ML20113G538

Rev 5 to 00260-C, Hazardous Substance & Waste Control

ML20113G538
Person / Time
Site:	Vogtle
Issue date:	10/24/1989
From:	Kitchens W GEORGIA POWER CO.
To:
Shared Package
ML20092F288	List: ML20092F604 ML20092F672 ML20092F802 ML20092F899 ML20092G696 ML20092G774 ML20092G779 ML20092G793 ML20092G802 ML20092H039 ML20092H055 ML20113G385 ML20113G538 ML20261F083 ML20261F087 ML20261F092 ML20261F097 ML20261F105 ML20261F115 ML20261F120 ML20261F124 ML20261F129 ML20261F135 ML20261F138 ML20261F145 ML20261F152 ML20261F155 ML20261F160 ML20261F165 ML20261F170 ML20261F175 ML20261F180 ML20261F183 ML20261F189 ML20261F195 ML20261F200 ML20261F206 ML20261F211 ML20261F216 ML20261F222 ML20261F227 ML20261F242 ML20261F249 ML20261F253 ML20261F257 ML20261F260 ML20261F264 ML20261F268 ML20261F273 ML20261F278 ... further results
References
CON-IIT05-002-116-90, CON-IIT05-278-90, CON-IIT5-2-116-90, CON-IIT5-278-90, RTR-NUREG-1410 00260-C, 260-C, NUDOCS 9202210452
Download: ML20113G538 (33)

Text

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1si peedure establishes guidelines and control for Jot'a substaneet used within the VEGP site b,or.,n#.rier.,

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' e11nes are entablished to ensure compliance 6

j.;j able codet, and regulations.

Thr.s (;t8tM ols are used to ensure a safe work 1.2 env2.~onibst when hazar dous substances are used.

f,5 NOTE

', Tbc use cf certain chercicale,

'..gl.uas, seclants, pt.ints.

l ub rica n t. c, cleaners, etc. on

. NSSS cor;<ponents are restricted.

The-use of those materiala on hSSS components shall not be allovt.d unless specifically stated in the Vogtle Chemical Centrol list.

For use,on NSSS c oreponen t s.

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/.. heme..i 's m chemical substance which may be herdul'to eititer persons or the plant if used or dispo. sed in an improper manner, m.

2.3.2 l'he.;A.'Enng chemicals are exenoted from requiring i

perd.ta out must appear on the chemical control list,

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I! abo atory chemicais.

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Bulk precess chemicals and resins.

Maintenance personnel use of small aerosol c.

chemical volumes used only in the Maintenance fSheps.

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How lubricating oils and greases, Household type cleaning products used for lavatory e.

or office purposes only.

2.

Sulk chemicals used by Decon and Building and Grounds parsonnel.

If these chemicals are used on NSSS compenants, they must be approved by Chemistry Superintendent or Chemistry Senior Regulatory Specialist.

t, 2.2 COMBUSTISLE AND FLAWAFLE GASES Gases determined by specified testing ;)rinciples to be easily iguitable.

Such gases include put are not limited to Hyd regen, MAPP Gas, Acetylene, and Methane.

2.3 COMBUSTIBLE LIQUID Any liquid having a flash point above 100 degrees Fahrenheit ('F).

This includes NFPA Class II and IIIA as indiceted in the preceding table.

See Table 3 for examples.

2.4 CONTRACTOR The parties, singularly or collectively, or legel counsel, contracting to furnish materials and/or p.arform the work covered by the specifications of c given purchasins document.

2.5 CONTROLLED CHEMICAL LIST The VEGP controlled chemical list represents an inventory of all chemicals which may be used on site, either by GPC or other personnel.

Inclusion of a chemical in this list indicates that a Material Safety Data Sheet (MSDS) for that chemical is available for inspection.

2.6 CONTR0 LIED ISSUE AREA (CIA)

See Procedure 00262-C, " Control Of Chemicals / Fluids" for this definition.

l 2.7 DRUM l

A metal or plastic, cylindrical container which holds l

l 55 gallons or 80 gallons.

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3 of 33 2.8 DISCARDED MATERIAL A material is censidered " discarded" if it is abandoned by " disposal" or burned or incinerated or physically, chemically, or biologically treated instead of or prior to " disposal" and is not used, reused, reclaimed, or

recycled, 2.9 DISPOSAL Discharge, deposit, injection, dump, spill, leak, or placement of a substance into or on any land or water so that such material or any consti:uent thereof may enter the environment er be emitted into the air or discharged into ground or surface waters.

2.10 FLASH POINT The minimum temperature st which a liquid gives off vapor in sufficient concentration to form an ignitable mixture with air, near the surface of the liquid, as specified by appropriate test procedures and apparatus.

2.11 FLAMMABLE LIQUID Any liquid having a flash point below 106 degrees Fahrenheit.

This includes NFPA Class IA, IB, and IC liquids as indicated in the follovir.g table r i

NTPA 30

, CLASSIFICATION _

FLASH POINT BOILlNG POINT Class IA Below 73'T Below 100'F Class IB below 73'F At or above 100*F Ciscs IC 73*-100'F N/A Class II 100'-140'F N/A Class IIIA 140'-200*F N/A See Table 3 for examples.

NOTE For shipment purposes, RCRA regulations require any liquid having a flash point of less than 140F be classified as flammable.

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4 of 33 2.12 RAZARDOUS SUBSTANCE A substance by reason of being toxic, corrosive, oxidizing, reactive, eaplosive. flammable, combustible, or otherwise harmful, mcy cause personal injury or environmental damage.

The above terms can be found in the Code of Federal Regulations, Titles 29, 40 and 49, 2.13 RAZARDOUS WASTE A waste including liquids, semi-solids, solids or combined gaseous materials or combinations of wastcs which, because of quantity, concentration, physical, chemical, or infectious characteristics, may pose a substantial or potential hazard to human, animal, or environmental health when impro>erly treated, stored, transported, disposed of, or otaervise managed.

See Section 11.0 for Determination of Hazardous Waste.

2.14 OTHER WASTE MATEPIAL Any solid, liquid, semi-solid, or contained gaseous material which is " discarded" or being accumulated.

stored, or treated prior to being discarded, or has served its original intended use.

Sometimes it is d!.scarded or is a discarded manufacturing or mining by-product.

C.15 NFPA National Fi:c Protection Association 2.16 OXIDIZING GASES A gas that induces another substance to form a coat of o.xide on its outer surface due to the exchange of electrons for oxygen atoms and the valence of the substance in increased.

Such Sases include but are not limited to:

Chlorina, Oxygen, and Fluorine.

2.17 RCRA Resource Conservation and Recovery Act l

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$ of 33 2.18 SAFETY-RELATED AREA Any area in a Category 1 building which provides a passage to a piece of safety related equipment or contains a piece of safety related equipment.

2.19 SPILL OR LEAK Unintentional release of any hazardous substance into the environment.(This includes moats, concrete berms, retaining walls, etc.)

2.20 STORAGE The holding of hazardous waste for a period less than 90 days betore the end of which the hazardous vaste is transported offsite to be treated, disposed of, discarded, or stored with a licensed hazardous waste contractor.

2.21 TREATMENT Any method, technique, or process, including.

neutralization, designed to change the physical, chemical, or biological character or composition of any hazardous waste so as to neutralize such vaste, or so as to recover energy or material resources from the waste, or so as to render such waste non-hazardous, or less hazardousi safer to transport store, or dispose of: or amenable for recovery, amena,ble for storage, or reduced in volume.

3.0 RESPONSIBILITIES 3.1 CHEMISTRY SUPERINTENDENT I

The Chemistry Superintendent will ensure that:

1 NOTE The Chemistry Superintendent I

may request and receive assistance i

from the Industrial Hygienist for any of the following.

3.1.1 Chemicals used at VEGP, considered as hazardous substances, are identified (as required) on the i

" Controlled Chemical List", Procecure 00262-C, " Control Of Chemicals / Fluids".

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3.1.2 Requirement.s of Federal Regulations applicable to hazardous aubstances and wastes are met.

3.1.3 Each controlled chemical or hazardous substance has a Materials Safety Data Sheet (MSDS) on file prior to issue for use.

3.1.4 Requests from individuals for chemical orders are reviewed to classify items to be purchased to determine l

if a Material Safety Data Sheet (MSDS) is required.

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3.1.5 Hazardous substances / wastes are transferred for disposal per this procedure, j

3.1.6 Hazardous wastes are classified for storage and mixing compatibility, 3.1.7 Control of an adequate area for the bulk storage of hazardous wastes is pravided and maintained.

3.2 MATERIALS SUPERINTENDENT The Materials Superintendent will ensure that l

3.2.1 Each hazardous chemical has the proper hazardous substance label affixed to it per purchase order.

3.2.2 All chemicals should remain in the original packing and containers while in the warehouse unless delivered in bulk transport trucks or unless label warnings are transfcrred to smaller quantities.

3.2.3 All chemicals stored in the hazardous substance /wasto storage area are handled in accordance with this procedure and Procedure 00262-C, " Control of Chemicals / Fluids".

3.2.4 Chemicals are not issued until it is on the chemical control list.

3.2.5 Hazardous substances are issued per this procedure and l

Procedure 00262-C, " Control Of Cacmicals/ Fluids".

3.2.6 Inside hazardous substance storage area temperature controls are regulateo to maintain temperatures specified for storage by the manufacturer or other approved temperatures as determined by the Industrial Hygienist.

3.2.7 Hazardous substance contarners are inspected upon receipt per Procedure 00850-c, " Materials Receiving And Inspection

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7 of 33 3.2.8 Control of an adequate arco for the bulk storage of hazardour, substances is provided and reaintained.

3.2.9 Hazardous substances storage areas are designated.

3.3 MANAGER PLANT T"AINING AND EMIRGENCT PREPAREDNESS I

The Manager Plant trsining and Emergency Preparedness l

will en6ure that plant eersonnel who handle, control, or are responsible for imzardous substances or hazardous wastes receives annual training as required by 40CFR.

3.4 CONTROLLED ISSUE AxEA PERSONNEL i

CIA personnel will ensures 3.4.1 All chemicals remain in the original packing and containers while under CIA persopuel control unless delivered in bulk transport truck or unleno itbel warnin[pt, are transferred to smaller quantitics, 3.4.2 Used harardous chemicals in the CIA are transferred to a Hazardous Waste $torage Area.

4.0 ORDERING OF HAZARDOUS SUBSTANCES 4.1 The individual requesting the chemical / fluid for use at VEOP will covrplete the applicable sections of the i

sup ply requisition per Procedure 00800*C, " Requisition Ofliaterials And Services".

4.2 The requester will ensure the requisition requests the i

manufacturer / supplier to state storage level temperature.

l 4.3 The individual will review the Controlled Chemical List i

I and note, if known, under the "Co::codity l

Number / Articles and Description" that the chemicul/ fluid tr. a " HAZARDOUS SUBSTANCE" and state

" MSDS REQUIREDi'i also state " PROPER HAZARDOUS SUBSTANCE l

LABEL MUST BE AFFIXED FOR EACH HAEARDOUS CHEMICAL".

4.4 The Supply Requisition will start to be processed per j

Procedure 00600-C, " Requisition of Materiale And

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8 of 33 4.5 If not classified as a herardous substance or a I

" Controlled Chemical", the requesting individual will transmit a request for clusiticatten to the Chemistry Superintendent for classification, vhile holding the requisition.

e.6 The Chemistry $uperintendent will request from the i

proposed vendor MSDS and tequest the required data and product label.

This utn be done by phone or a letter to the manufacturer.

4.7 Vhen received, the NSDS and product label will be l

transmitted to the Chemistry Superintendent.

4.8 The Chemistry Superintendent will disporition the MSDS l

nnd product label and send the requesting individual a letter of recommendation concerning the classification of the chemical / fluid.

If the vender fails to provide the information, the vendor shall not supply the chemical or substance.

4.9 The requesting individual will forward the requisition I

f the letter of recommendatice is available.

4.10 The supply requisition will continue to be processed 1

ger the applicable portions of Procedure 00800-C, Requifition Of Materials And Services",

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[ECEIVING OF HNZARDOUS Ss3 STANCES 5.1 When the chemical / fluid arrives on site, Materials Section per sonnel will r eceive the chemienl/ fluid per l

Procelure 00850-C, " Materials Receiving And Inspection" 5.2

'dazardous subacances received from cffsite b Materials Section personnel will be entered on the Nuc car Plant l

Management Information System (NPM15) as a hazardous substanca.

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6.0 STORING OF NEk' HAZARDOUS SUBSTANCES NOTE All excess, surplus, damaged, or contaminated hczardeus substances will be brought t

to the attention of the Chemistry Lab Supervisor.

The Laboratory personnel will facilitate the disposal of all such substances.

6.1 Upon acceptance, the chemical / fluid will be stored in the designated storage area.

Hazardous Chemicals will not be stored in areas that contain or expose safety-related equipment.

6.2 The Materials Section will advise the Chemistry l

Superir.tendent of the receipt.

6.3 The Chemistry Superintendent will assign an inspector to check that the shipment has been correctly stored as shown on an Environmental Inspection Report.

6.4 If any discrepancies exist, the Chemistry Superintendent s;11 notify the Materials Section to l

correct the situation.

6.5 Flammable and combustible materials will be stored in I

accordance with Section 10.0 of this procedure.

7.0 RAZARDOUS SUBSTANCE ISSUE TO CIA l

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<.1 Control Issue Personnel will withdraw chemicals / fluids l

from the warehouse as follows:

i 7.1.1 Ccmplete a " Materials / Equipment Request" per Procedure 00853-C, " Material Identification, Control, and Issue".

l 7.1.2 A copy of the MSDS may be obtained from the Chemistry Superintendent or Chemistry Senior Regulatory Specialist.

If the Chemistry Superintendent or Chemistry Senior Re gulatory Specialist is not available, such as backshifts or holidays, the Chemistry Duty Foreman will have access to the MSDS files.

MSDS files are located on the second floor of the Service Building in the Chemistry Support Group section.

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4 7.2 control Issue Personnel will log request for chemicals / fluids on the " Hazardous Substance Request r

Log" (Figure 1).

8.0 STORING OF HAZARDOUS WASTE MATERIAL I

S.1 Except in emergencies, the onsite transfer of hazardous waste shall not be performed in adverse weather conditions, and must be perfotued during daylight hours l

only.

8.2 No hazardous vaste may be stored at the VEGP Temporary Storage Area for a period of time longer than ninety (90) days, 8.3 Materials personnel will log all returned hazardoun i

substance / waste on the " Hazardous Substance / Waste Storage Log" (Figure 3).

8.4 Laboratory piirsonnel shall label per Subsection 8.9 and temporarily are the hazardous liquid waste in DOT 17C Open Head 55-gallon drums.

8.5 The liquid drums shall be ff.11ed only to within 2 inches of the top.

The remaining inches of air space are left for expansion of liquida.

t 8.6 Laboratory personnel will temporarily store hazardous solid or semi-solid waste in a DOT 17C Open Head

$5 ge11on drum.

8.7 Drums should be stored on wooden pallets.

8.8 The contones of each hazardous waste container must be identified and an appropriate label attached,.see Figure 2 and Toble i for applicable labels and codes.

The label shall contain the follov*mg informacion:

S.8.1 Generator's name and address:

Georgia Power Co.,.Vogtle Electric Generating Plant, Box 1600 Waynesboro, GA 30830 l

8.8.2 Generator's EPA I.D. Number:

CAD 094066321 8.8.3 EPA Waste I.D. Number:

.See Tab?e 1 8.8.4 Proper 007 Shipping Name:

See Table 1 8.8.5 DOT I.D. Number See Table 1 8.8.6 Accumulation Start Date:

The date filling of drum i

started.

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11 of 33 8.9 The following markings must be atenciled or printed on the top of each drum in 2 inch letters once they have started to be filled:

8.9.1 The Chemical Waste Management Alabata (CWMA) waste code:

See Table 2.

8,9.2 The word " Liquid" or " Solid", whichever is applicable.

8.9.3 The words "This End Up" or "This Side up" for drums containing liquids 8.10 The markings made in Subsection 8.9 must be:

Durable, in English, and printed on or affixed to the surface of the drum in the form of a label, tag, or sign.

The markings must sharply contrast with the background.

The markings must not be obscured by labels or attachments.

The markings must be located away from any other markings.

8.11 The side of each drum must bear the followin6 markings in 2 inch letters once it has started to be tilled:

8.11.1 Arrows showing drum orientation.(for 13 quids -

optional) 8.11.2 Generator's Name and Address:

Same as Sub-subsection 8.S.1.

8.11.3 Date of Content Classification:

Same as Sub-subsection 8.8.6 9.0

_ TRANSFERRING FOR DISPOSAL OF HAZARDOUS WASTE 9.1 The Hazardous Waste Manifest (Figure 4) shall be ccmpleted by tha Chemistry Senior Regulatory Specialist or Chemistry Supervisor and shall contain the following:

9.1.1 Manifest Document Number, 9.1.2 Generator Name:

Vogtle Electric Generating Plant.

9.1.3 Generator Address:

Same as Sub-subsection 8.9.1, 9.1.4 Generator Telephone Number:

404-724-1562, or 554-9961 X4135 9.1.5 Generator EPA Identification Number:

See subsection 8.8.2.

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12 of-33 3

e 9.1.6 The Name, Address, Phone Number, and Identification Number of the transoorter(s).

9.1.7 The Name, Address, Phone Number, and EPA Identification Number of the receiving facility.

9.1.8 A description of the waste that will include a.

Total number of containers, b.

Type of containers.

Proper shipping name of waste as shown on Table 1 c.

or 4.

d.

EPA Hazardous Waste ID Number, e.

DOT Identification Number preceded by "UN" or "NA" as appropriate.

See Table 2.

NOTE Hazard Class is not required when it is stated in the shipping name such as:

Flammable Liquid, Poison B, or Corrosive Liquid, f.

CWMA Wasce Code, g.

" Total Quantity" of each hazardous waste being

shipped, h.

If the proper name fer a hazardous waste is not included in Tables 1 or 2 and is a waste, then the word " WASTE" must precede-the name of the caterial.

10.0 CONTROL OF FLAMMABLE,AND COMBUSTIBLE LIQUIDS AND GASES 10.1 OUTDOOR STORAGE OF L1 QUIDS 10.1.1 Drum storage of ficmmable or combustible liquids must be located at least 75 feet from the nearest plant outdoor structure containing components necessary to assure safe shutdown.

The maximum number of drums per lot storable by class is as indicated in the following

table, e.

CLASS IA IB IC II IIIA Max. No.

of Drums 20 40 80 160 400 w..

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13 of 33 a

10,1.2 Multiple drum storage lots for flammable or ccmbustible liquids shall be separated by a minimum of 50 feet.

10.1.3 Where two or more classes of flammable or combustible liquids are stored in a single drum storage lot, the maximum number of drums in the drum storage lot shall be the maximum number for the highest individual class

( IA-highe s t ) represented in the lot.

10.1.4 Storage of Clasr IA liquids shall be sheltered from the direct rays of the sun.

10.1.5 Drums shall not be stacked.

10.1.6 Drum storage lots shall be provided with a surrounding curb at least 6 inches high or che lot shall be graded away from adjacent buildings and other exposures such that spills are diverted safely.

Curbed areas shall be provided with drains to relieve rain water.

Drains shall be terminated at a safe location which is accessible to operation under fire conditions.

10.1.7 A distance of 25 feet on any side of the drum storage lot shall be maintained comaletely free of grass, weeds, and foreign combustiiles.

10.1.8 Signs shall be posted and enforced such that there shall be no smoking or open flames within 25 feet of the Flammable and Combustible Liquid-drum storage lot.

10,1.9 Where flammable or combustible liquids are packaged together with ordinary combustibles, as in kits, the kit shall be stored on the basis of the most flammable or combustible commodity in the kit.

10 2 OUTDOOR RANDLING OF-LIQUIDS 10.2.1 Transfer of liquids between containers shall be done at a designated area at least 25 feet away from the drum storage lot and 75 feet from the nearest plant o

building.

The number.of drums allowed in this dispensing area shall be kept to a maximum of two.

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CAUTION Spring type clamps are not i

acceptable due to the possibility of the clamp slipping off of the container.

10.2.2 When transferring liquids in class IA, IB, or IC, the two containers shall be i; rounded and electrically connected to each other ay cables which are clatnped to each container by a bolt or screw clamp to reduce the possibility of static spark generation.

10.2.3 Transferring liquids by means of pressurizing the container with air is prohibited.

10.3 INDOOR STORAGE OF LIQUIDS 10.3.1 Flammable and/or combustible liquids shall NOT be stored within safety related areau of the plant.

10.3.2 Drum storage of Class IA, IB, or IC liquids is allowed ONLY in non-safety related plant build 2.ngs specifically I

designated " Flammable Liquid Storage Room".

10.3.3 Drum storage of Class II and IIIA liquids is allowed ONLY in the room referenced in Sub-subsection 10.3.2 or the Warehouse oil storage room.

10.3.4 Only original metal containers or specifically approved safety cans for use in handling flammable and i

combustible liquids may be used for storage purposes.

This includes the following liquid storage containers:

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DOT approved, b.

Underwriters Laboratories, Inc. (UL) approved, c.

Factory Mutual (FM) approved.

d.

Approved laboratory glass bottles for use in the laboratories only.

10.3.5 The following types of containers shall NOT be used for storage of flar::mable or combuscible liquids in plant buildings:

1 a.

Glass, b.

Plastic, c.

Other non-approved (non-safety).

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15 of 33 EXCEPT:

Liquids whose purity would be affected by a metal container Oh liquids which cause excessive corrosion of metal containers may be stored in glass containers of not more than one quart capacity.

Where required, glass containers must be stored in an approved metal cabinet.

Laboratory chemicals may be stored in one gallon glass containers.

10.3.6 If a total capacity of 25 gallons or more of flammable or combustible liquids which are not stored per Sub-subsection 10.3.2 need to be stored, they shall be stored in a metal cabinet specifically approved by UL or FM.

Each metal cabinet shall not contain more than 60 gallons of flammable or combustible liquids.

Of the 60 gallons, not more than 30 gallons shall be Class IA, IS, and/or IC.

'10.3,7 Not more than two metal cabinets specified in Sub-subsection 10.3s6 shall be located in any single fire zone.

10.3.8

'Each approved metal cabinet shall be labeled:

"FIJ M BLE - KEEP FIRE AWAY".

10.3.9 Flammable and combustible liquid storage cabinets shall not be used for storage of ANY OTHER MATERIAL except flammable or combur.tible li(uIda.

10.4 INDOOR-HANDLING OF LIQUIDS NOTE AEROSOL cans of 16 oz. or less are exempted.

10.4.1 F1-o2able or cocbustibia liquids snall be transferred frcm bulk _ supply containers into approved safety containers only by gravity through an approved self-closing UL and/or FM valve.

(Other previously approved mer.ns may be used as specified by the Fire Protection Engineer (FPE]).

10.4.2 All flammable and combustible liquids must be transported in an approved safety can (with flame arrester).

Under no circumstances shall the flame arrester-be removed from a safety can.

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EXCEPT:

Liquids whose purity would be affected by a metal container-OR liquids which cause excessive

-corrosion of metal containers may be stored in glass containers of not more than one quar: capacity.

Where required, glass containers must be stored in an approved metal cabinet.

Laboratory chemicals may be stored in one gallon glass containers.

10.4.3 Each flammable or combustible liquid container shall be conspicuously labeled to indicate the contents of the container.

The contents shall be icdicated by YELLOW letters on a RED background.

10.4.4 Closed areas where normal plant ven:ilation does not ventilate shall be provided with tenporary ventilation prior to using flammable or combusti>1e liquids in the area.

The temporary ventilation shall be provided to prevent accumulation of flammable or combustible vapors.

CAUTION Spring type clamps are not acceptable due to the possibility of the clamp slipping off of the container.

10.4.5 When transferring liquids in Class lA, IB, or IC, the two containers shall be grounded and electrically connected to each other by cables which are clamped to each container by a bolt or screw c'. amp to reduce the possibility of static spark generation.

10.4.6 During transfer operations, except is closed containers (closed loops), means shall be provided to control leaks or spills.

10.4.7 A Iransient Coiabustible Permit (Figure 1. Procedure 92015-C, " Control of Transient Combus tible s") shall be obtained for the movement of flammable or combustible liquida from, or into, safety related areas.

l 10.4.8 CLASS 1 Liquids shall not be used where there are open flames or other sources of ignition within the possible path of vapor travel.

10.4.9 Flammable and combustible liquids shall not be left unattended in any area of the plant, unless locked up.

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17 of 33 10.5 OUTUOOR AND INDOOR STORAGE OF GASES 10.5.1 Cylinders containing flammable and combustible gases shall not be permanently stored in areas that contain or expose safe shutdown equipment; normal storage shall be near the Maintenance Building and in the Gas Bottle Storage Room, 220' elevation, Level 1 of the Control Building.

For temporary storage of cylinders of compressed flammable and combustible gases, either near.its point of usage or otherwise, a Transient Combustible Permit (Figure 1, Procedure 92015-C,

" Control of Transient Combustibles") shall be obtained as necessary.

10.5.2 Cylinders containing oxidizing gases shall be separated from fuel gas cylinders or combustible materials (especially oil or grease) a minimum distance of 20 feet or by a barrier of noncombustible material at least 5 feet high having a fire resistance rating of at least 1/2 hour.

EXCEPTION:

This does not apply to welding units using MAPP or acetylene gas and oxygen or j

to laboratory equipment using multiple gases.

10.5.3 Cylinders containing compressed oxygen shall not be permanently stored in areas that contain or expose safe shutdown equipmenti normal storage shall be near the Maintenance Building.

10.5.4 Cylindets shall be physically restrained from falling by use of safety chains or equivalent restraints.

WARNING IF-A COMPRESSED-GAS CYLINDER VALVE ACCIDENTLY BREAKS OFF, N0ZZLE-REACTION WILL CAUSE THE CYLINDER TO MOVE VIOLENTLY AND ERRAf1CALLY.

10.5.5 Cylinders shall be stored with the valve closed, the protective cap securely in place, in the upright position, and with adequate ventilation.

10,5,6 Caution signs shall be placed at any entrance to the storage area warning of the dangers associated with flammable, combustible, and oxidizing gases.

i 10.5.7

~ Class IA, IB, and II gases shall be shielded from the direct rays of the sun.

• • JJ'

F20 EDURE No -

REvtSicN PAGE No.

• TGP 00260-C 5

18 of 33

-10.6 USE OF GASES 10.6.1 A Burn Permit (Fi Ignition Sources"gure 1, Procedure 92020-C, " Control Of

) shall be obtained-before using cylinders of compressed flammable or combustible gases or oxygen in burning or welding activities in an area containing flammable or combustible liquids or gases.

10.6.2 Cylinders of flammable or combustible compressed gases shall not be placed where they present a potential fire or explosion exposure to safety related cables or equipment, regardless of fire suppression provided in the area.

10.6.3 Non-ventilated, closed areas where flammable or combustible gases must be used shall be provided with temporary ventilation to prevent accumulation of explosive vapor mixtures.

10.6.4 Acetylene cylinders shall not be used when cylinder pressure falls below 35 psig.

10.6.5 Acetylene supply pressures in headers and hoses shall be maintained less than 15 psig.

11.0 HAZARDOUS WASTE DETERMINATION Hazardous materials or chemical prcducts that no longer have a commercial value and must be discarded or disposed of are subject to the-EPA Hazardous Was te Regulations.

To determine if a was:e material meets the definition of a hazardous _ waste, the generator (any_

f acility which disposes of a hazardous waste) must first_ determine if it is listed by name in Table 1.

If the hazardous waste is not listed by name, then the L

generator must determine (by chemical analysis) if it falls into ene of the following classifications:

l 11.1 IGNITABLE WASTE - (EPA NUMBER D001) l 11.1.1 Is a liquid that-has a flash point less than 60'C (140*F).

11.1.2 Is not a liquid but may cause fires by friction, absorption.of moisture, chemical change, or spontaneous chemical changes and when ignited burns so vigorously and persistently as to create a hazard.

11.1.3 Is_an ' ignitable compressed gas.

wn

~

PRoCCUAE Wo; REvistoM PAGE No.

VEGP 00260-C 5

19 of 33 e

11.1.4 Is an oxidizer that yields oxygen readily to stimulate the combustion of organic matter.

11,2 CORROSIVE WASTE - (EPA NUMBER D002) 11.2.1 Has a pH less than or equal to 2 or greater than or equal to 12.5.

11.2.2 Corrodes steel at a rate grearer than.250 inches per year at a test temperature of 55'C (131'F).

1 11.3 REACTIVE WASTES - (EPA NUMBER D003) 11.3.1 Is normally unstable and readily undergoes a violent chemical change without detonating.

11.3.2 Reacts violently with water.

11.3.3 Generates toxic gases, vapors, or fumes when mixed with water in quantities sufficient to present a danger to human' health or the environment.

11.'3.4 Is capable of detonation or explosive reaction if it is subjected to a strong initiating source or heated under continement.

11.3.5 It is a cyanide or sulfide bearing vaste which, when exposed to pH conditions between 2 and 12.5 can generate toxic gases,-vapors, or fumes in a quantity sufficient to present.a danger to human health or the environment.

12.0 REFERENCES

12.1 CODE OF FEDERAI. REGULATIONS 12.1.1 Title 40CFR, Part 260 12.1.2 Title 40CFR, Part-261 12.1.3 Title 49CFR, Part 172 12.1.4 Title 29CFR, Part 1926 12.1.5 Title 29CFR, Part 1910, OSHA Safety and Health Standards

'We t

-m

... ~....

-. -.. ~

'J P Acc I;U AE.No-92V!3 ON PAGE No

'TGP '.

.00260-C 5

20 of 33 12.2 Com)rehensive Environmental Response, Compensation, and

. Liability Act of 1980, Section 101 and 103 Public Law

.95-510,-December 11,-1980, 94 Stat. 2767.

'2.3

. Sections 3004 through 3008 of the Solid Waste Disposal-

-Act (as amended by the Resource Conservation and Recovery Act of 1976).

12.4-NFPA Standards Part 30, " Flammable and Combustible Liquids Code".

12.5 VEGP Hazard Communication Plan.

12.6

' PROCEDURES 12.6.1 00262-C,

" Control Of Chemicals / Fluids" 12.6.2 00800-C,

" Requisition Of Materials And Services" 12.6.3 00850-C,

" Materials Receiving And Inspection" 12.6.4 36205-C,

" Hazardous Waste Disposal" 12,6.5 920_15-C,

" Control of Transtent Combustibles" 12.6.6 92020-C,

" Control Of Ignition Sources" END OF PROCEDURE TEXT i

{

lL l

• 3w

.o, Proce&re Not Revlekm pqg VEGP.

00260-C 5

21.of 33

=_

llAZARDOUS WASTE IDENTIFICATION TABLE l-l EPA HA'I.

PROPER DOT HAZ. MAT'L.

DOT SHIPPING DOT LABEL PLACARD

• DESCRIPTION OR NAME WASTE t.O.

SHIPPING NAME

-DOT SHP. NO.

CI.ASSIFICATION REQUIRED REQUIRED 4-Aminopyridine P008 Waste UN2859 Poison B Poison Poison i

4-Aminopyridine Ammonium P008 Waste Ammonium UN2859 Poison B Poison Poison Metavanadate Metavanadate Potassium Cyanide P098 Waste Potassium UN1680 Poison B Poison Poison

-Cyanide Sodium Azide P105 Waste Sodium UN1687 Poison B Poison Poison Azide Crotonaldehyde U053 Waste UN1143 Flammable Flammable Flammable Crotonaldehyde liquid Dichlorodifluoro-UO75 Waste Dichloro-NA1956 Nonflamable Nonflam-Nonflam-l methane difluoromethane gas mable gas mable Gas 0-Toluidine U222 Waste UN1708 Poison B Poison Poison hydrochloride O-Toluidine hydrochloride Acetone U002 Waste Acetone UN1090 Flammable Flamable Flamable liquid liquid Formaldehyde U122 Waste UN2209 Combustible None Combust-Formaldehyde liquid ible Toluene U220 Waste Toluene UN1294 Flammable Flat::mable Flammable liquid liqutd Formic Acid U123 Waste Formic UN1779 Corrosive Corrosive Corrosive Acid Material a.

Prcredure No.

"b.t h Page No.

VEGP 00260-C 5

22 of 33

.IIAZARDOUS WASTE IDENTIFICATION TABLE 1 (CONT'D.)

EPA l!AZ.

PROPER DOT IIAZ. MAT ' L.

DOT SillPPING DOT LABEL ' PLACARD

• DESCRIPTION OR.NAME WASTE h0.

SilIPPING NAME DOT SHP. NO.

CLASSIFICATION REQUIRED REQUIRED Tetrachloroethene-U210 Waste UN1897 ORM-A None None Tetrachloroethene Methanol U154 Waste Methanol U1230 Flamable Flamable Flamable liquid liquid Cresylic Acid U054 Waste Cresylic U2022 Poison B Poison.

Poison Acid Ethyl Acetate U112 Waste Ethyl UNil73 Flamable Flamable Flamable Acetate liquid liquid Asbestos UOl3 Waste Asbestos None ORM-C None None Acrylic Acid U008 Waste Acrylic UN2218 Corrosive Corrosive Corrosive Acid Material Ethyl Ether Ull7 Waste Ethyl UNil55 Flamabl e Flamable F]amable Ether liquid liquid Methyl Ethyl Ketone U159 Weste Methyl UN1193 Flammable Flammablo Fl ama b l o Ethyl Ketone liquid liquid Phenol U188 Waste Phenol UN1671 Poison B Poison foison Mercury U151 Waste Mercury UN2025 Poison B Foison Poison Hydrazine U133 Waste Hydrazine UN2029 Flamable Flamable Flamable liquid liquid &

Poison 5 W %i0

~'

noce. no.

nus.on p.g.,e.

VEGP 00260-C 5

23 of 33 IIAZARDOUS.. WASTE IDENTIFICATION TABLE 1 (CONT'D.)

EPA HAZ.

PROPER DOT li AZ. MAT' L.

DOT SHIPPING DOT LABEL' PLACARD

• DESCRIPTION OR NAME WASTE NO.

SHIPPING NAME DOT SHP. NO.

CLASSIFICATION REQUIRED

' REQUIRED 7, 12-Dimethylamin - U093 7,

12-Dimethyl-osabezene

^ '

aminonzbezene n.o.i.b.n.

Methyl Chloro-U156 Waste Methyl UN1238 Flammable Flammable Flammable carbonate Chlorocarbonate liquid liquid &

Poison Methyl Chloroform U156 Waste Methyl UN2831 ORM-A None None Chloroform Hydrofluoric Acid U134 Waste Hydro-UN1790 Corrosive Corrosive Corrosive fluoric Acid Material Selenium Sulphide U205 Waste selenium NA2765 ORM-A None None Sulphide Silvex U205 Waste Silvex NA2765 ORM-A' None None 1, 2 Dichlorobenzene U070 Waste 1, UN1591 ORM-A None None 2 Dichloroben-Z t* fi t3 Creosote UO51 Waste Creosote NA1991 Combustible None Combust-liquid ible 1, 1, U226 Waste 1 1,

UN2831 ORM-A None None 1-Trichloroethane 1-Trichloro-ethane A etMs t

^

^

~

Procedurs No.

Ikvisbn Page No.

VEGP 00260-C

'S'.

24 of 33-HAZARDOUS: WASTE' IDENTIFICATION TAB'LE'1l(CONT'D.)-

^

. EPA HAZ...

PROPEREDOT.

- HAZ.. MAT'L..

DOT SHIPPING

. DOT-LABEL-PLACARD *-

DESCRIPTION OR NAME WASTE NO.

SHIPPING NAME DOT SHP. NO.

CLASSIFICATION : REQUIRED' 'REQUIKZD--

4 Degreasing:

<i Tetrachloroethy.-

F001 Waste-Solvent.

UN1702-ORM-A' None'

.None

.lene & Sludge N.O.S.

1 Trichloroethylene ;F001 Waste Solvent

'UN1710

'ORM-A-None None-5

& Sludge.

N.O.S.

LMethylene Chloride F001 Waste Solvent UN1593 ORM-A.

None None j

&. Sludge

' N.' O. S.

Spent Halogenated Solvents 1, 1, F002-Waste Solvent UN2831' ORM-A None

.None 1-Trichloroethane N.O.S.

& Sludge.

Chlorobenzene'&'

F002 Waste Solvent UN1134 Flamable Flammable Flammable' Sludge N.O.S.

liquid' liquid 0-Dichlorobenzene. F002 Waste Solvent UN1391 OMM-A None None

& Sludge

.N.O.S..

Trichlorofluoro-F002 Waste Solvent-UN1983 Non-'

Non-

' Chlorine.

methane &' Sludge N.O.S.

Flamable Flammable

. Gas

. Gas 4

I 5

i F

e l'

^^*

..2

Pmcedt:se No.

. flovtsion

~

. P y No.

VECP 00260-C 5

25 of 33 IIAZARDOUS WASTE IDENTIFICATION TABLE 1 (CONT'D.)

EPA IIAZ.

PROPER DOT HAZ. P.AT'L.

DOT SIIIPPING DOT LABEL PLACARD *-

DESCRIPTION OR NAME WASTE NO.

SilIPPING NAME DOT SilP. NO.

CLASSIFICATION REQUIRED REQUIRED Spent Non-lialogenated Solvents Recovered:

Xylene & Still F003 Waste Solvent UN1307 Flamable Flammable Flammable Bottoms N.O.S.

liquid liquid Acetone & Still F003 Waste Solvent UN1090 Flammable Flammable Flamable Bottoms N.O.S.

liquid

. liquid Ethyl Acetate &

F003 Waste Solvent UN1173 Flammable Flammable Flamable Still Bottoms N.O.S.

liquid liquid Ethyl Benzene &

F003 Waste Solvent UN1175 Flammable Flammable Flamable Still Bottoms N.O.S.

liquid liquid Ethyl Ether &

F003 Waste Solvent UN1155 Flamable Flacnable Flamable Still Bottoms N.O.S.

liquid liquid N-Butyl-Alcohol &

F003 Waste Solvent NA1120 Flamable Flammable Flammable S t.111 nottoma N.O.S.

liquid liquid Spent Non-Halogenated Solvents:

Cresols F004 Waste Solvent NA2076 Corrosive Corrosive Corrosive N.O.S.

Material Cresylic Acid F004 Waste Solvent UN2022 Poison B Poison Poison N.O.S.

Nitrobenzene F004 Waste Solvent UN1662 Poiscn B

. Poison Poison N.O.S.

I

i Procedure No.

Davision p,p pg VEGP

'00260-C 5

26 of 32

-11AZARDOUS : WASTE IDENTIFICATION TABLE 1 (CONT'D.)

EPA IIAZ.

PROPER DOT HAZ.. MAT'L.

DOT S111PPING DDT LABEL PLACARD

• DESCRIPTION OR NAME WASTE NO.

SiiIPPING NAME DOT SHP. NO.

C'LASSIFICATION REQUIRED REQUIRED Spent Non-

.t lialogenated Solvents:

[

Methanol F005 Waste Solvent UN1230 Flamable Flamable Flamable N.O.S.

liquid liquid Toluene F005 Waste Solvent UN1294 Flamable Flamable Flamable N.O.S.

liquid liquid Methyl Ethyl Ketone F005 Waste Solvent UN1193 Flamable Flamable F1smahle N.O.S.

liquid liquid Methyl Isobutyl F005 Waste Solvent UN1245 Flamable Flamable Flamable Ketone N.O.S.

liquid liquid Carbon Disulfide:

F005 Waste Solvent UNll31 Flamable Flamable Flamable N.O.S.

liquid liquid Isobutanol F005 Waste Solvent NA1120 Flamable Flamable Flamable N.O.S.

liquid liquid Pyridine F005 Wa s t. e Solvent UN1282 Fluernab le Flummable Fla nsnab l =4 N.O.S liquid liquid Carbon Disulphide P022 Waste Carbon UN1131 Flamable Flamable Flamable Disulphide liquid liquid t

Phosphonothioic Acid P097 Waste Phospho-NA2783 Poison B Poison Poison i

nothioic Acid I

na.,u

Prc edure No.

Ray 19on p,g, no, VEGP 00260-C 5

27 of 33 2

HAZARDOUS WASTE IDENTIFICATION TABLE 1 (CONT'D.)

EPA IIAZ.

PROPER DOT HAZ. MAT'L.

DOT SHIPPING DOT LABEL PLACARD

• DESCRIPTION OR NAME WASTE NO.

SilIPPING NAME DOT S!!P. NO.

CLASSIFICATION REQUIRED REQUIRED 0-dimethyl Ester P097 Waste 0-dimethy INA2783 Poison B Poison Poison Ester 0-ester With n P097 Waste 0-ester NA2783 Poison B Poison Poison With n N-dimethyl Benzene P097 Waste N-dimethyl NA2783 Poison B Poison Poison Sulfonamide Benzene Sulfonamide Phosphothioric P097 Waste Phospho-NA2783 Poison B Poison Poison

' Acid 0 thioric Acid 0 0-dimethyl P097 Waste 0-di-NA2783 Poison 3 Poison Poison (p-nitrophenyl) methyl ester (p-nitrophenyl) ester Sodium Cyanide P106 Waste Sodium UN1689 Poison B Poison Poison Cyanide

• If a vehicle has two or more types of hazardous waste and contains less than 5000 pounds, the placard indicating " Dangerous" may be used rather than two separate placards.

NOTE:

If a compound is not listed, contact the Chemistry Department, (primary contact Chemistry Senior Regulatory Specialist) for iurther instructions.

nma

--w

= * : e=

Procedure No.

fleviskm Pege Na VEGP 00260-C 5

28 of 33 TABLE 2 WASTE MATERIALS CURRENTLY AUTHORIZ8D FOR SHIPMENT TO CHEMICAL WASTE MANAGEMENT WASTE SHIPPING HAZARD DOT EPA HAZAPJ)OUS CWMA DOT LABEL PLACARD MATERIAL DESCRIPTION CLASS ID NO.

WASTE NO._

WASTE CODE REQUIRED REQUIRED Solvent Waste Flamable NA1993 D-001 MARA-39375 Flamable Flanunable Waste Flamable Liquid F-005 liquid (Flamable)

Liquid N.O.S.

Solvent Waste Combustible NA1993 D-001 MARA-39375 None None Waste Combustible F-001 (Combustible)

Liquid F-005 N.O.S.

liydraulic Waste Coa:bustible NA1270 None MARA-39540 None None and Motor Petroleum Liquid Oil Oil N.O.S.

Paint Waste Hazardous ORM-E NA9188 F-005 MARA-39333 Flamable Flaneable

. Waste Liquid D-001 liquid or Solid D-008*

Epoxy Resin Waste Resin Combustible UN2868 None MARA-39380 None None Solution Liquid

• Only used if material is lead based paint cm s

a

- s.

FAC;5:URE No AEVISloN PAGENo

• • EGP 00260-C.

5 29 of.33 r

TABLE 3 COMMONLY KNOWN FLAMMABLE AND COMBUSTIBLE LIQU_I_DS CLASS IA

- Ethyl Ether

- Methyl Ethyl Ether CLASS IB

- Acetone

- Toluol

- Denatured Alcohol

- Isopropyl Acetate

- Ethyl Alcohol

- Isopropyl Alcohol

- Gasoline Isopropyl Ether

- Oceane

- Me:ay1 Ethyl Ketone CLASS IC

- Ethyl Alcohol (50% and below)

- Hydrazine (Anhydrous)

- Styrene CLASS II

- Camphor Oil (light)

- Cleaning Solvent (140 class)

- Cleaning Solvent (Stoddard

- Mineral Spirits solvent)

- Fuel 011 1 & 2 CLASS IIIA

- Camphor

- Spindle Oil

- Cresote Oil

~

PAOCEUAE NO REVISION

' PAGE NO VEGP 00260-C 5

30 of 33 HAZARDOUS SUBSTANCE REQUEST LOG 6

4-($+6)=7 5

AMOUNT AMOUNT OF 1

1 2

3 4

AMOUNT OF USED SUBSTANCE REQUEST ISSUED HAZARDOUS QUANTITY 0F WASTE SUBSTANCE USED AND.

1 i

NUMBER TO SUB_ STANCE I ISSUED !RETURNEDiRETURNED NOT RETURNEI)

\\

1 I

i i

}

}

i FIGURE 1 (EXAMPLE)

I, L

PAC?!?UAE NO AEvlSiON PAGE NO

'[

'aGP 00260-C 5

31 of 33 i<

Hazardous Waste FEDERAL LAW PROHIBITS IMPROPER DISPOSAL

!! Found, Contset the Nurest Police, or Pubuc Safety Authodty, or the U.S. Environmental Protection Agency Proper 0.0,T. Shipping Name UN or NA #

0+wsw irwormenon Georgia Poww Company Accross City State Zlo EPAl.0, M EPA Waste h Accumutatkm Start Date Idamfest Document h HANDLE WITH CARE!

l,,

00:JTA: lS ltAZARDOUS OR T0XIC WASTES FIGURE 2 (EXAMPLE) 1

>:2m

- - - _ _ _ -__.__ _ __-__---_________-- _______ - -___-.____.-___ - __--_ -___ _-____-__-_---_________----________-___--- ~

rac:t:vaE NC p g,,,o VEGP 00260-C 32 of 33 4

HAZARDOUS SUBSTANCE / WASTE STORAGE LOG

~ QUANTITY NLMBER OF WASTE OF DRUM HAZARDOUS P.O.

RETURNED WASTE DRUM SUBSTANCE QUANTITY FROM 5

DEPOSITED START PRINT NAME/

P.O. NUMBER 1 WASTE

_ RECEIVED.0F FIG. 1 INTO DATE

-SIGNATURE i

l e

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m:

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PaOCEO.:E NO REVi$lON PAGE NO VE,P 00260-C 5

33 Of 33 F

9 AZARD0US WASTE MANIFEST (As Raouwed By The Alabama Depatrnent of Enworenental Management)

s. -. e see.,.ise air w ens ses nea, a.e. ww a

&i UNIFORM H AZAR DOUS

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WASTE MANIFEST

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Figure 4 (EXAMPLE) rems