,00____0 30.LI -0,0I~~ _____________ Operator S gnature Date Time Checked by igaueDate Time Checked by Signature Date Time Sensitivity Accuracy Results__ _ _ _ _ _ --K// O. 1%Notes: REDACTED VERSION

P'age biU oT "11 14 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix iU: C.alibration C~ertitcates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue University Sheet Ilof 1 Calibration Instrument Name and S.N.: --0!~ /42t Data Acquisition System: PC--,"* Gain: /00 Excitation Voltage: I 0 Channel: --Sensor: ________ Sensor S.N.: H- Measurand Voltage Measurand Voltage Measurand Voltage 0* 0 _ _i5.5 -0~o~bot5 ____ __ _____1Q.5 -0.00605-0-.5 uO, o _ __ __ __ __Operator Sign~tu~re -Date Time Checked by Signature Date Time Checked by Signature Date Time Sensitivity Accu racy Results -2%53K/v O. t%Notes: REDACTED VERSION

I-sage 4Uu oT 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 1U: CaIlibration Lertitlcates Calibration Documentation v.1 (Rev. 04/02/ 2012)Bowen Lab -Purdue University Sheet l of i Calibration Instrument Name and S.N.: 10441 72.Data Acquisition System: ?CI GZS9 Gain: Excitation Voltage: , Channel: M3O Sensor: .LUCAS -2Oo____ ___ ___ Sensor S.N.: __ _ _ __ _ 7250 _______ __ _ _ _ _Measurand Voltage Measurand Voltage Measurand Voltage I.35 -4.272 _________1. 500 -______.oo -o.25 ____ ____ ____2.t533_ ___0, 2-.5 __.__ ___ __Operator ignature Date Time Chckd ._ _ _ _atreDae _m Checked by Signature Date Time Sensitivity Accuracy Results Notes: REDACTED VERSION

I-age b41 ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 1U: Calidration Ldertilicates Calibration Documentation v.1 (Rev. 04/02/ 2012)Bowen Lab -Purdue University Sheet 1 of 1 Calibration Instrument Name and S.N.: 1W04i 72.Data Acquisition System: H" -100O0 Gain: I Excitation Voltage: 3 Channel: frI.3 1 Sensor: LUCA 2o000____________ Sensor S.N.: ________ 7251 _______Measurand Voltage Measurand Voltage Measurand Voltage 0.12Z5 4.1,..0 _ _ _ _ _ _ _ _ _ _ _ _ _ _0.5q7 __ __._ __ _ _ __ _ __ _ _o.}1f o.ozo_____ L.5o0 -2,4.14_____ ________, __ -4..02A5 _ _ _ _ _ _ _ _ _ _ _Operator Signature Date Time ChcedbPDt Tm Checked by Signatu re DaeTime Sensitivity Accuracy*Results Notes: REDACTED VERSION

b-UUU I-age b4z or 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 1U: C:alidration Lertitcates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue Universit' Sheet l of : Calibration Instrument Name and S.N.: ?U! D 10g!4I4'2. Data Acquisition System: MN, Scd.%-I 1000 I1 B Gain: I Excitation Voltage: 5. V Channel: Mt-0(Sensor: 'PA _ _ _ _ _ Sensor S.N.: __ _ _ _ _ _ _ _ _________0 Measurand ,Voltage Measurand Voltage Measurand Voltage 0.5/f o.95 __ _ __ __ __ _ __ _ _ _ _ _ _ I. i _ __-_ __ _ _ _ __ _ _._ _ _ _ _ _ _ _ _Operator Signature Date Time Checked by Signlature Date Time Cekdb .... -Signature Date Time Sensitivity Accuracy Results Notes: ~ u e.o' 4+ .% /D~ vi ~ 4 iw j 2-emx- r s 3 //REDACTED VERSION

b-UUU r-age ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars.Appendix 1U: (Caliaration Lertiticates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue Sheet i of 1 Calibration Instrument Name and S.N.: I N.ST 6-c N 109 4 I Data Acquisition System: KNh $C')(1 1000 ,SN IlI Gain: Excitation Voltage: 3 *3 53 \Sensor: _______ Sensor S.N.: _________ T00L' _______Measurand Voltage Measurand Voltage Measurand Voltage 4.5 ___._ __ __0.5 _____ _____ ____Operator Signature Date Time Checked by Signature Date Time Sensitivity Accu racy Results Notes: ,,4o -o.,°I REDACTED VERSION bbU3-UUU-ULi-(,U-UUU1 b-UUU Page OT 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendlx iu: Callbration (Certltlcates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue Universit'3 Sheet 1 of~Calibration Instrument Name and S.N.: I NJ N 1 0441 ',2_Data Acquisition System: NI[ S-C.) 1 1O0O 0 Gain: Excitation Voltage: Channel: M l- 2.Sensor: P,________ Sensor S.N.: ___0______ 0t Measurand Voltage Measurand Voltage Measurand Voltage 2 .5 (.2IOZ. G______-, I.8? __ _ _ __ _ _ __ _ _-_ _ _(o.5 2. .t__ __ ____ __Operator Signature Date Time Checkd by ignatre Dae Tim Checked by Signature Date Time Sensitivity Accuracy ResulIts Notes: Devickova." 0.2-%REDACTED VERSION bU-UUU-UbJ-UIU-UUU1Ii-UUU l-age b4b ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 1U: Calibration Certlticates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue Universit% Sheet 1 of :1 Calibration Instrument Name and S.N.: I \ , I A41 " TZ Data Acquisition System: 1000 11S86O0]Gain: Excitation Voltage: V Channel: __ _ __ _ __ _ __ _ __ _ __ _ __ _ __ _Sensor: PA -10_____ ____ SensorS.N.: __ __ _ __ _ __ _ __ __ _ __ _ __ _ __ _Measurand Voltage Measurand Voltage Measurand Voltage'I 8 _. _4.5 1.8~5 _ _ _ _ __ _ __ _ _ _ _Operator Signature Date Time Cheke by SignatueDatefTim Checked by Signature 'Date Time Sensitivity Accuracy Results_____________ .o?3. \JJ,/V\ 0.o3 %.'Notes: REDACTED VERSION

Irage b4g Ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 2U: Calibration Certllticates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue Sheet 1lof I Calibration Instrument Name and S.N.: _____ -______________0 __41 __________- Data Acquisition System: -C,)( c000 (IS 6(01 Gain: ___________________________ Excitation Voltage: 3. ; N Channel: t'A2- 0 Sensor: _______ Sensor S.N.: ____OO___O__ 4oo-Measurand Voltage Measurand Voltage Measurand. Voltage c3..54 ___._.__4.5" ' .841_ _ _ _ _S ." __ __Operator Signature Date Time Checed y6SgnaureDat Time__Checked by Signature Date .Time Sensitivity Accu racy Results__ __ __ _ __ __ _o.. o.____ I_ ___ _Notes: REDACTED VERSION bbY3-UUU-L.i-L5-L(-UUUlh-UUU l-'age b4( ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendlx 1Ui: Calibration Certiticates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue University Sheet l of I Calibration Instrument Name and S.N.: I ~\ .STE-o N 1044 [? 'Z Data Acquisition System: .SC X-I I00 t6 Gain: O00 Excitation Voltage: I OV Channel: Sensor: 44 3'_______ Sensor S.N.: 44 ______ ______Measurand Voltage Measurand Voltage Measurand Voltage-04-.1~o=0 0 sk -j-o, -0.002.1i Iok+-t-o4 -o.oo4,o _____I4-.6k--o., -o oo5s _____I9.04+o.1t -o.oo'8- _____ _____a4.ik+/- 04 -o.ooo~sg4 -o.Olla ____ ____ ___Operator Signature Date Time Checked by SDate Time Checked by Signature Date Time Sensitivity Accu racy Results_____________ -I. 5Thv iV/V @FSV o_______Io__ Notes: b'I~o r/ "a 5//a REDACTED VERSION bIUj-UUU-ULSJ-UIU-UUUIh-UUU H'age tbq. 071114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 1U: Calibration Lertinlcates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue Universit% Sheet 1 of I Calibration Instrument Name and S.N.: I N STZ-O A 104 41 ? 2..Data Acquisition System: .Scx 1000 GO7" Gain: 1O00 Excitation Voltage: 1 0 V/Channel: -Sensor: 4~4Z.__ _ _ _ _ _ Sensor S.N.: Measurand Voltage Measurand Voltage Measurand Voltage-o.,4+/-o.4k o~ooool ____ ____ ____4.J 0 5 -jo'I-oR __ __ __ __ _ _ __ _ _ __ _ __ _ _1%.1 k +o.4 -o.oo~ ______ _____04 -oom o_Operator Signature Date Time Checked_____by __ Signa____ure613Dae Time__Checked by Signature Date Time.Sensitivity Accuracy ResulIts Notes: LDev-v, 0,,. .2 REDACTED VERSION Project: Tests to Determine the Behavior of Spliced #11 Bars AppendilX LU: Calioration Certlrlcates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue Universit3 Sheet I of I Calibration .Instrument Name and S.N.: ) NJ ST NJ 104 4 1 : 'Data Acquisition System: NI ,SC)I 1000 Gain: I Excitation Voltage: 3 0 V/Channel: F -Sensor: LUCAS DODT -+-Z.."__ __ _ __ _ Sensor S.N.: JgZ O __ _ __ _ __ _ ___0_ _Measurand Voltage Measurand Voltage Measurand Voltage 1.5 ' -_ .__- _-1 ,,"_ __1 .o o .1 1 2 ._ _ _ _ __-_ _ _0.51 2. 4'_ __ _ _ _ _ __ _ _Operator Signature Date Time Checked_____by _Signature____ Date; '5Time Checked by Signature Date Time Sensitivity Accuracy Results Notes: Dvoiv.j 2 w /I' 4 REDACTED VERSION IibU ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendilx 1u: Lalibration C=ertli"lcates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue Universit% Sheet l of 1 Calibration Instrument Name and S.N.: INilS-T 1044[ Data Acquisition System: N I SX{ 1 I000 II SS 60 l" Gain: I Excitation Voltage: Channel: 1\11-- I Sensor: LUCA.-& bCJT ____ ___ ___ Sensor S.N.: ,__ __-___ ,. .25j __ _ _ _ _ _ _ _ _ _ _ _Measurand Voltage Measurand Voltage Measurand Voltage 0. 4A- . ______1.0" 0,1410 Operator Signature Date Time Checked by Signature Date Time.Checked by Signature Date Time Sensitivity ..Accuracy Results Notes: D v~ i' -REDACTED VERSION bbi-UUU-Ud::J-U.5"U-UUUIIh-UUU t-'age 1bl 1" o 1114ApeixU:alrtonettcte AppencllX 1u: Lallbratlorl Lertltlcates ! :~T I--t I r-r I F F- -- .-5 --REDACTED VERSION FIRST LOADING REDACTED VERSION FIRST LOADING REDACTED VERSION FIRST LOADING GIRDER A6-40 kip REDACTED VERSION RELOADING REDACTED VERSION RELOADING NoIRDEloAd GIRDERA3 (iIKUEK A4 -41 KIp REDACTED VERSION RELOADING GIRDER A5 -42 kip REDACTED VERSION FIRST LOADING REDACTED VERSION FIRST LOADING REDACTED VERSION FIRST LOADING REDACTED VERSION RELOADING No reloadI::Z -Loaa = ib Kip.REDACTED VERSION RELOADING 1 C~IRLThK 133- Load = 3b kip NoIReload4 GIRDER B4 REDACTED VERSION RELOADING GIRDER B5 -24 kio.REDACTED VERSION

• Project:

Tests to Determine the Behavior of Spliced #11 Bars Instrumentation Documentation v.1 (Rev. 04/01/2012) Specimen: A -I Sheet __ __of I Data Acquisition System: Channel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location Comments C) /11-o ( 3.3g3 OA-p-o -.': -Vt:2-zr Mj.o,-L 2.?-z5 I MI-I I " " 3Thoo't~ -6. I7- -l1=.o2 S. " .,S 2 I ', A-IO '-oolc5'r6, 3.'~l-5 !,% N5lc- 0,3l:t-.,2 3 hI-3 I " " 4oioioii 3.i6'=t 'f " b 2--0. I ____1__5 ",:-3! J 0..23 ,5 100 i0 '-,P1O 43 -______ o0,2D'C1 J, -. , /t1 1 oO 10 ___-- __ _.-_-___.__!l< s -_______m r-'v-o 3o 2_0 ooos -0o(30 "I 2'2-1O. o OOO So ." o., oooO Operator Signature Date Time Checked ___by__Signature_ 6 Date Time~'Checked by Signature Date Time Notes: 12-1 REDACTED VERSION v$*0 p~o~1 ~243~4*5 I.-id , .-- I-4 -I 4-U.- ;.---- ; --4----1;----I~--U- ... --U- --I~ -m -U -4 Noth III* qF *f 12 13 1 ! 15'I IF qF I-I '4II- II l --I -I I, I l- U I. --lI 4 4-2@10--20 A @520_ r 4 10Q10:100 r 4 1 4 E_1 _4 5=20_ 1 '21=-0 1 I--!I-.Back 4 Front 45qm Wv .... J ,4 I Specimen A -I LAORTRY Behavior of Lap Splices of No. 11 Reinforcing Bars 12-2 REDACTED VERSION Project: Tests to Determine the Behavior of Spliced #11 Bars Instrumentation Documentation v.1 (Rev. 04/01/2012) Specimen: Sheet I of _____Data Acquisition System:-,.T v Channel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location Comments 0 11I-O 1 3.333 'A-.20 3=,IOo~o -6.197-r -l::.oft ______- _ __ __ _ __ _, _ __ __ _ 3TlOOq -6,16=7- -jI-, I , " ;2 hlI-2 ____ "___ PA-Io ,9OOIOc 3.R-S i.2zr tJ.5Yv4 0.3B%3 14I-3 I r,"'40tolo~'=I O .4&O_____-_ I " ot~f' 3.17-3 O.qIi O,3!!9 frl2-; [6O JO L_.it,.soK ____-__5 0.3DeI -o.ooo'oo 4 10-0Lo 10 _____ L.-t2 -0.L[wJ s. =7- 113-0 ( 3o Lw'c.c 2. -J7-:2SO 0.0OO1 0,013 ht13-I I 30 "___ T+2Sz1 ,.209 -o,0oof $. "-o.5 OprtrSgaueDate Time Checked by ~SignatureDaeTm Checked by Signature Date Time Notes: 12-3 KEILAL I FU VLIOIbUI'J i i f I f , I 6.1 , Ii 9 A 6* qr *

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Specimen: Sheet I of I Data Acquisition System: Channel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location Comments 1 "~ I ___,,__" -&d,1T -_______ S. " ____. ___Z. "2.. I ,, 'A-Io 400 lo~to/ 3, 17. / OITM:-. N.. Spllcee_ 3 " .3 1 " 4o0 lo,)8s'5 / 6 ,7 A oI " __ __ _ -oo -5 / 0,ctI _ ._______ __,_____" 100 to L"o so 4 _______ C0,2 N.E -a -0O~btbf2 SMS-o .I 3ov Luc:8 J125o O..2O.f / ..N.. -.Ofi 8 1- I Sov "____ " J t951 O,20o / 00b0(o ,____,, -_ ,___-Operator Signature ,Date Time Checked by Signa ure \Date Time Checked by Signature Date Time Notes: 12-13 ml 1 39 40414243 44 45 46*A A-I-----4---41-----41-E-41-E-E-IE--lE .., m m -m m m m 1 -u.-------4.a.-~--u.-~-m.-u.~ I -. -m I m m m m m m m m I -i I 449605152 53 54 J/i v w v w v 4? 4849 505f w v 83 5,/North 34 Cl 1-* ! ! m ! m D m m I I ... ... i v ! V W W V= V V W V W I T I 7 zyz I Ia.1 9 55 565b75859690 61 62 ,_ Front-4436 6@10=60 2@10 --20, I- -- I 4@4.75=19 w _ , 4§4.75=19 LABORATORY Specimen -4I.Behavior of Lap Splices of No. 11 Reinforcing Bars 12- 14 REDACTED VERSION 0 Project: Tests to Determine the Behavior of Spliced #11 Bars (Instrumentation Documentation v.1 (Rev. 04/01/2012) Specimen: 6 -2, Sheet I of ..Data Acquisition System: Channel # Gain Excitation V. Sensor S.N. *Sensitivity Zero Offset Location Comments I hi-( I "_____ "5--I~ooq3 3 5,O L , 1 " .- +-iv. 0.352 5 fr-J2 10o _____ filC3 O.[ K] "3 [13-I I %or " -coosS , -O.O2fj Operator Signature Date Time Checked by _~Siapature Date Time Checked by Time Notes: 12-15* REDACTED VERSION 540414243 44 45 48 4 39 4041424344 45 48 A ---+---- 4 -4.L-------1 I U -~-J.I-.--I I *. I -I I-4 U -41 m m m m m m --d 1 ~ ~ aJ-4E -41 m m m m m m m m 4-I II 1~ 1~ 1~Ii P v 47 4849 5061 62 53 54 North 34 Cl.-I--------- I -I 1 I U -U -11 U -~ I -I -i h b -~ I ~ -*. *. *~ *. *. ---L -1r i m!2@10=201 37Ir Back a~~Front-, ,]_6@10=60 _i 2@10 --20, 4@4.75=19 4@4.75=19 12ft71in.LARATORY Behavior of Lap Splices of No. 11 Drawn by: .3P R Checked by: ZAJ/\_U____U"_,_____i___________ Reinforcing Bars Date: 12 -16 REDACTED VERSION Project: Tests to Determine the Behavior of Spliced #11 Bars 0 Instrumentation Documentation v.1 (Rev. 04/01/2012) Specimen: _______Sheet I of I Data Acquisition System: ill ul i Channel # Gain Excitation V. Sensor SN. Sensitivity Zero Offset Location Comments 0/-O tIii, 5533 PA2 Z~lOcsqio -6,yq-3.06 ,/2 t-'1-2 _____ ~ PA-4o ?: $~:7\\ s,,& O.305 3 tlI-3 .I " 9 ,oI0o~i 3,i6 of. H;i O.2-o3,______-0 I 3 , 0:7- S.pt~G. O,23(-/.S It-2 !oo0I e-1 c-1 3 -_____ 0o.3CR EK .£a,&. -- (0 = 10o ___ __ ____- __ --2_ _ o,2_[K7 5, ,~ Th 13-O I 30 2 C)25 __,___ O~ ~ '. , g,-,kp 0,o6- ,/ t1'- I 30o 3%5 o, of -o. oog Operator Signature Date Time Checked by Signature Date Time Checked by Signature Date Time Notes:.12 -17'I REDACTED VERSION U©t p ~!39 40414243 44 4548-F-0--@- + -63541 A A A A A A-I 48 49 50 51 52!fd)w A North 34 62-f---------t----~-------~. .I-I.-~-*--*-------~ fr-il -A. £ £ £

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us ST 585960 61 I_o m 2--- -, Front :*6@1 -0]_ .6@10=60 ::,Q 0--2 , 4@4.75=19 4@4.75=19/ 12 ft71In.LAORA TOR:Y Behavior of Lap Splices of No. 11 Drawn by: 1" Checked by: !....._____U_________R___!___ Reinforcing Bars Date: /Ic/.0 12-18 .(. U Project: Tests to Determine the Behavior of Spliced #11 Bars 0 Instrumentation Documentation v.1 (Rev. 04/01/2012) Specimen: __________________ Sheet I of _____I.Data Acquisition System: Channel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location Corn~ents o /pi-o 1 3.3353 PA.-2.o ---___._- ______2.I./"11 -2I P 1 oo______ 33. I :-6l-5 o.'1-,s G& .-l.2- I0 V'-i '/O~o4 I L O6' ____3 j--tc~'c4 3 ,- 15 ______.. j , -, -oooo~ jo-oJOooLo,4oP13-0 3 O"/ LDT TJ'so ___,____ -o~o05 "jjP.+-.Z~ L~1~o LJT T~-i ____ 0c? ' -o 014 Operator Signature Date Time__._"__.__ ____.__ ._ 3:41CaPM.Checked bySigatr Date Time Checked by Signature Date Time Notes: klI s~lil I/-12-19 KtL-UW.I I-U NJ A 39 40414243 44 kA b'45 46 , .1=.J A 4-ft------f?- U -U -I -. U -~--------~-~-----~ ~ I --+/- -v v w w w .v A w w A--m m m m -~j 7 -53 54 i!I a 48 495051 52 w North 34.-E -. --E,. --,-- I=_.. _,h __ *. *. .* .. .*- A .&1-1 1 S2010--2 1 37 :36-_Front -36Q06 2@10 --201 , 404.75=19 404.75=19 12fl7 in. I LAORTR.Y Behavior of Lap Splices of No.11 Dmwn by: "!I, Checked by:l _P___I____UI ______U__N___l_ Reinforcing Bars Date: 12 12 -20 REDACTED VERSION U Project: Tests to Determine the Behavior of Spliced #11 Bars 0 E-S Instrumentation Documentation v.1 (Rev. 04/01/2012) Specimen: Sheet !of 7 Data Acquisition System: Channel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location Comments 0 fl-c " "~3 .-,)s " .(vef ,:O2//;2pt-z I " Ai-IO 5 /11I-3 I "I 0 +/-,01:L/ 3 /o"WS OQ.LAo 053 /I &ov 2 'o,.oo pJ, s.1,,- -0oo2'3 t3-1I 30""-0-2 2 o..;o1 -FO.:o % 0, r0)OI Operator Signature Date Time s .l? UJOL_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Checked by Signature Date Time Checked by Signature Date Time~Noes ~ ~bj~12 -2.1-REDACTED VERSION 4 39 40 414243"44--m -mF ---t[ I -.- -.S. F 534..L....-I----4 I -4 I -U -4 I -I I- U -II -'-4 I -I I-~ U ---~ I m m m m m-4= -m m m lb j~p jgj9j~5 1 5 2!v v v v v v 47 4849 5051 62 North 34 Cl= = U. .=1-I 55 568 7"65960 61 82 12@Io=2o 37 ;,--36 ,351- Front =: , I=6Q10=60 _,2@10 -20 4@4.75=19 404.75=19 12ft71In.Specimen ~, -5 LABORATORY Behavior of Lap Splices of No.11 Drawn by~ 1@~P~. Checked by: Vy~PURDUE UNIVERSITY ReinforclngBars Date: ~/J6/U~.12 -22 REDACTED VERSION UJ 0 0 Specimen: Sheet 1 of 1-Project: Tests to Determine the Behavior of Spliced #11 Bars Instrumentation Documentation v.1 (Rev. 04/01/2012) Data Acquisition System:[>J Channel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location Comments I. /141-1 I " " B -F?,___ S, k 2 t- MI- I " !A- 10 9/OoOlCIf 3, 1:-5 O,.% 0,27--¥:3 14I-3 I "' " C010c11 "3,Aif _,5___,___po ______q/ I1)-O I ____ " -tooIO~ o -B,7.-3 IS 15 5 s\w _.______5 /12-2 100 boy _o____3 _____ O.Jo_ Ki -______s o ti- oo Io'J "I L/.I2 0.255 .O,2 CKJ <,___-o ___7- 113-b ! 3ov T 0 0.0oo 0.ooo I{ P13-1 30\I " -s .9o0o~o2 &. Operator Signature Date Time Checked by Signature Date Time Checked by Signature Date Time Notes: 12 -23 REDACTED VERSION Norlh 3 ,_ .Front _4@4.75=194(.. 12 ft7 In.I "Specimen g --LABRAOR Behavior of Lap Splices of No. 1:1 P URDUIE VER:S~ITY Reinforcing Bars 12 -24 REDACTED VERSION bbiL-UUU-U83-U.5"U.-UUU1bt-UUU I-'age bb or "1"114ApedX:Apoedls oede Appendtx Approved Iest Procedure 25539-O00-VIS-SY01-00001-003 Page I of 26 BECHTEL POWER CORPORATION SUPPUER DOCUMENT REVIEW Tests to Determine the Behavior CL.ASSIFICAT.ION & STATUS of #11 Bars with Lap Splices ...Bowen Laboratory ¶ El [] Purdue University El[ ,d ' El wodms Spring 2012 2-" *Test Procedure ., , == =1.1 Formwork -,(i The formwork shall be made using non-absorbent plywood. Its interior shall be caulked to prevent water leakage and it shall be covered with a thin layer of oil before casting. The dimensions of the formwork shall be checked and recorded using Form 1.1.2 Reinforcement Cages The steel reinforcement cages shall be built following the drawings attached.Reinforcing bars shall be supported by steel chairs placed away from lap splices. To ensure alignment, the bars shall be tied to chairs and to one another using gage-16 steel wire. The location of the reinforcement shall be recorded using Form 1. The locations of wire ties and rebar markings shall be recorded using Form 2.Tolerances (within the test region) are: 3/16" for horizontal cover and horizontal spacing measured to the surface of the bar (excluding ribs)1/4" for vertical distances shown in Form 1 1.3 Casting Fresh concrete properties to be measured include: Unit Weight Slump Air Content These measurements shall be made following the Specifications and recorded using Form 3.Revision 21 8-1 REDACTED VERSION boYJ-uUU-UdJ-ULUc-Uuu3 b-UUU r'age tbtU 011 114 Appendix 8: Approved lest Procedure 2bbJiY-UUU-ViS-:SYU1-UUUU1-UUit rage z oT Slump shall be measured before any other activity related to casting takes place to make sure that the delivered mix has ,satisfactory workability. The mixing truck shall deliver a ticket with the batched mix weights. These weights shall be examined to corroborate that the delivered mix has the specified proportions. Concrete shall not be accepted if it arrives more than 45 min. after leaving the batching plant. No water shall be added to the mix after the truck leaves the plant.Specimens and cylinders shall be cast and vibrated in two lifts following the Specifications. The vibrators to be used shall have the following cross-sectional dimensions: For cylinders: 3/4" -7/8" For Larger Specimens: 1-3/4" Their frequencies shall be between 50 and 200 Hz.Excess concrete shall be removed off the formwork. The exposed surfaces of the specimens shall be finished using cast magnesium floats. Lifting inserts shall be inserted in the fresh concrete as soon as the finishing is completed. Each test beam shall be cast using concrete from a single mixing truck. A complete set of concrete samples (cylinders) shall be obtained from each truck. Test beams and samples shall be marked with a number referring to the truck from which they were cast and the date of casting. In each casting day, trucks shall be numbered sequentially starting at 1. The number assigned to a truck shall be written clearly on the mix ticket describing the mix proportions for the batch. Test beams shall be cast and tested oriented in the North-South axis of the laboratory. During finishing, the north end of each beam shall be marked with the letter N.These activities shall be documented using Form 3 1.4 C:uring As soon as casting is completed all specimens shall be covered with impermeable sheets. When the concrete surface sets, wet burlap shall be inserted between these sheets and the exposed concrete. All formwork and molds shall be struck no later than three days after the cast.All exposed concrete surfaces shall be covered by wet burlap and impermeable sheets for a total of at least seven days after casting.Burlap shall be doused with water at least every other day during the curing period.Curing activities shall be logged using Form 4.Revision2 2 5-2 REDACTED VERSION

inage bU1 0? 11I 14 A~ppendix s: Approved lest Procedure 2bW3-UUU-V'15-bSYU'1-UUUU'1-UUtS frage it or 2u Test cylinders shall be stored and cured next to the test specimens and under similar conditions of temperature and humidity.The variation of concrete strength with time shall be monitored as specified in the Specifications. The results of cylinder tests shall be recorded using Form 5.2. Calibration Three types of measurements will be made: displacement, force, air content.The apparatuses to be used to calibrate sensors to measure these quantities are: Displacement Sensors: INSTRON Universal Testing Machine (S.N.:)Load Sensors: INSTRON Universal Testing Machine (S.N.:)Air Content: Calibrated Cylinder (S.N.)Load and displacement sensors will be calibrated following steps listed below: 1) Connect the sensor to the data-acquisition system that is going to be used in the test 2) Set and record the excitation voltage to the maximum possible value (not exceeding the maxima specified for the data-acquisition system and the sensor)3) Set the data-acquisition equipment to record voltage 4) Set the gain of the data-acquisition system to the first available level lower than the ratio of the maximum range of the system to the maximum expected output from the sensor.5) Mount the sensor on the universal testing machine 6) Apply a series of known displacement or force increments to the sensor ranging between 10% and 90% of the rated capacity of the sensor 7) Record the voltage read on the data-acquisition system at each known displacement or force increment 8) Create a plot of change in output voltage vs. change in force or displacement

9) Fit a line to the plot from 7) using "least squares" 10) Record the slope of the line from 8) (sensor sensitivity)

11) Label the cable used in the calibration with the serial number of the sensor Sensors shall be calibrated before the first test and after the final test.The apparatus used to measure air content of the fresh concrete shall be calibrated following the procedure described in ASTM standard 231. Form 6B shall be used to document the calibration.

Revision2 3 8-3 REDACTED VERSION bbg:i-UUU-LUdi-ULUL-UUU1 b-UUU i-'age bb2 01"1114. Appendix 8: Approved lest Procedure 2bbtJY-UUU-V1 -UUUU1 -UUi wage 4 07tLti All calibrations shall be performed by at least two persons: one leading each step and the other checking the work of the first independently. A log of each calibration shall be made using Form 6 and it shall include an estimate of the accuracy of the sensor.Sensors for which the sensitivity obtained in 9) above deviates by more than 10%from the nominal sensitivity (as reported by the manufacturer) shall not be used in any of the tests.3. Setup Each test beam shall be placed on two roller supports as described in the attached proposal. The final location of the supports shall be measured (to the nearest 1/16 in.j with maximum deviation of in and reported using Form 7. As-built external dimensions of each test beam shall be recorded using the same form.The maximum deviation from nominal dimensions in the test region shall be 1/4/ in.The test beam shall be placed with the reinforcement facing up as shown in the attached proposal.The shear spans shall be reinforced with external stirrups (pairs of 5/8-in threaded rods) installed at a spacing not exceeding 12 in. The locations of the stirrups shall be measured. The measurements shall be recorded using Form 7.The loading rigs (consisting of a loading tube, two hydraulic rams, two threaded rods, plates and nuts, and one load cell per rig) shall be placed on the test specimen and connected to "the strong floor" of the laboratory (without applying load to the specimen other than the weight of the rigs) as described in the attached proposal.The rams in each rig shall be connected to a single manifold and pump using 10,000-psi hydraulic hoses. All hoses and other hydraulic hardware shall be inspected visually and replaced -if defective-before testing.4. Instrumentation Displacement sensors shall be installed at midspan, at each support, and at each load point. They shall be secured to the strong floor of the laboratory directly below the point where displacement is to be measured.All sensors (displacement and force) shall be connected to the data acquisition system using the same cables used during calibration. The excitation voltage and gain shall also be set to the value used in calibration. The data acquisition system shall be set to record voltage changes caused by loading. Before applying load with the hydraulic rams, all sensors shall be set to read a voltage value between 10% and 90% of the voltage output of the sensor at its rated capacity. These voltages shall be referred to as the "zero offsets" of the sensors. If a sensor is set to have an initial Revision2 4 8-4 REDACTED VERSION

Hage o011114 Appendix 8: Approved lest Procedure 2bb68-UUU-Vl:5-bYU1-UUUU1-UUi Page b ot Zb voltage exceeding 20% of its output at rated capacity, the sign of the initial "zero offset" shall be opposite to the sign of the expected change in its signal.Set the data acquisition System to scan all sensors and save at least one record per sensor every 1 sec.Record a file of "zero offsets" capturing at least 10 min. of data before any load is applied with the hydraulic system.Means of initial voltages for all sensors (mean "zero offsets"), sensor serial numbers, the most recent sensitivity constants, excitation voltages, and the channels of the data-acquisition system used for each sensor shall be recorded using Form 8. The pairing of channels and sensors shall be checked by a second person working independently from the person making the initial connections. Infrared targets to be used to measure displacements as described in the attached proposal shall be glued to one face of the test beam using epoxy adhesive. The numbering sequence of these targets shall be recorded using Form 9.Video cameras (one for long-time lapse video and one for high-speed video) will be positioned to capture the response of the mid third of each specimen. To the extent possible, the location of the cameras shall be the same in all tests.5. Testing The following actions shall take place during each test: At the end of each loading increment: Mark Cracks: all visible cracks shall be marked using black permanent markers. Cracks shall be marked by drawing lines parallel to them and with an offset of approximately 0.25 in.Measure Crack Widths: Crack widths shall be measured using crack comparators or graduated handheld microscopes. Measure coordinates of infrared coordinates: A set of coordinates shall be obtained using an OptoTrack System 600 Pro. A set of four targets shall be attached to the strong floor. They shall be located at approximately the same distance to the OptoTrack cameras as targets attached to the test beam. Coordinates for these reference targets shall be obtained at each loading increment. They are to be used to monitor the stability of the Optotrack system by computing the variation in the distances between reference targets.Revision2 5 8-5 REDACTED VERSION

M'age bi40ot 1114 Appendix Approved lest Procedure l-'age 0 ot Zb In-Test Data Backup: At every loading increment the data being produced by the data-acquisition system shall be copied to an external hard drive.Photographs: a set of high-resolution photographs shall be obtained after cracks are marked at each loading increment. The photographs shall includes views of both elevations of the test beam and the top concrete surface above lap splices.The following data shall be recorded throughout each test: Sensor readings: to be recorded on a hard drive in volts. Conversion to engineering units shall be done after the test as follows:-Subtract zero offsets-Divide the result by the sensitivity obtained in the most recent calibration Lapse video photographs: to be obtained every 5 min.Actions to be taken at failure Trigger high-speed camera to record breaking away of the concrete cover and relative movement of the bars.Actions to be taken after test Generate a record of sensors that may have malfunctioned or been accidentally moved during the test Remove from all files recordings from sensors for which the results of the after-test calibration differ by more than 5% from the before-test calibration.

6. Reporting and Backup Produce all the captured data in two ways: By uploading data, photos, and video to a private project at nees.org.By recording all data, photos, and video on a magnetic hard drive Reports shall be produced as described in the Specifications.

Revision2 6 8-6 REDACTED VERSION Form 1 I 2 3 " SOUTH I NORTH I ..,-6 5 4.Section A-A 2 Spa. @3, 3'F A A KBKLc K D K EKF*For section B-Bthrough F-Fsee Sheet 3of 3 Series A Drawing: Series A Formwork As-builts Sheet: 1 of 3 BOWEN OWN , JLB YProject: Experimental Investigation of Drawn by: BPR Checked by: SP PURDUE UNIVERSITYCaatofLpSlcsfNo 11 Reinforcing Bars Date: 04/04/2012 8-7 R Form 1 I I -~2-I--31 SOUTH NORTH6 5 4 _Section A-A 2 Spa. @3 3 ,F A A K B LC KDKEKF*For section B-Bthrough F-Fsee Sheet 3of 3 Series B Series B Formwork As-builts Sheet: 2 of 3 Experimental Investigation of Drawn by: BPR Checked by: SP Capacity of Lap Splices of No.11 Reinforcing Bars Date: 04/04/2012 8-8 R E D IO0N Form 1 I" ~8 I" ~8 -6 4 5 2 '7 6 4- 5 7 1--3 1--3 Section C-C, D-D, & E-E*Facing North Section B-B & F-F*Facing North-- BOWEN PURDUE UNIVERSITY Formwork As-built Sections Sheet: 3 of 3 Experimental Investigation of Drawn by: BPR Checked by: SP Capacity of Lap Splices of No.11 Reinforcing Bars Date: 04/04/2012 8-9 RE N Form 1 Project: Tests to Determine the Behavior of Spliced #11 Bars As-built Dimensions v.1 (Rev. 04/04/2012) Specimen: Sheet ilof 2 Formwork As-built Dimensions Section 1 2 3 4 5 6 7 8 A-A B-B C-c D-D E-E F-F Recorded by: Signature Date Time Checked by: Signature Date Time Checked by: Signature Date Time Comments:*See formwork as-built drawings for dimension locations 8 -10 R IO0N Form I As-built Dimensions v.1 (Rev. 04/04/20 12)Project: Tests to Determine the Behavior of Spliced #11 Bars Specimen: Sheet 2 of 2 Formwork As-built Dimensions Key -Series A Section 1 2 3 4 5 6 7 8 A-A 14'-6" 10'-0" 14'-6" 14'-6" 10'-0" 14'-6" N/A N/A B-B 4-3/8" 6" 4-3/8" 23-5/8" 23-5/8" 30" 30" 17-5/8" c-C 3" 6" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8" D-D 3" 6" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8" E-E 3" 6" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8" F-F 3" 8-3/4" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8" Formwork As-built Dimensions Key -Series B Section 1 2 3 4 5 6 7 8 A-A 13 -10.5" 6'-7" 13 -10.5" 13'-10.5" 6'-7" 13 -10.5" N/A N/A B-B 4-3/8" 6" 4-3/8" 23-5/8" 23-5/8" 30" 30" 17-5/8" C-C 3" 6" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8" D-D 3" 6" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8" E-E 3" 6" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8" F-F 3" 8-3/4" 3" 23-5/8" 23-5/8" 30" 30" 17-5/8" 8-11 R E IO N Form 2ie Wire Ties NORTH Bar Marks NORTHOWENSpecimen: _ _B dTO YProject: Behavior of Lap Splices of No. Drawn by: Checked by: PUgR DU E UN I VE R SI TY 11 Reinforcing BarsDae Re~isi~n 2 REDACTED VERSION btUj-UuU-Ud-ULi3LP-UUU1U-UUU i-age h(1 ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 8: AI P'rocedure Casting Documentation v.1 (Rev. 03/30/2012) Mage 1i ot zb Specimen:_____________ Sheet 1 of 1 General Information Date Disp Ticket Num Truck No. JTime on Ticket Time of Arrival Temp. in Lab Measurements made upon arrival of concrete Slump (ASTM C143 -l0a) Air Content (ASTM C231 -10)Time 1 Result 1 Time 1 Result 1 S/N of Air Meter Time 2 Result 2 Time 2 Result 2 S/N of Scale Unit Weight (ASTM C138 -l0b)Time 1 Wt. of Cont.1 Total Wt. 1 Wt. of Conc.1 Result 1 = Wt. of Conc./Vol. of Cont.Time 2 Wt. of Cont.2 Total Wt. 2 Wt. of Conc.2 Result2 = Wt. of Conc./Vol. of Cont.Times of actions during and after casting Lae lcd Layer 1 vibration Layer 2 vibration Top surface struck Truck Departing complete Lae lcd complete off Lab Lifting Inserts Covered with Patcrmvd Covered with Burlap doused Covered with Placed plastic burlap with water plastic Recorded by Signature Date Time Checked by Signature Date Time Checked by Signature Date Time Comments:*The following ASTM standards and specifications will be followed during casting: C172-10, C192-07, C470-09 8-13 R EDAI~~~nLSI ON bbU3-UUU-Ud;J-UIUL-UUUl b-UUU -~age at 1114.Project: Tests to Determine the Behavior of Spliced #11 Bars Appendllx 8: Al 1 ymd4est Procedure Curing Documentation v.1'(Rev. 03/30/2012) Yb3-UUU-V15-:SYU1-UUUU1-UUj I-age 14 01" 2b Purdue University -Bowen Laboratory Sheet 1 of 1 General Information Specimen(s) Date Specimen Age Time Beginning Time Ending Temperature inside Lab (deg. F)Description of Work Performed Recorded by Signature Date Time Checked by Signature Date Time Checked by Signature Date Time Comments:*Test specimens and associated cylinders are to be cured under wet burlap for seven days 8-14 R E I O N Form 5 Project: Tests to Determine the Behavior of Spliced #11 Bars Cylinder Compression Tests Documentation v.2 (Rev. 04/01/2012) Specimen:* Sheet i of 2 Diameter [nearest 0.01 in.] Length [nearest 0.05 in.] Fracture Type Specimen Date Time of Test Wet/Dry Pmax [Ibf]1 2 1 2 3(1-6)1~2 3 4 5 6 S/N of Testing Machine: Recorded by: Signature Date Time Checked by: Signature Date Time Checked by: Signature Date Time Comments:*Cylinders to be test per ASTM C-39-22 and C-1231-20a with a loading rate of 60,0001bf/min at concrete ages of 3, 7, 14, 28 days, and on same day that test of correspondingspecimen is conducted. Specimens and caps free of defects unless otherwise noted in comments. Average cylinder diameter and area and unit compressive stress (f'c) calculated on sheet 2 of 2.8-15 R IO N Form 5 Project: Tests to Determine the Behavior of Spliced #11 Bars Cylinder Compression Tests Documentation v.2 (Rev. 04/01/2012) Specimen: Sheet 2 of 2 Average Cross-Specimen Date Age Time of Test Wet/Dry Measured sectional Area Prnax [Ibf] f' [psi] FrcueTp Dia. [in.] [in2](1 )2 0-Jan 12:00 AM 0 #DIV/0! #DIV/0! 0 #DIV/0! 0 2_____ 0-Jan 12:00 AM 0 #DIV/0! #DIV/0! 0 #DIV/0! 0 4 5 6 S/N of Testing Machine: d.Recorded by: Signature Date Ti me 0 0 0 Checked by: Signature Date Time 0 Sintr0________________ 0_________ Checked by: Signature_________ Date______Time ___Comments:*Cylinders to be test per ASTM C-39-12 and C-1231-10a with a loading rate of 60,0001bf/min at concrete ages of 3, 7, 14, 28 days, and on same day that test of corresponding specimen is conducted. Specimens and caps free of defects unless otherwise noted in comments. Recorded data is shown on sheet 1 of 2.8-16 R EDAljii(E:S IO N

I-age bib oT 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 85: est -'rocedure Calibration Documentation v.1 (Rev. 04/02/2012) Iage 1 ( ot Zb Bowen Lab -Purdue University Sheet 1 of 1 Calibration Instrument Name and S.N.: Data Acquisition System: Gain: Excitation Voltage: Channel: Sensor: Sensor S.N.: Measurand Voltage Measurand Voltage Measurand Voltage Operator Signature Date Time Checked by Signature Date Time Checked by Signature Date Time Sensitivity Accuracy Results Notes: Re~is~n 2 REDACTED VERSION

I-sage fbf ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 8: f~~l~ 6EtProcedure Calibration Documentation v.1 (Rev. 04/06/2012) I-'age id oT 2ti Bowen Lab -Purdue University Sheet 1 of 1 Meter S.N.+Tve fMee.4-Meter Brand Name Target Air Content Measured Air Content Operator Signature Date Time I + 4 Checked by Signature Date Time Checked by Signature Date Time Notes: Re~is~n 2 REDACTED VERSION Form 7 111+/- 111111 I I I I I I I I I I I I I I I I I I I I I Y II II I I I I I I III INORTH ILLLLLLLLLI__-LLLLLLLLLL ______________________________________________I I I I I I I I I I I I I I I I I I I I I F q................................. fT 111111111 I 111111111 I~8 NORTH 1 1 1 1. ..1 1 £ I---*-j 4~~~~~*a-I PURDUE UNIVERSITY Behavior of Lap Splices of No. 11 Reinforcing Bars 8-19 R EDgAl~i~icnESI ON Form 7 I SOUTH SOUTH I i-, ~2 Top Plan 2 Spa. @3' '-60" Ea. =' 3'KB Ko L LEL F Profile*For section B-B through F-F see Sheet 3 of 3 I" 3 " NORTH NORTH F-_I 4 Bottom Plan.. SOWEN D- LABORA TORY P U RD UE U-NI-VERS IT-Y Series A Concrete As-builts Sheet: 2 of 4 Experimental Investigation of Drawn by: BPR Checked by: SP Capacity of Lap Splices of No.11 Reinforcing Bars Date: 04/04/2012 8 -20 R E IO0N Form 7 I SOUTH SOUTH I NORTH 2 1 Top Plan 2 Spa. @3' ----39.5" Ea.--- 3'Profile*For section B-B through F-F see Sheet 3 of 3 V" 3 " NORTH I ,,I 4 Bottom Plan Series B Concrete As-builts Sheet: 3 of 4 Experimental Investigation of Drawn by: BPR Checked by: SP Capacity of Lap Splices of No.11 Reinforcing Bars Date: 04/04/2012 8 -21 R I0 Form 7 I" ~1 4 2-~3 -Section B-B, C-C, D-D, E-E & F-F*Facjng North__________ jr B W NDrawing: Concrete As-built Sections Sheet: 4 of 4___ __BO Experimental Investigation of Drawn by: BPR Checked by: SP P UR D.UE U NIVERS ITY Capacity of Lap Splices of No.11 Reinforcing Bars Date: 04/04/2012 8 -22 R E gAl~l~LS IO N Form 7 Project: Tests to Determine the Behavior of Spliced #11 Bars Setup and As-built Dimensions v.1 (Rev. 04/04/2012) Specimen: Sheet Ilof 2 Concrete As-built Dimensions Section 1 234 5 678 Plan B-B C-C D-D E-E F-F Recorded by: Signature Date Time Checked by: Signature Date Time Checked by: Signature Date Time Comments:*See concrete as-built drawings for dimension locations 8 -23 R Form 7 Setup and As-built Dimensions v.1 (Rev. 04/04/2012) Project: Tests to Determine the Behavior of Spliced #11 Bars Specimen: Sheet 2 of 2 Concrete As-built Dimensions Key -Series A Section 1 2 3 4 5 6 7 8 Plan 39'-0" 39'-0" 39'-0" 39'-0" N/A N/A N/A N/A B-B 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A C-C 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A D-D 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A E-E 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A F-F 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A Concrete As-built Dimensions Key -Series B Section 1 2 3 4 5 6 7 8 Plan 34'-4" 34'-4" 34'-4" 34'-4" N/A N/A N/A N/A B-B 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A C-C 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A D-D 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A E-E 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A F-F 17-5/8" 30" 17-5/8" 30" N/A N/A N/A N/A 8 -24 R I ON Form 8 Project: Tests to Determine the Behavior of Spliced #11 Bars Instrumentation Documentation v.1 (Rev. 04/01/2012) Specimen: Sheet __ __of____Data Acquisition System: Channel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location Comments Operator Signature Date Time Checked by Signature Date Time Checked by Signature Date Time Notes: Re~isi~n 2 REDACTED VERSION Form 9 Jj...1 1 1...1 1 1 1 jt ' -4 111111111 F I I [ ] I I I Th NORTH I I I I 4; 4" ,. , , ,-BOWEN flLABORA TORY PURDUE UNVRSIT Specimen Behavior of Lap Splices of No. 11 Reinforcing Bars Re~isi~n 2 REDACTED VERSION Purdue University Specimen: A-I Date: 4/LI/1 Average Joad North South North Splice Md (i) South Splice LVDT North LVDT South North Load Cell South Load Cell DG North DG South Tm (I- Overhang (in) Overhang (in) End (in) Mdpan (i) End (in) Support Support "J ." J! J" Overhang (in) Overhang (in) Time_____6 Q.-O."~ o.1S 0.o:7 0.o-i o.0 " .oQoo .-o.ooo 6 & O. i'l6 A_____, c?.c2 " 0. , o! c,0 0 ,If o.o" -O .oo0 -0,00 j"L- 7. O. 6H 0 .qO : "'A SI o.,9o Q. 4 .Q.It~ -c).ooo ooo !' !' 0.0060 0. /,O"/ 6 "tO 1.7. 1.L7 o.-I~ o.V. -0.Qoo -0.oo( -'o -'o- I./' VL.66 Io:ooA 6 tl.< tG -Ge4- O.gov "oQ o, oo ,.~.6A O i' .o0' "toS Q,?I oA&6 o.=1 -0ol.oo -o.oo' "V 6 L.38 IQ',.A" ' 1. 3.. ____ ______ _____ -oo,_-oo_ ___ ,!_.__ 0 q 13 1-.." I,0 , '[ 0. cj. L", O." 0,.1 -o.oo6' -o~o <?.'. q.o;F 15 iQ , "2.-I" ".-62 o.4" o .* c.4'i q -o.oog 1"1-..o I',O"IZ.16 3.?"'f 0.9;1. 0.70 0 .c G -.oo" -o.oo-f "A..Q. 2A.0. 12i":7P" O7 q q. .0:1O (\.o! o1$'7 -..c." ..o, LIL.\ Ho.o 20 __, ___ __.___ L.LI, 1 t. 1.Li( 1.15 -.oio -. 0 '.litH , __ __ __ __ _ _______9-I REDACTED VERSION I' ..0 U Purdue University Specimen: Date: Average Load North South North Splice Md ()South Splice LVDT North LVDT South North Load Cell South Load Cell 06 North D6 Sauth Tm (lbf) Overhang (in) Overhang (in) End (in) Misa i) End (in) Support Support *(Ibf) (]bf) Overhang (in) Overhang (in) Time____1 ~ .0 0 -0.0!l 0 -0.01 -0.001 -0.ool0. 0.2.. 0.7 .O~0 .!,-1 O.AI 0.0I .01 -0.00oo -0.00l S, G Q.W]L l1I" 0,-H'- O.-f-i 0.06 0.10 o~o 6 -.0.oo -0.001 V"L 11. 0.G3' Q.6?"t $'?5A , "1.qi16 .1"/ Q.!"1 O,"1,6 7.I1 0...0oo -0.00' %" ,IA t55~ ,.6"7 , .6 I.Q .2tz ;.3- 0.'Vl" -O.oO"t -0.0O1 30 t7Ol."e~ I.I'zQ T:J;A , _____ ..21 o..i-' o."z. -o.oo-. .-o.,:oo" ____ ____ 1.VI'/'- !.1t' 10 :3.,-- "z,"' "j,-' 0.33= -0.001 -o.o000o __ ___jj~ " 1o:S'JA 11 1O.g ";,6o; Q,q O."t'. o,.' -v.oo-i.- -o.ool 10,.6 "-II .. i:]"A 13'14 16 18"20 9-2 REDACTED VERSION 0 Purdue University Specimen: A-3 5 /~O/l2 Date: Averacejoad North South North Splice Midsa (In) South Splice LVDT North LVDT South North Load Cell South Load Cell DG North 06 South lm (fI<Overhang (in) Overhang (in) End (in) spn End (in) Support Support (1 Overhang (in) Overhang (in) Tm 1 Q.(6 0.00 0.00 0.00 Q.QQ Q.oO -Q.o0"L -o.0o'L 0.Lt ,0. 0 .1 o.(t40 2 ,' o(t Q.Iq o.o'z. Q0 0.0 1 .o. .-O.ooL -0.0o02 6 6.-i:. o.L g. ?Li." 0.q-H o.-I1 O,01 0.1! o.o-l .o.o'-L _o.OOi t1.. tiL.. Q.C'1 g:w;_____ 08 o.gO .' 0.-1.- Q.1- -oQo3 0.ooo ____ Q,9? -o:;1A2 1.V; 1.1-9 oI'z, 0,-1 *-o.oo,0 o.'oi- 20I I-tl , 1.',1[,b O.L O. q' .? 0.i.9 O.ooq L6'1$ t.S tO : f 10 11 12 13 14 17 ISi 19o 9-3 REDACTED VERSION 0 Purdue University Specimen: Date: 4,/3/12 Average Load North South " North Splice Misa i) South Splice LVOT*10rth LVDT south North Load Cell South Load Cell DG North DG South ,, (Ibf) Overhang (in) Overhang (in) End (in) lsan(n End (in) Support Support __ I_____If) Overhang (in) Overhang (in)} Time o,01 -o~oj -0.0 I -o.oQ -Q~oQ 0.00 -0.oo[ -0.00o O[ Q. 0.000 0.00 2 3..i. c atk ______3 6.0 0.11 0IGO1 0.0. 0.0'1 0.0"? -o.oo( -0.001 6.o 6-O 0.11 6 lL.1-O-I) O. CISoo Q.i.'l 0.0S -o.iool -o.oo0. 2:.I.O 'Li.I I.7lJ~ OI4~ To-IA' 3-J.S 1.-T? 0.1-c Q.-G -o-ooo -9.oo1 "i.'.9 L-1-fQ 1-iQE 9"1-IA N*,,~c VG __ __ ___ _ .oc'0 O.oO~10 N+" DG .- o.000 o-Qoo ,, "o.O ?.x' 7-ISo, O.61 Q.6G 0.c6 -o.oo? 0.-I"l O.'3" ,¢.,jj0 Is O.-SI 0.66Q O.c; o~o(- tO".",.. 03 __i___'zC ,, -1,Q o.',5 0.660,c.*I -0.0oo' 000o 7A.1 Ul:5JA 16 '.-: 7A.9 o.S9J Q.< Q.-&-f 0.o0Q3 ?6.o ___ .o_ VL:IbF 9-4 REDACTED VERSION U U U Purdue University / ll2 Specimen: Date: Average Load North South North Splice South Splice LVDT North LVDT South North Load Cell South Load Cell i DG North DG South rm (lbf) Overhang (in) Overhang (In) End (In) Mldspan (in) End (In) Support Support (lbf) (Ibf} Overhang (in) Overhang (In) Ti_____e _1 0.01 0.00 -O.oot. -o.oc-i. 01. o.ooo o.Qoo "]:3gA VL,.Q 0.11~ 0,0-j o.1 o.0, -.oO).o -a.0" VI.'t (i.Q Q-16= ' 0.86 o.9j -o0,0L -o.ooi I-Q I.Q 0.860 Q!~1'I g:-[s'A , ta~c) -o .oc~t o~ooo "IA.O .o +0. 1.1.;! __l__7_ : t' ?0,0 U,,I L.,5b 0.31 0,L-J -o.ooi o.ooI 30.0 Qo.O i.G2.? b&1,69 S-W'A , DC, ,.-, __'_"Q.ooo Q.OOQ , 6.o .o"1..O1 '),4Q o..4i -o.ooo o.oo1 ?6.0 36.0 Q.-f4;o~ o.'If fQ:o64 ii 'yc/qit -L.M1I Q2. 5' -o.o00 .O.ool ?1.7 '1 .q; O.e?" Q to':-A ,N14S" PG v-oQ4.- 'z.ooo 0.oQQ 13 3/4- 0.63 Q?.q 0.66 -Q.ooo -o.o0 o 2.0fo $.-]o iQ:ssA 1-9 -lo,1 '-1.6-i. ,0."i Q.'" o.o0o -0.001 '-!o.6 i~,-I-f P 9-5 REDACTED VERSION Purdue University Specimen: A-C, Date: Average oad North South NorthSplice Md n) South Splice .VDT North LVDT South North Loa.Cel South Load Cel DG North 06 South T--(6 Overhang (in) Overhang (in) End (in) M span [I) End (in) Support Support Overhang (in) Overhang (in) Tm O."V. 0.00 0.o0 0.00 -0.00 o.o0 -.0.0o0 -o~ooc' 0.? O... 0oo .000 F'Q- ot' 0.0'7, Q.o=; o.0ot -o.ooo 6.0 bQ O.i1!. oQ-i;i , ~z oA o Q,-o.+ 0,0-i ocoj 0.01 o.oo~ 0t.000 1'2..o ti..A I o .,913 I:'oP , o~g6 Q.%G 0.13 o.I9 v.007 -.001o {i~O 6 Vo ..67 I.61, 0."}.- O .'L6 o."js QOQ0 -0001" -2'fQ .0 Ao.. l. 6."3 L.6'1 "t.-{fP 8 12c ,voi4" 0.000 aQvQQ "1;bF'15 vo ,L -3,oo 3.1' 0 .i'- O*e6 osq-I 0.o00' -o.007 1.oQ.I "Lo.3 0.?3? O.q(;6 P 16 Q.tl," I.8 6 "i.. "..o Q,'j O.-jo 03.5 -o.0o7 O,1". O,"__-.0 _16 "1,'- 1 ."0 0 .Q O.&" -o..Oo" "_..__ .0_ ____ ___'9 '4..07 Q.(:,Q Q.g? 0.66 0.oo')J -0oo 3G .Q ?.o S-t- FP 20 t(Q,3 iJ?". -j.-i0 Q0.'0 Q0e..7 9.7 q.oo -c'.oo'9 4,Q,-7 _,__,_ _______9-6'REDACTED VERSION

• .r Purdue University Specimen: Date:_6.g.2 Average Load North South North Splice Midspan (in) South Splice LVDT North LVDT South North Load Cell South Load Cell DG North DG South Time (lbf) Overhang (In). Overhang (In) End (in)} ______ End (in) Support Support (lbf) (lbf) Overhang (in] Overhang (in) ______" -!. L.-0 L ,!-408; tt; .~ o o~t II H*.'. , F 23 24 26 27 28 29, 33 31, 32 33 34 36 17 43 9-7 REDACTED VERSION Purdue University

©Ii Specimen : DQ -_Date: -l0i: 71 ~T r Average North Overhang (in) South Overhang (in)North Splice End (in)Mldspan (in)South Splice End (in)LVDT North Support ILVDT South Support INorth Load Cell (lbf) ISouth Load Cell (Ibf)S o.'z -0.01 0 0 0 -o.00 -o.ooo o0 S .o5 .o o.oj o o 0 3.5 3. -6 0 ..o .5 o. 045- _ _ _ _ _ _S G 0.~ Io.14 O. oZ- 0.o'?_ O.oZ o.ooi 0.001 ___ __6 I o.j o 0.o5 d.oe o.0oo3 o.oo01 I 11 I0-o.- o.+/- 0.I _____o.I o..oo4r i 13 2-4 I.I I.o-+ o.15 O-Is o. 1j o.oo2 1, 1e .Po 1. 1 o.I_5 O.31 0.12 0.00 o.oo3 ______19 20 ZM vo 3 ~3A~414 9-8 REDACTED VERSION 0i ..Purdue University C)S Specimen: Date: Average Load North South North Splice Misa i) South Splice LVDT North LVDT South North Load Cell South Load Cell DG North DG South TnOverhang (in) Overhang (in) End (in) Misa I) End (in) ,- Support- Support ..a//,/ 't Overhang (in) Overhang (in) Time____1 o~. 0 o.oj 0 0 -Oofo -0.oo5 o.ool 0,3 0,L f-.0 0..o0Olo ?.:57-A___________ ______ O1 .0¢ 0 .O 0.'01 -0.005 0.001 0236 O~4 " 5o S 18 o.81 0. 8 0.1.1 0.13 O. Io -~o..oo____ ____ 0.__0_-__

1 , 0 14 o.2 0.2. .00~ I.s~ra bo~ooA-P.ELA'TJVE 10 If o.s, o.i.5 ol' o.11- o.OOS, I, Ig -O. 32o I1:1o A 12 19- I.% 1.9 o.j8 o.1- -ooo .17;9-9 REDACTED VERSION

...(0 Purdue University Specimen: Date: /_/i Average Load North South North Splice Mdan()South Splice LVDT North LVDT South North Load Cell South Load Cell DG North DG South lm 4Jf. ! Overhang (in) Overhang (in) End (in) __dspan___n) End (in) Support Support J4 Overhang (in) Overhang (in) Time____1 o .% o o o -0.o -o.oo' o 0 '-S G.2. 0.14 oXlf o.o'L 0.o2 ,-o.oal -coa.oo 6.z 6.g. o.j14 o.Ij, 2,io.A" 0.4. 0.40 0.05 0.0-4 0.05 -...ooo -o.oo~Z. )Z oQAo7 ,35A, S 8 oJ .0-jo. 0 o.3 o-JO -o.o04 -o..oo? 18 lB o.-?4-- 9):o{-6 z 4 1.o09 I.of- 0. 14 o049 0.15 .--o.0of .-0.002 4,, L. .057- (. o6o ¢/' 30 I.43 1.41 j.1 0.25 o2. -0.ood/ -cooo 30 zo I., " ." .'25 03.3 o."5 -o 0,.0o0oo 3C, o J.aao !o'zB4,q 0-o. Q44 o4 o.0? o.0J -o.oo~f o.,, oZ. o.,,/ (/;o5..4 1o 0% O 8G .1 O-Jk o.15 Oi12 -o.oo,0 -ooz 12.1 O.Saeto I1"1" 4 14 16 17'19 20 9-10 REDACTED VERSION Purdue University Specimen:, rh-H Date:_Averag Ove Nrthan (I) overhagin ENdr (pi) Mldspan (In) South Splice LVDT North LVDT South North Load Cell South Load C:ell DG North DG South (Ibf)_Overhan (in)____ Overhang__ ____n) __End _____in)_ End (In) Support Support (lbf) (Ibf) Overhang (in) Overhang (In) Time____.* o.o¢ 0 0 o0 o.ool 0. .. o. 4:jq/:' 04" 0 o o o o o ogp0 o. o.,'2 o. ,2o2 o.,loZ It z 24 26 28 27 28 29 30 31, 32 33 34 36 37 38 39 40 9-11 REDACTED VERSION Purdue University Specimen : Iz:-Date: -'Average Load North South North Splice Mlsa i) South Splice LVDT North LVOT South North Load Cell South Load Cell DG North DG South Tm (Ibf) Overhang (In) Overhang (in) End (in) Mldspan__in) End {in) Support Support (Ibf) (Ibf) Overhang (in) Overhang (in) im S 0 oo000 -o.ooyZ -o.0o1 _.___o. o._o..__._,_I-- 0 .. 0.o5 0 0 0 -o.ooi o __.__ 5.Z o.z45 oif_65 ______ 0.1 0z~.. 005 0o 0.00l ____ ii.__ 0.5 V(L 0.s'5 1_58____o. __ O.___ o._oo-I 0.08 0.00-3 o__o___ _____ __.__I o______ ____, L-> 'ST .S1Ll CI-, .Ac v. __ __ _ __ _ __ ____ _'24[ 0.c5 o. o.0o G.I5 O.0o-J g0 iAi~i' 1.i41' 3'3-, _ _ _ _. _ _r _ _. _- _ 0-I -o 2. l 0.W. o , o( o .oo 4 .I.Y /U :I.:9::/ I.:& 0. 0.2..,4 .___ .____ ___ -__ 4 12 13 14 15 16 17 18 14 20 9-12 REDACTED VERSION U Purdue University Specimen :_________ Date: Average Load North South North Splice Mi i) South Splice LVDT North LVDT South North Load Cell South Load Cell DG North DG South Tm (Ibf) Overhang (in) Overhang (in) End (in) ___span_____ End (in) Support Support ..II L-- Ia Overhang (in) Overhang (in) Tm 0.4 0 o 0 0 o 0 O _____ O~. o ' 0.2_ 0 0 0) 0 0 o-ool o.i_ o,-2 0 0.-900 _____ O.oO 0.c~ aOo2 0.0i o. oo'2. o.0oo1.. 6 0. I =P 6 ____ o,' 0.04 0.01 0.09 o. 04 o. ooZ ' ~ .oGO8 l4011P1 V 5 o.l. o5.9,5 o.o2. o-II oC4' 0c4 2e 15A -o.l o.92,5 2z'78'M* 1.oi 0.30 O.l9 o.17 o.I:7 0.05 20 30i 1-0.? I. 3:16W' z E ID & S ; _ _ _ _ ._ _ _ .o 00 ( J O)__ __o._ o.z8 o.Zf. o.00s o,0o/-osL L.5,Z.' 3:4411'"1 o o.59 0.39 0.05 0.o0 o.o5 o..oo3 o.oo'2 o ______ 12I 9.JG o.14 o~o 0.jI -o.Io .04 o.o0z __ __ _ .4_____o._______-_ 1.2l& .Q0 o0 I o.I .02 00o ___________. 14 3'._ 1.54 I. ¢ -_-___._ _ooo___ _____ --- -s ..o ?'M 15 16 18 19 20 9-13 REDACTED VERSION U 0 0 Date: S ,.5 Purdue University Specimen" Average Lgad North South North Splice Mda(n) South Splice LVDT North LVDT South North Load Cell South Load Cell DG North DG South re-]1 Overhang (in) Overhang (in) End (In) Midspan___n) End (In) Support Support 4J.f I c Overhang (in) Overhang (in) Tm o.1_ .O__ O.0', 0 0 0 -0.0b06 0. O.10O 2 k.: .c,_ __ _ __ _ _ _ __ _ __ _ __ _S6 04i o~ 0.01 0.01 -oo 0.005Ooo .6 o.105 'Z-9A 12 IO1.t 0.39 0.05 0.o0, 0.0ot -.xo~o, 12 V,2Z 1 8 0.:/5 0.1 0.0,9 o.ll 0.08 18 18 o.=jl %ob,4__________ .o__.$ O.l' o.oo,/ I.o3,L j4l~f _______.__-- i.0. ! oOZ ..1 -o.001 o.oob ffijZ- v.'S 1O-1i, 10 _____ L, [,'& O.i~l 0,1 -OOOI 0.005 ?,5 1.16ft 1.2.56 " o o.o~t 0.05 -oo o.oo. o.z o.ApL o.So5 I0oA.o 12 0.81 0.9,o o.11 0.13 0-!0 oR.o, 1l Z O.'Bo5 0.85 t2-IIo(,A 17 1.9 9-14 REDACTED VERSION bbY;5-UUU-Ut$;5-U1:U-UUUlth-UUU I-'age oT 1114ApedxU:alrtoneticas Appendix 1U: (JertlTicates TAKING ACCURATE THERMAOMETER READINGS COMMON TYPES OF THERMOMETERS AND FACTORS AFFECTING THEIR USE TOTAL IMMERSION thermometers are designed with scales calibrated to indicate the true temperature when the bulb and the portion of the thermometer that contains the mercury column are exposed to the temperature to be measured (practically,, less than an inch is permitted to extend above the surface,.o permit the reading to be made). Most total immersion thermometers can also be used in a condition of complete immersion, in which case the entire thermometer is exposed to the temperature being measured, such as in a freezer.PARTIAL IMMERSION thermometers are designed with scales calibrated to indicate the true temperature when the thermometers are immersed to specified depths. The portion that should be immersed is indicated on the back of each thermometer. COMPUTATION OF EMERGENT STEM CORRECTION When total immersion thermometers are used only partially immersed, a stem correction may he calculated and applied to the reading for precision results. To compute an emergent stem correction, the following variables must be defined: T = the reading of the thermometer in situ.N = the number of degrees on the thermometer scale between the liquid surface and the top of the mercury column.A = the average temperature of the emergent mercury column. To find value A, suspend alongside the subject thermometer a secondary or auxiliary thermometer with its bulb centered between the liquid level and the temperature indicated on the subject. thermometer. The temperature indicated on this auxiliary thermometer will he value A.Find the stem correction (SC) by computation from the following formula: SC = 0.00016 x (N x (T-A)) for Celsius temperatures, or SC = 0.00009 x (N x (T-A)) for Fahrenheit temperatures. Example: A thermometer graduated from -1° to 101°C., immersed to 20°C on its scale, reading 90°C. The auxiliary thermometer reads 42C. Hence, T=90, N=70 (90.20). A---42 Working the formula, SC =.00016 x (70 x (90 -42)) yields a value for SC of +.537. This value must he added to the observed indication of the subject thermometer to determine the true temperature of the liquid. Hence, the true temperature of the liquid is 90° + .54° (rounded result) = 90. 540 GENERAL CONSIDERATIONS FOR MAKING AN ACCURATE READ)ING The error due to parlla may be eliminated by taking care that the reflection of the scale can be seen in the mercury thread, and by adjusting the line of sight so that the graduation of the scale nearest the meniscus exactly hides its own image: the line of sight will then be normal to the stem at that point. In reading thermometers, account must be taken of the fact that the lines are of appreciable width. The best practice is to consider the position of the lines as defined by their middle parts." PERFORMING A CALIBRATION AT THE ICE POINT (0 DEGREES CELSIUS OR 32 DEGREES FAHRENHEIT) Select clear pieces of ice, preferably made from relatively pure water. Discard any cloudy or unsound portions. Rinse the ice with distilled water and shave or crush into sm~all pieces, avoiding direct contact with the hands or any chemically unclean objects. Fill a Dewar or other insulated vessel with the crushed ice and add sufficient distilled (and preferably precooled) water to form a slush, but not enough to float the ice. Insert the*thermometer, packing the ice gentiy about the stem, to a depth sufficient to cover the 0°C (32°F) graduation. As the ice melts, drain off some of the water and add more crushed ice.Raise the thermometer a few millimeters after at least 3 minutes have elapsed, tap the stem gently and observe the reading. Successive readings taken at least one minute apart should agree within one tenth of one graduation. APPLYING THE CORRECTION AT ICE POINT Record readings and compare with previous readings. If the readings are found to be higher or lower than the reading corresponding tO a previous calibration, readings at all other temperatures will he correspondingly increased or decreased. Reproduced in part from ASTM E77.KESSLER THERMOMETER CORP.Precision and ReliabilitY... from aname you can trust.REDACTED VERSION lbu)i-UUU-U.5IJ-U.1--U-UUU1Ii-UUU l-'age Ijuu ot 1114ApeixU:airtonetlcte Appendix 1U: L;allbratlon Cerl:lrlcates CALSER CORPORATION 302 N. BELT EAST SWANSEA, IL 62226 (618)277-0329 TESTING MACHINE CERTIFICATE OF CALIBRATION Owner : Purdue University Report #: Location : 1040 South River Rd. -Bowen Lab West Lafayette, IN 47907 Page : Machine : Fomey 600,0001bf Model F-600-DFM/1 Serial No. : 99058 -§ liaef wI Fomey DFM/1 Digital R/O #9902182 wI/Dynisco P/T #02-23-990747 This is to certify that the testing machine listed above has been calibrated by Calser Corporation personnel. The method Of verification and listed data are in accordance with ASTM E 4-09.Accuracy of all calibration devices is traceable to the National Institute of Standards and Testing (NIST)*and all calculations have been corrected for temperature where applicable. VN# 6560 2 of 20616111, Capacity Range Run 1 600,000lbf Range Run 2 600,0001bf Range Run 3 600,0001bf Range Loading Range 5,000 -600,000 5,000 -600,000 5,000 -600,000 Max. Error 1.20 %0.10 %0.08 %Verification Equipment Used: (400,000 Load Cell Set)Admet Gage Buster Digital Readout, Serial # GB-991 1092, and Load Cell(s) Listed Below.Serial # Ranne Calib. Date 901 120B 716.99 -10,000 lbf 08/19/2009 090716C (LO) 5,572.38 -100,000 lbf 08/10/2010 0907160 (HI) 39,281.95 -400,000 lbf 08/10/201 0 Uncertainty 1.792 16f 13.931 lbf 98.205 Ibf This cerlilicate is Issued as a statement of the fact that on the above date the listed testing machine has an accuracy as Indicated. It should not be construed or regarded as a Guarantee or Warra~nty of any kInd (In favor of the client, the client's customers, or the public at large) that the testng machine Will continue to retain the same percentage (%) of accuracy or efficiency as determined on the date when the calibration, and adjustments if required, was performed and reported by 'Calser Corqrration' since the calibrator has absolutely no control over the future operation, damage.maintenance, repairs, and overa~l condition of the testing machine and hereby expressly disclaims any and aDlliaLbility for damage or loss sustained by all parties adslng or resulting from th deterioration, obsolescence, malfunction or substandard perfonnance of said testing machine; wtrlch*shall remain the sole responsribiliy of the machine's regula custodian. owner. andlor user. This certilicate shall not be reporoduced except in full, without the written approval of Calser Corporation. CALSER CORPORATION Quality Control Director Form # 104-01-Rev 3 REDACTED VERSION bbi-UUU-LUb3-Utz-U-UUUId-UUU l-'age bU1 OT 1114ApeixU:alrtonertcas Appendix 1U: Calibration CertlTicates A.CALSER CORPORATION 302 N. Belt East, Swansea, IL 62226 (618) 277-0329 TESTING MACHINE CALIBRATION DATA AND REPORT ,-.Customer Purdue University _ Location 1040 South River Rd. -Bowen Lab' West Lafayette, IN 47907-1 Report #: VN# 6560 Page 1 of 2 Date of Service 06/06111 Cost order No. Verbal Order Date 06102/111 Temp. 74" F Date Done 05119110 Machine Serial No.Auxilay Equiprnent: ,Fomey 600,0001bf Model F-600-DFMI1 99058 w/ Fomey DFMfl Digital RIO #9902182I_____________w/D nisco P/T #02-23-990747 -_____AoppledForc __ _Ind'l cted Forel : rE, z I j)I " n l' et Frce r~ .E .I " 1 Idicted orc ErsIo" Run #1 _ Run #1 "As Formd" Co~rrdon __ Run #2 "As Left" Conclion Run #3 ."As Left" Condition 600,0001bf Range *__ l01bf/I DIV

• 0 0 60 0 0 0.00 60 0 0 0.00 6C 0 0 0.001 5.000 60 4,940 -60 1.20 60 5,000 0 0.00 60 5,000 0 0.00 10.000 7 9.880 -120 1.20 7 9.990 -10 0.10 7 10.000 0 0.00 20,,000 7 19.790 -2.10 1.05 7 19,990 -10 0.05 7 ,19,990 -10 0.05 40,000 8 39.530 -470 1.18 ,8 40.000 0 0.00 8 .40.000 0] 0.00 60.000 8 59,340 -660 1.10 8 60.010 10 0.02, 8 " 60.000 0 0.00 80.000! 8 79.1 50 -850 1.06 8 80.050 50; 0.06 8 80.030 30 0.04..00...00.............0..

.,8...........98940 ....0,05t1 -1.065 ... --.8 .... ...- 00 60*...........66(.....6 .6, -.80-.0........00.70 .100...070 .70 ...... 0.07007 125.000 8 123.600 -1,400 1.12 8 90 0.07; 8 125.100 100 0.08 150.0001 8 148.330 -1,670; 1.11. 8 150,150 150 0.10 8 150,120 120 0.08 200.000 8 197,650 -2,350 1.18 8 199,980 -20 0.0,1. 8 200,010 10 0.01 300,000 8 296,650 -3j30 1.12 8 300§6 60 0.02 8 300.040 40 0.01 400.000 8 395.880 -4.120 1.03 8 400.120 120 0.03 8 400,090 90 0.02 500,000! 8 495.110 -4.890! 0.98 8 500,260 260 0.05 8 500.210 210 0.04 600,000 8 593,770 -620 1.04 8 600.310 310 0.051 8 600,290 290 0.05 0 8 0 20 0.00 8 0 -100O.00i8 0 -30 0.00 Notes: D- Calibration in accordance with ASTM E4-09,! and Calser Corporation Procedure

1. 1-01, Rev 1.ACCURACY

SUMMARY

..capacity Rane Loadin Range Max. Error Run I1_____________

600,0001bf Range 5,000 -600,000 1.2.0 %Run 2 ______fl00,O001bf Range 5,000 -600.000 0.10 %Run3 3__________ 600,000!bf Range 5,000 -600,000 0.08 %*CAMBRATI.ON EQUIPMENT All verification equrlpmerf-Incuding dead weights, provin rings, load cells. etc., Is calibrated and traceable to the latest procedu'es $tipulated by the National Ins titute of Standards and Test~ng (NIST) and ASTM E74-06. All equipment is tr'aceable under 9ukleeines set forth In ISO/IEC 17025. Alt instrument readings have been corrected for temperature whiere necessary. _______ VERIFICATION EQUIPMENT _ _ _ _ _ _ _& Sertali ____ nd_ ncertalty(L.BF) & Date Strainsense 60 716.99 -10.000 Ibf Morehouse 901120B 1.792 lbf 08/19/09 Strainsense 7 5,572.38-100,O0001bf Morehouse 0907160 (10) 13.931 Ibt" 08/10/10 Strainsense 8 39,281.95 -400,000 lbf Morehouse 0907160 (HI) 98.205 Ibf 08110110 This report shall not be copied except in its entirety without express written approval of Calser Corp.Formi# 103-01-Rev 3 Calibraton Tedcnican Jerry Parker I)REDACTED VERSION bbW~-UUU-Ud~-UbU"UUU~~-UUU wags Uu~ ot VI14 Appendix W: uslieritian Lertilicitis CERTIFICATE OF CALIBRATION ISSUED BY: INSTRON CALIBRATION LABORATORY DATE OF ISSUE: 30-Jan-12 CERTIFICATE NUMBER: 340013012113643 Lab code: 200301-0~instron 825 University Avenue NSTRON~Norwood, MA 02052-2643 II C a" Teephone: (800) 473-7838 Fax: (781) 575-5750 Email: servicejreq uests~instran.cam Type of Calibration: Relevant Standard: ASTM E83-10 Page 1 of 3 pages APPROVED SIGNATORY Richard- Digh ineo d b ihr fDNcn=Rlchard Binford,:c=US, l=Norwaod, st=MA,---v -- -5'00'Date of Calibration: 30-Jan-I12 Name: PURDUE UNIVERSITY Address: 550 STADIUM MALL DR.WEST LAFAYETITEJ N 47907 KBROWER@PURDUE.EDU KEVIN BROWER PRO.Contract No.: Contact: Manufacturer. BALDWIN Manufacturer. INSTRON Serial Number. 120BTEC502040 Transducer ID: 2630-115/590 System ID:.Range Type: 120BTEC502040 Single Extensometer Type: Travel (Tension): Travel (Compression): Gauge Length: Mode: Type I lin 0.1 in 2in Static (Tension/Compression)-At,-&r A'~?? z&L.The following indicators of the extensometer system were verified and classed: Indicator Type Indicator Range Full Scale Units (%)System Class Description

1. Digital Readout strain 100 B-I All indicators listed above were verified on-site at customer location by Instron in accordance with ASTM E83.The verification and equipment used conform to a controlled Quality Assurance program which meets the specifications outlined in ANSIJNCSL Z540-I, 150 10012, ISO 900 1:2008 and ISO/lEO 17025:2005.

The testing machine was verified in the 'as found' condition. Instron Calpro Version 3.23 The results indicted on this certificate and the following report relate only to the items verifed. If there aremethods or data included that arc not covered by the NVLAP accreditation it wilt he identfifed in the comments. Any limitations of u.e as a result of this verification will be indicated in the comments. This report must nrot be used to chins product endorsement by NVLAP or the United States government. This report shalt not be reproduced, except in lull, without the approval of te issuing laboratory. REDACTED VERSION bb~6.UUUU~S-UbW-UUUlW-UUU rage wu~t or VI 14 Appendix iu: Lalibration Lartiticatma CERTIFICATE OF CALIBRATION NVLAP ACCREDITED CALIBRATION LABORATORY No. 200301-0 CERTIFICATE NUMBER: 340013012113643 Page 3 of 3 pages Indicator

1. -Digital Readout (strain)Range Run 1 Indicated (strai)Applied (in) I RunZ2 Indicated (st-ain)Applied (in)100% Range (Full Scale:l1.00016 in)Rim Temperature:

70.0 °F 40 J 0.19991 0.400580 701 0.34995 0.700010 100J 0.49985 1.000162 Run Temperature: 70.1 0 F 0.1995 0.400013 0.349987 0.700023 0.49899 1.000050 Verification Equipment: Serial Calibration Measurement Make/Model Number Description Agency Range Cal Date Cal Due Extech 445580 1003552 temp. indicator Tektronix NA 12-Feb-il 12-Feb-13 Epsilon 3590VH1R A5010 disp. indicator Instron Ltd 2.00 in 14-Feb-I11 14-Feb-12 (ASTM)* Instron US Gauge Bar 1902 gauge bar £4 Jansson NA 11l-May-10 1 1-May-12* HBM ML38 90630412 force indicator Instron NA 21-Jan-li 21-Jan-13* Epsilon 3590 VHR AS010 (Note: Also used for displacement measurements and listed above.)(ASTM)* Equipment used for gauge length measurements. Verification Equipment Usage: Measurement Serial Range Type Number (% Full Scale) Percent(s) of Range Displacement A5010 (ASTM) 100 0/10120140/70/100 Instron standards are traceable to NIST and/or other National standards. Verified by: Rich Binford Field Service Engineer NOTE: Clause 9 of ASTM E-83 states; It is recommended that extensometer systems be verified annually or more frequently if required. In no case shall the time interval between verifications exceed 18 months (unless an extensometer is being used in a long-time test running beyond the 18 month period). An extensometer system shall not be used after an adjustment or repair that could affect its accuracy without first veritying its accuracy utilizing the procedure described in this practice.instron Caipro Version 3.23 REDACTED VERSION

h~age tbU40oT 11 14Apeix1:ajrtonettcte Appenalx 3.U: Calibration (Jertltlcates INSTR:O:3N.CEAST/ Dynatup I Wilson / WOI.PE1RT itnstron-Service

825 University, Avenue .3-Norwood, MA 02062-2643 Tel" m

Fax

+1-78'1-575-5755 www.lnstron.com Field'Seivice Repor, Company: Address:*Contact;.

Service Order#: Field Engineer.Service Notes: '-550 Stadium Mail Drive Civi RoomG151*West Lafayette,'IN 47907.USA=Brower Kevin-.SV1201120017@§1 TCredit.Card 'Richard Binford :Reference

1. Contract Total Amount:.$2330.

Verified force,displcement~and~the extensometer. Keep aregular check on the pressure transducer oil~capsule

• gap regulatly to' insure the .030" gap for accurate force readings.Labor Activities-01130/2012-120BTEC502040

=0.02 S1400-003-A Zone 3 For Tensile Service 01.121 .120BTEC502040 .1.00 -1460-011-A Crosshead.Displacement Verification 0113012012 1208TECS02040 2.00 S1481-017-C-A ..Force Verification. 68K Ib-300K lb_______ __________ _________ _______ __________Compression ,, 01130/2012 2630-11'5/590 -120BTEC502040 .1.00 .$1490-003-A Strain Verification,. Static Ext or"__________________________ ______ _________Detfectometer Materialsi I I II .0113012012

• Technical Support: Service_Support@Instron.com Email: Serylcereq uests@lnstron.com Page I oilt REDACTED VERSION bbMI-UUU-.5-LdMI-Ub-JUU1U1-UUU 11196 iUb 0? 1114Apnax1:clirtnumrcts Appenalx 1U: Calibration Certificates CERTIFICATE OF CALIBRATION ISSUED BY :INSTRON CALIBRATION LABORATORY DATE OF ISSUE : 30-.Tan-2012 CERTIFICATE NUMBER: 340013012110833 Lab code: 200301-0 Page 1 of 3 INSTRON~Instron 825 University Avenue Norwood, MA 02062-2643 Telephone:

(800) 473- 7838 Fax: (781) 575 -5755 Email: serviceqrequests~instron.com APPROVED SIGNATORY Richard , icar Bi" " i=Narwc°cd, st-MA, au=OVR B Vno rd Customer Requested Due Date: 30-Jan-2013 Type of Calibration: 3D Relevant Standard: astm e2309 Date of Calibration: 30-Jan-2012 9us1m&4Lt,. PURDUE UN~IVERSITY 550 STADIUM MALL DR.WEST LAFAYETITE, IN 47907 I :~.ccw~gE~ 4'- .~ A..Serial No : Make : Model : C502040 BALDWIN 12OBTE P.O. Number : Contact : HARRY TIDRICK 1. Digital Readout (in)This certifies that the displacements verified with machine indicator 1 (listed above) were venifled byr Instron in accordance with ASTM E2309-05 (Follow-the-Displacement Method) and Instron work instruction ICA-8-07.The testing machine was verified on-site at customer location. Adjustments are noted in the comments section of this report with a reference to the "As Found" data.The verification and equipment used conform to a controlled Quality Assurance program which meets the specifications outlined in ANSI/NCSL Z540-1, ISO 10012, 1SO 9001:2000, and ISO/fEC 17025:2005. The Instron measurement equipment used for verification is traceable to NIST.Indicator 1- Digital Readout (in)Verified Range (in)Max Error Max Error (in) (%)Max Repeat Error (in)Max Repeat Error (36)ASTM System Resolution Resolution Lower Limit Class* (in) Class (in)0.2 0.00268 -0.355 0.001 12 0.257 B .001 B 0.2*Sys tern Class is derived from assessment of the following: error, repeatability, resolution, and standard device classification. The results indicated on this certificate and report relate only to the items verified. If there are methods or data included that are not covered by the NYLAP accreditation it will be identified in the comments. Any limitations of use as a result of this verification will be indicated in the comments. This report must not be used to claim product endorsement by NYLAP or the United States government. This report shall not be reproduced, except in full, without the approval of Irnstron.CalproSDS version 3.3 REDACTED VERSION

b-UUU P'age dUb5 07"1114ApndxU:airtoneticae Appendix 1U: Calibration Certlllcates CERTIFICATE OF CALIBRATION ISSUED BY :INSTRON CALIBRATION LABORATORY DATE OF ISSUE : 30-Jan-2012 CERTIFICATE NUMBER: 340013012110833 I IPage 2of 3 Direction of Displacement

Ascending Suggested Run I Runi1 Run 2 Run 2 Run 3 Run 3 Repeat Value IError Error Error Error Error Error Error Uncertainty Coverage (in) I(in) (%) (in) (%) (in) (%) (in) (in)* Factor = k 0.2 0.00007 0.035 -0.00045 -0.222 -0.00026 -0.129 0.00052 0.00081 2.26 0.4 -0.00110 -0.276 -0.00086 -0.213 -0.00091 -0.227 0.00024 0.00070 2.26 0.6 -0.00105 -0.153 -0.00214 -0.355 -0.00176 -0.292 0.00109 0.00150 2.78 0.8 -0.00268 -0.331 -0.00156 -0.189 -0.00162 -0.203 0.00112 0.00165 2.78 1 -0.00168 -0.164 -0.00142 -0.142 -0.00198 -0.196 0.00056 0.00086 2.26*ThW reported expanded uncertainty of measurement is based on a combined uncertainty multipied by a coverage factor k to provide a level of confidence of approximately 95 %.Runs 1 and 2 are performed to comply with the requirements of ASTM E2309, run 3 is performed to calculate the uncertainty of measurement.

Temperature at start of verification

67.9 0 F Run 1 Run 2 Run 3 Suggested Error Value Applied Indicated Class Applied Indicated 0.2 0.19993 0.200 A 0.20245 0.202 0.4 0.39810 0.397 A 0.40286 0.402 0.6 0.68605 0.685 A 0.60314 0.601 0.8 0.80968 0.807 A 0.82356 0.822 1 1.02568 1.024 A 1.00142 1.000 For runs 1 and2.' the worst Resolution Class is B and the worst Repeatability Class isA Temperature at end of verification

70 0 F Error Class Applied Indicated A A A A A 0.20126 0.40091 0.60176 0.79962 1.00798 0.201 0.400 0.600 0.798 1.006 Starting Point of crosshead

0 in Uncertainty of Make/Model Serial No. Description Cal Agency Calibration Resolution Cal Date Due Date Instron LDS-10 06105014 Linear Gage AA .IANSSON EXTECH 445580 1003552 Thermometer TEKTRONIX The standards used for this verification are traceable to NIST..000013 in 1 °F.00001 in 3-Aug-10 3-Aug-12.I°F 12-Feb-Il 12-Feb-13 CalproSDS version 3.3 REDACTED VERSION YiU-uuu-LUb-i-L-UU-uu1 d-UUU Page bUt oT 1114 Appendix 1U: Calibration certiticates CETIIATE OF CALIBRATION ISSUED BY : INSTRON CALIBRATION LABORATORY DATE OF ISSUE : 30-Jan-2012 CERTTFICATE NUMBER: 340013012110833 Page 3 of 3 Verified By: RICHARD BINFORD SNR.SERV.ENGR, CalproSDS version 3.3 REDALTED VERSION

~bbU-UUU-yU3-UbU--UUUltU-UUU Huge 01"1114 Apni U mirto ettcu Appendix 1U: Calibration CeFtltlCates CERTIFICATE OF CALIBRATION ISSUED BY: INSTRON CALIBRATION LABORATORY DATE OF ISSUE: 30-Jan-12 CERTIFICATE NUMBER: 340013012095410 IINF[ tIL_4j InstronLab code: 200301-0 825 University Avenue Page 1 of 4 pages ID "'R O N Norwood, MA 02082-2643 APPROVED SIGNATORY I T R~Telephone: (800) 473-7838 "Digitally signed by Richard EalFax: (781) 575-5750 sevc euss~nto~o ichoa rd ' Binford Emai: sevlceequets~istra~comU~ItI.C ON: cn=Rlchard Binford, Sc=US, I=Norwood, st=MA, Type of Calibration: @ V Date: 2012.01.30 11:08:19 o -05'00'Relevant Standard: ASTM E4-1 0 Date of Calibration: Customer Requested Due Date: 30-Jan-13 Name: PURDUE UNIVERSITY Address: 550 STADIUM MALL DR.WEST LAFAYETrE,IN 47907 KBROWER@PURDUE.EDU P.Ol/Contract No.: Contact: KEVIN BROWER Manufacturer: BALDWIN Manufacturer. BALDWIN Serial Number, 120BTEC502040 Transducer ID: 120BTEC502040 System ID: 120BTEC502040 Capacity: 120000 lbf Range Type: Single Type: Compression

1. Digital Readout -PASSED This certifies that the forces verified with machine indicator(s) (listed above) that passed are WITHIN +t 1 % accuracy, 1 %repeatability, and zero return tolerance.

All machine indicators were verified on-site at customer location by Instron in accordance with ASTM £4.The certification is based on runs 1 and 2 only. A third run is taken to satisfy uncertainty requirements according to ISO 17025 specifications. The verification and equipment used conform to a controlled Quality Assurance program which meets the specifications outlined in ANSIINCSL Z540-1, ISO 10012, ISO 9001:2008 and ISO/IEC 17025:2005. The testing machine was verified in the 'as found' condition with no adjustments carded out.Instroa CalproCR Version 3.23 The results indicated on this certificate and the following report relate only to the items verified. If there are methods or data included that are not covered by the NVLAP accreditation it will be identified in the comments. Any limitations of use as a result of this verification will be indicated in the comments. This report must not be used to claim product endorsement by NVLAP or the United Staten government. Thin report shall not be reproduced, except in fisil, without the approval of the issuing laboratory, REDACTED VERSION b~W5-UUU-I~iWj-tjbU-UUU~I~.UUU wage ~UU 0? VI14 Appendix w: Lalrnration Certaticates I CCIDTEIIP/ATE: ('Al IDDATIfiklI UI U vf I !, %f U VIrlLi.,U~lfall U fI 'I,11 CERTFIFCATE NUMBER: 340013012096410 NVL.AP ACCREDITED CALIBRATION LABORATORY No. 200301-0Pg o ae Temperature at start of verification: 67.00 0 F.Indicator

1. -Digital Readout (ibf)Range ASTM E4 ASTM E4 ASThI E4 Full Scale Tested Force Range Max Max Repeat Zero Resolution Lower Limit (%) (lbf) Mode Error (%) Error (%) Return (lbf) (IbI 100 -1194.4 to -119044.9 C 0.88 0.1I1 Pass 1 200 Temperature at end of verification:

67.80 0 F.-'s A 4'~ .... .... ". ... ...... ....... .' 2', g ' .&; "-COMPRESSION Run 1 Run 2 Run 3 ASTM E4 Relative Uncertainty of Error Error Error Repeat Error U~ncertainty* Measurement* % of Range (%) (%) (%) (%) (%) (+/- lbf)100% Range (Full Scale: -119044.9 INf)1 0.47 0.43 0.43 0.04 0.14 1.661 2 O.41 0.48 0.49 0.07 0.14 3.321 4 0.42 0.46 0.45 0.04 0.13. 6.213 7 0.77 0.76 0.77 0.01 0.14 11.254 10 0.82 0.75 0.76 0.07 0.14 16.908 20 0.88 0.77 0.78 0.11 0.15 36.187 40 0.81 0.81 0.80 0.00 0.14 64.283 70 0.81 0.80 0.81 0.01 0.14 112.494 100 0.80 0.81 0.81 0.01 0.14 160.702* The reported expanded uncertainty is based on a standard uncertairny multiplied by a coverage factor I = 2. providing a level of confidence of approxhnately 95%.COMPRESSION Indicated Applied Indicated Applied Indicated Applied% of Range (lbf) (b) (INb) (ibI (Ibi) (Ib)100% Range (Full Scale: -119044.9 Ibt)0OReturn 1 0 -1 1 -1200 -1194.4 -1200 -1194.9 -1200 -1194.85 2 -2400 -2390.3 -2400 -2388.5 -2400 -2388.2 4 -4800 -4780.1 -4800 -4777.95 -4800 -4778.5 7 -8400 -8335.52 -8400 -8336.7 -8400 -8336.11 10 -12000 -11902.07 -12000 -1191023 -12000 -11909.74 20 -24000 -23789.98 -24000 -23815.94 -24000 -23815.35 40 -48000 -47615.95 -48000 -47615.36 -48000 -47618.9 70 -84000 -83326.29: -84000 -83333.37 .-84000 -83327.47 100 -120000 -119044.89 -120000 -119034.86 -120000 -119034.86 Instran CalproCR Version 3.23 REDACTED VERSION ~bWs-UUU-UU~-U~U-UUU1U-UUU i~age wiU 0? VFI4 Appendix iu: Lallbratlan LartItacates f'lC r'AI IDDATrIflL ',lglx II U[1 Jfl/ I En %I flfl/ I IVI CERTIFICATE NUMBER: 340013012095410 NVLAP ACCREDITED CALIBRATION LABORATORY No. 200301-0 Page 3 of 4 pages The Return to Zero tolerance Is the indicator resolution, 0.1] % of the maximum force verified in the range, or 1 % of the low ast force ver f/led in the range, whichever is greater.100% Range 1.2 Compression 0.8 3 S ,, 0.4 N-t- Runi1 0 -0_____________________ -Run 2-1.00%*IU -0.4 ______________________________ -1.00%**t ASTM E4 Error Tolerance-0.8-1.2 o o o 0 0 .1 7 " Percent of Range Serial Calibration Make/Model Number Description Agency Capacity Cal Date Cal Due Extech 445580 1003552 temp. indicator Tektronix NA 12-Feb-l 1 12-Feb-13 HBM ML38 90630412 force indicator lnstron NA 21-Jan-il 21-Jan-13 Strainsense 050530 050530 load cell Instron 120000 lbf 10-Dec-10 10-Dec-12 HBM IOKFRR 688077 load cell Instron 12000 1Wf 24-Apr-10 24-Apr-12 Range Lower Limit fbr Full Scale Standard Standard Class (%) Serial Number Mode Percent(s) of Range A / Al (lb,1 100 050530 C 7/10/20/40/701100 5000 /5000 100 688077 C 1/2/4 200 /200 Instron standards are traceable to NIST.The standard Class A lower limit is used for systems with on accuracy of +/- 1.0% and the standard Closs A1 lower limit is used for systems with on accuracy of +1- 0.5%Standard forces have been temperature compensated as necessary. Instron CalproCR Version 3.23 REDACTED VERSION

-'age b1i 0i" 1114ApedxU:airaonertcte AppeFidlX 1U: Calibration Certlllcates CERTIFICATE OF CALIBRATION ISSUED BY: INSTRON CALIBRATION LABORATORY DATE OF ISSUE: 12-Apr-12 CERTIFICATE NUMBER: 516041212091759 Lab code: 200301-0 INS---RON 5 Type of Calibration: Relevant Standard: Date of Calibration: Instron 825 University Avenue Norwood, MA 02062-2643 Telephone: (800) 473-7838 Fax: (781) 575-5750 Email: service requests@instron.com Strain ASTM E83-10 12-Apr-12 Page 1 of 3 pages APPROVED SIGNATORY Jimm\ Digitally signed by Jimmy Warner g II I II I I UI N: cn=Jimmy Warner, c=US,/ \l=Norwood, st=MA, ou=OVR?¢ Reason: I attest to the accuracy A I e I and in~tegnty. of this document Vd -[11 [Date: Customer Requested Due Date: 23-Mar-13[Customer 'Name: Address: P.0./Contract No.: Contact: Purdue University 550 Stadium Mall Drive Civil Room G151 West Lafayette IN 47907 sarahh@purdue.edu Kevin Brower 1 Machine Transducer , .Manufacturer: Serial Number: System ID: Range Type: BALDWIN 120BTEC502040 120BTEC502040 Single Manufacturer: Transducer ID: Extensometer Type: Travel (Tension): Gauge Length: Mode: EPSILON 3543-0800-200T-ST/E89895 Type 1 2 in 8 in Static (Tension)Clsification ,-The following indicators of the extensometer system were verified and classed: Indicator Indicator Range Full Scale System Type Description Units (%) Class I. Digital Readout strain 100 B-i Certification Statement All indicators listed above were verified on-site at customer location by Instron in accordance with ASTM E83.S .,4t The verificationi and equipment used conform to a controlled Quality Assurance program which meets the specifications outlined in ANSI/NCSL Z540-l, ISO 10012, ISO 9001:2008 and ISO/IEC 17025:2005. The testing machine was verified in the 'as found' condition. Instron Calpro Version 3.23 The results indicated on this certificate and the following report relate only to the items verified. If there are methods or data included that are not covered by the NVLAP accreditation it will be identified in the comments. Any limitations of use as a result of this verification will he indicated in the comments. This report must not be used to claim product endorsement by NVLAP or the United States government. This report shall not be reproduced, except in full, without the approval of the issuing laboratory. REDACTED VERSION

r-age b512 or 1114 Apni U a~ainCriiae AppencllX 1U: Calibration Certltlcates PI::DTICIP^Ti: t"tl: PAl mL-I I I I r' I I. VI i i!.ii CERTIFICATE NUMBER: 516041212091759 NVLAP ACCREDITED CALIBRATION LABORATORY No. 200301-0 Page 2 of 3 pages[Summary of Results Indicator

1. -Digital Readout (strain)Range ASTM E83 Full Scale Tested Range System Resolution Resolution Lower Limit (%) (in) Mode Class* (strain) Class (in)100 0.2 to 2 Tension B-i 0.00000 1 A 0.0008* System Class for a range is the worst of the following classes: gauge length class, resolution class, individual point error class, repeatability class and is also based on the measurement capability of the laboratory.

[Gauge Length Measurement and Classification] Nominal Actual Error in ASTM E83 Uncertainty of Gauge Length Gauge Length Measurement Gauge Length Gauge Length Measuremnent*(in) (in) Type (%) Class (in)8 7.9897 Direct -0.13 B-i 0.0062* The reported expanded uncertainty is based on a standard uncertainty multiplied by a coverage factor k = 2, providing a level of confidence of approximately 95%.[Data Summary and Classification] Indicator

1. -Digital Readout (strain)Run 1 Error Run 2 Error RepeatI Uncertainty of% of Fixed Relative Fixed Relative Error[ Worst Measurement*

Range (strain) (% of strain) (strain) (% of strain) (strain) j Class (strain)100% Range (Full Scale: 2 in)10 0o00000 0o1 -0o0001 -0037 0.00001 A 0.000025 20 -0.00003 -0.0541 0.00000 -0.0041 0.000031 A 0.000042 40 0.00003 0.0281 0.00003 0.0341 0.000001 A 0.000079 70 0.00001 0.005 0.00005 0.028 0.00004 A 0.000137 100 -0.00016 -0.064 -0.00019 -0.074 0.00003 A 0.000195* The reported expanded uncertainty is based on a standard uncertainty multiplied by a coverage factor k = 2, providing a level of confidence of approximately 95%.[Data Indicator

1. -Digital Readout (strain)Runi 1j Run 2% fIndicated AppliedI Indicated Applied Range (strain) (in) (strain) (in)100% Range (Full Scale: 2 in)Run Temperature:

73.0 0 F Run Temperature: 73.3 0 F 0 0.00000o1 0.000000 0.000006 0.000000 1 0 0.025004 0.200000 0.024998 0.200010 20 0.049975 0.4000 10 0.050004 0.400000 Instron Calpro Version 3.23 REDACTED VERSION bbU;-UUU-Udi3-~LS~--UUU1b-UUU I-'age b1i o1T 1114ApedxU:alrtoneriits Appenalx 1U: L:allDratlon Certltlcates tIEDTIEIIPATI= flE fPAl II:DATIfltM mum--I I I I -1" I I. !.I l.lllIllU I CERTIFICATE NUMBER: 516041212091759 NVLAP ACCREDITED CALIBRATION LABORATORY No. 200301-0Pae3o3pgs [Data Indicator

1. -Digital Readout (strain)% fRuni 1 Apie Run 2%ojIndicated ApidIndicated Applied Range (strain) (in) j(strain) (in)100% Range (Full Scale: 2 in)Run Temperature:

73.0 °F Run Temperature: 73.3 0 F 401 0.100030 0.800010 0.100040 0.800000 701 0.175010 1.400000 0.175060 1.400040 100 0.249840 2.000000 0.249820 2.000000 Verification Equipment adUsage Verification Equipment: Serial Calibration Measurement Make/Model Number Description Agency Range Cal Date Cal Due Extech 445580 984437 temp. indicator Tektronix NA 28-Dec-il 28-Dec-13 Boeckeler Micrometer 20641 disp. indicator A.A. Jansson 2.00 in 07-Oct-il 07-Oct-12 1398 (ASTM)* Fowler Economy SH9J2879982 disp. indicator AA Jansson NA 20-Apr-10 20-Apr-12 Electronic

• Equipment used for gauge length measurements.

Verification Equipment Usage: Measurement Serial Range Type Number (% Full Scale) Percent(s) of Range Displacement 20641 (ASTM) 100 0/10/20/40/70/100 Instron standards are traceable to NIST and/or other National standards. [Comments] none Verified by: James Warner Field Service Engineer NOTE: Clause 9 of ASTM E-83 states; It is recommended that extensometer systems be verified annually or more frequently if required. In no case shall the time interval between verifications exceed 18 months (unless an extensometer is being used in a long-time test running beyond the 18 month period). An extensometer system shall not be used after an adjustment or repair that could affect its accuracy without first verify'ing its accuracy utilizing the procedure described in this practice.Instron Calpro Version 3.23 REDACTED VERSION bYi-UUU-Ubi3-UW(,-UUU1b-UUU h-'age til 4 o011114ApeixU:airaonettcts Appendix "IU: Calibration Cerl:lllcates CALIBRATION CERTIFICATE Address 86 Seabro Avenue Aniltyville, NY 11701 Website www.kessslerusa.com KESSLER THERMOMETER CORPORATION Telephone 631-841-5500 Facsimile 631-841-5553 E-mail KesslerUSA@aol~com CALIBRATION REPORT FOR THERMOMETER THIS REPORT OF CALIBRATION SHALL DOCUMENT THAT ThE INSTRUMENT DESCRIBED HEREIN WAS EXAMINED AND TESTED IN KESSLER'S CALIBRATION LABORATORY AGAINST NIST TRACEABLE REFERENCE STANDARDS, IN ACCORDANCE TO KESSLER'S PROCEDURE T-2008, WHICH IS BASED ON ASTM E-77-98 (2003) AND NIST PIBLICATION 250-23. THIS CALIBRATION MEETS THE REQUIREMENTS OF ISOIIEC 17025, ANSI/NCLS Z2540-1 -1 994 AND THE ISO 9000 AND QS 9000 SERIES OF QUALITY STANDARDS. CUSTOMER INFORMATION: GILSON COMPANY, INC..Purchase Order Number: P000096475 Date Calibrated: September 20, 2011 INSTRUMENT DESCRIPTION: Next Recommended Due Date: October 20, 2012 Serial No.: 689373 Scale Range: 30/124°F Marked: KESSLER USA Divisions: 0.2°F Catalog No.: 6340-FC Immersion: 3" RESULTS OF PHYSICAL EXAMINATION: ......This instrument was examined under a polarized lens and strains in the glass, if any, were juidged to be minimal and of no detriment to the function of the instrument. The capillary was examined under magnification and no irregularities or foreign material was.discovered. It was determined that this instruent was suitable for calibration. RESULTS OF CALIBRATION: TEST TEMP 32.00 60.00 80.00 100.00 120.00 READING 32.04 60.00 80.20 100.20 120.20 CORRECTION -0.04 0.00-0.20-0.20-0.20 UNCERTAINTY +/-0.06+/-0.06+/-0.06+/-0.06+/-0.06* The above readings were made under magnification and resolved to one tenth of one scale division.* The indications of this instrument cannot be adjusted or modified by ordinary means: accordingly, the readings given in the table above should be considered, in effect to be both "As Found" and "As Left" rfeadings* Laboratory Environment Conditions: Temperature: 25°C +/-+ 5 0 C / Relative Humidity: Between 40% and 60%* All temperatures given in this report are based on the International Scale of 1990 (ITS-90)TRACEABILITY INFORMATION: NIST Primary Standard: Rosemount Model 162CE Serial No. 5058 Transfer Standard: Hart Scientific 1502A Serial No. A 14422 / 547027 Approved By: John Lewis Calibration Performed By: Barbara Plaza Calibration Report Prepared By: RP Report No.: 092011-03 1 REDACTED VERSION

i-'age bib ot 1114ApeixU:alraonettcte Appendix 1U: Calibration (.:ertlllcates CALIBRATION REPORT PI TAPE[Report Number: I02221223040412 Date Issued:] Apr-04-12 Pi Tape Corporation Serial Number: 02221223 Tape Size: 2" -12" 0.0.Actual Findings and Procedure Numbers Tape Reads 4.9000 Over 4.9000" IProcedure 1 Remarks: New Gage Calibration Equipment Used S Gage I Serial Number I Test Date I Due Date I NIST Traceable Report Number 4.9" 102098 *May-12-I1 May-12-12 86903-1 This tape has been checked at one or more points over a calibrated measuring standard. Calibration performed in accordance with ANSI/NCSL Z540-1-1 994, ISO/IEC 17025 and the former MIL-STD 45662A.All standards are traceable to the National Institute of Standards and Technology Jerry Mathis, Quality Assurance Manager This calibration report shall not be reproduced, except in full, without the written approval of the issuing laboratory. Results listed relate only to the item beIng calibrated. Pi Tape Corporation 344 N. Vinewood St. Escondido, CA 92029 USA Phone (760) 746-9830 Fax (760) 746-9196 www.pitape.com Page 1 of 1 REDACTED VERSION

Jl-'age btl 0? A 1 1 4 CERTIFICA T D'ETALONNAGE KALIBRIER-ZERTIFIKA T CALIBRATION CERTIFICATE ~\ 2 N 0 26594 Date Datum Date 13.10.2009 Objet Gegenstand Object Type Typ Model Num6ro de s~rie Serien-Nummer Serial number Instrument vertical Vertikal-Messgerait Vertical instrument V1004+10473 /A Date d'dmission du certificat Ausgabedatum des Zertifikates Certificate issue date 13.10.2009 Ddclaration de confirmit6 L'instrument de mesure auquel se r~f~re ce certificat a et6 conformdment aux donnees techniques de TRIMOS contenues dans les documents de vente (prospectus, manuels d'utilisation). Ko nformititserkliirung Das Messgerat;,auf weiches sich dieses Zertifikat bezieht, wurde entsprechend den von TRIMOS in den Verkaufs-unterlagen (Prospekte, Gebrauchsanleitung) angegebenen technischen Daten hergestellt. Conformity declaration The measuring instrument to which this certificate refers to has been manufactured in acordance with the given TRIMOS specifications stated in sale documents (leaflets, instructions for use).Responsable departement qualit6: Leiter der Qualitatsabteilung: Manager of quality department: Gilbert Villard Contr61eur: Pn~ifer: Inspector: Philippe Desponds La publication ou Ia reproduction de ce document n'est autorls~e que dans sa forme Der Inhalt dieses Dakumentes darf nur in voltstindiger Form ver~ffentlicht oder weitergegeben werden.This document may not be published or forwarded other than in its entire form.Page Seite Page 118 I TRIMOS SA S++41 21 633 01 01 Av. de Longema lie 5 CH-1 020 Ren ens S++41 21 633 01 Switzerland htto://www.trimos.ch mtitiUUU-ubJ-u._i-UUU1 b-UUU l-h'age till ot )l 14 I CERTIFICA T D'ETALONNAGE KALIBRIER-ZERTIFIKA T CALIBRATION CERTIFICATE R MO~I N 26594 Date Datum Date 13.10.2009 Caract6ristique do r'objet mesur6 Merkmale des Gegenstander der Kalibrierung Features of the calibrated object Nornbre d'axes de mesures Anzahl der Messachsen Number of measuring axis 1 Etendue de mesure Messbereich Measuring range 0 -990 mm 0- ?~ci7~A(Coefficient de dilatation lin~aire Linearer Ausdehnu ngskoeffizient Linear expansion coefficient Etalonnage Kalibrierung Calibration Accessoire(s) utilis6(s) Verwendete Zubehore Used accessories Pas de mesure Messstufen Measuring steps Nombre de serie de mesures Anzahl von Messreihen Number of measurement series 11.5 V-1 20 mm t '-3 Principe de mesure Messprinzip Principle of measurement Condition de Referenzbedingungen Reference conditions En montant Antastung aufw~rts Upwards direction Temperatures / Temperatur / Temperature Humiditd relative / Relative Luftfeuchtigkeit / Relativ humidity Pression d'air / Luftdruck / Air pressure La publication ou la reproduction de co document n'est autoris~e que dans sa forina int6grale. Der Inhalt dieses Dokumentes daif nut in volistindiger Form ver(Tffeantliclht oder weitergageben wardenl.This document may not be published or forwarded other than in its entire form.20°C +/- 0.5°C 50% +/- 5%722 mm Hg Page Seite Page 2/8 I TRIMOS SA S++41 21 6330101O Av. de Longemalle 5 CH-1 020 Renens S++41 21 633 01 Switzerland! httD:llwww.trimos.ch I ti~-U-G~-U~5UURt-UU4M-'g bt i CERTIFICA T D'ETALONNAGE KALIBRIER-ZERTIFIKA T CALIBRATION CERTIFICATE N° 26594 Date Datum Date 13.10.2009 Etalon do rMf~rence et traa~bilit6 Bezugsnormal und R(Jckverfolgbarkeit Reference standard and tracability Los r~sultats de mesure contenus dans ce certificat se r~fdrent, par une tra~abilit6 documentf~e, aux dtalons reconnus sur le plan national et dont Ia conformit6 avec le syst~me international d'unit6 (SI) est ddmontrde. L'4talon do rf6frence est composd des dl~ments suivants:* Die in diesem Kalibrierzertifikat erhaltenen Ergebnisse von Messungen sind Bezugs-normale bsw. Einrichtungen auf national Normale rickverfolgbar. Deren Uboreinstimmung ist durch das Internationale Einheitensystem (SI) nachgew~iesen. Das Bezugsnormal besteht aus folgenden Elementen: All measurement results contained in this calibration certificat~e maintain a link, of tracability recognized by national standards. -Teir accordarl( with the international system (SI) is proved. The referonce standard is composed~of the fo/llowing cmp~nents: !Etalon do reference Bezugsnormal Reference standard N° des~re Serien-Nr. Serial no.N" du certi6fiat Zertifikat-Nr. Certificate no.Etalonn6 par Kalibriert durch Calibrated by Chock-Master 800002 81228 Fabricant Equerre 215-904 E310Z106 Kunz SCS Marbre 2000x1800 1644 R402B028 Kunz SCS* Mdtrologie et accre.ditation suisse La publication ou la reproduction de co document n'est quo dans sa forme int~grale. Der Inhalt dieses Dokumentes dart nut in vonlstindiger Form ver~ffentlicht odor weitergegeben werden.This document may not be published or forwarded other than in its entire form.Page Seite Page 3/8 I TRIMOS SA S++41 21 633 01 01 Av. de Longemalle 5 CH-1 020 Renens tt++4! 21 g33 01 0 Switzerland httD://www~trimns.ch ~1-UUU-U-ti~¶i-UUUTh-UUU ~ age tilti O]114 R MOS CER TIFICA T D'ETAL ONNA GE KALIBRIER-ZERTIFIKA T CALIBRA TION CERTIFICATE N 0 26594 Date Datum Date 13.10. 2009 Justesse Richtigkeit Freedom from bias* S~iel* S&1e2 AS&Srie3 I Valeur reelle Wahrer Wert True value mm 0.0000 9.9999 30.0003 50.0004 70.0007 90.0007 110.001 130.0009 150.0009 170.0009 190.0009 S6rle 1 Serie I Series 1 mm 0.000 10.000 30.000 50.000 70.000 90.001 110.001 130.001 150.000 170.000 189.999 S6rie 2 S6rie 3 Serie 2 Sele 3 Series 2 Series 3 mm mm Moyenne Ecart moyen Mittenwert Mittenabweichung Average Average deviation mm n 0.000 10.000 30.000 49.999 70.000 90,001 110.001 130,001 150.000 170.000 189.999 0.000 10.000 30.000 49.999 70.000 90.000 110.001 130.001 150.000 170.000 189.999 0.000 10,000 30. 000 49.999 70.000 90,001 110.001 130.001 150.000 170.000 189.999 0.0 0.1-0.3-1.1-0.7 0.0 0.0 0.1-0.9-0.9-1.9 La publication ou la reproduction de ce document n~est autodts~e que cdans sa forme int~grale. Der' Inhalt dieses Dokumentes dadt nur in vollstindiger Form Vert~ffentlicht oder weltergegeben werden.This document may not be published or forwarded other than in its entire form.Page Seite Page 418 I TRIMOS SA Av.de Longemalle 5 EATD CH-1020 Renens+ +41 21 633 01 01 -+-41 21 633 01 @trimosD h Switzerland htto;//www.trimos.ch

b-UUU tZU at 1 14 CERTIFICA T D'ETALONNAGE KALIBRIER-ZERTIFIKA T CALIBRATION CERTIFICATE N° 26594 Date Datum Date 13.10.2009 Valeur vraie Wahrer Wert True value mm 210.0009 230.001 250.001 270.001 290.0009 310.0009 330.0007 350.0006 370.0006 390.0006 410.0006 430.0006 450.0004 470.0006 490.0003 510.0004 530.0002 550.0002 570.0001 590.0001 610 630 650 670.0001 689.9999 709.9999 729.9997 749.9997 769.9998 789.9998 809.9997 829.9998 849.9997 869.9996 889.9996 909.9998 929.9997 949.9996 969.9995 989.9996 S6rle 1 Serie 1 Series 1 mm 209.999 230,000 249.999 269.998 289. 998 309.999 329.999 349.998 369.998 389.999 409.998 42.9988 449.998 469.998 489.998 509.998 529.997 549.998 589.998 609.997 629.998 649.997 669.998 689.997 709.998 729.997 749.998 769.997 789.997 809.997 829.997 849.997 869.998 889.997 909.997 929.997 949.997 969.997 989.997 S6rle 2 Serie 2 Series 2 mm 209.999 230.000 249.999 269.998 289.998 309.999 329.998 349.998 369.998 389.999 429.998.449.998 S469.998 S489.998 529.997 .569.997-589.998629.998 649.997 669.998 689.997 709.998 729.997 749.998 769.997 789.997 809.997 829.997 849.997 869.998 889.997 909. 997 929.997 949.997 969.997 989.997 S6rie 3 Moyenne Ecart moyen Serie 3 Mittenwert Mlttenabweichung Series 3 Average Average deviation mm mm p 209.999 230.000 249.999 269.998 289.998 309.998 329. 998 349.998 369.998 389.998 409.998 429.998-449.998 469.998!489.998 S52 9.998 S549.998 569.997 589.998.609.997 629.998 649.997 669.998 689.997 709.998 729.997 749.998 769.997 789.997 809.997 829.997 849.997 869.998 889.997 909.997 929.997 949.996 969.997 989.996 209.999 230.000 249.999 269.998 289.998 309.999 329.998 349. 998 369.998 389.999 i409.998 429.998'469.998 S489.998 1 509.99829.997997 , 5!89.998 629.998 649,997 669.998 689.997 709.998 729.997 749.998 769. 997 789.997 809.997 829.997 849.997 869.998 889.997 909.997 929.997 949.997 969.997 989.997 Page Seite Page-1.90-1.00-2.00-3.00-2.90-2.23-2.37-2.60-2.60-1.93-2.60-2.60-2.40-2.60-2.30-2.40-2.87-2.20-3.10-2.10-3.00-2.00-3.00-2.10-2.90-1.90-2.70-1.70-2.80-2.80-2.70-2.80-2.70-1.60-2.60-2.80-2.70-2.93-2.50-2.93 5/8 La publication ou la reproduction de ce document n'est que dlans sa forme int~grale. Der Inhalt dieses Dowumentes dadf nur in vollstindiger Form ver6ffentlicht oder weitergegeben werden.This document may nat be published or forwarded other than in its entire form.I TRIMOS SA Av. de Longemalle 5 CH-1 020 Renens S++41 21 633 01 01 ++41 21 633 01 oFEDACTED VElf~Itrimos,¢h Switzerland httD://www.trimos.ch )agebLz]ot 1114 CERTIFICA T D'ETALONNAGE KALIBRIER-ZER TIFIKA T CAL.IBRATION CERTIFICA TE fRtMOS N° 26594 Date Datum Date 13.10.2.009 R6sultas do mesure Messergebnlsse Measurement results Erreur maximale autorisee Max. Fehlergrenze Maximum permissible error Erreur maximale Gr~sste gemessene Abweichung Maximum error measured 5.8 ptm 3.2 p.rm Fid~Iite Wiederholpraizision Repeatability +/- 2s <2 ji Incertitude do mesure ',. Messunsicherheit

• i ..Uncertainty of measurement L'iceritue d meure"U"indiqu~e pouir la determination erreurs de mesures englobe: l'objet r'~talon de r&f&ence, l'0tendue de mesure et les conditions de r~f~rence.

Die nachstehend angegebene Messunsicherheit "U" fi~ir die Ermittlung der Messabweichungen umfasst folgende Komponente: das kalibrierte Objekt, das Bezugsnormal, den Messbereich und die Referenzbedingungen. The uncertainty of measurement "U" for the determination of the errors of measurement given hereafter includes the calibrated object, the reference standard, the measuring range and the reference conditions. le niveau de confiance est de 95%Das Vertrauensniveau betr~igt 95%Confidence probability is 95%Incertitude de mesure Messunsicherheit Uncertainty of measurement K =2 U 95 = 2.5 jm + (L(mm) / 300 )La publication ou la reproduction do co document n'est autodis~e quo dans so fornme int~grale. Der Inholt dieses Dokumentes dadt nur in volistindiger Form verbffentllcht odor weitergegeben worden.This document may not be published or forwarded other than in its entire form.Page Seite Page 6/8 I TRIMOS SA S++41 21 6330101O Av. de Longemalle 5 CH-1 020 Renens& ++41 21 6330 OlO[EDACTED VEfl~~trimos.ch Switzerland htto:I/www.trimos.ch

b-UUU t-'age t>LZ ot 114 CERTIFICA T D'ETALONNAGE KALIBRIER-ZERTIFIKA T CALIBRA TiON CERTIFICATE R!I N 0 26594 Date Datum Date 13.10.2009 C6ntrole de la perpendicularite ( direction de mesure )Kontrolle der Rechtwinkligkeit ( Messrichtung )Checking of the squareness ( measuring direction )10.0 I I t I-2 ~Q~04Q~__600 700 800 90010-10 Hauteur Hohe Height mm 0 50 100 150 200 250 300 350 400 450 500 Ecart Abweichung Deviation 0.0-1.0-2.0-2.0-2.0-2.0-3.0-3.0-2.0-2.0-4.0 La publication ou Ia reproduction de ce document n'est autorisie que dans sa forme Der Inhalt dieses Dokumentes dalrf flur in vo~llstindiger Form ver~ffentlicht oder weitergegeben werden.This document may not be published or forwarded other thian in its entire form.Page Seite Page 7/8 I TRIMOS SA S++41 21 63301 01 Av. de Longemalle 5 CH-1 020 Renens S++41 21 633 01 0 VE~!tI!;rimos~ch Switzerland http://www.trimos.ch I-age tiuj or CER TIFICA T D 'ETAL ONNA GE KALIBRIER-ZERTIFIKA T CALIBRATION CERTIFICA TE N 0 26594 Date Datum Date 13.10.2009 Hauteur Hohe Height mm 550 600 650 700 750 800 850 900 950 1000 Ecart Abweichung Deviation-4.0-4.0-4.0-6.0-6.0-6.0-8.0-8.0-8.0-8.0 Resultats du contr~le do la perpsndicularit6 ( dane s !direton de mes.* ) : Ergebnisse der Rechtwinkllgkeltprflfung (in MessuiChtun~g)

Resulits of squareness In

....Erreur maximale autoris~e

-Max. angegebene Fehlergrenze

Maximum permissible error -Erreur de la perpendicularit6 mesur~e Gemessene Rechtwinkl igkeitsa bweichung Squareness error measured 12.0 j!tm 8.0 j~m La publication ou la reproduction de ce document n'est autoris~e que dans sa forrme int~graie.

Der inhalt dieses Dokumentes darf nur in volistindiger Form verbffentlicht oder weitergegeben werden.This document may not be published or forwarded other than in its entire form.Page Seite Page 818 I TRIMOS SA S++41 21 633 01 01 Av. de Longemalle 5 CH-1 020 Renens S++41 21 6;33 01 Switzerland htto://www.trimos.chI -tM UU(b3- -UUU I-age b24 Or 1114 AppendllX 1U: Calloratlon Lertmtcates TROEMNER Henry Troemner LLC C libration Certificate 201 Wolf Drive o P.O. Box 870 T"horofare, NJ 08086-0087 oPhone: 856-686-160Q o F~x: 856-686-1601 o www.troemner.com o e-mail: troemner@troemner.com Page 1 of 7 Pages Weight SECTION 1: NAME AND ADDRESS OF CUSTOMER End user Purdue University 1040 S. River Road Bowen Laboratory West Lafayette IN 47907 SECTION 2: APPROVED SIGNATORY Manager SECTION 3: PERSON PERFORMING WORK Daniel Foglio SECTION 4: CERTIFICATE INFORMATION Certificate Number 663 364-1 Date of Calibration 30-APR-2012 Client Precision Weighing Balances 30 South Cross Road Bradford MA 01835-8232 Description of Masses: Grip Handle, Accuracy Class

• NIST 105-1 Class F Date Received Order Number : 100001369

"'Date of Calibration Construction

• Two Piece N, Date of Issue Material
• Cast Iron N5 'Weight Range SECTION 5: ENVIRONMENTAL CONDI'TIONS TEST: 30-APR-20 12: 30-APR-2012
• 30-APR-20 12: 1001b Temperature:

21 .84 0 C Pressure: 769.06 mm Pig--, Relative Humidity: 48%SECTION 6: PERTINENT INFORMATION The Weights listed on this .calibration report have been compared to reference mass standards that are directly traceable to the National Institute of Standards and Technology under Test No. 822-275872-il. Reference standards and balances used to perform the calibration are listed in Section 10.* The weights calibrated for this report have been calibrated in accordance with Troemner's ca~libration process. The calibration performed meets Level III criteria as described in the NIST/NVLAP Technical Guide 150-2.This calibration also meets specifications as outlined in ISO 9001, iSO/IEC 17025, ANSI/NCSL Z540-1-1994, NRC Document 10CFR50 Appendix B, and applicable documents. This certificate of calibration shall not be reproduced except in full, without the written approval of Troemner, LLC. This certificate of'calibration must not be used by the customer to claim product endorsement by NIST, NVLAP or any agency of the U.S. government." ."-,REDACTED VERSION -. u cjL b-uuu -age ot 11 14 Appendix 1U: Lalibratlon (ertificates LKROEMNER Henry Troemner LLC Calibratdon Certific te 201 Wolf Drive =P.O. Box 87

• Thorofare, NJ 08086-0087 o Phone: 856-686-1600 oFax: 856-686-1601 o www.troemner.com o e-mail: troemner@troemner.com Page 2 of 7 Pages Weight*NAME AND ADDRESS OF CUSTOMER End user Purdue University 1040 S. River Road Bowen Laboratory West Lafayette

[N 47907 Certificate Number 663364-1 Date of Calibration 30-APR-20 12 Client Precision Weighing Balances 30 South Cross Road Bradford MA 01835-8232 SECTION 7: TRUE MASS (MASS IN VACUUM) CALIBRATION DATA Nominal Mass Value.Serial Number Density'of Weight Uncertainty (+ or-)True Mass 100 ib 45362.709 g 7.2000 g/cm 3 450 mg y N I Density is assumed unless otherwise stated REDACTED VERSION UU (, -bIUUUllb-uuu Page bJ~b ot 1114 Appendix 1u: Calibratlon LSertmcates TROEMNER Henry Troemner LLC Calibration Certificate 201 Wolf Drive °P.O. Box 870o Thorofare, NJ 08086-0087 o Phone: 856-686-1600 o Fax: 856-686-1601,o www.troemner.com o e-mail: troemner@troemner.com Page 3 of 7 Pages Weight NAME AND ADDRESS OF CUSTOMER End user Purdue University 1040 S. River Road Bowen Laboratory West Lafayette IN 47907 Certificate Number 663364-1 Date of Calibration 30-APR.2012 Client Precision Weighing Balances 30 South Cross Road Bradford MA 01835-8232 SECTION 8: MASS IN AIR CALIBRATION VALUE VS, REFERENCE DENSITY 8000 kg m-Nominal Mass Value Serial Number Conventional Mass Value 45361. 953 g Uncertainty (+or-)Tolerance (+ or-)4. 5000 g 100 lb 450 mg\REDACTED VERSION -J L-L-UUUllb-UUU I-'age or 1114 Appendix 1U: CSalibration C:ertitcates LKROEMNER Henry Troemner LLC Calibration Certificate 201 Wolf Drive oP.O. Box 87 oThorofare, NJ 08086-0087 oPhone: 856-686-1600

• Fax: 856-686-1601.

www.troemner.com o e-mail: troemner@troemner.com Page 4 of 7 Pages Weight NAME AND ADDRESS OF CUSTOMER End user Purdue University 1040 S. River Road Bowen Laboratory West Lafayette IN 47907 Certificate Number 663364-1 Date of Calibration 30-APR-2012 Client Precision Weighing Balances 30 South Cross Road Bradford MA 01835-8232 SECTION 9: MASS IN AIR CALIBRATION DATA VS. REFERENCE DENSITY 8000 kg m-Nominal Mass Value Serial Number Conventional Mass Correction Uncertainty (+ or-)450 mg Tolerance (+ or-)4. 5000 g i00 lb 2716 mg N Ad REDACTED VERSION Y -UUU -. I-'age b2z5 Ot 11 14 Appendix 1U: (Jalibration C~ertmtcates IROEMNER Henry, Troemner LLC Calibratdon Certiflcate 201 Wolf Drive o P.O. Box 870o Thorofare, NJ 08086-00870o Phone: 856-686-1600 o Fax: 866-686-1601 ° www.troemner.como e-mail: troemner@troemner.com Page 5 of 7 Pages Weight NAME AND ADDRESS OF CUSTOMER End user Purdue University 1040 S. River Road Bowen Laboratory West Lafayette IN 47907 Certificate Number 6633 64-1 Date of Calibration 30-APR-20 12 Client Precision Weighing Balances 30 South Cross Road Bradford MA 01835-8232 SECTION 10: CALIBRATION PROCEDURE DATA Nominal Mass Value Serial Number Standard Cal Set No. Due Balance Used Cal Due Procedure Used 100 lb Sl104 05/31/12 XP64003L-A01 11/30/12 Multi A-B A 1 .'1 REDACTED VERSION

I-'age rdZ90t q 114 Appendix 1U: Calibration Certltlcates L<TROEMNER Henry Troemner LLC CalibratinCriia e~lboOO3 201 Wolf Drive

• P.O Box 870 Thorafare, NJ 08086-0087
• Phone: 856-686-1600 o Fax: 856-686-1601
• wvww.troernne~corn o e-nail: troemner@troernner corn Page 6 of 7 Pages Weight Certificate Number 663364-1 NAME AND ADDRESS OF CUSTOMER Date Of Calibration 30-APR-2012 End user Client Purdue University Precision Weighing Balances 1040 S. River Road 30 South Cross Road Bowen Laboratory Bradford MA 01835-8232 West Lafayette IN 47907 SECTION 11: GENERAL INFORMATION This calibration was performed in Troemner's High Precision Level I Mass Metrology Laboratory at 201 Wolf Drive, Thorofare, New Jersey 08086 unless otherwise noted on page one. The internal procedures used are CAL-CLASSI and NIST HB 145.SECTION 12: DEFINITIONS AND TERMS MASS IN A VACUUM -The mass of a weight as if it were measured in a vacuum. Also known as True Mass.MASS IN AIR -The conventional value of the result of weighing in air, in accordance to International Recommendation OIML D 28. For a weight taken at 200 C, the conventional mass is the mass of a reference weight of a density of 8003 kg~m" 3 which it balances in air of a density of 1.2 kg~m-3.AS FOUND MASS IN A VACUUM -The ~easured value of the mass(es) as they were receivdbrrenr AS LEFT MASS In A VACUUM -The value of the mass(es) after-they were adjusted,:repaird-

.or replaced when necessary. The As Found\"Mass in a Vacuum willequal the As Left Mass in a ,--;::,;, if the mass(es) did not require adjustm.ent, or replacement. -.:. .--.NOMINAL MASS -The mass value-isg marked on the w ight."...'....." CORRECTION -The difference between the mass value of a we~ight..and its nominal value. A positive correction indicates that the mass value is greater than the nominal value by the amount of the correction. AS FOUND CONVENTIONAL MASS CORRECTION -The conventional correction of the result, as it received by Troemner, of weighing in air in accordance to International Recommendation D 28. ForI a weight taken at 20° C, the conventional mass is the mass of a reference weight of density 8000 kg.m 3*. which it balances in air density of 1.2 kg'm -3 If the customer requires cleaning prior to clibration,; the after cleaning correction would be reported. AS LEFT CONVENTIONAL MASS CORRECTION -The conventional correction of the result, after moent repair, or replacement of weighing in air in accordance to International RecommendationiD 28.g a weight taken at 200 C, the conventional mass is the mass of a reference weight of density 8000 3 which it balances in air density of 1.2 kg~m 3.The As Found will equal the As Left Conventional Mass Correction if the mass(es) did not require adjustment, repair or replacement.(continued on next page)REDACTED VERSION Y-UUU ci-Uuu UUl -'U age ot 1114 Appencdlx 1u: Calibration Certitcates TROEMNER 7 Henry Troemner LLC I;201 Wolf Drive oP.O. Box 87 o Thorofare, NJ 08086-0087 ° Phone: 856-686-1600,a Fax: 856-686-1601

• www.troemner.com, e-mail: troemner@troemner.com Page 7 of 7 Pages Weight Certificate Number 663364-1 NAME AND ADDRESS OF CUSTOMER Date of Calibration 30-APR-2012 End user Client Purdue University Precision Weighing Balances 1040 S. River Road 30 South Cross Road Bowen Laboratory Bradford MA 01835-8232 West Lafayette IN 47907 SECTION 12: DEFINITIONS AND TERMS (continued)

UNCERTAINTIY -The standard deviation associated with the result of the measurement that characterizes the dispersion of the values that could reasonably be attributed to the measurand. The uncertainty is calculated in accordance with NIST TechNote 1297 / UKAS M3003 using a coverage factor of k = 2 (k= 2 defines an interval having a level of confidence of approximately 95 percent). The uncertainty does not include possible effects of magnetism. -Defines the limits in which the correction value and the uncertainty must fall to meet the tolerance specification for the given Class.AS FOUND CONVENTIONAL MASS VALUE -The measured value of the mass(es) as they were received by Troemner, of weighing in air in acc¢ordance to International Recommendation OIML D 28. For a weight taken at 200 C, the conventional mass is the \'nqass of a reference weight of density 8000 kg~m" 3 which it balances in air density of 1.2 kg~m-3.If the requires cleaning prior to calibration, the after cleaning value would be reported. F denotes Out of Tolerance Weight.AS LEFT CONVENTIONAL MASS VALUE -measured value of the mass(es) after they were adjusted, repaired or replaced when necessaVy-sf air in accordance to International Recommendation OIML D 28. For a weight taken at* the Conv~nftio~nal Mass is the mass of a reference weight of density 8000 kg.m'3 which it balances in air density of 1.2 kgrmn The As Found will equal the As Left Conventional Mass Value if the mass(es) did not require adjt~stmnent, repair or replacement. ASTM E617-97 -Weights meet the tolerance specification for ASTM E617-97. Weights 2kg -I g screened for magnetism using a Gaussmeter. REDACTED VERSION

l-age t531 0! 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix LU: Calibration (Jertificates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue University Sheet Ilof 2 Calibration Instrument Name and S.N.: Instron 1044172 Data Acquisition System: OptroTrack Pro Series 600 Gain: NA Excitation Voltage: NA Channel: NA Sensor: OptroTrack pro Series 600 Sensor S.N.: _________OptroTrack Pro Series 600 Input [in.] Output [in.] Input [in.] Output [in.]0 0 6.5 6.507 0 0 6.5 6.507 1 1.001 _____ __ 4 3.999________ 1 1.001 _____ __ 4 3.999________ 4 3.998 _________1.5 1.499 4 3.997 ________1.5 1.498 6.5 6.502 _________ _ _ _ _ _ _ _ _ __ _ _ _ _ _ _ _ ____ ____6.5 6.502 ________ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ____ ____9 9.007 __ _ _ _ _ _ _ __ _ _ _ _ _ _ __ _ _ _ _ _ _ __ _ _ _ _ _ _9 9.007 ____ ___Operator Sig nature Date Time Chce y intreDt ime~Checked by Signature Date Time Sensitivity Accuracy 1euls0.007 in.REDACTED VERSION bbEJ-UUU-U~tl4-UWI:-UUUIU-UUU P'age b;.t2 oT 1"114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 1U: CaliDration Lertlricates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue Sheet 2 of~Notes: The accuracy of the INSTRON sensor is 0.003 in.REDACTED VERSION Page bi at 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 1U: Calibration Certitcates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue University Sheet I of i.Calibration Instrument Name and SN'.: Data Acquisition System: /\31." t ?CJ 02.3 Gain: I Excitation Voltage: Channel: MVQ " Sensor: PA HJ1G- D-L3M Sensor S.N.: 3IJ100 0 Measurand Voltage Measurand Voltage Measurand Voltage ,4oZU 0.03 ____2____4,553 0°&75 ___________ Operator Si nature Date Time Checked by Signat ure Date Time Checked by Signature Date Time Sensitivity Accuracy Results__ _ _ _ __ _ _ __ _ _o.1 %Notes: REDACTED VERSION

l-UUU I-age ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix LU: Calibration Certificates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue University Sheet Ilof I Calibration Instrument Name and S.N.: 1044-172-Data Acquisition System: -(1 tOQO ?"'I Gain:__________________________ ExcitationVoltage: ___________________________ Channel: l i" Sensor: ?A"2Ot" iJC" Sensor S.N.: _______ 37i~910_______ ______Measurand Voltage Measurand Voltage Measurand Voltage__,____ 1.35 _ _ _ _4. 0/A I Operator 'ignature Date Time Checked by Sig ur Date Time Checked by Signature Date Time Sensitivity Accuracy Results 6, o. °I%Notes: REDACTED VERSION

I-age oT 11 14 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendilx 1u: Lalidration Lertlticates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue University Sheet i of 1 Calibration Instrument Name and S.N.: 1044 I72, Data Acquisition System: I -1000 P&i :) 2$Gain: I Excitation Voltage: -3333 Channel: Hv I -2 Sensor: BA -10 2L°___________ Sensor S.N.: 40 0k8 _______________ Measurand Voltage Measurand Voltage Measurand Voltage6.447 __ _. ____ __ _40,,o0 ______Operator Signature Date Time Checked by SgaueDate Time Checked by Signature Date Time Sensitivity Accuracy ResulIts__,___ ______ 3°/-Notes: REDACTED VERSION

-'age bil ot 1114 Project: Tests to Determine the Behavior of Spliced U11 Bars Appendix iU: C~alo~ratlon L~ertitlcates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue University SheetlIof 1 C)Calibration Instrument Name and S.N.: 1-/i'T1 /,O 4 1Z 04 !4 12-Data Acquisition System: MIJ PC. I 6'2 Gain: "I Excitation Voltage: 3. 3:3 Channel: M J-o"3 Sensor: P)A- IC-___ ___ Sensor S. N.: _ _ __ 400oI09&5_ _ _ __ _ _ _Measurand Voltage Measurand Voltage Measurand Voltage____ ____~4 O2.5 Operator ii~gnature Date Tim e s-.p. -z Checked by Signature Date Time Checked by Signature Date Time Sensitivity Accuracy"Results Notes: REDACTED VERSION

I-'Uage ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 1U: Lalibration Lertiticates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue University Sheet l of 1 i Calibration Instrument Name and S.N.: IIJSTO/') 044172 Data Acquisition System: $ [X 11O00 P;CI Gain: __________________________ Excitation Voltage: 3), 355 Channel: 2 Sensor: RA -__________ Sensor S.N.: ______ 4o010 l 77 ______Measurand Voltage Measurand Voltage Measurand Voltage g4.2 0_ 2~.5qo____ 4.bo7 !o33t _ __ _Operator Si nature Date Time sip,.Checked by Signa lre Date Time Checked by Signature Date Time Sensitivity Accuracy Results 3, Notes: frjZ-o REDACTED VERSION

I-age bad oT 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 1U: Lailibration C~ertlTicates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue University Sheet 1 of 1 0©Calibration Instrument Name and S.N.: '" l0 e..-j H V?':.. -Data Acquisition System: t'JQ-- -S C 4T -1000 ['C-T Gain: .00 Excitation Voltage: !. " .Channel:/" -0 Sensor SN: _ _ _ _ _ _ _ _ _ _ _ _ _Measurand Voltage Measurand Voltage Measurand Voltage.0.02o 153B -0,00600:25.3 -o0,00____0 30.LI -0,0I~~ _____________ Operator S gnature Date Time Checked by igaueDate Time Checked by Signature Date Time Sensitivity Accuracy Results__ _ _ _ _ _ --K// O. 1%Notes: REDACTED VERSION

P'age biU oT "11 14 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix iU: C.alibration C~ertitcates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue University Sheet Ilof 1 Calibration Instrument Name and S.N.: --0!~ /42t Data Acquisition System: PC--,"* Gain: /00 Excitation Voltage: I 0 Channel: --Sensor: ________ Sensor S.N.: H- Measurand Voltage Measurand Voltage Measurand Voltage 0* 0 _ _i5.5 -0~o~bot5 ____ __ _____1Q.5 -0.00605-0-.5 uO, o _ __ __ __ __Operator Sign~tu~re -Date Time Checked by Signature Date Time Checked by Signature Date Time Sensitivity Accu racy Results -2%53K/v O. t%Notes: REDACTED VERSION

I-sage 4Uu oT 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 1U: CaIlibration Lertitlcates Calibration Documentation v.1 (Rev. 04/02/ 2012)Bowen Lab -Purdue University Sheet l of i Calibration Instrument Name and S.N.: 10441 72.Data Acquisition System: ?CI GZS9 Gain: Excitation Voltage: , Channel: M3O Sensor: .LUCAS -2Oo____ ___ ___ Sensor S.N.: __ _ _ __ _ 7250 _______ __ _ _ _ _Measurand Voltage Measurand Voltage Measurand Voltage I.35 -4.272 _________1. 500 -______.oo -o.25 ____ ____ ____2.t533_ ___0, 2-.5 __.__ ___ __Operator ignature Date Time Chckd ._ _ _ _atreDae _m Checked by Signature Date Time Sensitivity Accuracy Results Notes: REDACTED VERSION

I-age b41 ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 1U: Calidration Ldertilicates Calibration Documentation v.1 (Rev. 04/02/ 2012)Bowen Lab -Purdue University Sheet 1 of 1 Calibration Instrument Name and S.N.: 1W04i 72.Data Acquisition System: H" -100O0 Gain: I Excitation Voltage: 3 Channel: frI.3 1 Sensor: LUCA 2o000____________ Sensor S.N.: ________ 7251 _______Measurand Voltage Measurand Voltage Measurand Voltage 0.12Z5 4.1,..0 _ _ _ _ _ _ _ _ _ _ _ _ _ _0.5q7 __ __._ __ _ _ __ _ __ _ _o.}1f o.ozo_____ L.5o0 -2,4.14_____ ________, __ -4..02A5 _ _ _ _ _ _ _ _ _ _ _Operator Signature Date Time ChcedbPDt Tm Checked by Signatu re DaeTime Sensitivity Accuracy*Results Notes: REDACTED VERSION

b-UUU I-age b4z or 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 1U: C:alidration Lertitcates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue Universit' Sheet l of : Calibration Instrument Name and S.N.: ?U! D 10g!4I4'2. Data Acquisition System: MN, Scd.%-I 1000 I1 B Gain: I Excitation Voltage: 5. V Channel: Mt-0(Sensor: 'PA _ _ _ _ _ Sensor S.N.: __ _ _ _ _ _ _ _ _________0 Measurand ,Voltage Measurand Voltage Measurand Voltage 0.5/f o.95 __ _ __ __ __ _ __ _ _ _ _ _ _ I. i _ __-_ __ _ _ _ __ _ _._ _ _ _ _ _ _ _ _Operator Signature Date Time Checked by Signlature Date Time Cekdb .... -Signature Date Time Sensitivity Accuracy Results Notes: ~ u e.o' 4+ .% /D~ vi ~ 4 iw j 2-emx- r s 3 //REDACTED VERSION

b-UUU r-age ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars.Appendix 1U: (Caliaration Lertiticates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue Sheet i of 1 Calibration Instrument Name and S.N.: I N.ST 6-c N 109 4 I Data Acquisition System: KNh $C')(1 1000 ,SN IlI Gain: Excitation Voltage: 3 *3 53 \Sensor: _______ Sensor S.N.: _________ T00L' _______Measurand Voltage Measurand Voltage Measurand Voltage 4.5 ___._ __ __0.5 _____ _____ ____Operator Signature Date Time Checked by Signature Date Time Sensitivity Accu racy Results Notes: ,,4o -o.,°I REDACTED VERSION bbU3-UUU-ULi-(,U-UUU1 b-UUU Page OT 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendlx iu: Callbration (Certltlcates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue Universit'3 Sheet 1 of~Calibration Instrument Name and S.N.: I NJ N 1 0441 ',2_Data Acquisition System: NI[ S-C.) 1 1O0O 0 Gain: Excitation Voltage: Channel: M l- 2.Sensor: P,________ Sensor S.N.: ___0______ 0t Measurand Voltage Measurand Voltage Measurand Voltage 2 .5 (.2IOZ. G______-, I.8? __ _ _ __ _ _ __ _ _-_ _ _(o.5 2. .t__ __ ____ __Operator Signature Date Time Checkd by ignatre Dae Tim Checked by Signature Date Time Sensitivity Accuracy ResulIts Notes: Devickova." 0.2-%REDACTED VERSION bU-UUU-UbJ-UIU-UUU1Ii-UUU l-age b4b ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 1U: Calibration Certlticates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue Universit% Sheet 1 of :1 Calibration Instrument Name and S.N.: I \ , I A41 " TZ Data Acquisition System: 1000 11S86O0]Gain: Excitation Voltage: V Channel: __ _ __ _ __ _ __ _ __ _ __ _ __ _ __ _Sensor: PA -10_____ ____ SensorS.N.: __ __ _ __ _ __ _ __ __ _ __ _ __ _ __ _Measurand Voltage Measurand Voltage Measurand Voltage'I 8 _. _4.5 1.8~5 _ _ _ _ __ _ __ _ _ _ _Operator Signature Date Time Cheke by SignatueDatefTim Checked by Signature 'Date Time Sensitivity Accuracy Results_____________ .o?3. \JJ,/V\ 0.o3 %.'Notes: REDACTED VERSION

Irage b4g Ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 2U: Calibration Certllticates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue Sheet 1lof I Calibration Instrument Name and S.N.: _____ -______________0 __41 __________- Data Acquisition System: -C,)( c000 (IS 6(01 Gain: ___________________________ Excitation Voltage: 3. ; N Channel: t'A2- 0 Sensor: _______ Sensor S.N.: ____OO___O__ 4oo-Measurand Voltage Measurand Voltage Measurand. Voltage c3..54 ___._.__4.5" ' .841_ _ _ _ _S ." __ __Operator Signature Date Time Checed y6SgnaureDat Time__Checked by Signature Date .Time Sensitivity Accu racy Results__ __ __ _ __ __ _o.. o.____ I_ ___ _Notes: REDACTED VERSION bbY3-UUU-L.i-L5-L(-UUUlh-UUU l-'age b4( ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendlx 1Ui: Calibration Certiticates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue University Sheet l of I Calibration Instrument Name and S.N.: I ~\ .STE-o N 1044 [? 'Z Data Acquisition System: .SC X-I I00 t6 Gain: O00 Excitation Voltage: I OV Channel: Sensor: 44 3'_______ Sensor S.N.: 44 ______ ______Measurand Voltage Measurand Voltage Measurand Voltage-04-.1~o=0 0 sk -j-o, -0.002.1i Iok+-t-o4 -o.oo4,o _____I4-.6k--o., -o oo5s _____I9.04+o.1t -o.oo'8- _____ _____a4.ik+/- 04 -o.ooo~sg4 -o.Olla ____ ____ ___Operator Signature Date Time Checked by SDate Time Checked by Signature Date Time Sensitivity Accu racy Results_____________ -I. 5Thv iV/V @FSV o_______Io__ Notes: b'I~o r/ "a 5//a REDACTED VERSION bIUj-UUU-ULSJ-UIU-UUUIh-UUU H'age tbq. 071114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendix 1U: Calibration Lertinlcates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue Universit% Sheet 1 of I Calibration Instrument Name and S.N.: I N STZ-O A 104 41 ? 2..Data Acquisition System: .Scx 1000 GO7" Gain: 1O00 Excitation Voltage: 1 0 V/Channel: -Sensor: 4~4Z.__ _ _ _ _ _ Sensor S.N.: Measurand Voltage Measurand Voltage Measurand Voltage-o.,4+/-o.4k o~ooool ____ ____ ____4.J 0 5 -jo'I-oR __ __ __ __ _ _ __ _ _ __ _ __ _ _1%.1 k +o.4 -o.oo~ ______ _____04 -oom o_Operator Signature Date Time Checked_____by __ Signa____ure613Dae Time__Checked by Signature Date Time.Sensitivity Accuracy ResulIts Notes: LDev-v, 0,,. .2 REDACTED VERSION Project: Tests to Determine the Behavior of Spliced #11 Bars AppendilX LU: Calioration Certlrlcates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue Universit3 Sheet I of I Calibration .Instrument Name and S.N.: ) NJ ST NJ 104 4 1 : 'Data Acquisition System: NI ,SC)I 1000 Gain: I Excitation Voltage: 3 0 V/Channel: F -Sensor: LUCAS DODT -+-Z.."__ __ _ __ _ Sensor S.N.: JgZ O __ _ __ _ __ _ ___0_ _Measurand Voltage Measurand Voltage Measurand Voltage 1.5 ' -_ .__- _-1 ,,"_ __1 .o o .1 1 2 ._ _ _ _ __-_ _ _0.51 2. 4'_ __ _ _ _ _ __ _ _Operator Signature Date Time Checked_____by _Signature____ Date; '5Time Checked by Signature Date Time Sensitivity Accuracy Results Notes: Dvoiv.j 2 w /I' 4 REDACTED VERSION IibU ot 1114 Project: Tests to Determine the Behavior of Spliced #11 Bars Appendilx 1u: Lalibration C=ertli"lcates Calibration Documentation v.1 (Rev. 04/02/2012) Bowen Lab -Purdue Universit% Sheet l of 1 Calibration Instrument Name and S.N.: INilS-T 1044[ Data Acquisition System: N I SX{ 1 I000 II SS 60 l" Gain: I Excitation Voltage: Channel: 1\11-- I Sensor: LUCA.-& bCJT ____ ___ ___ Sensor S.N.: ,__ __-___ ,. .25j __ _ _ _ _ _ _ _ _ _ _ _Measurand Voltage Measurand Voltage Measurand Voltage 0. 4A- . ______1.0" 0,1410 Operator Signature Date Time Checked by Signature Date Time.Checked by Signature Date Time Sensitivity ..Accuracy Results Notes: D v~ i' -REDACTED VERSION bbi-UUU-Ud::J-U.5"U-UUUIIh-UUU t-'age 1bl 1" o 1114ApeixU:alrtonettcte AppencllX 1u: Lallbratlorl Lertltlcates ! :~T I--t I r-r I F F- -- .-5 --REDACTED VERSION FIRST LOADING REDACTED VERSION FIRST LOADING REDACTED VERSION FIRST LOADING GIRDER A6-40 kip REDACTED VERSION RELOADING REDACTED VERSION RELOADING NoIRDEloAd GIRDERA3 (iIKUEK A4 -41 KIp REDACTED VERSION RELOADING GIRDER A5 -42 kip REDACTED VERSION FIRST LOADING REDACTED VERSION FIRST LOADING REDACTED VERSION FIRST LOADING REDACTED VERSION RELOADING No reloadI::Z -Loaa = ib Kip.REDACTED VERSION RELOADING 1 C~IRLThK 133- Load = 3b kip NoIReload4 GIRDER B4 REDACTED VERSION RELOADING GIRDER B5 -24 kio.REDACTED VERSION

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Tests to Determine the Behavior of Spliced #11 Bars Instrumentation Documentation v.1 (Rev. 04/01/2012) Specimen: A -I Sheet __ __of I Data Acquisition System: Channel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location Comments C) /11-o ( 3.3g3 OA-p-o -.': -Vt:2-zr Mj.o,-L 2.?-z5 I MI-I I " " 3Thoo't~ -6. I7- -l1=.o2 S. " .,S 2 I ', A-IO '-oolc5'r6, 3.'~l-5 !,% N5lc- 0,3l:t-.,2 3 hI-3 I " " 4oioioii 3.i6'=t 'f " b 2--0. I ____1__5 ",:-3! J 0..23 ,5 100 i0 '-,P1O 43 -______ o0,2D'C1 J, -. , /t1 1 oO 10 ___-- __ _.-_-___.__!l< s -_______m r-'v-o 3o 2_0 ooos -0o(30 "I 2'2-1O. o OOO So ." o., oooO Operator Signature Date Time Checked ___by__Signature_ 6 Date Time~'Checked by Signature Date Time Notes: 12-1 REDACTED VERSION v$*0 p~o~1 ~243~4*5 I.-id , .-- I-4 -I 4-U.- ;.---- ; --4----1;----I~--U- ... --U- --I~ -m -U -4 Noth III* qF *f 12 13 1 ! 15'I IF qF I-I '4II- II l --I -I I, I l- U I. --lI 4 4-2@10--20 A @520_ r 4 10Q10:100 r 4 1 4 E_1 _4 5=20_ 1 '21=-0 1 I--!I-.Back 4 Front 45qm Wv .... J ,4 I Specimen A -I LAORTRY Behavior of Lap Splices of No. 11 Reinforcing Bars 12-2 REDACTED VERSION Project: Tests to Determine the Behavior of Spliced #11 Bars Instrumentation Documentation v.1 (Rev. 04/01/2012) Specimen: Sheet I of _____Data Acquisition System:-,.T v Channel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location Comments 0 11I-O 1 3.333 'A-.20 3=,IOo~o -6.197-r -l::.oft ______- _ __ __ _ __ _, _ __ __ _ 3TlOOq -6,16=7- -jI-, I , " ;2 hlI-2 ____ "___ PA-Io ,9OOIOc 3.R-S i.2zr tJ.5Yv4 0.3B%3 14I-3 I r,"'40tolo~'=I O .4&O_____-_ I " ot~f' 3.17-3 O.qIi O,3!!9 frl2-; [6O JO L_.it,.soK ____-__5 0.3DeI -o.ooo'oo 4 10-0Lo 10 _____ L.-t2 -0.L[wJ s. =7- 113-0 ( 3o Lw'c.c 2. -J7-:2SO 0.0OO1 0,013 ht13-I I 30 "___ T+2Sz1 ,.209 -o,0oof $. "-o.5 OprtrSgaueDate Time Checked by ~SignatureDaeTm Checked by Signature Date Time Notes: 12-3 KEILAL I FU VLIOIbUI'J i i f I f , I 6.1 , Ii 9 A 6* qr *

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Reinforcing Bars Date: /31/.2.12 -4 REDACTED .VERSION Project: Tests to Determine the Behavior of Spliced #11 Bars Instrumentation Documentation v.1 (Rev. 04/01/2012) Specimen: A-3 Sheet I of i*Data Acquisition System: j- PIe. s/lq/1l ?jeqet Channel # Gain Excitation V. Sensor S.N. Sensitivity \ ZrOfset Location Comments O u-c1- i 3.333 PA-2.0 -g*lt:- I t1l-I ______ 3Thloo~' -6;. I: -(7u.13 5. " .-2 tlI-.2 " °A-IO ffooioQ 3.1I/- LI19 _______ ___,__3th11-3 I " " ooio~cuq 3.6 O.clO l,¢:s= ______--- ____ "___" .I. 5 O, 362.5 p~-j2- (00 10 Le~ocwSOK '-I'13 -- .5S56 -o~ocoo3f T¥ -30 o .4-0,oigI 5o am T"-2s- -O.OOI iS. OO Operator SgaueDate Time S Checked .by Date Time Y.N-. I .'.-i.., -_ __ _ __ _Checked by Time N otes: 12-5 i REDACTED VERSION I I i_2@10--20 i 4@:2 10010:100 _1405=20 i ~2@10:20 ,_~ Back e=Front-.-349' l6fL.LAB RA OR Behavior of Lap Splices of No. 11 Drown by: Checked by: vA'_____. ____________ Reinforcing Bars Date: /"12 -6 REDACTED VERSION U 0 0 A-N Project: Tests to Determine the Behavior of Spliced #11 Bars Instrumentation Documentation v.1 (Rev. 04/01/2012) Specimen: Sheet I of !Data Acquisition System: Channel # Gain Excitation V. Sensor S.N. Sensitivity ZrOfset Location Comments I I " 2-(~ -l=/-.HS $. " 2- -I-2 1 ____ IP#--0 '1oo1o0t' 3.1=/-5 __,__ IkJSrFe."E O.'f'3 tIt-- " qoojo7j 3.1'? o.'a¢ _______, L 1M12-- ___ ____ "___ ~,i?3 1.0.5 5.%,; 0.3.32.S M.2--2.' 100 )0 0K -c.5( IJ RJ A.. 6 /t 2-3 100 10 _____ L,LI 0 ;5= ,3C1 s.g&- -o.c5~oss_____ _-0__ 30 L~s 2 J-.2:50 0.. 2- O.O ____._oA O o g h -I! 30 ____ Q o -o~ooTh 5. " -oxo3s1 Operator Signature Date Time Checked by Signature Date ..Time Checked by Signature Date Time N otes: 12-7 U 0!2 I1=2I4 =2 141014 'Back 45= Front_ 1BfL LAB RAOY Behavior of Lap Splices of No. fl PURDUE: Reinforcing Bars 12-8 REDACTED VERSION U Specimen: /-A -- $Project: Tests to Determine the Behavior of Spliced #11 Bars Instrumentation Documentation v.1 (Rev. 04/01/2012) Sheet -l of Data Acquisition System:_,_ /,,T v Channel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location Comments 0 ,-1l-0 PA-.Do :-Ioo~o -q¥ -lht,0o u.o¢ 3 I M-'I-i _____" -6.16=/ -f16,fV 5. " 2.3-5o 2. Mj-2 ____" cloolOerS( 3.1=-5 [,10 __,_l,__ cO3Lqci, ,, 90 0 1cj991 3.1c C , /'- -42,.3,,. O. 2z LfjM2-O I ,-tQooc(3ql' 3.1F?3 _,____ L. pI65a= S ttL- oo IC Le OA:::( HI /3 -______* c3.2fl P. -0oo 4o P -3 LOO 10 ______ -______ C.2-[)<] 5. " -ooog g M3-1 j 30 " V¥5I 0.:201 -0,oo5 '5. " ,06i!Operator Signature Date Time Checked by Date Time Checked by ture Date Time N otes: 12-9 ©12-10 REDACTED VERSION U Project: Tests to Determine the Behavior of Spliced #11 Bars Instrumentation Documentation v.104/01/2012) Specimen: A -0 Sheet I of.J..Data Acquisition System: Channel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location Comments 0 [-0 1 3.333 PA -~- -6,i _____- __'___ _,__0 I I -I I ,,3 -6& ,6 -~--L0 ______. _.__-_3o MI -I ii "t '-tC 1 QQ 0 O9 3,j(:c1 o______- Mokt'sp,,,. 0, ..;" Hftr1.O I ,,f,0,0o1c09f 3,F?3 Oo.,Syl('c-C O, 3i4 4 /12-3 coo 10 £-IL-2 --2s63 e--e -CK S. -.,ooao_34 c t135-1 3 0 "i Y+P~sI 0.-o -~o~oo 5. "-oof Operator Signature Date Time__ __ _ __iOQ )Checked by Signature Date Time_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ C -_M -I°o Checked by Signature Date Time Notes: 12-11 464 14 94 4-qF Jr *

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Specimen: Sheet I of I Data Acquisition System: Channel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location Comments 1 "~ I ___,,__" -&d,1T -_______ S. " ____. ___Z. "2.. I ,, 'A-Io 400 lo~to/ 3, 17. / OITM:-. N.. Spllcee_ 3 " .3 1 " 4o0 lo,)8s'5 / 6 ,7 A oI " __ __ _ -oo -5 / 0,ctI _ ._______ __,_____" 100 to L"o so 4 _______ C0,2 N.E -a -0O~btbf2 SMS-o .I 3ov Luc:8 J125o O..2O.f / ..N.. -.Ofi 8 1- I Sov "____ " J t951 O,20o / 00b0(o ,____,, -_ ,___-Operator Signature ,Date Time Checked by Signa ure \Date Time Checked by Signature Date Time Notes: 12-13 ml 1 39 40414243 44 45 46*A A-I-----4---41-----41-E-41-E-E-IE--lE .., m m -m m m m 1 -u.-------4.a.-~--u.-~-m.-u.~ I -. -m I m m m m m m m m I -i I 449605152 53 54 J/i v w v w v 4? 4849 505f w v 83 5,/North 34 Cl 1-* ! ! m ! m D m m I I ... ... i v ! V W W V= V V W V W I T I 7 zyz I Ia.1 9 55 565b75859690 61 62 ,_ Front-4436 6@10=60 2@10 --20, I- -- I 4@4.75=19 w _ , 4§4.75=19 LABORATORY Specimen -4I.Behavior of Lap Splices of No. 11 Reinforcing Bars 12- 14 REDACTED VERSION 0 Project: Tests to Determine the Behavior of Spliced #11 Bars (Instrumentation Documentation v.1 (Rev. 04/01/2012) Specimen: 6 -2, Sheet I of ..Data Acquisition System: Channel # Gain Excitation V. Sensor S.N. *Sensitivity Zero Offset Location Comments I hi-( I "_____ "5--I~ooq3 3 5,O L , 1 " .- +-iv. 0.352 5 fr-J2 10o _____ filC3 O.[ K] "3 [13-I I %or " -coosS , -O.O2fj Operator Signature Date Time Checked by _~Siapature Date Time Checked by Time Notes: 12-15* REDACTED VERSION 540414243 44 45 48 4 39 4041424344 45 48 A ---+---- 4 -4.L-------1 I U -~-J.I-.--I I *. I -I I-4 U -41 m m m m m m --d 1 ~ ~ aJ-4E -41 m m m m m m m m 4-I II 1~ 1~ 1~Ii P v 47 4849 5061 62 53 54 North 34 Cl.-I--------- I -I 1 I U -U -11 U -~ I -I -i h b -~ I ~ -*. *. *~ *. *. ---L -1r i m!2@10=201 37Ir Back a~~Front-, ,]_6@10=60 _i 2@10 --20, 4@4.75=19 4@4.75=19 12ft71in.LARATORY Behavior of Lap Splices of No. 11 Drawn by: .3P R Checked by: ZAJ/\_U____U"_,_____i___________ Reinforcing Bars Date: 12 -16 REDACTED VERSION Project: Tests to Determine the Behavior of Spliced #11 Bars 0 Instrumentation Documentation v.1 (Rev. 04/01/2012) Specimen: _______Sheet I of I Data Acquisition System: ill ul i Channel # Gain Excitation V. Sensor SN. Sensitivity Zero Offset Location Comments 0/-O tIii, 5533 PA2 Z~lOcsqio -6,yq-3.06 ,/2 t-'1-2 _____ ~ PA-4o ?: $~:7\\ s,,& O.305 3 tlI-3 .I " 9 ,oI0o~i 3,i6 of. H;i O.2-o3,______-0 I 3 , 0:7- S.pt~G. O,23(-/.S It-2 !oo0I e-1 c-1 3 -_____ 0o.3CR EK .£a,&. -- (0 = 10o ___ __ ____- __ --2_ _ o,2_[K7 5, ,~ Th 13-O I 30 2 C)25 __,___ O~ ~ '. , g,-,kp 0,o6- ,/ t1'- I 30o 3%5 o, of -o. oog Operator Signature Date Time Checked by Signature Date Time Checked by Signature Date Time Notes:.12 -17'I REDACTED VERSION U©t p ~!39 40414243 44 4548-F-0--@- + -63541 A A A A A A-I 48 49 50 51 52!fd)w A North 34 62-f---------t----~-------~. .I-I.-~-*--*-------~ fr-il -A. £ £ £

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us ST 585960 61 I_o m 2--- -, Front :*6@1 -0]_ .6@10=60 ::,Q 0--2 , 4@4.75=19 4@4.75=19/ 12 ft71In.LAORA TOR:Y Behavior of Lap Splices of No. 11 Drawn by: 1" Checked by: !....._____U_________R___!___ Reinforcing Bars Date: /Ic/.0 12-18 .(. U Project: Tests to Determine the Behavior of Spliced #11 Bars 0 Instrumentation Documentation v.1 (Rev. 04/01/2012) Specimen: __________________ Sheet I of _____I.Data Acquisition System: Channel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location Corn~ents o /pi-o 1 3.3353 PA.-2.o ---___._- ______2.I./"11 -2I P 1 oo______ 33. I :-6l-5 o.'1-,s G& .-l.2- I0 V'-i '/O~o4 I L O6' ____3 j--tc~'c4 3 ,- 15 ______.. j , -, -oooo~ jo-oJOooLo,4oP13-0 3 O"/ LDT TJ'so ___,____ -o~o05 "jjP.+-.Z~ L~1~o LJT T~-i ____ 0c? ' -o 014 Operator Signature Date Time__._"__.__ ____.__ ._ 3:41CaPM.Checked bySigatr Date Time Checked by Signature Date Time Notes: klI s~lil I/-12-19 KtL-UW.I I-U NJ A 39 40414243 44 kA b'45 46 , .1=.J A 4-ft------f?- U -U -I -. U -~--------~-~-----~ ~ I --+/- -v v w w w .v A w w A--m m m m -~j 7 -53 54 i!I a 48 495051 52 w North 34.-E -. --E,. --,-- I=_.. _,h __ *. *. .* .. .*- A .&1-1 1 S2010--2 1 37 :36-_Front -36Q06 2@10 --201 , 404.75=19 404.75=19 12fl7 in. I LAORTR.Y Behavior of Lap Splices of No.11 Dmwn by: "!I, Checked by:l _P___I____UI ______U__N___l_ Reinforcing Bars Date: 12 12 -20 REDACTED VERSION U Project: Tests to Determine the Behavior of Spliced #11 Bars 0 E-S Instrumentation Documentation v.1 (Rev. 04/01/2012) Specimen: Sheet !of 7 Data Acquisition System: Channel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location Comments 0 fl-c " "~3 .-,)s " .(vef ,:O2//;2pt-z I " Ai-IO 5 /11I-3 I "I 0 +/-,01:L/ 3 /o"WS OQ.LAo 053 /I &ov 2 'o,.oo pJ, s.1,,- -0oo2'3 t3-1I 30""-0-2 2 o..;o1 -FO.:o % 0, r0)OI Operator Signature Date Time s .l? UJOL_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Checked by Signature Date Time Checked by Signature Date Time~Noes ~ ~bj~12 -2.1-REDACTED VERSION 4 39 40 414243"44--m -mF ---t[ I -.- -.S. F 534..L....-I----4 I -4 I -U -4 I -I I- U -II -'-4 I -I I-~ U ---~ I m m m m m-4= -m m m lb j~p jgj9j~5 1 5 2!v v v v v v 47 4849 5051 62 North 34 Cl= = U. .=1-I 55 568 7"65960 61 82 12@Io=2o 37 ;,--36 ,351- Front =: , I=6Q10=60 _,2@10 -20 4@4.75=19 404.75=19 12ft71In.Specimen ~, -5 LABORATORY Behavior of Lap Splices of No.11 Drawn by~ 1@~P~. Checked by: Vy~PURDUE UNIVERSITY ReinforclngBars Date: ~/J6/U~.12 -22 REDACTED VERSION UJ 0 0 Specimen: Sheet 1 of 1-Project: Tests to Determine the Behavior of Spliced #11 Bars Instrumentation Documentation v.1 (Rev. 04/01/2012) Data Acquisition System:[>J Channel # Gain Excitation V. Sensor S.N. Sensitivity Zero Offset Location Comments I. /141-1 I " " B -F?,___ S, k 2 t- MI- I " !A- 10 9/OoOlCIf 3, 1:-5 O,.% 0,27--¥:3 14I-3 I "' " C010c11 "3,Aif _,5___,___po ______q/ I1)-O I ____ " -tooIO~ o -B,7.-3 IS 15 5 s\w _.______5 /12-2 100 boy _o____3 _____ O.Jo_ Ki -______s o ti- oo Io'J "I L/.I2 0.255 .O,2 CKJ <,___-o ___7- 113-b ! 3ov T 0 0.0oo 0.ooo I{ P13-1 30\I " -s .9o0o~o2 &. Operator Signature Date Time Checked by Signature Date Time Checked by Signature Date Time Notes: 12 -23 REDACTED VERSION Norlh 3 ,_ .Front _4@4.75=194(.. 12 ft7 In.I "Specimen g --LABRAOR Behavior of Lap Splices of No. 1:1 P URDUIE VER:S~ITY Reinforcing Bars 12 -24 REDACTED VERSION}}