ML20138P613
| ML20138P613 | |
| Person / Time | |
|---|---|
| Site: | Comanche Peak, 05000000 |
| Issue date: | 10/14/1983 |
| From: | Wells M BROWN & ROOT, INC. (SUBS. OF HALLIBURTON CO.) |
| To: | |
| Shared Package | |
| ML20138M609 | List:
|
| References | |
| FOIA-85-59 CCP-40-02, CCP-40-2, NUDOCS 8511070285 | |
| Download: ML20138P613 (24) | |
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.o :Z JOB 35-1195 COMANCHE PEAK STEAM ELECTRIC STATION Construction Procedure DOCUMENT CHANGE NOTICE NUMBER 6 Notice applicable to Construction Procedure No. 35-1195- CCP-40 Rev. 5 .
This change will be incorporated in the next revision of the procedure. Change the procedure as follows: Please replace the following pages with the attached: ATTACHMEllT 5; Special Coating Procedure C-1 Rev.1 Pages 1 through 5 Reviewed by: tty 1 Origiqator
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Approved by: TUGC0 'Qdali.ty'Assuranc e Date d - f te d // //2 / g d October 14, 1983 Construction Project ManagerDate Effective Date lg100g5851016 0 GARDE 85-59 PDR J
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. i JOB 35-1195 COMANCHE PEAK STEAM ELECTRIC STATION Construction Procedure DOCUMENT CHANGE NOTICE NUMBER s Notice applicable to Construction Procedure No. 35-1195- CCP-40 Rev.s .
This change will be incorporated in the next revision of the procedure. Change the procedure as follows: Please replace the following page(s) with the attached: Page 7 of 13 Reviewed by: 14/l l.~l1lU 8ll9181 Do , $ ~. ;; Q i:' C2
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W // / r ik.#C .E.1-- Auaust 30. Ice Construction Project Manager Date Effective Date
% a JOB 35-1195 COMANCHE PEAK STEAM ELECTRIC STATION Construction Procedure DOCUMENT CHANGE NOTICE NUMBER 4 Notice applicable to Construction Procedure No. 35-1195- CCP-40 Rev. 5 . This change will be incorporated in the next revision of the procedure. Change the procedure as follows: Please replace the following page(s) with the attached: Page 7 of 13 Reviewed by: W lb/8} Brown Yh& Root . w. Quality Assurance Date Origin / tor 4 ate'
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. ,6 J08 35-1195 Comanche Peak Steam Electric Station Construction Procacure DOCUMENT CHANGE NOTICE NUMBER 3 5
This notice applies to Construction Procedure No. 351195. CCP-40 Revision This change will te incorpcratec in the next revision of the procedure. Change the procedure as fo11cws: Replace the following pages with the attached: Page 3 of 13 Page 4 of 13 Page 5 of 13 Page 13 of 13 Add pages: Page 13a of 13 ATTACHMENT 4 Page l o~f 2 Page 2 of 2 ATTACHMENT 5 Page 1 of 5 Page 2 of 5 Page 3 of 5 Page 4 of 5 Page 5 of 5 Reviewed by: M/ lA j 3 2hf?} Uk I t WY J 5'bb Orig ator Cate / 3rown & Acot quait:y Assurance Data Revieve v
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JOB 35-1195 Comanche Peak Steam Electric Station Sheet 1 of 3 Construction Procedure DOCUMENT CHANGE NOTICE NUMBER 7 This notice applies to Construction Precedure No. 35-1195 CCP-40 Revision 5 . This change will be incor: orated in the next revision of the procedure. Change the procedure as follows: Replace the following pages with the attached: Page 6 of 13 Page 7 of 13 i Reviewed by: pf A !x/ o' 2 "I9-? ] hl [ < . JNl ,$ I?Y7' , Cate / srown & Aoot Qu lity Assurance Qa:e Or1g;nator Ravi e' . EE
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J08 35-1195 Comanche Peak Steam Electric Station Sheet 1 of 3 Construction Procedure 00CtJMENT CHANGE NOTICE NtJMBER 1 This notice applies to Construction Procedure No. 35-1195 CCP-40 Revisfon 5 . This change will be incorporated in the next revision of the procedure. Change the procedure as follows: Replace the following pages with the attached: Page 12 of 13 Page 13 of 13 Reason for change: Additional requirements. Reviewed by: [h '1- fh l . I WEJ l~(O Or191n,etor Date drpn&AcatQuailtyAssurance Date 7* P , EP
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l PROCEDURE EFFECTIVE BROWN & ROOT, INC. NUMBER REVISION DATE PAGE CPSES JOB 35-1195 CCP-40 5 8/18/82 2 of 13
1.0 INTRODUCTION
I 1.1 PURPOSE 1.1.1 The purpose of this procedure is to establish the methods by which the surfacer and finish coats are to be applied to concrete surfaces in accordance with specification, draw-ing, and manufacturer's requirements. I I 1.2 SCOPE 1 1.2.1 The scope of this procedure covers the surface preparation and coating of cementitous surfaces inside the reactor build-ing and radiation area as delineated by Reference 1. 1.3 GENERAL DISCUSSION 1.;.1 All coating materials addressed by this procedure shall be as manufactured by Imperial Professional Coating of New Orleans, Louisiana. The coating system will consist of a surfacer ' coat of NUTEC #115, touch-up with NUTEC #115 or NUTEC #11, and a finish coat of NUTEC #1201. In order to prevent finish l coat damage, the finish coat will normally be applied as close as possible to turn-over of the area to the owner or as required due to the setting of equipment or other items which would make an area inaccessible. Any permanent equipment located in the area to be coated will be adequately protected from contamination caused by surface preparation or coating application. 2.0 DEFINITIONS OF TERMS, ABBREVIATIONS AND SYMBOLS Z.1 TERMS 2.1.1 Substrate - The uncoated surface to which a coating is applied. 2.1.2 Pinhole - A minor discontinuity in the coating film which exposes the primer. l 2.2 ABBREVIATIONS 2.2.1 (NONE) 2.3 SYMBOLS 2.3.1 (NONE)
I t PROCEDURE EFFECTIVE BROWN & ROOT, INC. NUMBER REVISION DATE PAGE CPSES JOB 35-1195 CCP-40 5 8/18/82' 3 of 13 3.0 SPECIAL ITEMS AND OPERATIONS 3.1 QUALIFICATION OF PERSONNEL 3.1.1 Coating Application Personnel shall be qualified per pre-vious experience and/or demonstrated ability. In addition, each applicator shall have been certified by the Paint Dept. Superintendent or his repersentative per technical data and demonstrated ability. Application procedures shall be in compliance with this procedure. This shall be verified by completing a form similar to Attachment I which will be exe-cuted by the B&R Paint Superintendent or his representative. A coating manufacturer's representative will be available for technical supervision upon initial painting effort. 3.2 SAFETY REQUIREMENTS 3.2.1 All appropriate health, safety, and fire protection require-ments pertaining to surface preparation and coating applica-tion shall be followed. It shall be the responsibility of the
- Safety Department representative who will be present to randomly monitor safety during coating application.
3.3 INSTRUMENTS AND THEIR USE 3.3.1 The Painting Foreman and General Foreman shall have access to and be familiar with the use of thermometers, wet film gauges, and psychrometers for measuring relative humidity. Viscosity measuring devices will not be used. Wet film gauges will be randomly used during coating application; readings will be limited to the minimum necessary to control coating thickness. 3.4 00CUMENTATION 3.4.1 Records shall be maintained on Attachment 1 and 4 listed in Section 5.1. Af ter completion, each form shall be forwarded to The Brown & Root Document Control Center for filing and distribution to the various parties as listed on the distribution list. l l l l
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- CCP-40 Ru c nr.N #1 6/24/83 ShmR 9 of 11
PROCEDURE EFFECTIVE BROWN & ROOT, INC. NUMBER REVISION DATE PAGE CPSES JOB 35-1195 CCP-40 5 8/18/82 4 of 13 3.5 RECEIVING, STORAGE AND DISPENSING OF COATING MATERIALS 3.5.1 Receiving and Storage 3.5.1.1 Upon receipt of a shipment of coating materials, the B&R QC Representative accepting shipment shall be responsible for completing all necessary receiving inspection documen-tation. General receiving procedures shall be in accord-It and with Brown & Root Construction Procedure CP-CPM 8.1. shall then be segregated from "Non-Q" materials and stored in the Paint -Storage Building where temperatures will be b Rises in air temperature maintainegF up to 120 ktween 400F and 1000Fs acceptable f. or as long(Ac- as fourteen d cumulative). Infrequent dips (for periods not to exceeg 24 hours) in air temperature in storage areas as low as 33 F is acceptable; however, prior to application the coatings shall be brought back into the 500 - 90 range. Temporary storage may be required at the Receiving Warehouse due to receiving or other problems. 3.5.2 Dispensing . 3.5.2.1 When coating materials are needed in the field, it shall be t*ansferred from the controlled area to a designated temporary storage area or area of intended use in the field. Due to limited shelf-life of coating materials, this shall be done on a "first-in" "first out" basis. After materials have been partially used from an individual container, the said container cannot be resealed and returned to "Q" storage area for later use. Containers opened and partially distributed from the "Q" paint storage area may be resealed and the remaining contents used for "Q" painting. Except for thinners, the contents from partially used containers shall not be reused after a period of 7 days has elapsed from date of initial opening. 3.6 Special Coating Procedure 3.6.1 When items require special coating not covered under the content of this procedure, Attachment 4 shall be completed by the Protective Coatings engineer and transmitted to painting supeintendent for construction. Special coatings procedures issued via Attachment 4 shall be attached to this procedure after completion. 3.6.2 Special Coating Procedures added by Attachment 4 shall recieve a unique identification number issued in sequence beginning with C-1. The scope of the procedure shall describe the working limits of the special procedure with pertinet storage and coating require- ' ments listed under the requirements section. The approvals section shall have the signatures of the Project Civil Engineer, TUGCo QA Manager if safety related, Originator, and the Construction Project l l Manager. Each procedure shall exhibit the revision number and I issue date. - i 6/24/83 Sheet 3 of 11 _ - _ CCP 40._Rev.._. 5 DC.N #3_ _
~* ' PROCEDURE EFFECTIVE BROWN & ROOT, INC. NUMBER REVISION DATE PAGE CPSES JOB 35-1195 CCP-40 5 8/18/82 5 of 13 4.0 PROCEDURE 4.1 PREPARATION OF SUBSTRATES AND C0ATING MATERIALS 4.1.1 Preparation of Surfacer 4.1.1.1 Normal surface preparation shall consist of water blasting with 4,000 P.S.I. to 10,000 P.S.I. Additionally, surface preparation may be accomplished by the use of approximately 2,500 P.S.I. water blasting ,with sand injection, acid etching with an Imperial recom-mended solution, or straight sand blasting. Any heavy oil or grease deposits shall be removed by steam cleaning, trisodium phosphate washing with a mixture of 3-6 pounds T.S.P. per gallon of water, or use of an Imperial recomended detergent. Following surface preparation, the surface shall be free of construction dust, laitance, and loose deposits. If cleaning
. does not remove oil and grease, the contaminated concrete surface will be chipped away and patched before coating. All T.S.P. cleaned areas will be flushed with clean water. Holes or voids in the concrete surface that exceed 1/2" in depth shall be repaired with dry-pack or epoxy grout. Detrimental surface irreg- .
ularities such as projections, fins, or ridges shall be reduced by bush-hamering, power grinding, or stoning. Wood particles of
" fuzz" remaining after water blasting is acceptable. Recomended surface preparation shall include power tools which are capable of removing liatance and curing membranes from concrete' surfaces.
4.1.1.2 Markings on concrete - Before application of 115,11 or 1201, all markings (ink, pencil, chalk, or felt tip markers) on wall and floors shall be solvent wiped in accordance with SSPC-SP-1 using DL-6A or comercially available MEK or Xylol. Marking paint (surveyor marks) shall be removed by solvent wiping, water blasting, sandblasting, or power tool cleaning. Discolored coatings due to aging or stains shall be abraded and solvent wiped to remove the discoloration. Residual marking or discoloration remaining in pores below the plane of the surface is acceptable. 4.1.1.3 Repair of embedded foreign objects - Embedded foreign objects such as nails, rebar chairs, bolts, wood, or plastic shall be repaired per the following guidelines before application of NUTEC 11S surfacer.
- 1. Objects protruding from the surface shall be ground or cut smooth until the object is flush with the concrete surface prior to application of 115.
- 2. If the object is loosely adhered in the concrete, it shall be removed (in case of wook splinters or wood " fuzz" an attempt shall be made to remove by high pressure water blast-ing). Rever to section 4.1.1.1.
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CCP-40 Rey, 5 DCN #3 6/24/83 Sheet 4 of 13
l BROWN & ROOT, INC. PROCEDURE NUMBER ' REVISION l EFFECTIVE OATE PAGE l CPSES i JOB 35-1195 i 8/ 18/82 1 6 of 13
! 5 CCP-40
- 4. Metal objects larger than four square inches sh CCP-30.
5. Objects which are recessed to a depth greater than 1/2" sh be repaired using a " dry pack" or epoxy grout. Surface appearance - Surface srnoothness or " glossy" appea 4.1.1.4 concrete will not be detrimental to the performance of NUTEC providing the surface is free of water, oil, grease, laitance, efflorescence, deleterious Ifcuring NUTEC membranes, or isother contamin 10 curing membrane as outlined in this procedure. present with thickness sufficient to give a g cation of 11S surfacer. 4.2 PREPARATION OF C0ATING MATERIALS 4.2.1 Surface Coat The surfacer, NUTEC #11S, is packaged, in The a three base component 4.2.1.1 kit consisting of a base, curing agent, and filler. If necessary, and curing agent shall be thoroughly mixed first. box the The mixture to assure filler shall then be slowlythat added allunder the constantThe base andpatching cure used. agitation and mixed until a smooth blend is achieved. Partial mix material, NUTEC #11, is prepared the same way.NU 4.2.2 Finish Coat 4.2.2.1 The finish coat, NUTEC #1201, is a two component epoxy consisting of a base and cure. under constant agitation until a homogeno ment 3. Minimum induction times shall be as follows: ' O INDUCTION TIMES TEMPERATURE F 45 min. 50-59 30 min. 60-69 20 min. 70-79 10 min. 80-90 NONE 91-100 Sheet 2 of 3
EFFECTIVE PROCEDURE DATE PAGE NUMBER REVISION BROWN & ROOT, INC. CPSES JOB 35-1195 8/18/82 7aof 13 5 CCP-40 4.3 APPLICATION OF SURFACER & FINISH C0ATING 4.3.1 Surfacer Coat Coating material shall be applied using a bottom feed con-To facilitate 4.3.1.1 ventional pressurt. pot-mastic gun arrangement. application on areas such as floors and for repair work, trowe squeege or float application without the use of the masticUn arrangement may be used. surface shall be allowed to cure a application of protective coatings. C to be applied to pour backs, grouting, or patc , after a minimum of 6 days has elapsed from NUTEC 10 application time. Abandoned hilti bolt holes, tie holes, and spalled conerete as defined in CEI-20 and patched per CCP-1 Material shall
~ to be coated, may Le coated af ter 48 hours cure.be a A single extra material being added to large noles or depressions. Care blade rubber squeege is then used to smooth out the material.
shall be taken to eliminate as many cinholes as po a back and forth motion.
- 1. Minimum and maximum 0 0values of surface and ambient tempe shall be between 50 F and 100 F, to 40 F is permissible during application ang/or cure; however, the elapsed time the temperaturePotislifbelow the cure time. e 50 the surface temperature is 5 F above the dew point.
shall be as stated in the ch1rt below. FCTUF5 HRL I us .
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Humidity may vary as high as 100%; however, free standing w Coating application uver a damp surface is shall be removed. Under no condition shall NUTEC permissible. Free115 be applied standing water to a surface containing free standing water. may be identified by: 1 t eg~~'
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~ 8/30/83 Sheet 2 of 2
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EFFECTIVE PROCEDURE DATE PAGE NUMBER REVISION BROWN & . ROOT, INC. CPSES l JOB 35-1195 8/18/82 8 of 13 5 CCP-40
- a. Reduced viscosity of 115 during application, and excessive sagging from bug holes.
- b. Wet rings around bug holes.
- c. Failure of 115 to adhere to the substrate during the squeegeeing or trowelling process.
- d. Visible signs of surface water,
- e. Running hand over the surface resulting in moisture on the hand, Product instability resulting in white streaks.
f.
- 3. Thickness of surface for level 1 service may vary Forbetween 10 and 35 mils, depending on the surface roughness.
areas other than level 1, the recommended dry film thicknesses for surfacer is 10-60 mils. ,
- 4. Tack free times shall be as follows:
#11 #11S TEMPERATURE OF 6 hrs. 8 hrs.
50-59 6 hrs. 60-79 4 hrs. 2 hrs. 4 hrs. 80-99 2 hrs. 100 1 hr.
- 5. Curing time shall be as follows:
CURING TIME BEFORE O TOPC0ATING WITH 1201 TEMPERATURE F_ 72 hrs. 50-59 48 hrs. 60-69 24 hrs. 70-79 18 brs. 80-89 12 hrs. 90-100 t ! I
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EFFECTIVE PROCEDURE DATE PAGE NUMBER REVISION BROWN & ROOT, INC. CPSES 4 8/18/82 9 of 13 JOB 35-1195 CCP-40 5 , f FULL CURE 11. 11S_ i TEMPERATURE O F_ 10 days 50-59 8 days 60-69 7 days 70-79 6 days 80-89 5 days 90-100 No appreciable cure 0 takes place below 0 50 F, therefore, main , tain 0area coated above 50 F.to 40 F is permissible; however, d , added to cure time. I
- 6. NUTEC 11S may be recoated with #11 or #11S as soon as the initial coat has dried such that the paint shall not adhere to the thumb when downward 0 angle. pressure is exerted on(this d the paint film while turning a 90 Dry time will vary refer to a two pass application method).At thicknesses greater with film thickness.a minimum of 24 hours shall be allowed prior to ,
full coat of NUTEC 11. l 7. NUTEC 115 may be touched up with #11S or #11 as soon as it
#11S and #11 may be subjected to personnel set to touch.
foot traffic after 24 hours cure and lay down of material after full cure. 8. Thinning of #115 is not normally required; however, at lower temperatures, it is permissible to thin up to 5% by volume with Imperial's OL-54 thinner. 4.3.1.2 Imperial coatings may be applied in the Millage followingper requirements sequential o
#11S/1201/1.1S/1201 or 11S/1201/11/1201.
ccat are as follows: Service Level 1 NUTEC 115 10-35 Mils NUTEC 11 3-20 Mils l NUTEC 1201 3-16 Mils Areas other than Service Level 1 NUTEC 11S 10-60 Mils NUTEC 11 3-20 Mils l NUTEC 1201 3-16 Mils Repair and recoating of NUTEC 115 - Remove all loose coatin 4 . 3 .1 '. 3 and concrete by sanding or wire brushing and feather edge ad The area shall then be blown off with compressed to the coating. air, washed with water or DL-54 thinner (No
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EFFECTIVE PROCEDURE DATE PAGE NUMBER REVISION BROWN & ROOT, INC. CPSES JOB 35-1195 5 8/18/82 10 of 13 CCP-40 ' 4.3.1.4 Repair of Pinholes, blowholes, or overworked areas Apply - Remove any contaminants by compressed air or clean water.NUTE in area. -NUTEC #115 surfacer may be smoothed by spraying a mist after itsof application. Imperial DL-54 thinner on the #115 film 15-30 minu can be worked over the surface to smooth or polish the ffim, thus eliminating the defects due to overworking of the 115, Mudcracking - Area shall be repaired by means of grinding, sanding, 4.3.1.5 The area will then be blown down with compressed or wire brush. , air and then wiped with DL-54 thinner. 4.3.1.6 Repair of Sags and Runs - Inside containment, runs or sags shallO be abraded down to adjoining thicknest. - coating is sound, sags and runs will not be repaired. 4.3.1.7 Repair of Embedded Foreign Particles - Embedded foreign shall be removed by abrading. then area shall be repaired in accordance with Section 4.3.1.4.
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4.3.1.8 Treatment of Rust Stains - Remove residue, thou Treatment of Interfaces with Other Coatings - Interfaces with 4.3.1.9 projecting coated items shall be constructed by abutting theInterfa 11S up to the projecting item. coated items shall be constructed by feathering the 11S into the coated item, 4.3.1.10 Repair of Scorched Areas - If the concrete is not damaged, scorch areas shall be repaired by abrading the surface until the dis-colored area is removed. Visuti inspection ofThe thearea area shall then should be conducted to assure the area is acceptable. be coated with 11 or 11S as appropriate. 4.3.1.11 Coating of Expansion Joints - Expansion joints will not be coated. Coatings will be feathered b,ack at the edges. 4.3.1.12 Repair of Scratches and Similar Damage - Any s If the damaged area extends to con-adherent particles are removed. crete and is k" or less in diam applied . If the damage extending to concrete substrate is greater than
" in diameter but 2 sq. inches or less in area, the area may be repaired with 11 or 115 for surfacer prior to topcoating., Damages involving areas larger than that stated above shall be repaired with ;
normal coating system. ! N&
-,_ EFFECTIVE PROCEDURE DATE PAGE NUMBER REVISION ~
BROWN & ROOT, INC. CPSES JOB 35-1195 5 8/18/82 11 of 13 CCP-40 4.3.2 Finish 4.3.2.1 Finish coat shall be applied by brush, roller, conventional airless spray methods. care The materialmust shall be taken to ensure be allowed to become a smooth
" tack free" uniform finish su before any other construction operations proceed which could create con-Pinhole crite tamination by dust or other foreign matter. "B". Any runs shall be in accordance with NACE T-6F-3, condition or sags having a detrimental The following effect on theparameters application coating system shall ,
be removed and repaired. shall govern: 1. The permissibfe range Infrequent of surface and dips ambient temperature in temperature to be between 50 F and 100 F. 4CPF is permissible during application and/or c Application shall not begin unless theIf from the cure time. 0 surface temperature is at least 5 F above the dew point.#1201 may b increased workability is desired, Reacti It is normally . up to 30% by volume with Imperial DL-6A thinner. using conventional spray equipment. . W 3
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MRPERATVME *F 2. Thickness of 1201 topcoat for Service Level 1 and Service Le II areas shall be as specified in Section 4.3.1.2.
- 3. Coating materials shall be applied as a hea 50%.
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! EFFECTIVE l PROCEDURE DATE PAGE REVISION l NUMBER '
BROWN & ROOT, INC. ' l CPSES - . l 1 JOB 35-1195 8/18/82 i 12 of 13 5 CCP-40
- 4. Recoating time of NUTEC #1201 is 24 hours.
- 5. Tack free time is as follows:
O F_ TACK FREE TIME TEMPERATURE 8 hrs. 50 4 hrs. 60 2 hrs. 80 1 hr. 100
- 6. Full cure time is as follows:
O FULL CURE TIME _ TEMPERATURE F 11 days 50-59 8 days ' 60-79 7 days 80-99 5 days 100
#1201 may be subjected to personnel foot traffic af ter 24 hour org above surface temperature 0 of 80PF.50 F little or n '
maintain temperature above 50 F. 4.3.2.2 Repair of RunsRuns andorSags - Runs or sags showing evidence sags inside Service Level I areas which must be removed. exhibit no other coating defects, shall be abraded to the thickne Runs or sags outside Service Level I areas of adjoining coating.which exhibit no other coating defect need no 4.3.2.3 Repair of Embedded Foreign Particles - Embedded forei shall be removed by abrading.Any loose particles shall be removed by overcoat of #1201. ing, vacuum, or compressed air. 4.3.2.4 Repair of Pinholes and Discontinuities -The Any loose pinholes andparticle be removed by brushing, vacuum or compressed air. discontinuities shall then be repair-d by use of a brush or squeege Pinholes and small discontinuities tr y be repaired at time of If the re-inspection without a later reinspection of the repair. paired coating will be subjected to a high moisture d envir placement into service, the placement into service shall not until full cure of the repair. as il 4.3.2.5 Repair of Scratches andIf the Damaged Areas damaged area extends d area loosely adherent particles are removed.to concr n-less may be coated with NUTEC #1201. f crete substrate is greater than k" in diam m
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1/11/83 Sheet 2 of 3 N
EFFECTIVE PROCEDURE DATE PAGE NUMBER REVISION BROWN & ROOT, INC. ! CPSES : 5 8/18/82 13 ofl3 CCP-40 JOB 35-1195 NUTEC #1201. Damaged areas to concrete substrate larger than the above values shall be repaired with the normal coating system. 4.3.2.6 Treatment of Rust Stains - If the topcoat surface and water or solvent wiping with Thinner OL-6A. not acceptable from a cosmetic viewpoint will be covered by a light overcoat of NUTEC #1201. 4.4 FINAL ACCEPTANCE TESTING - Full cure of the coating system shall be maintained prior Final to testing acceptance 4.4.1 and/or inspection for other than visual inspection. ins after topcoat has cured per paragraph 4.3.2.1(4). After final inspection, and resolution of all discrepancies are com-pleted, the QC Inspector shall document the final acceptance by com pleting and signing the Final Acceptance Record and will transmit a copy of this record to the B&R Paint Superintendent as soon as ' possible after final acceptance is made. , 4.5 HOLD POINTS 4.5.1 On-site receipt of coating material. Substrates before preparation if blasting or bush hanraering is to be 4.5.2 utilized and following all methods of preparation. 4.5.3 Mixing and preparation of coating material for application. 4.5.4 Film characteristics after drying and curing. Control of ambient conditions and surface temperatures during all 4.5.5 phases of the coating work. 5.0 SUPPORTING INFORMATION 5.1 ATTACHMENTS
- 1. Painter Qualification Record
- 2. Table for Partial Mixes of NUTEC 115
- 3. Table for Partial Mixes of NUTEC #1201
- 4. Special Coating Procedure .
- 5. Special Coating Procedure C-1
- 6/24/83 Sheet 5 of 13
f EFFECTIVE PROCEDURE DATE PAGE NUMBER REVISION ' BROWN & ROOT, INC. CPSES 8/18/82 13a Of 13 5 CCP-40 JOB 35-1195 S.2 REFERENCES 1. Gibbs & Hill Specification 2323-AS-31, " Protective Coating" Latest Revision
- 2. Steel Structures Paint Council, Vol.2, Second Edition
- 3. Imperial Data Sheet NUTEC #11S and NUTEC #1201, Dated 7/7
- 4. NACE Publication T-6F-3 N
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i EFFECTIVE PROCEDURE DATE j PAGE BROWN & ROOT, INC. , NUMBER l REVISION CPSES i ! l 1 of 1 JOB 35-1195 5 8/18/82 CCP-40 l ATTAC MENT 1 Painter Qualification Record GENERAL DATA Report Number _ Date TECHNICAL DATA _ Name of Painter Summary of Field Experience ._ Experience with Following Product Types Application Test for Specified Substrate . Additional Qualifications (School) SignatureApplicator's Field Supervisor Distribution: Painting Supt. QC Department TUGC0 QA Vault (Original) [ 8 G_ .
i EFFECTIVE ; PROCEDURE PAGE REVISION DATE BROWN & ROOT, INC. NUMBER , CPSES I, JOB 35-1195 8/18/82 i i of 1 S I CCP-40 ATTACHMENT 2 NUTEE 115 PEMI551BLE CuaE FILLER mgmEn 8ASE pts. 03. Ibs. oz. Ibs. oz. Ibs. ot. 1 0 3 1.6 10.6 0 i 5.3 3 < 0 Gal . - 1 Qt. l3.2 5 0 0 I 5.1 0 12.6 2 at. 0 Gal . .. -. 9 0 0 i'8 0 91. . 3 Ot. 1 ,15.7 1
)3 10.2 1 9.3 12 0 0 f6.4 0 Ot. 2 1 Gal . -
15 0 0 S 3 4.9 1 15.6 1 Gal . . I at. la 0 0 9.6 3 15.4 2 5.9 1 kl . . 2 Qt. 0 0 11.2 4 9.9 2 12.2 21 1 na t . . 3 Qt. 24 0 0 ;12.S 5 4.5 3 2.6 0 Qt. . . 2 Gi.. - L. _ 15.0 3 3.9 27 0 0 g 14.4 1 Ot. 5 2 Ga! . . ' 16 15 2' 30 0 0 - j 2 Ga1. . 2 Ot. 6 f 9.6 3 - - _ . _ _ . . _ _ _
, 33 0 1 1.6 7 4.2 ,a 5.5 2 Gal . . 3 ct.
14.7 4 11.3 36 0 1 l 3.2 0 Ot. 7 ;- f 3 Gal. . 9.3 5 2.2 39 0 1 i4.8 I Ot. 8 3 21, . . 3.5 , 22 0 1 l 5.4 9 3.3 5 3 21. . 2 at. 9 14 5 14.3 45 0 1 l9 3 Gal . . 3 ct. 43 0 1 9.5 10 9 5 5.1 4 Gal. . O Qt. I 0 1 Qt. 11 3.5 6 11.4 51 l11.2 4 Gal. . I 1 12.3 11 14.1 )7 1.! $4 0 1 4 kl. . 2 Ot 3 57 0 1 11.4 12 3.6 7 s.1 4 kl. . 3 Ot. 0 2 0 12.4 50
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. i ' I EFFECTIVE PROCEDURE DATE PAGE NUMBER ; REVISION l BROWN & ROOT, INC. CPSES ; JOB 35-1195 5 8/18/82 1 of 1 CCP-40 l l ATTACHMENT 3 TABLE FOR PARTIAL MIXES OF NUTEC #1201 Maximum Base Cure Permissibl e Thiener qts. oz. Gal. Qts. lbs.oz. lbs.cz. , 2 96 0 5.4 0 9.6 0 1 2 5 3.2 0 12.E 0 ISi2 0 7 3.2 0 23.0 0 3 5 14 . t. 1 8 1 3 1 6.4 1 0 10 14.4 16 1 1 13 1.6 1 1 2 15 11.2 2 4.8 1 23.6 , 1 18 4.8 2 11.2 2 3.2 1 3 0 20 14 . ', '3 1.6 2 12.3 2 1 23 3 , 3 0 2 22.4 2 ; 14./' 3 0 2 2 26 3.2 3 23 12.8 4 3.2 3 9.6 2 3 31 5.4 4 9.6 3 19.2 3 0
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EFFECTIVE PROCEDURE PAGE REVISION DATE NUMBER ' BROWN & ROOT, INC. CPSES CCP 40 5 8/18/82 JOB 35-1195 1 of2L_ Sheet _ of ATTACHMENT 4 "Q" Coating Procedure # R ev . _ _0 ate "Non-Q" Coating SPECIAL COATING PROCEDURE NO. SCOPE REQUIREMENTS: APPROVALS REFERENCE C2CUMENTS ORGINATOR PROJECT C.E. TUGC0 QA
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- PREPAPACON CA3 r P gCccT TD 3E TESTED: NUTEC 11/REACTIC 1201 2 TTFE SUBSTRAM: Concreto SI2: 2"'x 4" x 2"
- 3. SURFACE PREPAEAC::lN (DesdA): All surfaces mandewept with Crosblast #4 blasting sand.
3530 4* FECCCT CAna SAMPI.Z NO. (s) : SL CAM AND CME C3:NG COMPCCND CR PR::MER APPI.:ZD N/A PECCCT APPI. C1=ON G w s.CNS MICI:ESS TI:2 & CATE
- APP' m COAT PRCDCCT CCCES BATCH 4 SETECD R/M(CT) % R.E. (ins.) -
i NOTEC 11 2671/I3150/I.B149 Squaegee 82 F/55% See below 10/18/77 1 p.
- NU':EC 11 2671/I.B150/L3149 Squeegee 70*F/72% . 003 .005 11/4/77 11 a.
REACC C 1201 3070/2568 Spray 71 F/69% See below 11/7/77 9 a.. t J *Csed for tcuch-up caly Total film thickness range: .004 .331 11 1201 f 32.n. .001 .002 .003 .005 l avg. .003 .005 .007 .008 j anx. .010 .015 .010 .011 l l S. C3:NG CO!CICONS: AMBIINT TEMP. 70 - 80 F RC. ECMIDITT 45 - 65 %
,I MI2CMCM C3E 11 CAIS i
7 "EST PRCCI::CRE: CBA per Bechtal CP 956
- 1. "ES b G'PERICRMED BY: Coastal Science :,As sc33: m 11/18/77 4:4 '
APPEVED BY: - CATE: i 77 [ PREPARED BY: M . .S c# /[< u d5 4 CATE: 12/77 t l CST xEPCR: NC.: 210-77
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- 3. SCRTA G PREPARAC CN (Desh) : 111 sur' aces mandmuset wi+3 crocht met a4 b1.. 4-e . . .4 1
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" 3530 SIDE ONEs NO FLAKES, BLISTERS, DELAMINATION SIDE TVO NO FLAKES, BLISTERS, DELAMINATION SIDE THREE: NO FLAKES, BI.I STERS, DELAMINATION SIDE FOUR NO FLAKES, BLISTERS, DELAMINATION
.. NOTE: PINHOLE ON SIDE #3 THERE PRIOR TO TESTING.
I 1 3534 SIDE ONE: NO FLAXIS, BLISTERS, DELAMINATIONS
! SIDE TV0: NO FLLAKES, DLISTERS, DELAMINATIONS i
SIDE THREE: NO FLAKES, BLISTERS, DELAMINATION S SIDE FOUR NO FLAXES, BLISTERS, DELAMINATIONS i i r R EP O RT NUMBER-- ----0 5 41 122 7--------------- i Appgoygg gy . l I I i , I i l CCCPER ATIVE STUCIES e TECHNICAL PROGRAM EVALU A TION
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Design Basis Accident Testing J Nutac 1201 and Nutec 1202 over Bare Concrete l FOR CUSTOMER j Submitted by: cerald E. Arn Id
! Accepted by: M [ redf _ , Approved: y y Date: July 2, 1980 SOUTHERN DiPERIAL COATLNGS C RPORATION, LNC.
P. O. Box 29077, + New Orle: s, Loumana 70189 Phone: (504) 254-1 41 ZO.7E*."/EUZU7O~=*7=E.$C7.LYIO."".., n:
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.i T.R. #412-80 Page 1 I SC0FE - The purpose of this test was to evaluate the DBA performance of Nutec 1201 and Mutec 1202 over bare concrete. '
- BACKCROUND - During the application of the Nutec 11S/11/*.201 system, bare con-crete is sometimes exposed due to overworking of the h..ec 11S or Nutec 11, or stoning or abrading of the surfacer to the substrate. In Service Level I and Service Level II areas it is essential that the concrete be shielded from rad-ioactive nuclides and that the surface be easily decontaminable. It is al-ready known, from past testing that Nutec 1201 seats these requirements - that decontamination f actor is well within the ANSI N5.12 criteria. However, in addition to the above requirements, the Nurec 1201 (and 1202) naast be demon-strated to withstand the rigors of a Loss of Coolant Accident - that is, it must remain intact on the surf ace, to prevent clogging of the strainers and to faci-11 tate decontamination work.
PROCEDURE - Two concrete coupons, measuring 2 x 4 x 2" and prepared in accord-ance with the proposed ASTM D01.43 concrete procedure, were topcoated with Nutec 1201 and Nutec 1202 epoxy polyamide topcoats. Each topcoat was applied to two faces on each concrete specimen. Details of the application and curing of the coatings are outlined in the attached panel preparation sheets. Cai The panels were then suhr.itted to Cak Ridge National Laboratories for Design
'C Basis Ac=ident Testing at the ASTM D01.43 proposed PWR curve (307 F., 60 psig).
Refer to the attached ORE procedures. RESULTS - No defects were noted en either coupon. Refer to t'le attached CRNL results sheet. CCNCLUSION - In those instances where the concrete remains exposed, applicatien of Nutec 1201 or 1202 is satisfactory provided the application is pinhole free. 4 l e 1
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TEST PANEL PREPAPATICN CATA l'. PICDOCT TO BE 2 SED: Nutec 1201 and Nutec 1202
- 2. T'TPE SUBSDA2 : tw e-... SI2: 2 x 4 x T'
- 3. SURFACE PREPAEA20N (Describe): vir, brush elemned to remove e!!1erescense frem
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- 4. PRODUCT DAM: SAMPLE NO. (s) :
- 5. DA2 AND TDIE C:TRING COMPCCND CR PRIMER APPLIED: N/A
; PICDUCT APPLICA20N CONDITICNS MICKNESS TDfE & OATI i COAT PROCCC"' CODES BATCH 4_ MD R/M ("F) % R.E . (ins.) APPLIED 1 Epory *1202 8333/7939, Spray 44' 71% .005 .006 02/07/80 02/08/80
, 2 Nutec **1201 6637/6333 Spray 44* 712 .005 .006 02/07/80 02/08/80
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- Sides 1 & 2 coated with 1202 t- ** Sides 3 & 4 coated with 1201 -
40 - 45 0 7 m , gugg3 m 70 - 75 g
- 6. b u CONDI2ONS: AME N TEMP.
ICNIMUM CTRE 35 CAYS l DBA .
- 7. 2ST P.M l
S. TIS 2 NG PERItRMED BY: Cak Ridge DA2 SUBMI m 03/15/80 APP!CVED: TEST ,R* "2CRT IC. e s
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- 1. PRODUCT TO BE ESTED: w. . ., 19n1 .A m e., 1969
- 2. $rPESIMSTRAM: Concrete SI2: 2 x 4 x 2"
- 3. StmPac PREPARAT!CN (Describe): Wira brush cleaned to remove efflorescence from coupon.
i- 4. PEDCCT DA3s SAMPI2 NO. (s) _ 41 A1 DATE AND TIME CURING COMPCCND f,R PRIMER APPLIID: N/A 5. 8 PEDUCT APPLICATICN CONDITICNS SIC:CIESS TIME & CATI CCAT PECCCT CDDES BATCH # .6D R/M (*F) % R.H . (ins.1 APPLIED 1 Epory *1202 8353/7939 Spray 44' 71% .005 .006 02/07/80 02/80/80 2 Nutec **1201 6637/6333 Spray 44* 71% .003 .006 02/07/80 l. e6 02/80/80
- Sides 1 & 2 coa ted with 1:02 ,
** Sides 3 & 4 coated with 1:01
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- 6. CURING CONDITIONS: AMBI:CET TEMP. 40 - 45 *r REL. atMIDITY 70 - 75 g MDC' MUM CORE 35 cars l
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- 7. TEST PROCE::CRE: USA i
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- 8. TESTING PERFCRMED ST: cak vief e. OA2 SCBMIT:ED 01/1t/no f
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f' Imeerial Analytical Chemistry Division Manufacturer: _ k Ridge Na al Laboratory New Orleann Louisiana f*,g l . Report of Irradiation and DBA Testing The irradiation and design basis accident (DBA) tests are conducted, respectively, in accordance with Bechtel Corp. Scandard Specificatwn Coat-ings far Juelser Power Plants.. specs. CP-951 and CP-956 (or with modifi-cations as noted in Table 2. DBA test conditions). The tests are designed 101.2-1972, Pm-to meet the specifications set in both A.N.S.I. report N sective Coatings (Paints) for Light Water Nuclear Reactor Castainment facilitiss, and N 5.12-1974, Protsetive Coatings (Paints) for the Ructsar -
; Industry. The DBA test spray solution and the test conditions are listed in Tables 1 and 2.
After both the DBA and the irradiation tests, the coatings are examined for signs of chalking, blistering, cracking, peeling, delamination, and flaking, according to ASTM standards where applicable.
- All test panels are returned to the coating manufactu:er.
The irradiation tests are run using a spent fuel assenbly, removed from the High-Flux Isotope Reactor (HFIR) at ORNL, as the source of radia-
'.. . . tion. .These fuel asramblies are stored under 20 feet of demineralized water. The fuel is U% enriched U23s as U 3 0s combined with aluminum.
The spent fuel assemblies are removed after each 23-oegawatt day period. Irradiation is done using the gansna energy frem the accumulated mixed fission products. This more readily simulates cenditions areund a reactor Also, the higher gamma activity affords than does a cobalt source. The dose rate four shorter irradiation time to achieve accianulated doses. rads /hr. days after renoval of a fuel assembly from the reactor is 1 x los The fuel assembly is 20 inches high. A 20-foot long, 3-1/2-inch diameter pipe, with one end capped, is used for the air irradiation tests. The capped end is lowered into the four-inch opening of the center of the fuel assembly. The open end, above the water level, is covered with an "0" j ring sealed flange to which is attached a steel cable and an air outlet The test speci-hose. The air inlet is located at the bottom of the pipe. l 8 mens are connected to the bottom of the cable and lowered into the radia field. Also at the center of the fuel assembly is a stainless steel clad cadmitsu tube used as a neutron absorber. This prevents contamination of the test specimens by induced radiation. Evaluated /. J/ /
' Approved I,,N [Mb '
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t Analytical Chemistry Division Manufacturer: Imoerial _ Oak Ridge 'icnal Lacoratory Date: -May 14, 1980 9 New Orleans. Louisiana ORNL Log Book No. A 7562; A5-5-80 Table 1. 08A solution composition, distilled water Reagent Concantration 1 Boric acid, H 803 3 0.28 # Sodium hydroxide, Nadi Required to adjust pH to 9.5 Table 2. 08A test conditions -- T ture P t h nts Time Autoclave preheated. Start 307 60 (10 s) Steam injected. 10 s 60 Pressure maintained by relief valve. 2 h 47 min 30 7 4.5 min 307-270 30 Spray solution added at 75'F. 25 min 270-250 30 4 days 250 30 250-230 0 Fresh spray rolution added at 75'F 3 min after draining autoclave. 10 min 230-200 10 3 days 200 10 i End of test i I i Evaluated , fu Approved I O
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- tienal Laboratory Date: N , 14, 1780 New Orleans. .ouisiana
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-Steel panel x Concrete block System Identification
. 1201/1202 1 .
t DBA Test Results l GUIL Master Analytical Manual Method No. 2 0922. ORNL Log Book No. A 7562; as-s-so 08A phase Connents Sample No. spray Coatings intact, no defects, sides 1, 2, 3, and 4. 6163 spray Coatings intact, no defects, sides 1, 2, 3, and 4. 6165 as ( S 4 D 1 i O f- .
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ECElVE Y 1 TECHNICAL REPORT NUMBER i 346-79-G y . s TITLE l 8 L R CC"* CfST* DBA Test Results-Short Intercoat Ti:ses: Nutec 11S/Nutes 11, Nutec 11/Nutec 1201 PRCJECT W15. I FOR PSECT act. l , QA ER. l/ PRCJECT CONT. (MR.l)s/ CUSTOMER 0 QA l PRCJE*TGO.!a*J.l ARMS */y[ Submitted by: Gerald E. Arnold g ppt ved b d [/ c g_ g [ 4 ,/ !j { g)
' Date: Dece=ber 27, 1979 l i
I/)?g l)N t i SOUTHERN btPERIAL COATLNGS CORPORATION. INC. P. O. Box 29077, + New Orleans. Louisiana 70139 Phone: (504) 254 1433
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1 T.R. 4346-79-G Fage 1 1 SCOPE: The purpose of this test was to determine the feasibility of applying two coatings (Nutec 11S and 11 or, Nutec 11 and 1201) in a single day, for touch up purposes.
, ' E&CK0ROUND: When applying the 11S/11/1201 concrete coating system, it is some-j times necessary to conduct repair or touch up work. Voids or pinholes may be left in the Nutec 11S coated surface. It would be advantageous to touch up these
. voids the same day prior to applying the next full coat.
I j Similarly, before applying the 1201 topcoat, the 115 or 11S/11 coated concrete
-' should be pinhole free. If pinholes do exist they should be touched up with
'j Nutec 11 prior to topcoating. Again, it would be ideal if both the repair and
. final coats could be applied in the same day.
3 .
-5
SUMMARY
- Dasign Basis Accident testing conducted by Coastal Science Associates 4
revealed no significant defects on specimens which had the Nutec 115 and Nutec 11 applied at 6 hour Latervals and others which had the Nutec 11 and Nutec 1201 ap-
]
plied with a 4 hour intercoat period. Because the cure time of each coating is dependent on film thickness, temperature, amount of thinning, and to some extent relative humidity, this practice is only recommended for touch up applications and not full coats. yg FROCEDURES: Three concrete coupons, -easuring 2 x 4 x 2" sere all coated with _is Nutec 11S. Of these, two coupons were coated with Nutec 11, 24 hours later, and one was coated with Nutec 11 aft 2r only 6 hours. The one specimen with the 6 hour 115/11 incarcoat cure was then topcoated with Nutec 1201 follsving a 24 hour cure of the Futee 11. The remaining two coupons with the 24 hour 113/11 intercoat cure were handled as follows: Cne specimen was copcoated 4 hours after the application of the Nutec 11, while the other was copcoated following 'a 24 hour curing of the Nutec 11. To summarize: Counon # Descriotion 3535 11S/11 6 hour intercoat cure 3537 11/1201 4 hour intercoat cure
> 3539 Standard 24 hour intercoat times f
- Refer to the attached panel preparation sheets for details of application and l cur ing.
The coated specimens were allowed to cure approximately 22 days, then submitted to Coastal Science Associates for DBA Testing in accordance with the Houston Lighting and Power / South Texas Project conditions: 291*T. and 58PSIG (zaximum). j The duration of the test was four days-see attached diagrau. i
! RESULTS: See attached Coastal' Science Reports.
l l CONCLUSIONS: All test specimens, including those coated using short intercoat
- cure cines, performed well under DBA conditions, exhibiting no significant de-
,e facts. Por sinor repair applications, Nutec 115 =ay be coated with Nucee 11 as soon as the 115 has set to touch. The same is also true for cepcoating Nutec 11 s .
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% thinning, temperature, and to some extent relative humidity. Because of the n eber of variables that can effect the set time and the corresponding release of solvent, the practice of using short intercoat times is recommended only for small areas.
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REFERENCE:
Lab Notebook 133 pg.155. L i'g t f e 4 A % l e e, e
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e T"ST PANEL PREPARATION *:A*
- 1. Product to be Tested: Nutec 11S/Mutec 11/Mutec 1201
- 2. Type substrates concrete SIZZ: 2 x 4 x 2"
- 3. Surface Preparation (describe): 100 osi comoressed air 1
- 4. PfCDCCT ".UL"K Sample- No(s) : 3535
- 5. Date and Time Caring ^ v d or PFm Appliad N/A TOG: &
P CCCCT APPL:ckT:cs m 220NS TIICCIESS ::A=E CCAT P1cDCC" COCE _ BA*CI 4 ME"5CD R/M (OF ) % R.R. fins.) APPt.IED Nucee
- 11S 2671/I.3150/I.5148 Squeegee 75/54 .015 .020" 10/17/77 11 a.m.
Nucee 11 2671/L3150/I.3149 Squeesee 82/48 .003 .005" 10/17/77
, 5 p.m.
{ 84/56 .004 .006" 10/18/77 Nutec 1201 2467/2568 Spray j 4 p.m.
, ,)'
- '. Total dry film thickness .022 .031" t
70 - 80 or Ra1. Humidity 45 - 602 g
- 6. Curing canditions: Ambient Temp.
M' n 4 == cure 22 g
- 7. Test Precedure DBA car HI.&P/ South Texas Testing Perf rmed By: Coastal Science Associates Oata 11/11/77
! 8. Prepared Syr ..
! Data 'l=2 ~21- 7 9 Approved By:- N/f cata: //f/stv
- Raport No.
t i
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"57 PA:.E PREPARATI::N llA" i
- 1. Product to be Testad Nutec 115/Nucee 11/Nutec 1201
< 2. Type substrata: Concrete SIZI: 2 x 4 x 2" ,
- 3. Surface Preparation (describe): 100 psi compressed air i
'b i 4. PacDDCT DATA: Sgle No(s): 3537 S. Data and Time Curing FW cr Primer Applied:
N/A TIME: & i FICDDCT APPLICATICN CONUITIONE "JECINESS CATE COAT PRCDUC'" COCE BATc3 9
- METECD R/M (*?) % R.E. (ins.) APPLIZ:3 Nutec 115 2671/LN150/L3148 Squeegee 74/54 .015 .020" 10/17/77 11 a.m.
Nutec 11 2671/L3150/L3149 Squeesee 82/55 .003 .005" 10/18/77 11:40 am i Nutec 1201 2467/2568 Spray 84/56 .004 .006" 10/18/77
' 3:45 p.m.
Total dry film thickness: .022 .031"
- 6. 70 - 80 Ra1. Numidity
$~ g Curing conditions: Ambient Temp; F
.w4 n4 == C:xre 22 Days
- 7. Test Procedurer DBA per F.&P/ South Texas
, 8. Testing Perforand By: e,..,,5 ges .., r , asgeeines Cate: 11/11/77 j Prepared By: 8 [. b d l Dates /4-47-79 AFPrzed 3ys. MZ/ > e t.: //_.</h Report No. i i D i ! l t : 1
~ * ~ * * ' '
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~257 PA::E* PFIPA.M"'!::N llA" i
- 0 L. Product to be Tested: Nutec 115/Nutee 11/Nutec 1201
- 2. Type substrates Concrete SIZE: 2 x 4 x 2"
- 3. Surface Preparation (describe) : 100 psi compressed air n
j i 4. FICDDCT DA*."
- Sgle No(s): 3539 S. Date and "."as curag "W or Prmd Appl.ied: N/A m&
PEDDOCT APPLI 3TICN N CNE .YICKNESS cA:= C37 PRCDCCT COCE BATCI 4 ' . METICD , R/M (OF) % R.E.. (ins.) APPTI C Nutec 115 2671/L3150/L3148 Squeegee 74/54 .015 .020" 10/17/77 i 11 a.m. Nutec 11 2671/L3150/L3149 Squeegee 82/55 .003 .005" 10/18/77 11:40 am Nutec 1201 2467/2568 Spray 80/68 .004 .006" 10/19/77 11 a.m.
?
Total dry film thickness: .022 .031" QT. ?
- 6. Caring canditions: Ambiene Temp. 70 - 80 o f g g g g7 45 - 60 g
.w<,4,.,. Care 22 c,y,
- 7. Test Procedura: DBA per E&P/ South Texas
- 8. Testing Perfczmod 3y: ,,...., os..,,. 3,,,,rs ... :: ate: 11/11/77 Prepared Eye Dater /2"22~7f Approved By:- N//
Date: / /J//0 asport No. I 9 es.am
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I ~ A, i ASSOC 2ATES h u (504) 283 4 258 l COASTAL 6900 C AN A L SOU L EV A RD SCIENCE e NEW O RL E A N S, LOUISI AN A 70124 4 < PRINT DATE: 11/14/77 PRODUCT IDCJTITICATION r 1 CONCRETE DBA TEST CONDITIONS: HOUSTON LIGHTING AND PC'JER, SHORTCJED TO 96 HOURS. CCMMENTS SAMPLE NUMBER
-- .................g..........................................
?. SIDE ONE: NO ELISTERS, CRACKS, TLAX NG, DELAMINATIONS, 3
3535 OR OTHER DETECTS DETECTED SIDE TV0 NO ELISTERS, CRACXS, FLAXING, DELAMINATIONS, OR OTHER DETECTS DETECTED. SIDE THREE: NO ELISTERS, CRACKS, TLAXING, DELAMINATIONS, OR OTHER DEFECTS DETECTED. SIDE TOUR: NO ELISTERS, CP.ACX S, FLAXING, DELAMINATIONS, l OR OTHER DETECTS DETECTED. 1 REPCRT NUMBER 352111477 l I APPROVED f 1./ i COOPER ATIVE STUDIES
- TECHNICAL PROGRAM EVALUATICN
- POLLU'*lGN A S A TEMEN T MARINE COATINGS & TESTING
- CHEMICAL / PHYSICS CCNSUuTING i
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l CC ASTAL SCIENCE ASSOCIATES g} _ (504) 283-7158 0900 C AN AL SQULEV ARD e NEW QRLEANS,gougSgANA yog24 _ '! PRINT DATE: 11/14/77 PRODUCT IDENTITICATION: 1 CONCRETE DSA TEST CONDITIONS: HOUSTON LIGHTING AND POWER, SHORTENED To 96 HOURS. 1 SAMPLE NUMBER CDMMENTS 3537 SIDE ONE: NO SLISTERS, CRACKS, FLAKING, DELAMINA*ICNS, OR QTHER DETECTS DETECTED. SIDE TWO: NO ELIS*ERS, CRACKS, FLAKING, DE:AMINATIONS, OR OTHER DETECTS DETECTED. SIDE THREE: NO ELISTERS, CRACKS, FLAKING, DELAMINATIONS, OR OTHER DETECTS DETECTED. SIDE FOUR: N0 ELISTERS, CRACKS, FLAKING, DELAMINATIONS, OR OTHER DETECTS DETECTED. I l REPORT NUMSER 3 521114 7'T AFPROVED / t.f.A., d'dv i 4 CCCPER ATIVE STUDIES
- TECHNICAL PROGRAM EVALUATICN , POLLUTION AS ATE VENT MARINE COATINGS & TESTING e CHENICAL / PHYSICS CONSULTING
" * * " ' * *
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W.f ". ' . - R;*.,:1d ?- gMS--?'.qGY*--@r t ~%~3?W.f'. e 4 o l COASTAL SCIENCE ASS OCI ATES 6 900 C AN A L B O U L EV A RD e NEW O R L E A N S , s,0 U I S I A N A 70I24 w (504) 183 72SI h 1 4 1 l PRINT DATE: 11/14/77 PRODUCT IDCJTIFI CATION : 1 CONCRE*E DBA TEST CONDITIONS: HOUSTON LIGHTING AND POWER, SHORTENED TO 96 HOURS. SAMPLE NUMSER COMM DJTS
-...................g..........................................
3539 SIDE ONE: NO SLISTERS, CRACKS, FLAKING, DELAMINATIONS, 2 OR OTHER DEFECTS DE*ECTED. v
^
SIDE TV0: CNE FLAKE, ABOUT 1/4", LOVER HALF. SIDE THREE: NO ELISTERS, CRACKS, FLAKING, DELAMINATIONS, OR OTHER DEFECTS DETECTED. t, SIDE FOUR: NO ELISTERS, CRACKS, FLAKING, DELAMINATIONS, OR OTHER DEFECTS DETECTED. l 1 1 REPORT NUMBER 252111477 '{ g,y W APPRCVED [/ e I
! ( !(-
C00PER ATIVE STUDIES
- TECHNICAL PROGRAM EVALUATICN
- POLLUTICN ABATEMENT MARINE CO ATINGS & TESTING e CHEMICAL / PHYSICS CONSUL TING u
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WN$.., ? 1, _ I i i TECENICAL REPORT NOlBER .
" 115-3-78 4
1
.a TITLE CBA, RADIATICN. CEC 0!C2MI?aTION, TI.T" RIST*S #10/11S/11/1201 FOR t
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' CL*STO.\lE R I
Subtritted by: cak Ridge Natieral Libersecries i Approved: Date: 4/5/78 , SOLTHED L\tPERIAL COATINGS CORPORATION. LNC. P. O. Box 190'~
- New Orleans. Lou:suna 70130 Phone: 1504i2541432 l
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'** "S? PAN"*.: PREPARA'."!CN CAT"4 f PRCCDCT TO 3E 'l'ESTED: NUTC #10/NUTEC 411S/NUSC #11/PE.ACTIC #1201 Concrete e.Bechtal CP-956 SHE: 2" x 4" x 2"
- 2. TryE SUBST3ULTE:
- 3. SURFACE PREPARACCN (Desc=1.he): All surfaces blasted with 100 psi compressed air.
~
1 4' PRCCUC:l' DATA: SAMPLZ NO.(s): 2377 SL CAC AND CME CC1L'%. CCMPCCND CR PRIMER APPLIEDs 3/11/77 4., 4 PRCDUC'l* APPLICACCN COND CICMS *:'EICK:ESS . 2 ".!E & CA O l COCES
~
BATCH # ME."1CD R/M(CT) % R.H ._ ' (ins.) APPLEO CCAT PRCCCCT. ,
#10 1297/1315/1347 Spray 75 F/78%
- 3/11/77 1 . NUTEC
#115 1310/1556/1312 . Squeegee 75 F/58% " 4/8/77 2 NUNC NUT C #11 1313/1314 Squeegee '78 F/64% ** 4/9/77
'3 41201 7497/7434 Spray 82 F/48% " 4/11/77 4 REACTIC 7
'Nutec #10 Spray Applied at 400 ft / gal.
I NL'1TC #115 i NU"ZC ell i REACTIC #1201i
** .su.=um I.'ucxt. ass
, , y m q ,,,. , ,.,,, .) yg y,q m, 3, ,, g ny, nn, g ,
Average Thi kaess Sides adjacent to .015 .020ir .005 .010 in .007 .008 in 6 nroemed surface f
- Maxist$a Thickness Side opposite * .025 .0351: .015 .020 in .010 .012 in Broomed surface j Total Dry Film ':hickness Range - .016 .067 inches -
- i. * .
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- 6. CORING C::NDICONS: AMBIENT TIMP. 70-a0 F REL. EI2COCT 40-45 %
l CAZS MINIMCM CORE 11 I t
- 7. TEST PFA w :
Radiation - CBA Bechtel CP-951 and CP-956 Cak Ridge National Laboratories 4/22/77
,:A g 3:33 ,,3
' 8. TESC NG PZ3ECE'ID BY:
APPPCVE3 BY: /d M . -. - ' f g, 4/5/76 s PPIPAPIO BT: CATE: I. 4/5/78
$ ((5$ .
TEST RIPOK" NO. : 115-3-79 l . 12 n- ~, ,- . m.- - - - .
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1 i . 1 1 CBA AND RAOIACON ~OLI27*;C s O*" '+ TEST PANC. PREPARA*":0N SA"7. s 4 l yEDCCT TO BE SSED: NU30 910/NURC DllS/NITITC ell /RECC 41201 Conerete,- Bechte1 CP-956 3:::lg3 2" x 4" x 2"
- 1. TFFE SUBSTRAM :
All surfaces blasted with 100 psi ccmcrossed at:
- 1. SURFACE PREPARATION (D'sc::ibe) :
~
2379
; PEDCCT DATA: SAMPLZ NO.(s):
1/11/7-1.. DATT AND 2 CORING NCMD OR PRIMER APPL:ID: . APPLICATICN ' CONDITIONS SICCZESS T : E 4 ::A~ T PEtx CT * (ins.) AP7LIEO
$ BATCH 4 .6 R/M(CT) % R.H.
*::AT PPcCCCT- CCDES - .
,J 510 1297/1315/1347 Spray 7$ F/784
- 3/11/77 1 .
NUEC NUED #115 1310/1556/1312 Squeegee 75 F/58s ** 4/8/77 2 911 1313/1314 Squeegee 78 F/64% ** ,4/9/77
*3 NtTITC
#1201 7497/7434 Spray 82 F/48% ** 4/11/77
- 4 PIET:C
*Nutec 910 Spray Applied at 400 ft / gal.
' Nt?ITC ells I NUU C 411 REACTIC #1201i
_co,_ ocs . _ec3. ,c= 4.
** ! Minimum rnicxness L u e ,,,.,w. .eto. . cis t.t _
Average Thicknest Sides adjacent to 015 .020 in .005 .010 i$- .007 .008 in n e = d sm;" ace Maximum Thickness Side opposite- .025 .035 in .015 .020 in .010 .012 in Br somed surface Total Dry Film Thickness Range - .016 .067 inc.%s -
- 6. CORING CONOITIONS: A:GIINT TIMP. 70-80 F REL. iiUMIDITT 40-65
. M i CORE 11 CATS .
- 7. =ST ypcc :URI: * :BA - Bechtel CP-956 Cak Ridge National I.abora'tcries CA2 SC3MI.a 4/22/77
- 8. TIa.-.lG PERFCEMED BT r ./
APPPCVED 3Y: W N s CNTE: 4/5/78 PRIPARID BY: db . b, CATE: 4/5/78 -
- j. ,
i
' TEST PIPCRT NO. : **5_3.-e 13
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- 1 a
s % L. TEST PANEL PREPARA""0N CA"'A i 1 i I PRCCOCT TD SE 25 2 3: NUSC 410/NUTEC 911S/NCTIEC #11/REACTIC 41201
; L. TyyE SUBSTRATE: Concrete . Bechtel CP-956 SI2: 2" x 4" x 2"
- 3. SURPACE PREPARAT:CN (Desc=1be): m . , ,,, , , . u . . . . a .2 4 % 3no .. ~., . a .4..
4' PICDUCT CA A SAMPLZ NO.(s): 2381 4
- 5-. DA2 AND T3E CURING COMPCCND CR PRIMER APPCED: 3/11/77 APPC CATICN .CONDIC CNS 5 :CKNE.SS 2 & 'A~~
PICCCCT PICCUCT CDDES BA"CH 4 METECD 7/M (C'E*) t R.H . fins.) APPLII: CCAT , NUTEC #10 1297/1315/1347 Spray 759E78%
- 3/11/77 1 .
ells 131J/1556/1312 . Squeegee 75 F/58% ** 4/8/77 2 NUTEC 911 1313/1314 Squeegee 78 F/64% ** 4/9/77
~3 NUSC 91201 7497/7434 Spray 82 F/48% " 4/11/77 4 REACT!*
- NUTEC 910 spray applied at 400 ft / gal.
I NMTC #115 i NUTEC 411 I REACU C #12011
** m a m m ess
. , ,,._ ,, ,,,,,,,m-e '
-998 0M i n .0H .020 in ' .010 .012 in i Average 'Ihickness Sides adjacent to .015 .020 in .005 .010 in .007 .008 in Broceed surface Minimum Thickness Side opposite .010 .015 1rt .003 .005 in .003 .005 in Breemed sur" ace Total try Film Thickness Range - .016 .067 inches
# 40-45
- 6. CTR3G CONDICCNS: AM5 3 2 *E.MP. 7b-80 F REL. ECMCITY %
. 6 CORE 11 CAYS .
7*. "ST PPCCIOCKE: . Radiatien - CBA - Bechtel CP-951 and CP-956
- 8. TEST D C PI JCEMED BY: Cak Ridge National Laboratories CA:3 S:3Mn g3 4/22/77 APPPCVED BT:." " Y b m
CATE: 4/5/78 PREPAPID ST: ( [
CATE: 4/5/78 4 TEST REPORT NO. ,,,_,_- f
- 14 f' --- . . _ . . . . , , - .. . , _ . . _ , , _ . . ,,
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l DBA AND RAOIACON **':LIPXT 9' . EST PANE:. PPI7 ARA'l' ION CA"'A I PRODUCT TO BE 3333: NCTEC 410/NC3C tilS/NUSC til/REACIC #1231
- 2. TYPE SUBSTRATE: Concrete.- Bechtel CP-956 sue s 2" x 4" x 2" 3, gggract PREPARA= cN (Describe) : All surfaces blasted with 100 psi compressed air.
= ~
4~ PICDUCT DATk: SAMPI.E NO.(s): Sint 5-. DA2 AND N C "4CNC CCMPCCMD CR PRIMER APPI.IID: 1/11/77 PEIX3C APPI.: CATION CONDIT!CNS MIC2 CESS ", M & CAO
- APPLIZO CCAT' PRCOUCT CDDES EATCE 4 METICD R/M(87) % R.R. (ins.)
1 . NMEC #10 1297/1315/1347 Spray 759F/784
- 3/11/77 o "
2 NMEC ells 1310/1556/1312 squeegee 75 r/58% . 4/8/77
~
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's NUTEC ell 1313/1314 Squeegee 78 F/64% " 4/9/77 REAC'"IC 91201 7494/7434 Spray 82*F/48% " 4/11/77
^
- NUTEC #10 spray applied at 400 f t / gal. .
I NUlTC 4115 i NUSC ell i REACTIC #1201(
.. w ,. 4 -,, me t, ,. . . . u -A m, se. i . net _oss u ots .o20 in I .010 .012 in t Average nickness Sides adjacent to .015 .020 in .005 .010 in .007 .008 in
,, g , g ,,,
Minimum' Thickness side opposite- .010 .015 in .003 .005 in .003 .005 in a m mad surface Total Dry Film Mickness Range - .016 .067 inches 8
- 6. C3.3G CCMDICCNS: AMBIENT TZMP. 70-80 7 . m 3:Ty 40-65 g MINIMCM CORE 11 CAYS .
7 *, =sT PRCCEEURE: . CBA - Bechtel CP-956
- 8. TES=NG PERTCP.MED BY: Cak Ridge National Laboratories CA 2 57EM m 4/22/77 i APPICVEO BY: . M~ , * .
t - gg, 4/5/78 PRIPARED BY: d a.IO [. j CATE: 4/5/79 .
. l TEST REPORT NO. its., ,.
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" Southern Imcerial Analytical Chemistry Division Manufacturer: Oak Ridge National Laboratory l'
Nov Orleans. t.A Cata: 5/11/77 1 1 System Identification: Steel X Concreta Block 10/115/11/1201 (7-day cure) , 4 08A Test Results: ORNL Master Analytical Ma6ual Method No. 2 0922;
- 5echtal Corp. Spec. No. CP-956; ORNL Log Book No. A 7562; 4-29-7 08A Phase Ccfuents "
Samole No.
*2377 scrav Coatinos intact: no defects, all sides.
2379 serav Coatinos intact: no defects, att sides.
*2381 sorav *
- Coatines intact no defects, all sides.
2382 scrav Coatinos intact: no defects, all ' sides.
' Irradiated. "($A) = sand blast; (SH) = shot blast; (GR) = grit blast. .1 l -
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4 1 i . 4 O. - i s i RADIATION TCLIRANCE TEST R2 UL:s O I f I 4 a e I e I
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] . . . - . ._ ,, i <. Analytical Chemistry Divisic.9 Ta~#g ' Manufacturer: Soutaern Imoerial , Cak Ridge Mtional Lancracry New Orleans, LA Data: 5-31 -77 d System Identification: Steel Panel X Concreta Block 1 10/115/11/1201 (7-day cure) Radiation Toleranca Test Results: ORNL Master Analytical Wnual Method No. 2 0921; 8echtal Corp. Spec. No.. CP-951; ORM. Log Book No. A 7562; 4 7 Initial Dose Rata: 1.55 x 107 rads /hr Test Conducted In: X air water Cumulative Oose Rate: Consents l'I 10' rods 1 x 10' esds Samole No. Coatinos intact; no defects. 2377 2381 Coatinos intact: no defects. Additional Ccnnents: Evaluated E 4. rs Aporoved__ _ e ed
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- 'EC': TAM *'!AT!.**; TEST BECR':Ti, CP-95 2 A:C A.N.S . I . N-5. l*
TEST PANET. PPIPAEA"."CN CATA -l 1. PRCDUCT TO BE TES2D: EACTIC #1201 ASTM A-36 Carbon Steel S:23 2" x 4" x 1/4"
- 2. TTFE SUBSTRATE:
l 3. SCEFACE PREPARATION (Describe) : Sandblasted per SSPC-SP-10 with Crosblast $4 Blasting Sand. Surface profile between 1370 and 2570 as read on a Keane-Tator Profile Cosq:arator Disc.
- 4. PRODUCT CATA: SAMPI.E NO. (s) : 688 PICDCCT . APPI. CATICN CC'CICONS THIC: CESS OA2 CAT PRCOCC'" CCCES BATCH 4 METHCD R/M( F) % R.E. (ins) APPI.II:
1 NUTIC #6 '6169/6170 Spray 82 T/63% .0024- 7/ 29/76
.0033 5:00 p.m.
2 MAC=C #1201 6171/6172 Spray 92 r/59% .0056- 8/5/76
.0077 12:00 noca Total Dry Film Thickness .0080 .0110 O,:'
v . 4 75 + - 5 c 60 A 10 g - i 5. CTRING C::NOICONS: AME:I C TEMP: T FI:. EC2C::: T I l 7 M3:MCM CURE: DAYS
- 6. TEST PRCC::URE Decen*= hmtion
- 7. TES CNG PERYORMED BY: Cak Rides National I4boratories cA;g 3;3xIngs:8/12/76 t
321FCIED: * ' /,!. - TIST FI7CRT NO. ite_s-7e . l r I . PREPARED BY: M d,' [,d , W" 4/5/98 1,.
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. Itanufacturer: Sout en imeerial r. Analyt il Chemistry Divisien
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Oak Ridge National Laboratory
> Ovleans. U Date: Secteet:er 15, 1976 i 3 v.
l Decontamination Test Results: These tests performed according to ORNL Master Analytical Manual
! Method No. 2 0920 and Bechtel Corp. Spec. CP-952.
ORNL Log Book No. A 7562; 8-12-6 . Pe ent of
.' Decontamination Factor (OF)
Water Acid Acid Sample Contaminant 925'C 925'c 980*C Overall Activit{ Removed
. Numoer 673 Co-144 87 1.9 -
1.6 270 , (1203) Ru-106 41 1.6 1.6 100 Cs-137 680 1.2 1.7 1400 Zr-95 20 1.5 1.0 31 TOTAL 70 1.6 1.5 170 99.4 688 Ce-144 120 2.1 1.0 250 OT ' (1201) Ru-106 Cs-137 68 160 1.6 1.3 1.1 1.4 120 280 Zr-95 17 1.6 1.1 29 . TOTAL 85 1.6 1.1 160 99.4 772 Ce-144 1.7 4.0 1.8 13 . Ru-106 2.3 1.7 1.4 5.5
. (555)
Cs-137 20 2.6 1.9 98
'Zr-95 1.1 1.9 2.0 4.3 TOTAL 2.7 2.4 1.6 10 90.0 .
Ce-144 Ru-106 Cs-137 Zr-95 . TOTAL Ce-144 Ru-106 Cs-137
- l. Zr-95
- TOTAL l .
3 Percent of total activity removed = (1 - g) x 100, i
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i O ~ . _ _ _ _ . ggggg ,a PRCFESSICNAL CCATINGS R Q. Son 29077 New crears. Lousara 70189 U.SA. 504 2541433 lv -1 VBR-7496 .J April 13, 1978 Mr. Don Sutton c/o Brown & Root Comanche Peak Steam Electric Station P.O. Box 1001 GLDI RCSE, TX 76043 .
SUBJECT:
Markings on Concrete Attached is a copy of Technical report $246-78-G, describing the ecmpatibility
/ testing of Nutec filS and Reactic #1201,over felt-tipped marking inks on ccacrete and Nutec ills.
CBA testing over black and white felt-tipped markings revealed no significant
, c,' difacts, other than bleeding through of the black markings (black =a.rking inks *
'< - ot ells bled through the topccat) .
It is strongly reccamended that a solvent dissolvable marker be used, such as a felt tip marking pen. A white marking pen would be desirable to prevent bleeding. Prior to application of the coating, I recosenend the =arkings be se 1 vent wiped per S$PC-SP-1 with CL-6A Universal solvent, or Xylol. The cleaned surface shall be allowed to dry thoroughly before the coating is applied. Marking stains imbedded in the concrete and not removable by this procedure should not be deleterious to the coatings performance. PREPARE 3 3Y: I< N APPRCVED BY 7 .
/
CATE: 4/19/78 d I.
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u TECHNICAL REPORT f NUMBER 246-78-G w'
- TITLE Effects of felt-tip Markers en 9113/1201 system FOR Company Knowledge
- S'.R.41396 I CUSTOMER -
I i i Submitted by: c s1:a cience Associates Approved: -
! Date: 4/78 SOtJTHERN L%iPERIAL COATLNCS CORPORATION. INC. ' P. O. Box 29077, + New Orleans. Louisiana 70189 Phone: (104) 154 1433 l
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i l t O T.R.4246-78-C i page 1. 1 , 4 l
SUMMARY
- Black and white felt tip markings were applied to concrete and 1
Nutec fus surfaces. The test specimen was completely coated with the Nutec ens /Reactic 01201 system and than CBA tasted to determine the effect of the markings. The coated test specimen was exposed to DBA conditions in an autoclave for 24 houp (Coastal Science Associatas) with maxistaa tasperature and pressure of 307 F. and 58 psig.
- Careful inspection of the specimen revealed co defects other than bleeding through of the black markings.
INTECCtrTICN Se objective of this test ma to dataraine what effect, if any, felt tip marXings on concreta and Nutec $113.would have on the 4113/1201 systas.
,52THCCS: .. .
- a. Specimen: the tast specimen used was a concrete coupon, measuring
- 2" x 4" x 2". and prepared in accordance with the proposed ASTM D1.43
*' (modified) mix and ASTM C192-69 procedure. The concreta specimen was cured by applying Nutac $10 as a curing membrane within 24 hours of the removal of the concreta from the forms.
- b. Mazkings: Two types of felt tip markers were used:
- 1. Whita - white marker Cartar's Ink Company Cambridge, Mass. 02142
. 2. Black - Graphi 500
. Graphic Industries ,
L.A., Calif. 90038 , Each marker was applied to the concreta and to the applied Nutec filS. I Markar tocation of Surface applied to
, Harking
. Whita Bottom face Concrete white Side B Nutec Sils Black Tcp face Concreta Black Side D Nutac fils
< c. Application: Nutac fils was applied to four faces of the ccacrete
{ .. .,.. . . coupon and wasz al.l. .- owed to.c.ure fully. The marking inks were applied
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G' T.R.#246-78-G l Page 2. <
' liberally to the top and bottem faces (bare concrete) and to tw of the four faces coated with Nutec 9115. Nutec $115 was applied I
i to the top and bottom faces after the markings had dried for 24 hours. The entire coupon was then topceated with Rmactic #1201. No s-cface preparation was used between coats to rezcvs the markings. Essentially, two systans were applied for tasting:
- 1. Markings /Nutec filS/Reactic 01201
- 2. Nutac fllS/ Markings /Emactic 81201 See attached panel preparatica sheet for application and curing details.
- d. Testing: D.e test specisen was allowed to cre for 17 days and then submitted to Coastal Science Associates for ::EA testing at the Houst=n Lighting and Power curn, Revision 0, 10-22-75. The ==v % temperature and pressure achieved was 307*F. and 58 psig.
RESULTS : No defects other than bleeding through of the black marking ink were no ted. Coastal Science reportad dense #6 blisters on Side D, however, micro-scopic inspection of the surface in question, revealed only the usual rough' surface.
~
Apparently the rough, sandpaper-lika surface, ccatrasted by the bleeding-through black marking ink was mistaken to be uniformly covered with small blisters. Although the test indir=ted no ecmpatibility problems, as a precaution it is suggestad that the markings be removed as well as possible by solvent wiping with Xylol, in accordance with SSPC-SP-1. i I RETTRENCIS: Lab. Notabook 056, p.p.53,54,56 i i l l . t c l l me - ( e t t
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CDASTAL SCIENCE ASSOCIATF'e INC.
' 4900 CANAL BLVD.
NEIJ ORLEANS, LOUISIANA 70124 4 ... TEL. 504-283-7051 . I ... . " 4
SUBJECT:
DESIGN BASIS ACCIDENT CCATINGS TEST REPORT.
- \
DATE: 3/21/78
- DBA TEST CONDITIONS:
24 HR. HLSP, REVISION O , RUN..... 307 DEG. F. HIGHEST TEMPERATURE DURING 58 LBS./ SO.,IN. HIGHEST PRESSURE DURING RUN..... SAMPLE TYPE: CONCRETE COUPON . SAMPLE NUMBER: 3790 SAMPLE 6 DESCRIPTION
, 3790 SITE 1 NO. DEFECTS .
d. SIDE 2: NO DEFECTS SIDE 3: NO DEFECTS
- SIDE 4: DENSE COVERAGE OF NO. 4 BLSSTERS, SURFACE COAT .
f.
. REPORT WRITTEN FOR:
- SOUTHERN IMPERIAL REPORT e 049032178 APPROVED SY..
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41 c r . s I e l ^ DBA AND RACIA*" ION TII?XIC" ' O::y < SST PA rE:, PPZFAMTICt! OA*:A_ NtTIEC 410/ NUTIC 4115/?'2 T C 41201 L PMcCCT M RE 253D: 2" x 4" x 2* SIZE 2 ., TTFE SUBSTRA3: Concrete 100 psi air bl="t j 3. StmrACE PREFARAT*.ON (Describe) : 7300CCT CA*:'As SA;@!J: NO. (s) : 379o 4' 5L DA3 AND ""IyJ: C 2. NG COMPCCND CIL PLT. A77L3D enm . T5:CCIESS TIME & OATE PMDCCT AFFLICAT:CN CONO TIONS AI?" 33 METECD R/M(OT) % R.R ._ ' (i:18. I CCAT PECOCC'" COCES _ BATC5 4 92*r/53% 400 ft / gal. 8/2/77 1 mmEC' 810 .6526/6531 spray , , Squeegee 64 P'/60% .025 .025 2/21/78 I 2 Ntr2EC fils 3227/3228/3229 , Spray 65 F/66% .005 .006 3/3/78 3 EEACTIC 01201 3952/3953 i
.. .041 Y' ,
Total dry film thickness .030
- 4 *
' a aa %
AME ENT 3 MF. in.sn F REL. 31:M 3:T s tii. CUR:2G CONO TIONS ~ MIMIMCM C RE 17 CATS DsA per Houston Lighting & Power, Revision 0, 10/22/75 , 7., g ,,gegggyg, Coastal Science Associates DA3 20BM:m 3/16M8
- 8. TEST 2tG 7ERTCRMED ST: .
Q M 7 AFFK:VED BT , 4/19/?9! DdTE: _ l . nEnREo T . - . A JDL 6.A~-CL
,,....,.DA:Z: 4/19/?g j
SST REPCIC No.: 246-78.C
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; Je TECHNICAL REPORT NUMBER y 249-78-G J
u/ M Effects of "Muderacking" on CBA perfor: nance of NU':ZC #115 FOR S.R.91401 CUSTOMER Brown & Root, Inc. Comanche Peak i ' Submitted by: as g seience Associatas Approved: ! - i , Date: 4/78
/
SOLTHERN LMPERIAL COATINGS CORPORATION. INC. P. O. Box 29077,
- New Orleans Loumana 70189 Phone: (504) 154-1433
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1 l T.R.9249-78-G Page 1. StDegutra ne purpose of this test was to determine what effects cracking of the Nutec 911S film has on the performance of the concrete coating system. l ,1 m
" No defects were noted on the test specimen fonowing DBA testing. ,
IEFFEODUCTION: "Muderacking" of Nutec SMS has been noted on two occasions; in the laboratory and at the t'a-a-ha Peak jobsite. The "mudcracking" phaaa=maaa was ; observed when rapid changes in surface or air temperatwo took place, immediately fonowing application of the Nutec 0113. E1cometer adhesion and Designed Sasis Accident tests were conducted on the laboratory speciana to assure that this phenomenon was not deleterious to the performance of the coating sys,tes. No defects were noted on the test specimen fonowing DBA testing at 307 F. and i 54 peig. Elconstar adhesion was also demonstrated to be escenent at 650 psi
' and 100% failure in the concrete. Me laboratory data was further supplemented by tests conducted by Brown & Root Quality Control at the Comanche Peak jobsita.
Elcoaster adhesion tests were performed with values greater than 500 psi. j MTscos Lab. panel 93795, a concrete coupon measuring 2" x 4" x 2" was coated with Nutec $US. The concrete had been previously coated with a concrete curing membrane, Res 1. The specimen was placed under running water, in search Y of water beads which would indicate the presence of a Res X surface film. Satisfied that such a surfacg film was not present on the concrete, the specimen was placed in an oven at 120 F. for 15 minutes in order, to espedite the applica-j Me room tion. The concreeg was still warm when the Nutec #113 was applied. Overnight the
- temperature was 54 F. and dropping due to a heater malfunction.
' temperature in the laboratory plunged to 28,F. film (which had modcracked overnight) was curet for an additional
- S 5 days 4 70-40 An E1 counter Adhesion test was conducted on the zuderacked e Nutec ells,F.
- SMS film.
t ! Shortly after the anderacking incident at Comanche Peak, the Elcometer' Adhesion damage was repaired with Nutec 0115 and the entire coupon topcoated with i Reactic 91201. Design Basis Accident testing was performed at Cogstal Science ' ' Associates with the =awi== temperature and pressure reaching 307 F. and 58 psig. Se DBA test was conducted over a 24 hour period and performed in accordance wita } ; nouston U ghting & Power, Revision 0, 10/22/75. l Refer to attached Test Panel Preparation ::ata sheet for details of surface preparation, coating application, and curing. ! RESULTSe
- a. E1cometer Adhesion - 650 psi with 1004 breakage in concrete
! h. CSA testing - No defects: all sides \ l
- (See attached Results sheet from Coastal Science Assoc.)
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CONC:,USIONS: h "mudcracked" film exhibited excellent adhesion to the concrete substrate and demonstrated the ability to withstand the high.
- temperature and pressures of a Designed Basis Accident test. Se laboratory test results were further supported by on-site E1 coaster Adhesion tests conducted by Brown & Root Quality control. The lowest value obtained in these tests was 500 psi.
The "auderacking" p h a w n is believed to occur because of large differences in surface and air temperatures resulting in varying degrees of expansica or contrac-tion within the thick ells film itself. Such changes can occur wneuever space heaters are used and also as in the case of the laboratory application. Because of its density, the concrete exhibits a greater resistance to tampera-ture cage than does the surrounding air. Se tenparature of the ills film in proximity with the concrete, closely approximates that of the concrete, whereas the fils exposed to the air, more closely approximates the air temperature.
REFERENCES:
I4b. Nce=M 956, pp. 35,58 i c
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* - PNYSICAL PRCPER S 6
BEG TE,CP-954 and A.N.S.I. N-5.12 6.. PECCCT 233 3: Nutec 0115
; 2. TFPE SUBSTRA N s 2" x 4" x 2" concreto coupon
- 3. SURFEE PREPARATION: Sandswept with Crosblast 94 blasting sand.
l
- 4. PICDOCT DAM: SAMPLE NOS. 3795 P30DCCT APPLICATICN CCNDITICNS MICENESS CA2 CDAT PRODUCT COMS BATE 9 ME3CD R/M ("F) 4 R.*H . (ins.) APPL 3D 1 Res x Brush 70 F/48g 200 ft / gal. 12/8/77 j 2 NC3C tils 3386/3388/*J149 Squeegee 58 F/28% .015 .025 12/10/77 l.
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- First day curing temperat=rs ranged from 28-58 F.
O 5. CUENG DAM: APSIENT EMP.
- 70-80 F REL. ' avaa.,A;-1: 45-60 g tc.7. C:nu: TI.g 5 Cays
- 6. EST PROCEDURE: Bechtel Standard CP-954 and A.N.S.I. N-5.12
- 7. EST RESCL"Si
7.1 ABRASION
Federal Test Method SemnAn d 141 Test Method 6192, 10C0 cycles with a CS-17 Wheel and a 1000 gram lacd. LCW - N/A EGE - N/A AVERAGE - N/A
7.2 AIEESICN
Determined by use of the ELCCMES R ACEESICN ESIER
~
650 ;si t 7.3 DIRECT IMPACT RESISTANCE: N/A J M APPRC r ,- 7 TEST REPCRT NC. 249- 8-G PREPARED 3Y: <- f
- CATE: 4/78
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SST PANC. PSIPARATON CA".'A 1 PRCCCCT TO at 232 3: NUSC #115/REACTIC 41201
- 2. TTPE SUBSTRATE: Concreto S:2 2" x 4" x 2"
- 3. SURFACE PREPARA20N (Desc:dhe): Sandswept with Crosblast #4 blasting sand.
J 4'. PICDCC: DA3 SAMPI.E NO. (s) : 3795
- 1. CATE AND TDC CORING COMPCCTD CR PR*MER APPI.IID: 12/8M7 i
PMCT APPLICA2CN COasuor ,NS 2:C'TIESS 2ME s CA 2 COAT PRCCCC'" CCCES BATCH # .MD R/M(C71 % R.E.
- fi:".s.) AFPI,IIO N
1 RES X Brush 70 F/48% 200 ft / gal. 10/8/77 2 NCNC fils 3386/3388/ Squeeges 58 F/38% .015 .025 10/10/77 fB149 o 3 REAC2C 01:01 3952/3953 Spray 62 F/66% .003 .004 3/3/78
- [-
Total Dry Film Thickness: .018 .029" 4 8 C
- 6. we aw CON !=ONS: AMB 2NT N . 70-80 y ;a=,, grynm 40-65 g
. M CORg 8 CATS l -
l l 7 ~. ESTss.u a: DBA per Housten I.ight.ing & Power, Revision 0, 10/22/75
- 3. "TST NG PERFORMED ST: r-...., e-4 . e.. a,wr4=t., CA 2 SC3M:2 ID 3/10n8 APPICVED BY: , _.
( CA2: 4/19/78 [ PREPARD SY: Id ((M - cA2: 4/19/78 j TEST REPCRT NC.: -.o_-o_,- l i l . _ _. . . . . . ~ . _. . . . . - _ . . . - . . . . . - - - . - . -
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1 COASTAL SCIENCE ASSOCI A"S, INC.
' 6900 CANAL BLVD.
l NEW ORLEANSr LOUISIANA 70124f
' TEL. 504-283-7251 < -e3 2
SUBJECT:
DESIGN BASIS ACCIDENT COATINGS TEST' REPORT. 4 1 DATE: 3/13/78 ", .
, DBA TEST CONDITIONS: ABREVkATEDHLSP (24 HOURS)
HIGHEST TEMPERATURE DURING RUN..... 307 DEG. F. HIGHEST PRESSURE DURING RUN..... 58 LBS./ SG. IN. SAMPLE NUMBER: 3795 SAMPLE TYPE: CONCRETE COUPON
~' **
SAMPLE 4 DESCRIPTION 3795 SIDE 1: NO DEFECTS I{' SIDE 2: NO DEFECTS b/ SIDE 3: NO DEFECTS SIDE 4: NO DEFECTS
-REPORT 'tRITTEN FOR: SOUTHERN IMPERIAL CDATINGS REPORT 4 068031 8 I APPROVED BY. ...... ... ....p ........
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I l TECHNICAL REPORT NUMBER
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167-77 TITLE Repairability of Nutac 11S/Nutec 11/*sactic 1201 FOR
~ .
CUSTOMER Submitted by: old j f Approved: Date: July 15, 1977 . SOLTTHERN IMPERIAL COATINGS C0iGORATION. LNC. l
- New Orleans, Louisiana 70189
' P. O. Box 29077 I
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- Phone: (504) 254-1433 l
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5 Repairability of Damaged Concrete Systems a The following report describes the repairability of the three systems i outlined below:
- 1. Conamet C cleaned /Nutec llS/Nutec 11/Reactic
- 2. Nutec 10/ Conamet C cleaned /Nutec 11S/Nutec 11/Reactic 1201
- 3. L & M cure-ft71tive dye /Nutec 11S/Nutec 11/Reactic 1201 Since, however, the damage incurred by the E1cometer adhesion tester occured in the concrete, the actual repairability evaluations reflect only the Nutec 11S/Nutec 11/Reactic 1201 system.
The tested specimens were damaged by means of an Elecmeter adhesion tester A high strength aluminum dollie was applied to each coupon with an epoxy resin type adhesive in accordance with 'c ial Test Method 03. The adhesive was allowed to cure thoroughly, then removed with the E1cometer. Failure Yi occured in the concrete. The purpose of this procedure is two folds to gen-erste adhesion data, and to inflict damage.
~.
- The damaged coupons were repaired with the original three ccat system:
Nutsc 11S/Nutec 11/Reactic 1201. The affected areas were hand sanded to re-move loose concrete and to feather edge the adjacent coating system. Compressed air, 100 psi, was used to remove any dust and cont =mination from the substrate prior to applying the Nutec 11S surfacer. Refer to the following panel preparation sheets for application and airing data of the applied touch up system. -
" Novsaoov h7u.sActs ,
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l i l T!lST PANEL PREPARATION G 9, i IEPAIRAB" .!TT & MA'T. ITNANCZ
- 1. Product to be Testads NU"TC ells /NtmtC All/REAC=;C al201
- 2. Type Subetrata Concrete - Bechtel CP-956 Size 2" x 4" x 2"
- 3. - Surface Preparatica (dancribe): All surfaces blasted with 100 esi comeressed air.
- 4. PEDDOCT DA2A: Sample No(s): 2369
- 5. Data and Time Curing '*-d or Primer Applied: L s M cure /fucitive dve acplied 3/3/77 N&
PEDDUCT APPLICATICN CCNDITI0tC MICENESS CATE COAT P'tCCCC"' COCE BA"C5 4 MES CD R/M (C?) g R.H. (ins.) APPL Z 1 L & M/ Fugit'. re Dye Spray 72/73
- 3/3/77 2 NUTEC 411S 1310/1556/1312 Squeegee 76/59 .015 .020 4/4/77 3 NUTEC #11 1313/1314 Squeegee 74/58 .005 .010 4/6/77
! 4 IEAc-IC 41201 7497/7434 Spray 82/48 .007 .008 4/11/7-29 e;! ~
* *L & M Cure / Fugitive Dye Mixture applied at a spread rate of 250 ft / gal.
- 6. C:zring Cmditions: Ambient Temp. 70-80 F ital. Inmidity 40-60 g 44 a4 == Cure 27 Days ,
l ,, I 7. Test P a - : CBA - $ usten Lichtine s Power (Rev. O. 10/22/75)
, 8. , Testing Perf=rmed By: Coastal Sciences Dated 647/iO
/ / /
.. F Approved By: , --
Data ~1 f/ W 7 9 l h ' Prepared By: AM[ ' i Dates /JP /'/2 Itaport No. 167-77 e 9 O .sp m
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TEST PANIT. PREPARACON CJL . O']. REPAI3ABILITT & .%MC2
- 1. Product to be Tested: m ells /NDTEC dil/REACTIC #1201
- 2. Type substrates Concrete - Bechtel CP-956 Size: 2" x 4" x 2" All surfaces blasted with 100 psi compressed
- 3.
- Surface Preparation (describe):
-; air.
- 4. PICDUCT DATA: Sample No(s):
- 5. Date and ".".no Curing "m-d or Primer Applied: L- & v. cure / fugitive dye applied 3/3/77 TIME &
l PRCDUCT APPLICACCN CONDITICNS "JCCZMESS CATE I C0&T PICCCC'f COCE BA M 8 ME".5CD R/M (C?) % R.H. (ins.) APP' m 1 L & M/ Fugitive Dve Spray 72/73
- 3/3/77 2 NUTEC ells 1121/1122/1123 Squeegee 80/60 .015 .020 3/10/77 s3 3 NUTEC #il 1124/1125 Squeegee 74/56 .005 .010 3/14/77 4 REACTIC 41201 7497/7434 Spray 80/68 .C07 .008 3/16/77 q, ., *L E M Cure /Fucitive Dye Mixture applied at a spread rate of 250 ft / gal.
, . ,, , z 70-80 40-60 g
- 6. Curing Condi"_cas: Ambient Temp. F Rel. Ruaidity pi n 4 9== Cure 27 ,
DBA'- Nbuston Lignting & Power (Rev. O, 10/22/75) 7 Test Procedures Coastal Sciences Da W 6/7477
- 8. Testing Performed By:
P / e ' _7 Approved Dates By: _%%/-. - / Prepared By: M'd[b Date: 7,//f,h79 3,pegg g, 167-77 O
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i 2ST RESULTS MR TOUCE-CP AND REPA3 i PRODUCT h T.a aCATION: Steel Panel Concrete Sicck lat Coat: See Panel Preparation 2nd Coat: 3rd Coats -- TotX2-CP PM: Methed of Damage: Eleemeter adhesien test - break in ecnerate Surface Preparatica Damaged area hand sanded and feather edged Touch-Co Coating: 1st Coat: NOTEC 4115 4/22/77 .015 .020
' 2nd Coat NUT C 411 5/2/77 .005 .010 3rd coat: REACTIC 41201 5/11/77 .005 .007 DBA 2 s? RESULTs:
CENL Master Analytical Manual Me*%i No. 2 0922. Sample No. Comments CBA Phase rM " See Coastal Science Beport 4043G60iii b g-
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l EST RESCT.TS ICR TCUCE-CP AND REPAIR PRODUCT MCICATION: Stael Panel X Cencrete Block ist Coat: 2nd Coat See Panel Prepara* den l. 3rd Coat T*?UC5-UP PRCCDCRE: gg ,g Elcometer adhesien test - break in concreta Surface Preparation: Damaged area hand sanded and feather edged Tcuch-Un Coating: 1st Ccat NUSC 4113 4/22/77 .015 .020 2nd coat: NUTEC $11 5/2/77 .005 .010 3rd Coat: REACTIC $1201 5/11/77 .005 .007 DBA 257 . M TS: CRNL Master Analytical Manual Method No. 2 0922. Sammle No. ::SA Phase Conuments k.', See Coastal Science Recort 4040060777 4 j . . l l0 l_ Approved By: M
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l 1 . EsT REsm.:s FCR TCCCH-CP AND IEPAIR A.. . X Concreta 31cck PRODUCT I::E3rrIFICATICN: Steel Panel l let Coat: See Panel Preparation 2nd Coat:
-i 3rd coat:
l j TOUG-CP PEOCECIE: 4 Method of Damage: *E1cometer adhesion test - break in concrete Surface Preparation: Oamaged area hand sanded and feather edged f Touch-Un Coatings lat Coat: NUTEC #11S 4/22/77 .015 .020 2nd coat: NUTEC 411 5/2/77 .005 010 3rd Ccat: REACTIC 41201 5/11/77 .005 .007 DBA EST RESCI.TS: CENL Master Analytical Manual Met.%d No. 2 0922. 1 Sample No. CBA Phase F"'Its See Coastal Science Report 9040060777 A$[
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TEST RESW.TS FCR TCtX3-CP AND REPA22 PICDUCT I E!!TIFICATION: Steel Panel X Concrete Sleck lat Coat: 2nd Coat: See Panel Precaration
/ 3rd coats d .. TCt3CI-UP PICCEDU1E 1 ! Method of Oamage: Elcometer adhesien test - break in concrete Surface Preparatica: Damaged area hand sanded and feather edged a Touch-Co Coating: 1st Coati NUTEC #11S 4/22/77 .015 .020 1
1 2nd Coat: NUTEC 411 5/2/77 .005 .010 3d Coat: REACTIC #1201 5/11/77 .005 .007 J, OBA *.*ST RE3ULTS: 9 CRML Master Analytical Manual Method No. 2 0922.
-]
Samuple No. CSA Phase Comments : g;' y See Coastal Science Report 4040060777
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Report No. 167-77 l eig** 4+ e=9- p ...q..,gp , , , ,
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. TEST PANC. PREPARACCN L A'A O3. REPADABL"! & .CMNCE
- l. Product to be Tested: NUTEC 410/NUTEC 411S/NUTEC til/REACC C #1201 1
- 2. Type Substrates Concrete - Bechtel CP-956 Size: 2" x 4" x 2"
- 3. Surface Preparation (describe): NITTEC 410 cured concrete scrubbed and rinsed with i
diluted conamet C (Engineered Design Products)
- 4. PRODUCT DATAs Sample No(s):
- 5. Data and Time Curing Pd or Primer Applied: Primer / Sealer applied 7/9/76 TOS &
PICDCCT APPL *CATICN CONDITIONS TRICENESS CATE CCAT PN CCCE BATCH 8 MEMCD R/M (CF) % R.H. fins.) AP"_.*EO 1 NUTEC 410 6154/6155 Spray 86/70
- 7/9/76 j 2 NtT?EC #11S 1310/1556/1312 Squeegee 76/59 .015 .020 4/4/77 3 NUTEC 411 1313/1314 squeegee 74/58 .005 .010 4/6/77 4 REACJIC 41201 7497/7434 Spray 82/48 .007 .008 4/ 11/77
- NUTEC 910 applied at a spr' e ad rate of 350 ft / gal.
# 40-60
- 6. Curing canditions: Ambient Temp. 70-80 F Rel. Humidity g
*4 == Cure 27 g
- 7. Test Procedure: CBA % Houston Lighting & Power (Rev. O, 10/22/75)
- 8. Testing Performed By: Coastal Sciences c. , , 6/ M 7
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. REPAIRAB L*TT & F N CE
- 1. Product to be Tested: NUTEC 411S/NUTEC dll/REACM C 51201
- 2. Type Substrates Concrete - Bechtel CP-956 Size: 2" x 4" x 2"
- 3. - Surface Preparation (der.cribe) : Concrete scrubbed and rinsed with concentrated i
Conamet C (Enginee ed Design Products)
]
- 4. PEDDUCT DATA: SJaple No(s): 2361
- 5. Date and Time Curing "T=A or Primer Applied: N/A
':DG: (.
PR: DUCT APPLICATICN C::NDISCNS THICK:ES3 CAT 3 COAT PRCCCCT CCt2 BATCH 4 ME"NCD R/M (O*) 4 R.H. (ins.) . APPC
; # 1 Nt7FEC 4115 1310/1556/1312 Squeegee 76/59 .015 .020 4/4/77 1 2 NUTEC fil 1313/1314 Squeegee 74/58 .005 .010 4/6/77 3 REACTIC #1201 7497/7434 Spray 82/48 .007 .008 4/11/77 ti%
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- 6. C:zri.ng Conditions: Amt:ient Temp. _70-80 F Rel. Humidity 40-60 g w4 n 4,"= C::re *7 Days
- 7. Test uh .: OBA - souston Lighting & Power (Rev. O, 10/22/75)
. 8.
.. Testing Performed Sys Coastal Sciences Da
/ 6/7/77 Approved By: Q er-
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Date M/9//? [ Prepared By: JI f A
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Date: 7//W77 167-77 Report No. l l s . .e.
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f i l COASTAL SCIENCE ASSOCIATES e NEW O R LE AN S, LOUISl AN A 70124 (504) 283 72Sl l 6 900 C A N A L S O U L E V A R D I 5 Date: July 14, 1977 Product Identifications _ Steel Panel _koncrete Eleck DEA Test conditions: Houston Lighting and Power Curve, nev. O, Oct. 22, 1975 Sample No. Comments 2367 No cracks, blisters, flakes, or loss of adhesion on any side. 2369 No cracks, blisters, flakes, or less of adhesion on any side. 2364 No cracks, blisters, flakes', or loss of adhesion on any side. g, 2361 No cracks, blisters, flakes, or loss of adhesion on any side. Approved M M u
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Report #046060777 l l l I C00PER
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ATivE STUCIES
- TECHNICAL PROGR AM EVALU ATioN
- PCLLUTl0N AB ATE'NEN MAPINE COATINGS & TESTING e CHEMICAL / PHYSICS CONSULTING l
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J ggggfgg ; PROFESSICNAL CCATINGS JM February 24, 1978 4 Consaanche Peak Steam Electric Sption Brcwn & Ecot, Inc.
; P.O. Box 1001 G:ZN BCSE, TX 76043 v'
ATIENTION: Mr. Don Sutton
Dear Mr. Sutton:
Enclosed is a copy of Imperial's Technical Report 4215-78-G demonstrating the compatibility of Concresive 1411 Epoxy .trtar, with Imperials s tCTIC $11S/ c REACTIC #1201 System.
@+~ , ' Sincerely, Gitrald E. Ar::ald Technical Support Representative Nuclear GEA/rai Enclosure i
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TECHNICAL REPORT NUMBER 215-78-G 3, s - w: nns CCNPAT":BrITY TESTING - CONCRESIVE 1411 EPCXY NCICAR FOR CUSTOMER BBCNN & RCCT Submitted by: Gerald E. Arnold 1 Approved: g Date: 1/25/784 l SOtmIERN IMPERIAL COATINGS CORPORATION LNC. P. O. Box 29077, + New Orleans. Louinana 70189 Phone: (504) 254 1433
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l j - Q w T.R.8215-78-G Page 1. Stnegut! - Compatibility testing was initiated at the request of Brown and spot engineers relative to the South Texas Project. Elcometer
' adhesion and Dak tests were conducted to d==an=trata the compatibility i
of Concresive 1411 to Imperial's NUTEC 11S/1tEACTIC 1201 systan. ".Sta results of these tests 4=Henta that the Concrasive 1411 is compatible with the Imperial products. , Dml0 DUCTION - Concresive 14H is a 1004 epoxy ansonry and concrete nortar which is designated for use in repairing concreta damage at the South Texas Project. Brown and Boot engineers requested that Imperial conduct tests to demonstrate that the proposed NUTEC llS/REACTIC 1201 coating system and concresive 14 n are compatible. ETEDDS - 4 a) Spae4==ns - 2" x 3 " x 2" concreta v 4 = = prepared in accordance with Bechtel CP956 4 4 Coupon No. Batch Pour Data Curing Cospound
..g r 478, 479 1-53 .5-6-76 NOTEC 810 (5606/5607)
& 486 509, 512, 1-53 5-6-76 NOME s 513 h) Surface preparation - 100 psi compressed air c) Application and Curing Data Product Batch 8 Data and Time F/t R.H. DFf Cure Oata Applied 70*F/644 Fin 4 days 6 70-80*
Concresive Ict 77654 '2-5-78 len 9:30 a.m. voids' 45-654 1.E. I 'i
-t NUIEC ells 3227/3228/ 1-9-78 58'F/46% .020" .025" 3 days 9 70-80*
3229 1:30 p.m. 45-65% R.H. l
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.005" .006" 4 days 9 70-a0*
I ItEAC"'IC #12012467/2563 1-12-78 58'F/66% 45-654 R.H. 10:00 a.m. l l *Concresive 14H was applied to the entire surface - not just voids. 8 i An approximata DFT of 5-10 mils was obtained. l i-i ' l d) Testing 1 t 1. E1cometer adhesion tasting was perfor:ned (
' in accordance with Imperial Test ' Method 03.
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i J . 4 T.R. 0215-78-G
' Page 2.
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Eigh strength a11minum dollies were applied to the 4
' coated specimens by means of an epoxy resin-type adhesive.
i The dollies were placed 1-13-78 at 11:00 a.m. and rem ved with an E1cometer adhesion tester 1-16-78 at 9:00 a.m.
- 2. Ttso of the six concreta W -= were then submitted to 4 Coastal Science Associates for DBA testing in accordance with the test parameters established for the South Texas Project. The concrete coupons were subjected to 24 hours of p simulated conditions with a anximum temperature of 307 F. and a s=wi== pressure of approximately 57 psig.
The coating damage inflicted by the E1cometer testing was not repaired prior to WA testing. RESULTS - ) a) E1cometer Adhesion Lab. Panel # Concrete Coupon 9 Fcree required Mode of to remove dolly Failure 3706 478 350 psi 1004 concrete failure 3707 479 500 psi 80s 1411/concr. 20tconcrete 3708 486 475 psi 1004 concrete failure 3709 509 450 psi 100% concrete i 1 failure l
.3710 512 500 psi loot concrete failure 3711 513 400 psi 1004 concrete failure l
I b) DBA Lab. Panel 4 Concrete Coupon e Results 3710 479
- Coati =g intact. Scme d=1-4 "= tion en broemed i
and smooth surfaces, I t 37 07 512 No Defects.
- Delamination was determined by " sounding" the tes: specimen. Siis ....
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1 O, .. T.R.#215-78-G Page 3. . l observation was ~=*4 W by reseving the coating in the
" defective" areas. Se failure was found to occur betwoen d the Concresive 1411 and the concrete surface.
l . CORIC.USIONS - Se results of the E1cometer adhesion and DBA testing demonstrates the compatibility of Concresive 1411 with the Imperial coating system. In all tests, the bond between the Concresive 14H and the NtTEC 4115 was excellent. Some failures, however, did occur between the concrete surface and the Concresive 1411. S,~ h a # 3707 exhibited some loss of adhesion at the substrate in the adhesion test and specimen #3710 exhibited signs of 4 1 dalamination in the ERA test. 2Lis potential problem can be avoided by good surface preparation practices. Se concrete speeMnm used had aged i for 20 months. Apparently some contamination was present which was not readily removed by 100 poi compressed air , Use of Concresive 1411 should ]
. be restricted to damaged concrete, voids, and tie holes where a " physical bond" will be achieved and improve the performance of the overall system.
Excess Concresive 1411 should be reenved to avoid any potential adhesion problems. - IEFERENCE - Lab. Notebook #56, p.39 l l I 9 } 6 1 l - 1-
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I COASTAL SCIENCE ASSOCIATES, INC. 6969 CANAL BLVD. NEW ORLEANS, LOUISI ANA 78124 4 TEL. 594-283-7251 11
SUBJECT:
DESIGN BASIS ACCIDENT COATINGS TEST REPORT. h. DATE: 1/18/78 MOUSTON LIGHT AND POWER, 24 HR. SCREEN TEST DBA TEST CONDITIONS: 397 HIGHEST TEMPERATURE CDEG. T) REACHED DURING RUN 3787. SAMPLE TTPE: CONCRETE COUPON SAMPLE NUMBER:
~".. l SAMPLE # DESCRIPTION 3757 SIDE 1: NO DETECTS SIDE 2 NO DETECTS SIDE 3: NO DETECTS .
SIDE 4: NO DETECTS i n ' REPORT VRITTEN .FORs SOUTHERN IMPERIAL COATINGS i REPORT # 859911778 APPROVEDBY....[..... $2....... s.... 9 e 5 4 I .
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CCASTAL SCIENCE (4SSCCIATES, INC. 6998 CANAL BLVD. NEW ORLEANS, LOUISIANA 78124 TEL. 584 283-7251 i
SUBJECT:
DESIGN BASIS ACCIDENT COATINGS TEST REPORT. 1 l
+ DATES 1/18/78 1
i HOUSTON LIGHT AND POWER, 24 HR. SCREEN TEST 3 DBA TEST CCNDITIONS: l i 387 1, HIGHEST TEMPERATURE (CEG. F) REACHED DURING RUN 3718 SAMPLZ TYPE: CONCRETE COUPCN SAMPLE NUMBER:
.g.
/ SAMPLZ # DESCRIPTION
.............. - ...~......................................
3718 SIDE'1: C SIDE WITH SAMPLE #) NO DETECTS SIDE 2: DELAMINATION OVER MOST OF SIDE. NO CRACHS OR BLISTERS.
- 4 4
I SIDE 3: NO DETECTS - { SIDE 4: DELAMINATICN BELOV ACHESICN TEST CUT. NO OTHER DETECTS 1 i i E b REPORT VRITTEN FOR: SOUTHERN IMPERIAL r I
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REPORT # 35991 778 APPROVED BY... ......... ...... .... . 4
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- rJ P, 6 A l\. P. M6 s wl f L SU11SER 205-1-78-G I TITLE CO.UATISI!.ITY OF tis X with NUTEC 411S SCRFACER 4
FOR Cceanche Peak Stes:2 Electric Station I CUSTO51ER TrxAs UTI:.ITIIs 1
! Submined by: Gerald E. Arnold Apptcved: g / t ,, ' Date: anuary 26, 1978 SOLTriER.N L\tPERIAL COATISGS CORPORATION. LNC.
P. O. Box 29077,
- S'ew Orleans. Lcuisiana 70139 Phone: (504) I'4-1433
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- q T.R. #205-1-78-G -
4 Page 1. 5 SUMP.ARY - Extensive testing was conducted to determine if Imperial's NUTEC tilS surfacer is compatible with Burke's RES X concrete curing compound. Based on results of Elcometer adhesien and Design Basis Accident testing, it was concluded that the RES X is a dissipating membrane only if exposed to the ultraviolet rays of sunlight or to heet. Without these agents, the RES X remains on the conrete indefi-sitely. On porous well surfaces the RES X penetrates easily leaving no
- appreciable surface film to interfere with the chemical adhesion of the NUTEC '115 to the concrete. The floors, especially steel trowelled finishes, however, pose a pechlem because of the lack of porosity and the build up of a RES X film on the surface. This film is incompatible with the NUTEC #115 and must be removed by physical means, specifically a high pressure water blast, sand . blasting, or a cembination of tra two methods. ,
DITRCDUCTION_ - Tasting of Burke's RES X was performed at the request of Brown & Root in connection with the Texas Utilities' Comanche Peak Nuclear Power Plant. RES X is a dissipating concrete curing membrane consisting of a solution of resinous solids and petroleum solvents. The RES.X film, according to literature, disintegrates by oxidation. ary for this reaction to occur. Heat and ultraviolet read rate'srays are are nectsg/ 200ft. gallon for rough surfaces and Recosunended 200 - 300 ft. sg/ gallon for smooth and steel trowel finishes. - The pur-pose of this test was to determine if NUTEC #115 is compatible with e RES X. METHCD - Elcometer adhesion (cinder blocks) a) RES X was applied to two 3 " x 7" 2" high density cinder j blocks at a spread rate of 200 f t.,g/gallen. The RES X was cured in the laboratory at 70 - 80 F. and 45-65% R.H.
)' NUTEC #115 was applied to one block after 24 hours and to the second block after 30 days. No surface preparation was performed between coats. Both specimens were topccated with REACTIC 91201. Three high strength aluminum dollies were applied to each specimen and removed with an Elec=eter adhesion tester following sufficient cure of the coating system. Tests were conducted in accordance with :=perial i' Test Method 03. For cocparative purposes, 2 control speci-
-- = ens were coated with the Imperial system only.
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- 1. Application and curing Data _
i j PDODUCT BA1'CH # Date Aeplied ~F./% R.H. OTT (inches) (24 hour intercoat time - RES X/NUTEC #11S) 2 1 1 RES X 10/31/77 - 1:50 p.m. 84 70 200 ft. 7 ,1, NUTEC #115 LB150/2671/ 11/1/77 - 1:00 p.m. 80 75 .020 .025 LB148 NUTEC #11 LB150/2671/ 11/4/77 - 8:00 a.m. 70 7 .005 .007 LB149 . REACTIC 3070/2568 11/7/77 - 9:20 a.m. 71 69 .006 .009
< #1201 Dollies applied 11/9/77 Dollies removed 11/14/77 I
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# (32 day intercoat time - RES X/NT.TIEC #11S)
RES X' 10/31/77 - 1:50 p.m. 84 70 200 ft. / gal. NUTEC ells 5386/3388/ 12/2/77 - 9:00 a.m. 70 64 .020 .23 LB148 3070/2568 12/8/77 - 5:00 p.m. 67 71 .003 .005 REACTIC
#1201 Dollies applied 12/13/77 Dollies reseved 12/16/77 I
- 2. Panel designation Panel # System RES X/NUTEC 9115 intereca: time 3448 11S/11/1201 24 hours 3464 RES X/11S/11/1201 24 hours 3449 11S/1201 32 days 3465 RES X/115/1201 32 days I
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- 205-1-78-G Page 3.
b) . - E1cometer adhesion (concrete coupons) 1 RES X was applied to four 2" x 4" x 2" concrete coupons I prepared i accordance with Bechtel CP954, at a spread rate of 100 ft.g/ gallon. The RES X coated coupons were cured in the laboratory at 70 - 80 F. and 45-65% R.H. Two coupons were coated with NUTEC $11S af ter 48 hours. S e remaining specimens were surfaced af ter 50 days, following a 3000 psi water blast whica was achieved using a Graco Bulldog (30:1) and a .043" tip. All concrete blocks were topcoated with REACTIC #1201. One high strength aluminum dolly was applied to each specimen by means of an epoxy resin-type adhesive and removed with an Elcometer adhesion tester following sufficient cure of the coating system and adhesive. Tests were perfor:ned as directed by Imperial Test Method 03. Control specimens were also coated with the Imperial system only. The concrete substrates were allcwed to stand for 48 hours and 50 days as were the RES X coated specimens.'
- l. Applicatica and curing cata PROOUCT BATCH e rste Acclied F./%R.H. OFT (inches)
(48 hour intercoat time - RES X/NUTEC fils RES X 11/17/77 - 1:00 p.m. 78 65 100f t. / gal. LB150/2671/ 70 .018 .024 NUTEC 511S LB148 l11.13.77-11:00a.m.72 2467/2491 11/26/77 - 10:00 a.m. 74 58 .005 .007 REACTIC .
$1201 Oc111es applied 12/1/77 Dollies re::cved 12/3/77 f
I (50 day intercoat time - RES X/NUTEC 9115) RES X 11/17/77 1:00 p.m. 78 65 100ft. / gal. NUTEC 4115 3227/3228/ 1/9/78 11:00 a.m. 78 67 .018 .022 3229 REACTIC 2467/2568 1/12/78 10:00 a.m. 58 66 .004 .026 41201 Oc111es applied 1/13/78 Dollies removed 1/16/78 I i
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R[ .y $ _ t ,_ <.c9 . - - 4 T.R.s 205-1-78-G j Page 4. 5 2 1 1 2. Panel designation a a I4b. Panel # Concrete # ES X/4115 intercoat time Surface Prep. 3493 632 48 hours None (11S/1201)
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3494 667 48 hours None (115/1201) 3495 801 50 days 3000 psi water (11S/1201) I [ 3496 861 50 days 3000 psi water (11S/1201 3525 602 48 hours None p' . (RES X/11S/1201) i v l 3526 680 48 hours Ncne (RES X/11S/1201) 3527 793 50 days 3000 psi water (RES X/115/1201) 352S 803 50 days 3000 psi water (RES X/115/1201) I c) Elecmeter adhesion (concrete coupons) rate coupons were coated with RES X at Four spread2"rate x 4"of x 2" cong/ gallon. The specimens were stored in 250ft. darkness at 70-4s0 F. and 45-65% R.H. for 120 days prior to the application of the next coat. NUTEC #11S was applied to each j' coupon following a 100 psi compressed air blast. One high strength aluminum dolly was applied to each specimen directly to the #11S surfacer by means of an epoxy resin-type adhesive. O.e adhesive was allowed to cure for 72 hours. The dellies were removed with an E1cometer adhesion tester and the force rege. ired to remove the dollies and the sm:de of failure were recorded. The E1cometer adhesion testing was performed on the smooth surface of the concrete coupons. I 4-t i 1-i h -
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- T.R 8205-1-78-G i Page 5.
- 1. Application and Curing Oata 1
1 PRODCCT BA"IH # Date Applied F./% R.H. CFT (inches)
. .I 8/8/77 8:00 a.m. 81 87 250ft.2/ gal.
RES X 12/10/77 9:00 a.m. 58 38 .020 .025 3386/3388/ NUTEC #11S LB149
- 2. _anel Designation Iab. Panel # Concrete # RES X/811S Intercoat time 3283 163 120 days 3284 171 120 days 3285 172 120 days c.
3286. 188 120 days J d) Design Basis Accident Concrete coupons previously used in adhesion tests (see b) 2.) were submitted to Coastal Science Associates for an autoclave screen test designed to simulate Loss of Coolant Accident temperature and pressure conditions. The ma.dmum temperature and pressure obtained was 307 F. and 57 psig respectively. All specimens were inspected within one hour of their re:noval frem the autoclave for signs of visual damage and then " sounded" by tapping with a solid instrument to determine if any disbond-ing had occurred at the substrate.
- 1. Application and Curing Cata See b) 1.
- 2. Panel designation Iab. Panel B System RES X/115 Interceat Oate subnitted time fer testin-3493 #11S/1201 48 hours 12/12/77 3525 M:s X/11S/1201 48 hours 12/12/77 l 3495 *115/1201 1 50 days 1/16/78 3527 RIS x/115/1201 50 days 1/16/78 1
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I j RESM.TS - a) E1cometer adhesion (cinder blocks) Panel"9 System Intercoat Torce Required Tailure time to remove dolly ::cde 3448' 11S/11/1201 24 hrs a) 250 psi 100% concrete (Control) b) 200 pst 100% concreta c) 300 psi 100% concreta 3464 RES X/11S/ 24 hrs a) 50 psi 954 115/ con-g crete. 1 11/1201 54 concrete b) 100 psi 90s 115/ con-crete. 10% concrete c) 250 psi 100% concrete 3449 11S/1201 32 days a) 450 psi 100% concrete (Control) b) 600 psi 100% concrete c) 200 psi 100% concrete 3465 11S/1201 32 days a) 50 psi 90% 11S/ con-crete. 10% concrete b) ~'00 1 psi ~ 90i liS/ con-
- rete.
104 concrete c) 100 psi 90% 115/ con-crete. j 10% concrete k I,
' DISCUSSION - Cinder blocks used were of high density concrete. Although the surface is rough, the porosity is low and the KES X accu =ulates en the surface as a fil:n. Siis adhesion test de:nonstrates that FIS X cured under j
laboratory conditions without heat or ultraviolet rays has detericrated j very little, if any, thus resulting in poor adhesion of the MO #11S to i the substrate. Excellent adhesion was cotained with the control specimens. t r I' t
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b) E1cometer Adhesion (concrete coupons) Panel 9 System Intercoat Surface Force required to Failure Mode l Remove dolly time Preparation 115/1201 48 hrs None 450 psi' 100% concrete 3493 I 11S/1201 48 hrs None 800 psi' 100% concrete
] 3494 RES X/11S/ 48 hrs None 500 psi' 50% concrete 3525 1201 504 115/concreta Mone 500 psi' 904 concrete 3526 RES X/115/ 48 hrs 1201 104 11S/ concrete 50 days 3000 psi 450 psi'* 100% concrete
] 3495 11S/1201 water 50 days 3000 psi 300 psi ** 100% concrete 3496 115/1201 water
~
I RES X/11S/ 50 days 3000 psi 700 psi'* 100% concrete 3527 1201 water 3528 RES X/11S/ 50 days 3000 psi 450 psi ** ,80s concrete 1201 water 204 11S/concreta
- Adhesien tests performed on simulated wall surface.
" Adhesion tests perfor:ned on simulated floor surface.
DISCt:SSION - Specimens 3493, 3494, 3525, and 3526 represent adhesica tests on simulated wall surfaces. Even though the RES X had cured only 48 hours penetration into the porous concrete was sufficient to allow the NOTEC 115 to bond to the substrate. The values obesined (500 psi for both specimens) indicates good adhesion of the 115 to the concrete, however, the mode of failure (seme disbonding between the 115 and the concrete) reveals a I' decrease in the bonding that is not normally observed with the .WTIC 11S r i surfacer. Note that in all centrol specimens f ailure occurred 100% in the concrete. l Specimens 3495, 3496, 3527, and 3528 represent adhesion tests on si=ulated floor surfaces. The surface tested is smooth and porosity is low. The i RES X was allcwed to stand for 50 days prior to the application of the f f N73C 115. Because the test coupons.were stored in the laboratory under ' controlled conditions, any appreciable dissipation of the RES X film was l unlikely. The improvement in adhesion is due to the 3000 psi water blast l used to remove the RES X film. Both ES X specimens exhibited goed adhesion i f1 values with the majority of the failure in the concrete. Coupon g3528
' demonstrated approximately 20% adhesion loss between the 115 and the RES X l
l sealed concrete, indicating the water blast did not rs=cve all of the l residue en the surface. i e I
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c) E1cometer adhesion (cencrete coupons) i
! Panel 9 System Intercoat Time Force required to Failure lede reseve dolly 3283 RES X/115 120 days 700 psi 100% concrets 3284 RES X/11S 120 days 350 psi 100% concra e , 3285 RES X/115 120 days 200 psi 100% 11S/ ! concrete j 3286 RES X/11S 120 days 400 psi 100% 115/
concrete DISC::SSION - The results here are inconsistent, two specimens exhibiting excellent adhesion and the remaining two demonstrating peor bonding between the NOTEC 115 and the ES X sealed concrete. Specimens 3283 and 3234 were
.: originally designated for other testing. The concrete coupons had previously (18 months) been treated with a 1% Silane solution which may have promoted adhesion.
Coupons 3285 and 3286 may better represent the potential problems on steel trowelled floors. The adhesion t.sts were performed on the smooth surface of each coupon. The smoothness of the concrete is a result of the method in which the coupons are prepared. In this case, the surface tested was very smooth and glossy thus simulating a steel trowelled finish. The RES X was eured for 120 days in the laboratory at 70-80 F. and 45-65% relative humidity, with no exposure to sunlight (ultraviolet rays). Prior to the i application of NU'2C 115 only a 100 psi compressed air blast was used to remove any dust or other contamir. ants which may have accumulated over the
+ four month period. The E1cometer testing indicates very poor adhesion of the 115 to the ES X sealed concrete. "herefore, . it can be concluded that the RES X film will not disintegrate without heat or ultraviolet lignt.
d) Design Basis Accident Panel # System Intercoat Time Results 3493 11S/1201 48 hours ., No defects 3525 RES X/11S/1201 48 hours' . Two h" diameter areas
' of delaminatica - coat-ing intact. ,
3495 115/1201 50 days No defects j 3527 RES X/11S/1201 50 days No defects. I-h k 9-... . m-...._. % . ..._,7-, . . . _ .. _ _ _ _ _ , . _ , e
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- The tested coating system was intact and no defects were visually discovered.
i However, upon " sounding" the specimen two areas of apparent delamination or
-1 disbonding were noted. This finding was confirmed by removing the coating J in the questionable areas with a sharp instrument to determine the degree of dishonding. .
3 DISCUSSION - This test demonstrates that if proper surface preparation
, procedures are used to remove the RES X, the adhesion of the NUTEC llS surfacer to the concrete is assured.
-4 More importantly, specimen 3525 indicates that if the RES X film dces not I dissipate with time or is not removed by some physical means, an adhesion
, problem is inevitable.
]
CONC .USICNS - Burke's RES X is a dissipating concrete curing merbrane consisting of a solution of resinous (hydrocarbons) solids and petroleum solvents. As an intact film the RES X is a poor base for subsequent coatings. This fact is substantiated by the results of this testing and is readily admitted to by the RES X manufacturer. The dissipation rate of the RES X curing membrane depends upon oxidation
> resulting from heat and ultraviolet rays. The length of time which the RES X is exposed is irrelevant; the accumulative and quantitative amount of sunlight and heat is important. Without exposure to the ultraviolet rays
- of sunlight or heat, the RES X remains on the concrete as a surface film and can only be reimaved by physical means.
The major concern, therefore, is how effective the surface preparation is
- in removing any remaining surface film. Whether or not a 7 day, 30 day, or 120 day dissipation period is allowed, is unimportant. Based en laboratory tests, high pressure water -(3000 psi) is sufficient to remove the RES X and
. providing anadequate base for adhesion of the NUTEC llS surfacer. The only time lhaitation that should be imposed is the 28 day cure period established by 1LCl 301. . 2 The main factor controlling build up of a surface film is the porosity of the concrete. Throughout the adhesion and DBA testing, simulated wall surfaces coated with RES X posed no compatibility problems because of the degree of porosity. The RES X penetrates well into formed wall surfaces, leaving no surface film to interfere with the adhesion of the NUTEC 115 surfacer. I Despite this finding, high pressure water is reccamended as a safeguard. The simulated floor surfaces, especially very smooth surfaces with very little porosity, pose a definite problem. Because of the icw porosity, penetration is impeded and a surface film is effected. Without the natural breakdown of the film or procer physical preparation (e.g. waterblasting, sandblasting) to remove the film, poor adhesion of subsequent coating will occur. i a sue
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) T.R.4205-1-78-G Page 10.
I Based on the results of the RES X testing program and discussions with Mr. Al Brownlee with Conspec Marketing and Manufacturing Company, the following recommendations are made. RES X should be applied to concrete surfaces in accordance with the manufacturer's recommendations. Care
~
should be taken to avoid an unnecessary build up of RES X on the concrete, especially floor surfaces. The concrete shall be allowed to cure a minimum of 28 days as directed by AC1 301. Prior to application of
~
Imperial's coatings, 4000 psi water blasting, 2500 psi water blasting with I sand injection, or sand sweeping shall be used to remove any remaining RES X. Adequate surface preparation shall be nade by visually inspecting the concrete surface for " water beads". Beading of the water indicates the presence of-the RES X and additional surface preparation will be required until this heading is eliminated. F4
- RETERENCES - LAB. Notebock 56, p.p. 1-17
! LAB. Notebook 33, p. 147 4
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- COASTA1. SCIENCE ASSOCIATES, INC.
~ 6900 CANAL ELVD.
NEW ORLEANS, LOUISIANNA 70124 TEL. 504-283-7251 SUSJECT: DESIGN BASIS ACCICENT COATINGS TEST REPORT. i DATE: 12/19/77 DSA TEST CONDITIONS: HOUSTON LIGHT AND POVER, SHORT TO 48 HRS. 3493 SAMPLE TYPEt CONCRETE COUPON SAMPLE NUMBER: DESCRIPTION [$- S AMPLE #
............................................................ I 3493 SIDE ONE: NO DEFECTS .
SIDE TV0: NO DETECTS SIDE THREE: NO DETECTS SIDE FOUR NO DETECTS REPORT VRITTE23 FOR: SOUTHERN IMPERIAL REPORT # 05712 977 e APPROVED BY .....n........p........ i I t
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COASTAL SCIENCE ASSOCI ATES, INC. 6983 CANAL BLVD. NEW ORLEANS, LOUIS! ANNA 78124 J TEL. S84-283-7251 I
SUBJECT:
DESIGN BASIS ACCIDENT COATINGS TEST REPORT. I DATE: 12/I5/77 HOUSTON LIGHT AND POV ER, SHORTENED TO 48 HRS. DBA TEST CONDITIONS: SAMPLE f(?Es CONCRITE COUPON SAMPLE NUNSER: 3525 DESCRIPTION SAMPLE # SIDE ONE: CELAMINATION, UPPER LETT CORNER
- 3525 .
SIDE TV0: NO VISISLE DEFECTS, NO DELAMINATION l SIDE THREE: N0 VISIELE DETEC'TS, NO DELAMINATION SIDE FOUR NO VISIBLE DEFECTS, NO DELAMINATION i
'I REPORT VRITTEN FOR: SOUTHERN IMPERIAL 956121577 ,~ ,-
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J 1 _ g 1 COASTAL' SCIENCE ASSOCIATES, INC. 6908 CANAL ELVD. NE'J ORLEANS, LOUISIANA 72124
- TEL. 534-253-7251 SU3JECY: DESIGN SASIS ACCIDENT CCATINGS TEST REPORT.
DATE: 1/18/78 DSA TEST CONDITIONS: HOUSTON LIGHT AND Pok'ER, 24 HR. SCREIN TE37 HIGHEST TEMPERATL"-1E (DE3. T) REACHED DURING RUN 337 SAMPLE NUMEER: 3527 SAMPLE TYPE: CONCRETE COCPON O,l. l SAMPLE i DESCRIPTION 3527 SIDE !: NO DETECTS SIDE 2: NO DFTECTS SIDE 3: NO DEFECTS SIDE 4: NO DETECTS REPORT k*RITTEN FOR: SOUTHERN IMPERIAL CCATINGS REPORT # 359011778 APPROVID EY... I. 4 . . .Th ... t .
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COASTAL SCIENCE ASSOCIATES, INC. 6963 CANAL BLVD.
/ NE*4 ORLEANS, LOUISIANA 73124 TEL. 534-253-7251
SUBJECT:
DESIGN SASIS ACCICENT. COATINGS TEST REPORT. DATES- t/15/75 DBA TEST CCNDITIONS: HOUSTON LIGHT AND PC'.*ER, 24 HR. SCREEN TEST HIGHEST TDiPERATURE (DEG. T) REACHED CURING KUN 337 SAMPLE NUMSER: '3495 SAMPLE TYPE: CONCRETE COUPON SAMSLE # DESCRIPTICN 3495 SIDE la NO DETECTS
- t. SIDE 2 NO DETECTS SIDE 3: NO DEFECTS SIDE 4: NO DETECTS 4
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8" l' f i l TECHNICAL REPORT i i NUMBER 175-1-77 TITLE DBA, PADIATION TOLERANCE OF NUTEC #11S/11/1201 Over Sandblasted Concrete FOR SICC 1 l
' CUSTOMER l l ' Subr'nitted by: Ri National Libs Approved:
I Date: 12/77 l
' SOLTHERN IStPERIAL COATINGS CORPORATION [NC.
P. O. Box 29077,
- New Orleans. Louisiana 70189 I
Phone: (504) 254 1433 l r %.-............,.,,ww.-<e.ec.....o.,,...,..,
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. Analytical Chemistry Division v
- Oak Ridge National Laboratory 4 Date: 5-31 -77 Report of Irradiation and 08A Testing Southern Imperial, New Orleans, Lo91siana The Irradiation and Design Basis Accident (08A) tests are conducted, respectively, in accordance with Bechtel Corporation Standard Specification Coatings for Nuclear Power Plants Spec. Nos. CP-951 and CP-956. The tests y are designed also to meet the specifications set in both A.N.S.I. Report N 'l 101.2-1972 Protective Coatings (Paints-) for Light Water Nuclear Reactor Con-tainment Facilities, and N 5.12-1974, Protective Coatings (Paints) for the Nuclear Industry. The 08A test spray solution and the test conditions are 1 listed in Tables 1 and 2. After both the DBA and the irradiation tests, the coatings are examined for signs of chalking, blistering, cracking, peeling, de-lamination, and flaking, according to ASTM standards where applicable. All except the decontamination test panels are returned to the coating manufacturer.
Th'e' irradiation tests are run using a spent fuel assembly, removed from the High Flux Isotope Reactor (HFIR) at ORNL, as the source of radiation.
. , .. These fuel assemblies are stored under 20 feet of domineralized water. The 5 fuel is 93% enriched U23s as Us so combined with aluminum. The spent fuel as-semblies are removed after each 23-megawatt day period. Irradiation is done using the ganna energy from the accumulated mixed fission products. This more readily simulates conditions around a reactor than does a cobalt source. Also, the higher ganza activity affords shorter irradiatian tima ta ee W ye accumu-lated doses. The dose rate four days after removal of a fuel assembly from the reactor is 1 x 10s rads / hour.
The fuel assembly is 20 inches high. A 20-foot long, 31/2-inch diameter pipe, with one end capped, is used for the air irradiation tests. The capped end is lowered into the four-inch opening of the center of the fuel assembly. t The open end, above the water level, is covered with an "0" ring sealed flange to which is attached a steel cable and an air outlet hose. The air inlet is located at the bottom of the pipe. The test specimens are connected to the
! bottom of the cable and lowered into the radiation field. Also at the center t-I of the fuel assembly is a stainless steel clad cadmium tube used as a neutron f absorber. This prevents contamination of the test specimens by induced radiation.
Evaluated '$M A4 Approved .
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e DBA AND RADIATICN TCI.'*3ANCE
' SST PANEL PREPARATICN CA3
- 1. PRODUCT TO BE TESTED: NUTEC #115/rsuu C #il/REACTIC #1201 f SI2E: 2" x 4" x 2"
- 2. TYPE SUBSTRATEs Concrete - Bechtel CP-956
#4
- 3. SURFACE PREPARATICM (Descri.be): All Concrete surfaces sandsweet with Cresblast Blastina Sand to exoose all rock ocekets and voids.
- 4. PRODCCT DA m s SAMPI.E NO. (s) : 2373 None
- 5. CATE AND TIME CURING COMPCCND CR PRIMER APPLIID:
.T5ICKNESS TIME & DATE PRODUCT APPLICATION CCNDITICNS APPLIID BATCH #_ METICD R/M("Fl%R.E. (ins.) _
CCAT PPCCCCT_ CCDES _ Squeegee 76"/59%
- 4/4/77 1 NUTEC 115 1310/1556/1312 Base / Cure / Fill
- 4/6/77 NUTEC 11 1313/1314 Squeegee 74"/584 2 Base / Cure 7497/7434 Spray 82 /48%
- 4/11/77 3 REACTIC 1201 Base / Cure q
lNUTEC #11S NUT C #11 REACTIC #1201
.003 .005 in .003 .005 in
- Minimus: Thickness Bic~s d Surface LO10 .0151n sides Adjacent to.015 .020in .005 .010 in. .007 .006 in.
Average Thickness Broomed Surface Side Cyposite .025 .0351n. .015 .020 in. .010 .012 in. Maximus Thickness r 9 .. . _ _
.. . 8_.4et.edec.e Total Dry Film Thickness Range 016 to .067 inches.
F REL. ICtIDITT 40-65 g
- 6. CTRI:iG CCNDITICUS: AMBIENT TIMP. 70-80 f 11 CAYS i ! MINI:C4 CTRE
- 7. IIST PRCCEOC"AEs DBA - Bechtel CP-956 CATE SUBF.ITIED 4/22/77 8 TESTI:tG PER.NRMED BT: Oak Ridce National Laboratories
[/' .O APPRCVED: TIST RIPCRT NO. 175-1-7h l ( DATE: 12/77 PPIPARED BY:_ d
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M DBA AND RADIATICN TCLIRANCE TEST PANEL PREPARATICN CATA i 1. PRODUCT TO BE ESTED: NUTEC #11S/NUTEC #11/REACTIC #1201 SIZE 2" x 4" x 2"
- 2. TTPE SUBSTRATE: Concrete - Bechtel CP-956 All concrete surfaces pndswept with Crosblast #4
- 3. SURFACE PREPARATIt3t (Describe):
Blasting Sand to expose all rock pockets and voids.
- 4. PRCDCCT DATA: SA. m NO.(s): 2374 None
- 5. CA2 AND TDE CURING COMPCCND CR PRIMER APPfl7'S APPLICATION CONDITIONS MICKNESS TI:E E DATE PRODUCT APPLIID BATCH # 'ETECD R/M(CF) t R.E ._ (ins.)
CCAT PICDUC" CODES _ 11S 1310/1556/1312 Squeegee 76 /594
- 4/4/77 1 NUTEC Base / Cure / Fill 1313/1314 Squeegee 74 /584
- 4/6/77 2 NUTEC 11 Base / Cure 7497/7434 Spray 82*/484
- 4/11/77 s
3 REACTIC 1201 Base / Cure 07- NUTEC $11S NU'IEC 411 REACTIC #1201
- Brc,cced Surface ,025 .035 in . 015 . 02 0 in . .010 - .012 in Maximum Thickness Average Thickness Sides Adjacent to,015 .020 in .005 .010 in. .007 .008 in.
Broceed Surface Side- Opposita' . 010 . 015 'in .003 .005 in. .003 .005 in. Minimum Thickness Bic-:-M Surface Total Dry Film Thickness Range .016 to .067 inches. 70-80 40-65 g
- 6. CURING CONDITIONS: AMBIINT TEMP. F REL. ECMIDITY MI:rIMUM CTRE 11 CAYS
- 7. TIST PROCICURE: DBA - Bechtel CP-956 Cak Ridge National Iaboratories cagg sg33:m 4/22/77
- 8. TISTOiG PERFCRM:"3 BY:
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o / /. 22PPCVED: Vk[ " f TEST RE7CRT NO. 178-1 77 { DATEI 12/77 8 PPIPARED BY , 8 6 e
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y: - . q, . DBA AND RADIATION TOLERANCE T ST PANEL PREPARATION DATA
- 1. PRODUCT TO BE TESTED: NOTEC #115/NUTEC #11/REAC nC #1201
- 2. TTPE SUBSTRATE: Concrete - Bechtel CP-956 SIZE: 2" x 4" x 2"
- 3. SURFACE PREPARATION (Describe): All Concrete surfaces sandswept with Crosblast #4 blastine sand to expose all rock pockets and voids.
- 4. PRODUCT DATA: SAMPLE NO.(s): 2375
- 5. DATE AND TIME CURING COMPOUND OR PRIMER APPLIID: None l
PRODUCT APPLICATION CONDITIONS THICKNESS TIME & CATE COAT PRODUCT CODES BATCH # METHOD R/M(CF) t R.E. fins.) APPLIED l 1 NUTEC 115 1310/1556/1312 Squeegee 76*/594
- 4/4/77 1 Base / Cure / Fill 2 NUTEC 11 1313/1314 Squeegee 74*/584
- 4/6/77 Base / Cure 3 REACTIC 1201 7497/7434 Spray 82*/48%
- 4/11/77 a s Base / Cure NUTEC lls NUTEC 11 REACTIC 1201
- Maximus Thicknessi Broomed Surface .025 .035 .015 .020 .010 .012 Average Thickness Sides Adjacent to Broomed Surface .015 .020 .005 .010 .007 .008 Minimum Thickness Side Opposite Broomed Surface .010 .015 .003 .005 .003 .005 7 -" *"y ~! 1r C.;.de. :: rs.r.ga ..lii te .06' 1:.:hes
,i
- 6. CURING CONDITIONS: AMBIINT TE.T. 70-80 F REL. HUMIDITY 40-65 %
l MINIMUM CURE 11 DAYS i
- 7. TEST PROCEDUPE: CBA Bechtel CP-956
- 8. TESTING PERECPMED BY: Cak Ridge National Laboratories CA 2 SUBMITTED 4/22/77
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DBA AND RADIATICN E LERANCE 2ST PANEL PREPARATION DA S
- 1. Plt 0D0CT TO EE ESTED: NUTEC #11S/NURC #11/REACTIC #1201 SIZES 2" x 4" r 2"
- 2. TYPE SUBSTRAM: Concrete - Bechtel CP-956
- 3. SURFACE P1tEPARATICIf (Describe) : att eene ete eur emens =mmdewone v4*h (*n =himm* e4 Blastina mand to erv de att mek neckets and *inid s.
- 4. PRODCCT DA ns SAMPLE NO. (s) : 2376
- 5. DA2 AND TI.T C:TRING COMPCCND CR PRIMER APPLIED: None APPLICATICN CONDITICUS TEICETESS TIME & DATE P1CDGCT METHOD R/M(C7)tR.H. (ins.) APPLIED COAT PM:DCCT CODES _ BATH 4 NOTIC 115 1310/1556/1312 Squeegee 760/59%
- 4/4/77 1
Base / Cure / Fill 2 NUTEC 11 1313/1314' Base / Cure Squeegee 74 /5C%
- 4/6/77 REACTIC 1201 7497/7434 Spray 82 /4Ps
- 4/11/77 3
' - Base / Cure
' ' - NUTEC ells NJ:EC ell $ REACIC 41201
- Minimuri Thickness Breemed Surface .010 .015in .003 .005 in.) .003 .005 in.
Sides Mjacent to .015 .020
.005 .010 in. .007 .008 in.
A'.*erage Thickness iA* Broomed Surface Side- Cpposite .025 .035 .015 .020 in. .010 .012 in. Maximum Thickness Brc,cr d Surface in. Total Dry Film Thickness Range .016 to .067 inches. 70-80 40-65 g
- 6. CORING CONDITIONS: AMBIINT TEMP. F REL. HChIDITY 11 CAYS MININUM CURE
?
6
- 7. IIST PPCCIDORE: DBA - Bechtel CP-956
- 8. TESTING PERFORMED BY Cak Ridge National Laboratories CATE S'3:CT".'_D 4/22/77 4 .9
/ !,
APPPCVID 7 IIST REPCRT No. 175-1-77 DATE: nm PREPARID BY: - _Q, 9
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Southern Imperial Analytical Chemistry Division 64, Manufacturer: Oak Ridge National Laboratory New Orleans LA Date: 5-31-77 System Identification _: Steel X Concrete Block 115/11/1201 DBA Test Results: ORNL Master Analytical Manual Method No. 2 0922;
}
Bechtel Corp. Spec. No. CP-956; ORNL Log Book No. A 7562; 4- 29 -7 Sample No. 08A Phase . Connents**
*2373 _
spray _ Coatings intact; no defects, all sides.
*2374 spray Coatings intact; no defects, all sides.
,s.
2375 _
<erav enatinet int =c+- nn defac+<- all <4dae 2376 spray Coatings intact no defects. all sides.
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. ri. Manufacturer: Southern Imperial Analytical Chemistry Division
" J' Ridge N ti nal Laboratory New Orleans, LA ,
System Identification: Steel Panel X Concrete Block . 115/11/1201 Radiation Tolerance Test Results: ORNL Master Analytical Manual Method No. 2 0921; Bechtel Corp. Spec. No. CP-951; ORNL Log Book No. A 7562; 4-29-7 Initial Dose Rate: 1.55-1.8 x 107 rads /hr Test Conducted In: X air water Cumulative Dose Rate: Coments Sample No. 1 X los rads 1 x 10' rads 2373 Coatings intact; no defects. 2374 Coatings intact; no defects. T
! Additional Coments: . .l '
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Manufacturer: Southern Imoerial Analytical Chemistry Division
- Oak Ridge National Laboratory New Orleans, LA Datet 5-31-77
- 08A Solution Composition, Distilled Water.
Table 1. 0.28 1 boric acid (3,000 ppm baron) 0.064 M sodium thiosulfate Adjusted to pH 9.5 with sodium hydroxide Table 2. OBA Test Conditions.
. Time Temperature (*F) Pressure (psig) Consnents l
Start 170 - Autoclave preheated. 20 seconds . 340 70 (10 see) Steam injected. 6 hours 340 70 Pressure maintained by relief valve. 20 seconds 220 30 Spray solution added at 75*F. 20 minutes 220-250 30
- 4 4 days 250 30 I
20 seconds 170 . -15 Fresh spray solution added at 75*F after draining autoclave. j 25 minutes 170-200 10 3 days 200 10 End of test ORNL Log Book No. A7562; 4-29-7.
' " Approved I, ~
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' OFFICE MEMOR ANDUM . ~
George Bentinck / 3,. November 14, 1980 s To Richard Curtise -- 0A/ Site Survie11ance cr.n N T.za. Soutnern Imperial Test Report #175-1-77 uw JOS NO. 35-1195 COMANCHE PEAK STEAM ELECTRIC STATION .
..y .,-e-o ;. I y c p 3 k ::w 01 1' igab y gy -
w i e E C E I V E a == Please find attached Southern Imperial Test Report #175-1-77 concerning 08A testing of the coating system Nuter #115/11/1201. Please advise if further infonnation on this system is needed. l g.s ~ [-
' Mark Wells
- Coatings Eng.
MW/bgf Attachments cc: ARMS OL 8 & F IOO ^!37. . . . . . l .. _ . .._. 7/.cC7 "S e e.' e et {, g i i i r. : m F C F.',f I gl i AR:.3 l , , i .. . _ i l 1 ' _ - . ,l e l d& l 0 GPA , i l
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,7 TECHNICAL REPORT NUMBER
#495-61 TITLE Nutec 11S/Nutec 1201 Nutec llS/Nutec ll/Nutec 1201 Radiation Tolerance, Design Basis Acci g Testing (ORNL)
Company Knowledge l i CUSTOMER Submitted by: Gerald E. Arn ld 1 a/0 ,h W MprwABy: . . l Date: June 10, 1981 l SOUTHERN IMPERIAL COATINGS CORPORATION, INC. P. O. Box 29077,
- New Orleans Louisiana 70189 Phone: (504) 254-1433 i
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SCOPE: The purpose of this test is to evaluate the performance of Nutec 11S applied at film thicknesses of .020 .115" under design basis accident conditions specified for the South Texas Project. The effects of various mixing techniques and compressed air cleaning are also studied. BACKGROUND: The six test specimens were included in the South Texas Project test to generate data on Nutec 11S at film thicknesses higher than the currently qualified 35 mil. maximum DFT imposed in Service Level 1 areas, to comply with the newly revised STP test require-ments and to provide data on surface preparation other than abrasive blasting.
SUMMARY
All six specimens exhibited no defects when subjected to the STP designbasisaccidentconditions{291*F.,70PSIG). Two of the' specimens were irradiated to 2x10 rads; radiation tolerance was excellent. PROCEDURES: Concrete coupons, measuring 2x4x2",'were coated as described in the attached panel preparation sheets. On coupons A32.A34, and A38, Nutec 11S was applied at various film thicknesses and in 1-3 coats. Some faces also received a tight coat of Nutec 11. Coupons A78,A83, and A85 were coated with Nutec 11S and Nutec 11 which had either been hand mixed with a spatula or with a Cowles
., mixer. One face of each coupon received no Nutec 11. Therefcre, the coupons in both sets represent both the Nutec 11S/11/1201 and the Nutec 115/1201 system.
The test specimens were submitted to Oak Ridge National Laboratories. Coupons A32 and A83 were irradiated to 2x108 rads; all coupons were DBA tested per the South Texas requirements, with maximum temperature and pressure, of 291*F. and 70 PSIG, respectively. (See attachment summary) Refer to the attached ORNL statement for a description of the tests performed. RESULTS: Refer to individual ORNL results sheets. DBA Coupon No. Irradiation Results A32 Yes No defects A34 No A38 No A78 No A83 Yes A85 No
o..... .
' Technical Report #495-81 i Page 2
/
CONCLUSION: , h At the LOCA conditions simulated in this test, the Nutec concrete system performed satisfactorily: A) Without Nutec 11 (Nutec 11S/1201) B) At Nutec 11S thicknesses of .020 .070" (one coat) { C) At Nutec 11S thicknesses of .040 .115" (two-three coats) D) At Nutec 11 thicknesses of 1001 .010" E) At Nutec 1201 thicknesses of .003 .012"- F) Regardless of dispersion speed (mixing) G) Over various prepared surfaces The date demonstrates that both the 11S/11/1201 and 11S/1201 systems met the acceptance criteria of ANSI N5.12 and ANSI N101.2, when subjected to a radiation exposure level of 2x108 rads and DBA conditions of 291*F and 70 PSIG. This report should be reviewed.in conjunction with imperial's technical report #505-81, which describes the results of a second DBA test series on the Nutec concrete coating system.
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e
SUMMARY
OF TEST PROCEDURES Max. Coupon # Surface Prep. System DFT Rad. Levels Comments (Mils) 8 A 32 11S/1201 70 (llS) 2x10 rads 11S/11S/1201 60 (11S) A 34 Broomed surface 11S/1201 25 (11S) No radiation llS/11/1201 was abrasive 40 (115) blasted; all 11S/11S/1201 115 (11S) other surfaces 11S/115/11S/11/1201 75 (11S) were stoned follow-A 38 ed by compressed 11S/11/1201 45 (115) No radiation ! air cleaning. 11S/11S/11/1201 70 (11S) 11S/11S/1201 70 (115)
- A 78 11S/11/1201 30 (11S) No radiation #11S & #11 ,
10 (11) were hand
, Broomed surface 12 (1201) mixed.
was abrasive , lasted; all 8 A 83 11S/11/1201 30 (11S) 2x10 rads #11S & #11 other surfaces 10 (11) were hand 12 (1201) mixed. bru he ollow-ed by compress- No radiation #11S and #11 A 85 ed air cleaning. 11S/11/1201 30 (11S) 1 10 (11) were mixed
. 12 (1201) on a Cowles dissolver.
l 4
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y 1 S s = R TEST PROCEDURES 4 e e f I
Manufacturer: Imperial Analytical Chemistry Division
' Oak Ridge National Laboratory New Orleans, Louisiana Date: May 26, 1981 REPORT OF IRRADIATION AND.DBA TESTING The irradiation and design basis accident (DBA) tests are conducted, respectively, in accordance with Bechtel Corporation specifications CP-951 and CP-956 in Standard Specification Coatings for Nuclear Power Plants (or with modifications as noted in Table 2, DBA test conaitions). The tests are designed to meet specifications set in both ANSI report N 101.2-1972, Protective Coatings (Paints) for Light Water Nuclear Reactor Containment Facilities, and N 5.12-1974, Protective Coatings (Paints) for the Nuclear Industry. The DBA test spray solution and the test conditions are listed in Tables 1 and 2. After both the DBA and irradiation tests, coatings are examined for signs of chalking, blistering, cracking, peeling, delamin'ation, and flaking, according to ASTM standards where applicable. All test panels are returned to the coating manuf acturer.
The irradiation tests are run using a spent fuel assembly, removed from the High-Flux Isotope Reactor at ORNL, as the source of radiation. These fuel assemblies are stored under 20 ft of demineralized water. The fuel is The spent fuel as-93% enriched U-235 as U 03 8 combined with aluminum. semblies are removed after each 23-megawatt-day period,. Irradiation is done using the gamma energy from acpumulated mixed fission products. This more readily simulates conditions around a reactor than does a cobalt source. Also, the higher gamma activity affords shorter irradiation time to achieve accumulated doses. The dose rate four days after removal of a fuel assembly from the reactor is 1 x 108 rad /h. The fuel assembly it 20 in. high. A 20-f t-long, 3-1/2-in . -d i ameter pipe, with one end capped, is used for air irradiation tests. The capped end is lowered into a 4-in. opening at the center of the fuel assembly. The open end, above water level, is covered with an 0-ring-sealed flange to which is attached a steel cable and an air outlet hose. The air inlet is 1 located at the bottom of the pipe. Test specimens are connected to the bottom of the cable and lowered into the radiation field. Also at the center of the fuel assembly is a stainless steel-clad cadmium tube used as a neutron absorber. This prevents contamination of the test specimens by induced radiation. (
/ :
Evaluated rt([ ( O Approved [,
.- ' Manufacturer: Imperial Analytical Chemistry Divisi:n Oak Ridge National Laboratory )
New Orleans, Louisiana Date: May 26, 1981 l ORNL Log Book No. A9675, A5-5-1 Table 1. DBA solution composition, distilled water Reagent Concentration Boric acid, H3803 0.28 N Sodium hydroxide, NaOH Required to adjust pH to 9.5 Table 2. DBA test conditions Temperature Pressure Time (*F) (psig) Comments Start 150 ' Autoclave preheated.
'10 min 150-291 Steam injected at 260*F.
20 min 291 70 Pressure maintained by relief valve. 45 min 291-260 80 min 260 39 Pressure adjusted with N2-15Dmin 260-220 180 min 220 20 210 min 220-160 21 h 160 5 10 d 125 2 Placed in fresh spray solution in constant temperature bath. End of test O Evaluated 'M i / Approved
1 2 PANEL PREPARATION DATA s A
'e 2
t k0 - ' - -
TEST PANEL PREPARATION DATA
.. .0 DUCT TO BE TESTED: y,,edl3efv,..,39nv .. . . _ !. TYPE SUBSTRATE: Concrete Size: 2x4x7
- 1. SURFACE PREPARATION (Describe): Carborundum stone used to re=ove hich lichts and lonne particles l broomed surface blast swept to remove efflorescence. Cleaned with 100 owf ecm-pressed air
- i. PRODUCT DATA: SAMPLE NO (s): A-32 DATE AND TIME CURING COMPOUND OR PRIMER APPLIED: N/A 5.
PRODUCT APPLICATION CONDITION!! THICKNESS TIME & E-20AT PRODUCT CODES 3ATCH f METHOD R/M(*F):R.H. (ins.) AFFLIE-Nutec llS 2519/2530/2517 Squeegee 66*F/53
- 2/4/81 3:00 p.c Nute$ llS 2519/2530/2517 Squeegee 60*F/85% ** 2/5/81 9:00 a.t Nutec 11S 2519/2530/2517 Squeqgee 64*F/55% *** 2/9/81 9:30 a.tr Nutec 1201 9772/1959 Spray 73*F/52: ***** 2/16/81.3:
FILM THICKNESS TOP VIDT C (ins.)' lls
- 11c ** 11e *** 11 **** 1201 ***** COUPON
.On3_ nns - 3 'Sida 1 max. .060 .070 _
4 2 min. .040 .050 .co,.ons Sidt 2 1 Sida 3 .010 .020 .030 .040 .003 .005 i Numbered and
.010 .020 .030 .040
~
.003 .005 broomed surf Sid2 4 TOTnL DRY FILM THICKNESS RANGE - Side 1 0'63 .075 ' Side 3 .043 .065 Side 2.043 .055 Side 4 .044 .074 .
*F REL. HUMIDITY 45-65 %
~;URING CONDITIONS: AMBIENT TEMP. 70-80 MINIMUM CURE 7 DAYS TF PROCEDURE: DBA and Rad ORNL DATE SUBMITIED 4-28-81 TESTING PERFORMED BY:
APPROVED, , TEST REPORT NO. 495-81
TEST PANEL PREPARATION DATA
. JDUCT TO BE TESTED: Nutec 11S/Nutec 11/Nutec 120L Nutec 11S/Nutec 1201 Sizer 2y 4y 2 . TYPE SUBSTRATE: Concrete , . SURPACE PREPARATION (Describe): Carborundum stone used to remove hieh lichts and lnnne particles; broomed surface blast swept to remove efflorescence. Cleaned with 100 nmi cnm-pressed air . PRODUCT DATA: SAMPLE NO.(s): A- 34 . DATE AND TIME CURING COMPOUND OR PRIMER APPLIED: N/A PRODUCT APPLICATION CONDITIONS THICKNESS TIME & D.
3AT PRODUCT CODES ~ 3ATCH f METHOD R/M(*F)%R.E. (ins.) APPLIE-Nutec 11S 2S19/2530/2517 Squeegee 66*F/53%
- 2/4/81 1
3:00 P.t ' Nutec 11S 2519/2530/2517 Squeegee 60*F/85% ** 2/5/81 9:00 a.m. Nutec 11S 2519/2530/2517 Squeegee 62*F/55% *** 2/9/81 9:30 a.m. Nutec 11 2476/2102/2444 Squeegee 62*F/43% **** 2/13/81.2:( Nutec 1201 9772/1959 Spray 73*F/52: ***** 2/16/81,3:( FILM THICKNESS TOP VIEW 0: (ins.) 11S
- 11s ** 11g *** 11 **** 1201 ***** COUPON Sida 1 Min. .020 .025 .003 .005 3 Sid1 2 .025 .040 .001 .004 .003 .005 1
Sida 3 Max. .025 .035 .030 .040 .030 .040 .001 .004 .003 .005 t Numbered'and Sida 4 ,
.020 .035 .030 .040 .003 .005 broomed surf.
TOTAL DRY FILM TEICKNESS RANGE - Side 1 .523.030 Side 3 .086 .124 Side 2 .029 .049 Side 4 .053 .080 . URING CONDITIONS: AMBIENT TEMP. 70-Rn ' *P REL. HUMIDITY 45-65 Z MINIMUM CURE 7 DAYS E!- 'ROCEDURE: DBA ESTING PERFORMED BY: ORNL DATE SUBMITIED 4-28-81 < APPROVED, TEST REPORT NO. 495-81 s-- - , , - , , , . , - .--e, n-,- , , , . , , , - . _ y --
TEST PANEL PREPARATION DATA l
. JDUCT TO BE TESTED: Nutec 11S/Nutec 11/Nutec 1201 , Nutec llS/Nutee 1201
. TYPE SUBSTRATE: Concrete Sirer 2w4x2 SURFACE PREPARATION (Describe): Carborundum stone used to remove hirh lichts and inna, particles broomed surface blast swep.; to remove efflorescence. Cleaned with 100 nef ens-pressed air
. PRODUCT DATA: SAMPLE NO.(s): A- 38
. DATE AND TIME CURING COMPOUND OR PRIMER APPLIED: N/A PRODUCT APPLICATION CONDITION!! THICKNESS TIME & D.
- OAT PRODUCT CODES 3ATCH i METHOD R/M(*P)%R.H. (ins.) APPLIE.
Nutec lls 2519/2530/2517 Squeegee 66*F/53%
- 2/4/81 3:00 P2 Nutee llS 2519/2530/2517 Squeegee 60*F/85% ** 2/5/81 9:00 a.m.
Nutet 11S 2519/2530/2517 Squeegee 62*F/55% *** 2/9/81 9:30 a.m e Nutec 11 2476/2102/2444 Squeegee 62*F/43% **** 2/13/81,2:t' Nutec 1201 9772/1959 Spray 73*F/52% ***** 2/16/81,3:( FILM THICKNES,5 TOP VIEIT 0: (ins.) lis
- 11s ** 11e *** 11 **** 1201 ***** COUPON Sidt 1 min. .030 .045 .001 .004 .003 .005 3 4 2 Sidt 2 nax. .025 .030 .030 .040 .001 .004 .003 .005 1
Sida 3 .025 .030 .030 .040 .003 .005 4 Numbered and
.025 .030 .030 .040 - .003~. 005 broomed surf.
Sida 4 TOTAL DRY PILM THICKNESS RANGE - Side 1 034 .054 Side 3 .058 .075 Side 2 059 .079 Side 4 .058 .075 ,
'0 RING CONDITIONS: AMBIENT TEMP. 70 go *P REL. HUMIDITY 45-65 %
MINIMUM CURE 7 DAYT
.'E' "ROCEDUR'E: DBA ORNL DATE SUBMITTED 4-28-81 TESTING PERFORMED BY:
APPROVED / , 's TEST REPORT NO. 495-81
>.e -- , - - , - - - - - , , - r-- ,,-n -
+ , . , TEST PANEL PREPARATION DATA l'.. PRODUCT *:0 BE TESTED: Nutec llS/Nutec ll/Nutec 1201, Nutec llS/Nutec 1201 2.. TYPE SUBSTRATE: Concrete SI2:E: 2" x 4" x 2"
- 3. SURFACE PREPARATION (Describe): Blast sweet on broomed surface to remove efflorescence; remaining faces wire brushed and blown down with 100 psi compressed air to-remove dust and loose concrete.
- 3. PRODUCT DATA: SAMPLE NO. (s) : A-78
- 3. DATE AND TIME CURING COMPOUND OR PRIMER APPLIED
~
[ PRODUCI APPLICATION CONDITIONS THICKNESS TIME & DA _MT PRODUC"' __ CODES BA'ICH # METHOD R/M(OF) % R.H. (ins.) APPLIE Nutec 11S* 2519/2086/2516 squeegee 71/73 See below 3-27-81 Nutee 11* 2476/2683/2444 squeegee 73/64 4-2.-81 Nutee 1201 2606/2607 spray 69/51 4-5-81 F M yins I Nutec lls Nutec 11 Nutec 1201 RAIG CO i Sida ,1 .020 .030 .006 .010 .008 .012 . 034 .052 Side 2 Min. .020 .030 .008 .012 . 028 .042 4 2
,Sida 3 .020 .030 .006 .010 .008 .012 . 034 .052 1 Sida 4 .020 .030 .006 .010 .008 .012 . 034 .052 Numbere+d a2 broomed surfac
. CURING CONDITICNS: AMBIENT TEMP. 65-80 F REL. EUMIDITY 45-90 g MINIMUM CURE 7 DAYS
. ITST PROCEDURE: DBA
. TESTING PERFORMED BY: ORNL DATE SUBMITTED 4-28-81
- Hand mixed APPROVED: ..
TEST REPORT NO: 495-81
-.~ .- -.n-_ , , , - -. . - ,n --- - -
..m. ,,
, 'EST PANEL PREPARATION DATA 1 PRODUCT ':0 BE TESTED: Nutec llS/Nutec ll/Nutee 1201. Nutec llS/Nutee 1201 2 TYPE SUBSTRATE: Concrete SIZE: 2" x 4'" x 2"
- 3. SURFACE PREPARATION (Describe): Blast swept on broomed surface to remove efflorescence:
remaining faces wire brushed and blown down with 100 psi compressed air to remove dust and loose concrete.
- 4. PRODUCT DA"a: SAMPLE NO. (s) : A-83
- 5. DATE AND TIME CURING COMPOUND OR PRIMER APPLIED N/A PRODUCT APPLICATION CONDITIONS THICKNESS TIME & DA
. TAT PRODUC'" CODES BA'ICH # METHOD R/M (*F) 4 R. H .
(ins.) APPLIE Nutec llS* 2519/2086/2516 squeegee 71/73 See celow 3-27-81 Nutec 11* 2476/2683/2444 squeegee 73/64 " 4-2-81 Nutec 1201 2606/2607 spray 69/51 " 4-6-81 FIIM THICYJT.SS TOTAL DFT TOP VIEW C (ins.} Nutec llS Nutec 11 Nutee 1201 RAIK"/ COUPON Sida ,1 ( '
.020 .030 .006 .010 .00a- E ~) .034 .052 Sida 2 ? min. 3 l .020 .030 .008 .012 .028 .042
4 2
-Sida 3. .020 .030 .006 .010 .008 .012 .034 .052 1 Sid1 4 .020 .030 .006 .010 .008 .012 .034 .052 Numbere+d an broomed surfac
. CURING CONDITIONS: AMBIENT TEMP. 65-80 F REL. EUMIDITY 45-90 %
MINIMUM CURE 7 CAYS
. TEST PROCEDURE: DBA / Radiation Tolerance . TESTING PERFORMED BY: ORNL DATE SU3MITTED 4-28-81
- Hand mixed
- APPROVED:
- TEST REPORT NO: 495-81
N , TEST PANEL PREPARATION DATA 1 PRODUCT 'IO BE ESTED:_ Nutec llS/Nutee ll/Nutec 1201, Nutee 11S/Nutee 1201 2 TYPE SUBSTRATE: Concrete SIZE: 2"x4"x2"
- 3. SURFACE PREPARATION (Describe): Blast swept on broomed surface to remove efflorescence remaining faces wire brushed and blown down with 100 psi compressed air to remove dust and loose concrete.
- 4. PRODUCT DATA: SAMPLE No. (s) : A-85 5; DATE AND TIME CURING COMPOUND OR PRIMER APPLIED PRODUCT APPLICATION CONDITIONS E ICKNESS TIME & DA'.
' OAT PRODUCT CODES BA'ITH # METHOD R/M( F)%R.H.
(ins.) APPLIE: Nutiec 11S* 2519/LN138-17-2 squeegee 71/73 See below 3-27-81 Nutec 11* 2476/LN138-17-1 squeegee 73/64 " 4-2-81 Nutec 1201 2606/2607 spray 69/51 " 4-6-81 FIIM THICE.TSS TOTAL DFT TOP VIEW C-(ins.) Nutec llS Nutec 11- Nutec 1201 RANGE COUPON Sidt _1 .020 .030 .006 .010 .008 .012 .034 .052 Sids 2; min. .020 .030 3 i
.008 .012 .028 .042 1 ' 4 2 -Sida 3 .020 .030 .006 .010 .008 .012 .034 .052 1 Sid2 4 .020 .030 .006 .010 ,.008 .012 .034 .052 Numbere+d a:x broomed surfac . CURING CONDIT!CNS: A: GIT.NT TIFP. 65-80 F REL. HUMIDITY 45-90 %
MIPIMUM CURE 7 DAYS
. TEST PROCEDURE: DBA TESTING PERFORMED BY: ORNL DATE SUBM.ITED 4-28-81
*Cowles Mixed ~~ ~-
4 APPROVED: TEST REPORT NO: toq_p,
e . 4 e h t RESULTS t S $
OAK RIDGE NATIONAL LABORATORY OPERATED BY union CARBIDE CoRPoRATloN NUCLEAR DIVl310N O P057 0FFICE BOX X OAK RIDGE. TENNESSEE 37830 May 26, 1981 Mr. Gerald E. Arnold Technical Representative Imperial Professional Coatings P.O. Box 29077 New Orleans, Louisiana 70189
Dear Jerry:
Enclosed are the test results on your recently submitted specimens. If we can be of further assistance,
- please feel free to call on us.
Sincerely yours,, 1 L./ d & - L. T. Corbin, Section Head
'- Analytical Chemistry Division LTC:dmw Enclosures I
r- 1 1 Manufacturer: Imperial Analytical Chemistry Division l Oak Ridge National Laboratory , New Orleans, Louisiana Date: May 26, 1981 l SYSTEM IDENTIFICATION Steel panel x Concrete block 115/1201 RADIATION TOLERANCE TEST ORNL Master Analytical Manual Method No. 2 0921; Bechtel Corpo' etion Specification No. CP-951; ORNL Log Book No. A9675, A5-5-1 . Initial dose rate: 1.0 x 107 rad Test conducted in: x air water Sample No. Cumulative dose Test results A-32 2 x 108 rad Coatings intact, no defects. f Evaluated 4/ I / , [/ -
,cm Approved ,/, M.~-
S
T 1
. Manufacturer: Imperial Analytical Chemistry Division 1 Oak Ridge National Laboratory New Orleans, Louisiana Date: May 26, 1981 SYSTEM IDENTIFICATION Steel panel x Concrete block 11S/1201 DBA TEST ORNL Master Analytical Manual Method No. 2 0922.
ORNL Log Book No. A9675, A5-5-1 Samole No. DBA chase Test results A-32 spray
- Coatings intact, no defects, all areas.
A-34 spray Coatings intact, no defects, all areas. A-38 spray Coetings intact, no defects, all areas.
- Irradiated.
Approved [. N
Imperial Analytical Chemistry Division Manufacturer: Oak Ridge National Laboratory New Orleans, Louisiana Date: May 26, 1981 SYSTEM IDENTIFICATION Steel panel x Concrete block 115/11/1201 RADIATION TOLERANCE TEST ORNL Master Analytical Manual Method No. 2 0921; Bechtel Corporation Specification No. CP-951; ORNL Log Book No. A9675, A5-5-1 . Initial dose rate: 1.0 x 107 rad Test conducted in: x air water Samole No. Cumulative dose Test results A-83 2 x 108 rad Coatings intact, no defects. j
$ f Approved I/ %
Manufacturer: Imperial Analytical Chemistry Division
. Oak Ridge National Laboratory New Orleans Louisiana Date: May 26, 1981 SYSTEM IDENTIFICATION Steel panel x Concrete block 115/11/1201 DBA TEST ORNL Master Analytical Manual Method No. 2 0922.
ORNL Log Book No. A9675, A5-5-1 Sample No. DBA chase Test results A-78 spray Coatings intact, no defects, all areas. A-83 spray
- Coatings intact, no defects, all areas.
A-85 spray Co,atings intact, no defects, all areas.
- Irradiated.
9
,- i Evaluated // ,/, // s .
Approved ,/ [
-L 12-4201 06/22/84 Allegation No. 12 If maximum limits are used, paragraph 4.3.1.2 of Procedure Number CCP-40, Rev. 5., allows a 102 mil thick coating system for 115/1201/11S/1201. Is this system thickness qualified, for example for environmental (irradition) conditions and DBA conditions, under ANSI 101.2-1972?
Evaluation of Validity This allegation, which relates to a repair procedure involving limited total surface area, is addressed in our response to Allegation Number 1. Additionally, data developed by Imperial (See Test Report No. 495-81, attached) includes the i results of irradiation and DBA tests of systems similar to those listed in t Allegations No. 1 and No. 12. The coatings thicknesses tested range from 10 to 115 mils. All systems tested met DBA requirements. The systems subjected to irradiation were at fil::t thicknesses of 10, 12, 30, 60 and 70 mils. These were - unaffected by irradiation. In view of the limited areas involved and the available data, this allegation is without technical significance. Safety Significance None , Generic Impliettions on Other Systems or Contractors Not applicable i
lE f %
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TECHNICAL REPORT i 1 NUMBER l
#495-81 l , ,
N mu Nutac 115/Nutac 1201 Nutec 11S/Nutac 11/Nucac 1201 Radiation Tolarance, Design Basis Acci g Testing (ORNL)
. Company Enowledge
' - CUSTOMER Submitted by: Gerald E.
, sD d/f ,
A$$ M 37 ~. ~ ~ l 1 Date: June 10 198i , l SOUTHERN IMPERIAL COATINGS CORPORATION, LNC. i P. O. Box 290 7 - New Orleans. Laum.m 70189 Phone: (504) 254-1433
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M The purpose of this rest is to. evaluate the performance of Nutec HS applied at-film thicknesses of .020 .115" undar design basis accident conditions specified for the South Texas Project. The effects of various mixing techniques and compressed air r1==ning , are also studied. BACKGROUND: The six rest spee4-= were included in the South Texas Project test to generate data on Nutec HS at film thicknesses higher than the currently qualified 35 mil. ==v1== DFI imposed in Service Level 1 areas, to comply with the newly revised STP test require-monts and to provide data on surface preparation other than abrasive blasting.
SUMMARY
AH six specimens exhibited no defects when subjected to the S'5P designbasisaccidentconditionsj291*T.,70PSIG). Two of the sper1==a= were irradiated to 2x10 rads; radiation tolerance was exceHanc. F10CIDURIS: Concrete coupons, measuring 2x4x2",' were coated as described in g " the attached panel preparation sheets. On coupons A32,A34, and A38, Nutec US was applied at various film thicknesses and in 1-3 costs. Some faces also received a tight coat of Nutec M. Coupons A78,A83, and A85 were coated with Nutac H S and Nutec H i which had either been hand mixed with a spatula or with a Cowles
.. mixer. One face of each coupon received no Nutec M. Therefore, the coupons in both sets represent both the Nucac 115/H/1201 and the Nutec HS/1201 system.
i The test spae4==== were submitted to Oak Ridge National Laboratories.
- Coupons A32 and A83 were irradiated to 2x108 rads; all coupons were DBA tested per the 56uth Tazes esquirements, with maxisma temperature and pressure, of 291*F. and 70 PETC, respectively.
(See ate =eh==at sumunary) Refer to the attached OIEL statement
- for a description of the testa performed.
RESULTS: Refer to individual ORNL results sheets. Du Coupon No. Irradt.ation Results A32 Yes No defects p;p A34 No l 438 No V. A78 No "
-(
M3 Yu . A85 " No (
Tarkniemi Report #495-81 Page 2 J CONCLUSION: At the LOCA conditions simulated in this test, the Nutac ;
.' concrete system performed satisfactorily:
A) Without Nutec 11 (Nutec 11S/1201)
, 3) At Nutac US thicknesses of .020 .070" (one coat)
; C) At Nutac HS thicknesses of .040 .n5" (two-three ie cau)
D) At Nutec n thicknesses of 1001 .010" E) At Nutec 1201 thicknesses of .003 .012" F) Regardless of dispersion speed (mixing) G) Over various prepared surfaces , The. data demonstratas that both the 11S/n /1201 and ES/1201 systems met the acceptance criteria of ANSI N5.12 and ANSI N101.2, when subjected to a radiation exposure level of 2x108 rads and DBA conditions of 291*T and 70 PSIO.
! This report should be reviewed.in conjunction with Imperial's t=a w4e=1 report #505-81, which describes the results of a second c ,. . DBA test series on the Nutec concrete coating system.
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%, SMBIARI QF TES FEDCEDURES
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Max. Coupon i Surface Prep. System DFT Rad. levels Comments (Mils) 8 A 32 11S/1201 70 (H S) 2x10 rads i 115/11S/1201 60 (115) ' 1 i A 34 3 roomed surface 11S/1201 25 (US) No radiation was abrasive HS/11/1201 40 (ES) blasted; all US/nS/1201 L15 (ES) other surfaces 11S/US/us/n/120175 (US) were stoned fonow-A 38 ed by compressed HS/n/1201 45 (nS) No radiation air cleaning. 115/115/u/1201 70 (us) us/us/1201 70 (ns) A 78 US/u/1201 30 (u S) No radiation ins & fu 10 (n) were hand Broomed surface 12 (1201) sized. was abrasive - O*- ted; C 8
</
i A 83 other surfaces 115/n/1201 30 (115) 2x10 rads ills & fn 10 W mW h one 12 (1201) aimed. j soEPress US/u/1201 #115 and fn A 85 g 30 (US) No radiation 10 (n) were sized
.. 12 (1201) 'on a Cowles dissolver.
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*4 TEST PROCEDURES O
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9
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i Manufacturer: Imperial Analytical Chemistry Divisitn Oak Ridge National Laboratory
}'.
New Orleans Louisiana . .Dat e: May 26, 1981 S - j REPORT OF IRRADIATION AND.DSA TESTING , t The irradiation and design basis accident (DSA) tests are conducted, respectively, in accordence with Bechtel Corporation specifications CP-951
- and CP-956,in Standard specification Coatinos for Nuclear Power Plants (or I with modifications as noteo in Taole Z, asA test conottions). Tne tests are designed to meet specifications set in both AMSI report N 101.2-1972,
, Protective Coatinos (Paints) for Licht Water Nuclear Reactor Containment Facilities, ano N 5.12-1974, Protect've Coatinos (Paints) for the Nuclear , Inoustry. The DBA test spray solution ano tne' test conottions are listeo in Tacles 1 and 2. After both the DBA and irradiation tests, coatings are t examined for signs of chalking, blistering, cracking, peeling, delanination, and flaking, according to ASTM standards where applicable. All test pana.ls are returned to the coating manuf acturer. . The irradiation tests are run using a spent fuel assencly, removed from
- the High-Flux Isotope Reactor at ORNL, as the hource of radiation. These fuel asseelies are stored under 20 ft of domineralized water. The fuel is 931 enriched U-235 as U 03 8 combined with aluminun. The spent fuel as-semblies are removed after each 23-megawatt-day period . Irradiation is done using the .ganna energy ' rom acpumulated mixed fission products. Th'.s
. more readily simulates conditions around a reactor than does a cobalt
. IV' source. Also, the higher gaseia activity affords shorter irradiation time to achieve accumulated doses. The dosg rate four days after removal of a fuel assembly from the reactor is 1 x 100 rad /h. The fuel assembly is 20 in high. A 20-ft-long, 3-1/2-in.-diameter pipe, with one end capped, is used for air irradiation tests. The capped
'and is lowered into a 4-in. opening at the center of the fuel asseely. The open end, above water level, is covered with an 0-ring-sealed flange to which is attached a steel cable and an air outlet hose. The air inlet is located at the bottom of the pipe. Test specimens are connected to the bott:mi of the cable and lowered into the radiation field. Also at the
- center of the fuel assembly is a stainless steel-clad cadmium tubt used as a rautron absorber. This prevents contamination of the test speci
- nens by l
induced radiation. l f ,s Evaluated 4[~t Approved I/,
- i f
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- r
$I Manufacturer: Imoe-ial Analytical Chemistry Division Oak Ridge National Laboratory
% 'New Orleans, Louisiana , Date: May 26. 1981
#N9 ORNL Log Book No. A9675, A5-5-1__ ,
Table 1. DBA solution composition, distilled water Resoent Concentrat. ion Boric acid, Hs50: 0.28 # Sodium hydroxide, NaOH Required to adjust pH to 9.5 Table 2. DBA test conditions l Temperature Pressure Time (*F) (psic) Comments
, . , Start 150 ' Autoclave preheated.
WO 10 min 150-291 Steam injected at 260*F.
. 20 min 291 70 Pressure maintained by relief valve.
45 min 291-260 80 min 260 39 Pressure adjusted with N2-
~
12b min 260-220 180 min 220 20 4 210 min 220-160 21 h 160 5 ( Placed in fresh spray solution in l 10 d 125 2 constant temperature bath. End of test I ' I , i Evaluated 4/d i / Approved [ / - [ $ G- . . i I I l . . l
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!. TF.ST FANI2. FREPARATION DATA e
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@ TO ME TEI22D: 3 3 e in..... ....
. mE sUnsm,, Co.erate -
u .. . 2,t , Carborundum stone used to remove hiwh 14. hen = net lan== e . SUEFACE FIDARATION (Describs): particles l broomed surface blast svent to remove afflorescence. Cleaned vdrh 100 c=4 c enn-pressed air
. FEODUCI DATA: SAMFLE NO.(s): A-32
. DATE AND T::20E CUENG COMPOUND DE FEIMER. AFFLIEDi N/A PRODUCI AFFLICATION CONDITIONS TEICKNESS TIME & DA:
Q _AT FRODUCI - CODES . RATCH f METBOD RfM(*F)TR.E. (ins.) AFFLIII Nutec 115 2519/2530/2517 Squeegse 66*F/53I
- 2/4/81 3:00 p.s."
Nute$ 11s 2319/2530/2517 Squaesse 60*F/85I ** 2/5/81 9:00 a.m. Nutec 115 2519/2530/2517 Squegsee 64*F/55I *** 2/9/81 9:30 a.m.
/-O. . .
i Nutec 1201 9772/1959 Spray 73*F/52I ***** 2/16/81.3:0: NM TOF TIIR OF fins.) 11e
- 15e ** ise *** 11 **** 1201 ***** g max. nng_ nns Side 1 .060 .070 3 4 2 Side 2 min. .040 .050 ons_ nne
-l 1 Side 3
.010 .020 .030 .040 .003- not i Numared and
.010 .020 .030 .040 .003 .005 broo W surfa' Side 4
~
ttrIA1. DEI FILM TIICENESS BANGE - Side 1.063 .075
- Side 3 .043 .065 I
Sida .2 043 .055 Side 4 .044 .074 ,
- UEING CONDITIONS: AMBIENT TEMP. 7n-an 'F REL. BUMIDITT t.5-65 :
MINDfDM CURE 7 DAYS i y PROCEDURE: DBA and Rad (.. .,$lac FxxFonszn n : onm. naz:. In xITIED 4-2s-si AFFROVID , TEST REPORT NO. 495-81
- I , .
1,
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'j . .-
~
t TEST FANI1, FREFARATION DATA i k .- .D 3E'TISTED: htec US/Nutee 11/Natee '1201 Wree 'nS/Nutee 1201 i
. TIFE 501STEATE: Concrete
- ci-,. ?,4,9
. gggyACg yggy m ?Trnt WMM): Carborundum stone used to remove hieh 14 ,hes n a 1an..
particles; broceed surface blast 4 event to remove efflorescence. Cleened tre ek 100 ned = n-pressed air
. TEggxx:r DATA: SAMFLE NO.(s): A- 34 DAZE AED TIME CORIEG COMP 0tDED DE 7EIMEE A?71.IED: R/A
- FttuxR:: A7FLIcA?Trra CONDITIONS TEICINE9i DAT PRODUC- CODES 2ATCH # TIME & D METROD 1/MC*7):1.E. (ins.) AFFLZZ kre: us 2519/2530/2517 Squeesee 66*F/53:
2/4/81 htac 3:00 P 115 2519/2530/2517 Squeegee
' 60*F/85: **
2/5/81 9:00 a.a-Bucae US
' 2519/2530/2517 Squeegee 62*F/55: *** 2/9/81 9:30 a.m heac n 2476/2102/2444 Squeegee 62*T/43: ****
2/13/81.2:1 Entec 1201 9772/1959 Spray 73*F/52: ***** 2/16/81,3:t yILu Twterwret _ (ins.) ilt
- 199 ** ile *** 11 **** 1201 ***** TOP VIEN C 3 , . g
! Side 1 Min. .020 .025
.003 .005 3
Side 2 .025 .040 .001 .004
' .003 .005 side 3 Max. .025 .035 .030 .040 I 1
.030 .040 .001 .004 ' 003~.005
' s e76 side 4 .02 %.035 .03b.%0 Numbered'and
.00%.005 broomed M TDTEI. DEZ FIIE nTcrWESS RANGE - Side 1 .523.030" Side 3 .086 .124 Side 2 .029 .049 Side 4 .053 .080 ,
UEIBG CORDITICKS: AMBIERT TIMP. 76-an * *7 2ZL. EDMIDIIT 45-65 : MINIMDM CURE 7 Dh's
*EST TRDCEDbEE: DBA i .t . .
CRNL (-$2FZ1FOIMEDIT: DATE SUEMITIZD 4-28-81 3 AFFE07ED j - ,
- -- . .. TEST REPOEI NO. 495-81 t - _.
-m-***y *=*=====- -eeum .e
.-m . . . . . . . .
s . ,,
~ - - ~ ~ !** TER FANEL FREFARATION DATA e
i TO 3E TESTED: Watee lis/Nutee 11/Nutee 1201 . Nutec lis/Mutee 1201 i
!.. M SM* COScTeca M49e= '1 y Aw 'l ? .
I
. sg3 FACE FIEFARAZIM (Deecribs): Carborundus stone used to r hieh 14 ehes-' ==A 1aae.
particles; broomed surface blast swept to remove affloreseenee. c1.-=.a e h too . 4 i . pressed air
.. FIODDCT DATA: SAMFLE NO.(s): A- 38
.c, DATE AED TIME CEZNG CCRIPODED OR,712MEL AFFLIED: N/A
- PsaDucr AFFLIcATzan CcarDrrzaEs TszcssEss TzuE & Da zur FnaDoe: codes 2ATCn d wrarm 1/M C*F):1.E. (ins.) AFFLIEE mucee ils 2519/2530/2517 squaesse 66*F/53:
- 2/4/s1 3:00 P**
autec 11s 2519/2530/2517 squaesee 60*F/as: ** 2/5/81 9:00 a.m. But.c 11s 2519/2530/2517 squeepee 62*F/552 *** 2/9/81 9:30 a.m.
. _. y Entee 11 2476/2102/2444 squeegee 62*r/43% **** 2/13/81,2:0 Butee 1201 9772/1959 Spray 73*F/52: ***** 2/16/81.3:0.
rzLu TnIC m ss Tar vzza ar 3 (ins.) 11e
- 11e ** 11e *** 11 *"** 1201 ***** COOFW i .
Side 1 min. .030 .045 .001 .004 .003 .005 3 4 ^2
- Side 2 ""** .025 .030 .030 .040 .001 .004 .003 .005 1
Side 3 .025 .030 .030 .040
.003 .005 Numbered'and
+
Side 4 .025 .030 .030 .040 .
.003 .005 broomed surfar TUZAL DEI FIIX TIICENESS BANGE - Side 1 0 b .054 ' side 3 .058 .075 Sida 2 059 .079 Sida 4 .058 .075 .
llDI23G CONDITIONS: AMBIENT TIMP. 7c sin ' *F REL. EDtED M 45-65 % MINIMuti CUEE 7 DAIS TEST.PRDCIDUR': E CBA T*' FERFORMID BY: OREL DATE SUBMIT 22D 4-28-81 t imo. Aa zh s TEST REF0ET NO. 495-81 e - - - ;. - - __ __ m - . . 5 a
1 -
- _"2:ST
. PANE
- PREPARA'"!ON DA"'A t,
.C .,
e .
'I M . TD RE TES".ED:
Nutec 113/Nutac 11/Nutec 1201. Nutec 11S/Nutec 1201 2- TFE SUBSTRA3: Concrete ' E lllZ: 2" x 4" x 2"
- 3. SURTA 2 PPEPARA CN (Desc=ibe): Blast swept on broomed surface to remove efflorescence f remainine faces wire brushed and blown down with 100 psi compressed air to remove dust and !
loose concrete.
- 4. PX3DDC DA".lk SAMPLZ IR3. (s) : x-vg i L. DL"E AND ":ME CURINC CttfPOUND DE PRIMER AFPLIED PEQDOCT APPLICRT205 CDHDZTION5 TEICENESS TIME & DR "l CAT PM3DDC" CCDES BATCE 5 _m R/M(CT)gn.g.
(ins.) APPLZZ Nutec lis' 2519/2086/2516 squeegee See below 3-27-81
"{1/73 Nutec 11* 2476/2683/2444 squeegee 73/64 "
4-2-81 Nutec 1201 2606/2607 spray 69/51 " 4-6-81 i . TIIM TirTemm total Dr; T3F VIEN C g m ,i Nutec 115 Nutec 11 Nutec 12011 RANGE - COUPCM Side 1 .020 .030 .006 .010 .008 .012 .034 .052 . Side 2 Min. 1 .C20 .030 .008 .012 .028 .042
,6 2l 0
Side 3 .020 .030 .006 .010 .008 .012 .034 .032 1 Sida 4 .020 .030 .006 .010 .008 .012 .034-
~ aan broceed su=fac
)
C3RIlBG CDEDITIC.NS: AMBZENT TEMP. 6S-80 *F 7.e.".. Et2CDITT 45-90 g
; -!E3CMCM CURE 7 Dars
.. EET FMmeF: DBA
- TESTZRG PERPCRMED IT: ORNL ggg, ggggg;;gg 4 23-31 f
enand r.1xed (-ho APPROVED:
, ! TEIT REPORT NO: 195-81 -
1
, , _ ,__ _ , , . . . . . ._ _ . . . -- - -- - - - ---- ' - - ~ '
. . . .. ._._. . . - . - ~ ~ - - - * * *
. t. .
TEST PANE" PIEPARACON DATA 3,
'3 w
jLNIElIDOCT ':0 RE TESTED: I Nutec 12S/Nutee 11/Nutee 1201. Nutee 11E /Nutee 1201 l
) 2- ':TFE SUBSTRA2: Concrate 5::llE: 2" x 4" x 2" .
1
,2. SURr3Wl:E PREPARACCN (Desc:l1be): Blast swept on broomed surface to remove affloresceneet r -mining faces wire brushed and blown down with 100 psi compressed air to remove dust and loose concrete. -
- 4. FX3 DUCT DATA: SAMPIZ M2. (s) : A-83 L DLC AND CME CURINC COMPOUND OR FRDfER AFFLIED N/A FRODUCll' AFFLICATION C:MDITIONS ':IICENESS TZME E DA: '
- DAT F1cDUC".' CDDES BA':t:I # m R/M(*T)tR.E.
(das. ) APPLIE: Nutec US* 2519/2086/2516 squeegee 7h73 See below 3-27-81 Nutec n' 2476/2683/2444 squeegee 73/64 " 4-2-81 . Nutee 1201 2606/2607 spray
. 69/51
- 4-4-41
) .
. q~:? .
TOTAL DFT TOP VIEN G T:l3 M TH I.CK:U:SS f4=e.1 Nutec 11S Nutec U Nutee 1201 RANGE CtXIPtlE Side _11 I
.020 030 .006 050 '
. m - 659 . 034 .052 Side 2( min. l .020 .030 3
.008 .012 . 028 .042 l I '* 4 2
. Side 3 l .020 .030- .006 .010 .3C8 .012 '
. 034 .052 '
1 (
.'stae 4 .020 .030 .006 .010
.00s .Ou . 034 .052 maemer7sama mee e4 u=e..e
.. CURING CDN:: =CNS: AMBIENT TEMP. 65-80 'F RE: EtLw"m 45-90 y M:3t: MUM C:DtE 7 DAYS
. - EST PROCE:XDtE: DEA / Radiation To'lerance
. TEE =NG FE3tFCIMED IT: ORRL-DA'!lE SUBMITTElD 4-28-81
- Hand mixed
- t..N APPROVED: '
J- )
. .g l TEST REPORT NO: 495-81 s
6
-,e --n--,..,--sn w- -,- . , - - . - --- --- -,
1 i . j TEST PANZ" PRDARATION DATA
.I RCDDCT TO E METED: Nutee llS/Nutee ll/Nutee 1201. Nutee llS/Nutee 1201 2 TPE SUBSTJtA= concrete 52:Z: 2"x4"x2" 5
- 3. SURFA2 PEFARATICK (Desc:=ibe): Blast swept on broomed surface to remove efflorescence:
remaininc faces wire brushed and blown down with 100 psi comoressed air a remove dust and loose concrete. f 4 F1CDDC: DA:ks SAMPLZ MD. (s) : A-85 l L DA:l2 AND N CURING COMPOUND DE PRDG1 AFFLIED l i l PMXECT
- APFLICATION COND "" CN5 MIC2 NESS T Mr. & CA <
"Oh!" _P1CDDC" CCDES BATCH # ME':ED R/M (*T) g R.E.
(ins.) APPL 22: l Nutec llS* 2519/LN138-17-2 squeegee 71/73 See below 3-27-41 Nutec 11' 2476/LN138-17-1 squeegee 73/64 " 4-2-31 Nutec 1201 2606/2607 spray 69/51
- 4-6-41 e '
- s. -
s 00ffAL QFT E
. TZut TEI.CE::2:35ft...) L u Nutec 1.15 Nutec 11- -l Nutec 1201 RANGI: COOPW rJde 1, . 020 .030 .006 .G.G .008 .012 .034 .052 Sina 2, ra.n. . 020 .030 .008 .012 l l.028 .042 3
'* -6 2 i
Side 3 .020 .030 .006 .010 '
.008 .012 l .034 .052 i
.020 .030 .006 .02-) I.004 .012 side 4
.034 .052 M and broamed sureae :
- s. CU3C3G CDEDIT:CRE: AMBIZET N.
65-80 F .EL. EUMIDI'IT 45-90 g ME!ENDf C3EE 7 C225
. SST PN: DEA
. TIITING N ET N mg= sg33z;ss 4 28-81 s
*Cowles Mixed ~~ - -
M L.! ,
; TEST REPQFT NQ: t e et_ o ,
}
i t 1 . i .
--.. . -- . ~
g--- -- , w g--,,--- -- , , , _ g-,,,-g--y p g a . _ w wwr - . - - - - - - , _,.,,, ,m---_-,,-, _ - - ~ -- - - - - - - - - -_-
-,-m.m - - --
F e e em** go * - . =ame. bene -e= M
---- - *N** em . **6 6 m. N' * *--oo. . . . . . .. .- ---- . . ..
m.sp*- , .,, .- g .
# b
- e
%4 4
3
-i S
e o D' I S 4 e e IESULTS 0 G 9 e
$+
eds 4 w
- 9 4
-. 4 l
9 0 1 .
.a.ee... _ ,,, ,
m
s.- OAK RIDGE NATIONAL LABORATORY i , s. = = . , Union'cARSlot CORPORATION O
. NilCLEAR OfVIsl0N e
Post OPPtCE 80X X - OAK RIOSE. TEmeeBASEE 37830 May 26, 1981 v Mr. Gerald E. Arnold
' Technical Representative Imperial Professional Coatings ,
P.O. Box 29077 New Orleans, Louisiana 70189 .
Dear Jerry:
Enclosed are the test results on your recently submitted specimens. If we can be of further assistanca,
- please feel free to n, call on us.
'1/
Sincerely yours,
, / .
sg s. - 3 . r-L. T. Corbin, Section Head Analytical Chemistry Division LTC:dat i Enclosures WN $e e m , l l .
,... .. * ~
l . l r i
. c.9 O - .
l l L-
6 j - Manufacturer: Imperial Analytical Chemistry Division
- Oak Rid 9e National Laboratory New Orleans, Louisiana Date: __ May 26, 1981
.h #
. !C SYSTEM IDENTIFICATION , _ Steel panel x Concrete block
! 115/1201 i
5 I RADIATION TOLERANCE TEST s
. ORNL Master Analytical Manual Method No. 2 0921; Eachtel Corporation i Specification No. CP-951; ORNL Log Book No. A9675, AS-5-1 .
'5* Initial dose rate: 1.0 x 107 rad Test conducted in: x air water
%: . A.:/
- Sample No. Cumulative dose Test results A-32 2 i 108 rad Coatings intact, no defects.
{ j .
== e )
E,aioat h w
! .' //,. //
?5 Approved I., 'l __
4
- .. . . .y 1
. g. .
?
. ,e .
. ! r;
* ***'**a'B=emee oc p w e** p - se ome am .
memog,eg, , , , ,9 g. . . _ , _ - , _ _ - . _ . . _ _ _ _ _ _ _ _ _ __ . - _ _ _ . . . , _ _ ..,m . ,_.
7.; _.- .
, j ..
-d . .'o
. Manufacturer: Imperial
~
Analytical Chemistry Division i .0ak Ridge National Laboratory
>q New Orleans, Lcuisiana Date: May 26, 1981 w
. SYSTEM IDENTIFICATION Steel panel ,
x Concrete block i 115/1201 I 1 DBA TEST ORNL Master Analytical Manual Method No. 2 0922. ORNL Log Book No. A3675, AS-5-1 Test results Samole No. DBA phase A-32 spray
- Coatings intact, no defects, all areas.
A-34 spray Coatings intact, no defects, all areas. A-38 spray Costings intact, no defects, all areas, f ,. . 6
.. .D
- Irradiated.
e i Evaluated s . N b. Approved ID [ __ - l I
.~_-
r
.\ .
s, s'
)
I l
~
r .,. _ . __ e. Manufacturer: Incerial Analytical Chemistry Division Oak Ridge National Laboratory How Orleans. Louisiana Date: May 26. 1981 i' D SYSTEM IDENTIFICATION Steel panel x Concrete block' 115/11/1201 RADIATION TOLERANCE TEST ORNL Master Analytical Manual Method No. 2 0921; Bechtel Corporation Specification No. CP-951; OENL Log Book No. A9575, AS-5-1 .
. Initial dose rate: 1.0 x 107 rad Test conducted in: x air water e
J . Sample No. Cumulative dose Test results A-83 2 x 108 rad Coatings intact, no defects. l f Evaluated W/ , 2, Approved I *
;- )
kJ . . .
- 6 i:
;-_. ~..~_.. .. _. .n;
- = . . . . _ . - . . _ _ .. - . .-..
1 1 .g, .
.] Manufacturer: Imperial Analytical Chemistry Division
,- Oak Ridge National Laboratory New Orleans, Louisiana May 26, 1981 Date: AO . SYSTEM IDENTTFICATION Steel panel x Concrett block , i? 'l
~
115/11/1201 i MA 72R f ORNL Master Analytical Manual Method No. 2 0922.
- j ORNL Log. Book No. A9675, A5-5-1 i
e Samole No. DBA chase Test results . i i A-78 spray Coatings intact, no defects, all areas. A-83 spray
- Coatings intact, no defects, all areas.
.]:
- A-85 spray Co,atings intact, no defects, all areas.
tb.^ f -
2 /
;
- Irradiated.
- j. .
/
. l i L -
l Evaluated
. ) 8
. fr/ // s , :
Approved I c i...
- . ~, *:-* gi
~i I 'i
$, k..
. ._}}