ML19095B335

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W6H-IMC-2079-S-P-4

ML19095B335
Person / Time
Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
Shared Package
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References
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Text

• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2079\\W6H-IMC-207 Report Generated On : 5/1/2017 9:50:02 AM Sample Title : W6H-IMC-2079-S-P-4 Sample Description :

Sample Identification : 2079-S-P-4 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 2.823E+002 grams Sample Taken On : 3/17/2017 12:00:00 AM Acquisition Started : 3/31/2017 10:31:47 AM Live Time : 1800.0 seconds Real Time : 1800.3 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 3/24/2017 Efficiency Calibration Used Done On : 5/1/2017 Efficiency ID : H-IMC-2079-S-P-4

Peak Analysis Report 5/1/2017 9:50:03 AM Page 1

• • • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W6H-IMC-2079-S-P-4 Peak Analysis Performed on: 5/1/2017 9:49:59 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 249-259 253.25 63.52 0.45 2.36E+001 13.57 5.50E+001 M 2 295-313 300.05 75.23 0.75 7.35E+001 22.44 8.02E+001 m 3 295-313 308.44 77.33 0.76 5.21E+001 18.42 5.62E+001 F 4 738-749 742.53 185.91 1.14 5.77E+001 18.59 3.15E+001 F 5 947-958 952.59 238.46 0.99 5.84E+001 17.99 2.85E+001 F 6 1173-1182 1178.85 295.06 0.47 1.94E+001 10.61 1.90E+001 F 7 1399-1411 1405.67 351.79 0.87 3.88E+001 14.98 2.60E+001 F 8 5825-5850 5836.92 1460.26 2.60 1.66E+002 24.02 7.22E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/1/2017 9:50:03 AM Page 2

• • • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W6H-IMC-2079-S-P-4 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.950 1460.82* 10.66 1.03951E+001 1.74692E+000 Pb-212 0.992 74.82* 10.28 6.14753E-001 2.25028E-001 77.11* 17.10 2.56647E-001 1.04412E-001 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 1.56351E-001 5.41586E-002 300.09 3.30 PB-214 0.851 74.82* 5.80 1.08960E+000 4.10584E-001 77.11* 9.70 4.52440E-001 1.88519E-001 86.83 1.70 87.35 2.24 89.78 0.82 241.99 7.25 258.76 0.53 274.80 0.35 295.22* 18.42 1.51555E-001 8.62018E-002 351.93* 35.60 1.87975E-001 7.77284E-002 462.02 0.21 480.43 0.34 487.14 0.43 533.66 0.18 580.14 0.37 785.96 1.06 839.07 0.58 Ra-226 0.988 81.07 0.20 83.79 0.32 186.21* 3.64 1.49779E+000 5.45255E-001 TH-232 0.987 63.81* 0.26 9.14626E+000 5.63478E+000 TH-234 0.996 63.29* 3.70 6.50126E-001 4.18845E-001 92.38 2.13 92.80 2.10 112.81 0.21

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/1/2017 9:50:03 AM Page 3

• • • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.950 1.039508E+001 1.746918E+000 Pb-212 0.992 1.715279E-001 4.750186E-002 PB-214 0.851 1.813948E-001 5.526640E-002 Ra-226 0.988 1.497785E+000 5.452550E-001

? TH-232 0.987 9.146263E+000 5.634780E+000

? TH-234 0.996 6.501263E-001 4.188448E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

• • • • • • • • • • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 5/1/2017 9:49:59 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified.

Nuclide MDA Report 5/1/2017 9:50:03 AM Page 4

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W6H-IMC-2079-S-P-4 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 1.036E+000 1.04E+000 1.040E+001 4.334E-00 CO-60 1173.23 99.85 1.833E-001 1.58E-001 -2.092E-002 8.410E-00 1332.49 99.98 1.584E-001 -7.935E-003 7.078E-00 CS-137 661.66 85.10 1.530E-001 1.53E-001 6.113E-003 7.125E-00 Pb-210 46.54 4.25 2.134E+000 2.13E+000 1.924E+000 1.011E+00 BI-212 288.20 0.34 1.858E+001 2.12E+000 4.876E+000 8.726E+00 328.03 0.13 5.918E+001 -6.419E-001 2.786E+00 452.98 0.36 2.290E+001 -2.535E+000 1.061E+00 727.33 6.67 2.119E+000 1.601E+000 9.863E-00 785.37 1.10 1.134E+001 7.690E+000 5.193E+00 893.41 0.38 4.482E+001 1.033E+001 2.085E+00 952.12 0.17 8.942E+001 1.140E+001 4.103E+00 1078.62 0.56 3.037E+001 -3.028E+000 1.395E+00 1512.70 0.29 4.311E+001 8.452E+000 1.834E+00 1620.50 1.47 5.366E+000 -4.403E+000 2.009E+00

+ Pb-212 74.82* 10.28 3.712E-001 8.16E-002 6.148E-001 1.743E-00 77.11* 17.10 1.851E-001 2.566E-001 8.590E-00 86.83 2.07 2.301E+000 1.332E+000 1.099E+00 87.35 3.97 1.189E+000 1.682E-001 5.677E-00 89.78 1.46 2.846E+000 -3.168E+000 1.351E+00 115.18 0.60 5.876E+000 2.894E+000 2.766E+00 238.63* 43.60 8.161E-002 1.564E-001 3.718E-00 300.09 3.30 1.942E+000 -3.260E+000 9.112E-00 BI-214 76.86 0.55 1.147E+001 3.21E-001 -1.553E-001 5.525E+00 79.29 0.91 5.183E+000 -1.096E+000 2.468E+00 89.26 0.11 3.861E+001 1.062E+000 1.834E+00 89.81 0.21 1.979E+001 -2.202E+001 9.392E+00 273.80 0.13 4.592E+001 -3.075E+001 2.155E+00 348.92 0.10 8.142E+001 -4.148E+001 3.848E+00 386.78 0.29 2.781E+001 1.501E+001 1.303E+00 388.89 0.40 1.920E+001 -7.829E+000 8.954E+00 405.72 0.17 4.672E+001 4.156E+000 2.175E+00 454.79 0.29 2.908E+001 -6.910E+000 1.349E+00 469.77 0.13 6.709E+001 -5.645E+001 3.115E+00 609.32 45.49 3.207E-001 1.023E-001 1.513E-00 665.45 1.53 8.922E+000 3.103E+000 4.167E+00 703.11 0.47 2.988E+001 -1.157E+001 1.393E+00 719.87 0.39 3.165E+001 -2.104E+001 1.459E+00 752.85 0.13 1.264E+002 7.304E+001 5.926E+00 768.36 4.89 2.947E+000 -1.001E-001 1.368E+00 786.35 0.32 3.679E+001 -1.738E+000 1.675E+00 806.18 1.26 1.101E+001 -4.391E+000 5.081E+00

Nuclide MDA Report 5/1/2017 9:50:03 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram BI-214 821.18 0.16 8.709E+001 3.21E-001 -1.924E+001 4.014E+00 826.45 0.12 1.132E+002 -3.484E+001 5.189E+00 934.06 3.11 5.116E+000 7.007E-001 2.360E+00 964.08 0.37 4.965E+001 4.165E+001 2.309E+00 1051.96 0.31 5.633E+001 -1.451E+001 2.598E+00 1069.96 0.27 6.514E+001 -5.412E+000 3.002E+00 1120.29 14.92 1.373E+000 7.453E-001 6.380E-00 1133.66 0.25 6.476E+001 4.231E+001 2.948E+00 1155.21 1.63 1.025E+001 3.118E+000 4.674E+00 1207.68 0.45 4.227E+001 2.597E+000 1.943E+00 1238.11 5.83 3.475E+000 -1.100E+000 1.603E+00 1280.98 1.43 1.441E+001 9.371E+000 6.642E+00 1303.75 0.11 1.735E+002 6.516E+001 7.909E+00 1377.67 3.99 3.398E+000 -9.032E-001 1.483E+00 1385.31 0.79 1.669E+001 -8.904E+000 7.256E+00 1401.52 1.33 1.115E+001 1.886E-001 4.918E+00 1407.99 2.39 5.607E+000 -3.998E+000 2.438E+00 1509.21 2.13 6.292E+000 -1.812E+000 2.709E+00 1538.53 0.40 3.189E+001 5.860E+000 1.356E+00 1543.34 0.30 4.200E+001 1.659E+001 1.787E+00 1583.20 0.70 2.497E+001 6.786E+000 1.111E+00 1594.75 0.27 6.219E+001 4.073E+001 2.743E+00 1599.37 0.32 4.633E+001 -1.937E+001 2.014E+00 1661.27 1.05 1.394E+001 -8.589E-001 6.004E+00 1684.01 0.21 6.674E+001 4.786E+000 2.857E+00 1729.59 2.88 4.707E+000 -2.567E-001 1.988E+00 1764.49 15.30 1.190E+000 7.948E-001 5.250E-00 1838.36 0.35 3.533E+001 -4.365E+001 1.448E+00 1847.43 2.03 6.483E+000 1.777E+000 2.688E+00 1873.16 0.21 5.526E+001 -6.661E+000 2.233E+00 1896.05 0.15 8.551E+001 3.986E+001 3.505E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2293.38 0.31 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 6.579E-001 1.37E-001 1.090E+000 3.089E-00 77.11* 9.70 3.264E-001 4.524E-001 1.514E-00 86.83 1.70 2.801E+000 1.622E+000 1.338E+00 87.35 2.24 2.107E+000 2.982E-001 1.006E+00 89.78 0.82 5.067E+000 -5.640E+000 2.405E+00 241.99 7.25 9.713E-001 -1.979E-001 4.636E-00 258.76 0.53 1.159E+001 1.188E+000 5.473E+00 274.80 0.35 1.691E+001 5.281E-001 7.946E+00 295.22* 18.42 1.795E-001 1.516E-001 7.919E-00 351.93* 35.60 1.365E-001 1.880E-001 6.170E-00 462.02 0.21 4.269E+001 4.250E+000 1.988E+00 480.43 0.34 2.859E+001 2.488E+000 1.334E+00 487.14 0.43 2.214E+001 -5.486E+000 1.031E+00 533.66 0.18 5.803E+001 5.778E+000 2.702E+00 580.14 0.37 3.521E+001 -6.282E+000 1.654E+00 785.96 1.06 1.124E+001 -1.574E-001 5.126E+00

Nuclide MDA Report 5/1/2017 9:50:03 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 839.07 0.58 2.789E+001 1.37E-001 5.215E+000 1.298E+00

+ Ra-226 81.07 0.20 1.962E+001 8.28E-001 4.930E+000 9.246E+00 83.79 0.32 1.379E+001 6.080E+000 6.557E+00 186.21* 3.64 8.285E-001 1.498E+000 3.791E-00 AC-228 89.96 1.90 2.059E+017 6.14E+016 -2.291E+017 9.774E+01 93.35 3.10 1.222E+017 6.181E+016 5.793E+01 99.51 1.26 2.566E+017 1.717E+017 1.207E+01 104.82 0.39 8.108E+017 4.971E+017 3.808E+01 105.60 0.74 4.197E+017 8.624E+016 1.969E+01 108.58 0.28 1.075E+018 -2.869E+017 5.032E+01 129.07 2.42 1.397E+017 2.976E+016 6.578E+01 145.85 0.16 2.305E+018 7.208E+017 1.087E+01 153.98 0.72 5.108E+017 2.317E+017 2.406E+01 191.35 0.12 3.503E+018 1.175E+018 1.652E+01 199.41 0.31 1.377E+018 -2.165E+017 6.480E+01 204.03 0.11 4.009E+018 1.187E+018 1.889E+01 209.25 3.89 1.197E+017 -4.876E+016 5.646E+01 214.85 0.76 6.639E+017 -4.941E+016 3.141E+01 270.24 3.46 1.626E+017 1.219E+016 7.646E+01 278.95 0.16 3.441E+018 -8.643E+017 1.612E+01 321.65 0.23 2.939E+018 3.277E+017 1.381E+01 327.44 0.12 5.921E+018 -1.320E+018 2.791E+01 328.00 2.95 2.362E+017 -2.562E+015 1.112E+01 332.37 0.40 1.668E+018 -1.475E+018 7.822E+01 338.32 11.27 6.140E+016 1.870E+016 2.883E+01 340.96 0.37 1.902E+018 6.185E+017 8.932E+01 409.46 1.92 3.882E+017 -5.568E+017 1.807E+01 440.44 0.12 7.187E+018 3.961E+018 3.363E+01 463.00 4.40 1.971E+017 9.668E+016 9.188E+01 478.33 0.21 4.386E+018 3.163E+018 2.047E+01 503.82 0.18 4.889E+018 -4.278E+018 2.268E+01 508.96 0.45 2.622E+018 1.686E+018 1.239E+01 523.13 0.10 8.829E+018 6.580E+017 4.091E+01 546.47 0.20 4.967E+018 0.000E+000 2.310E+01 562.50 0.87 1.261E+018 -1.830E+017 5.894E+01 570.91 0.18 5.734E+018 0.000E+000 2.667E+01 572.14 0.15 7.079E+018 1.709E+018 3.296E+01 583.41 0.11 1.180E+019 1.283E+019 5.563E+01 674.75 2.10 6.081E+017 -3.240E+016 2.836E+01 701.75 0.17 7.935E+018 3.104E+018 3.710E+01 707.41 0.16 8.433E+018 3.537E+018 3.926E+01 726.86 0.62 2.147E+018 1.622E+018 9.990E+01 755.32 1.00 1.539E+018 5.326E+017 7.215E+01 772.29 1.49 8.297E+017 -3.286E+016 3.821E+01 782.14 0.49 2.246E+018 -7.312E+017 1.021E+01 794.95 4.25 2.987E+017 1.993E+016 1.376E+01 830.49 0.54 2.543E+018 4.490E+017 1.175E+01 835.71 1.61 9.408E+017 5.043E+017 4.378E+01 840.38 0.91 1.723E+018 9.120E+017 8.036E+01 904.20 0.77 2.046E+018 1.082E+017 9.498E+01 911.20 25.80 6.296E+016 2.089E+016 2.928E+01

Nuclide MDA Report 5/1/2017 9:50:03 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram AC-228 947.98 0.11 1.286E+019 6.14E+016 -1.331E+018 5.874E+01 958.61 0.28 5.311E+018 -1.566E+018 2.444E+01 964.77 4.99 3.232E+017 7.345E+016 1.497E+01 968.97 15.80 1.007E+017 8.054E+015 4.654E+01 1033.25 0.20 7.309E+018 -4.425E+018 3.340E+01 1065.18 0.13 1.183E+019 3.254E+018 5.423E+01 1095.68 0.13 1.396E+019 2.552E+018 6.464E+01 1110.61 0.28 6.107E+018 -8.269E+018 2.817E+01 1153.52 0.14 1.148E+019 2.406E+018 5.238E+01 1247.08 0.50 4.127E+018 9.624E+017 1.915E+01 1459.14 0.83 4.991E+018 1.254E+019 2.393E+01 1495.91 0.86 1.550E+018 5.650E+017 6.738E+01 1501.57 0.46 3.071E+018 8.183E+017 1.345E+01 1557.11 0.18 7.292E+018 -8.733E+017 3.139E+01 1580.53 0.60 2.463E+018 -1.106E+018 1.079E+01 1588.20 3.22 5.369E+017 3.392E+017 2.400E+01 1625.06 0.25 3.828E+018 -3.724E+018 1.547E+01 1630.63 1.51 9.529E+017 5.083E+017 4.142E+01 1638.28 0.47 3.330E+018 9.147E+017 1.464E+01 1666.52 0.18 8.001E+018 4.157E+018 3.463E+01 TH-230 67.67 0.38 1.291E+001 1.29E+001 6.366E+000 6.119E+00 PA-234 742.81 0.11 1.311E+002 2.12E+001 -5.493E+001 6.085E+00 766.42 0.32 4.824E+001 1.679E+001 2.250E+00 1001.03 0.84 2.118E+001 2.368E+000 9.813E+00

+ TH-234 63.29* 3.70 1.208E+000 1.21E+000 6.501E-001 5.665E-00 92.38 2.13 2.000E+000 1.590E+000 9.512E-00 92.80 2.10 1.941E+000 1.830E-001 9.212E-00 112.81 0.21 1.637E+001 5.744E+000 7.699E+00 U-234 53.20 0.12 4.806E+001 4.81E+001 1.916E+001 2.256E+00 120.90 0.04 9.471E+001 -7.614E+000 4.441E+00 U-235 72.70 0.12 4.499E+001 3.69E-001 -1.032E+001 2.150E+00 89.96 3.43 1.211E+000 -1.347E+000 5.746E-00 93.35 5.54 7.256E-001 3.671E-001 3.441E-00 104.82 0.69 4.900E+000 3.004E+000 2.301E+00 105.60 1.31 2.516E+000 5.171E-001 1.180E+00 108.58 0.50 6.389E+000 -1.705E+000 2.991E+00 109.19 1.66 1.887E+000 -9.973E-001 8.823E-00 140.76 0.20 1.912E+001 -7.396E+000 9.017E+00 143.76 10.96 3.693E-001 2.136E-001 1.747E-00 163.36 5.08 8.018E-001 1.660E-001 3.779E-00 182.62 0.39 1.334E+001 -1.510E+001 6.344E+00 194.94 0.63 7.442E+000 1.089E+000 3.510E+00 202.12 1.08 4.333E+000 9.347E-002 2.040E+00 205.32 5.02 9.594E-001 -2.878E-001 4.521E-00 221.39 0.12 4.309E+001 -1.156E+001 2.030E+00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

5/1/2017 9:50:03 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2079\\W6H-IMC-207 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 1.04E+001 16.805 Pb-212 74.8 6.15E-001 36.605 3.932[50.396] 4.64 -0.850 77.1 2.57E-001 40.683 1.641[53.432] [ 0.534]

238.6 ^ 1.56E-001 34.639 1.000[48.987]

PB-214 74.8 1.09E+000 37.682 5.796[55.945] 5.53 -0.969 77.1 4.52E-001 41.667 2.407[58.703] [ 0.412]

295.2 1.52E-001 56.878 0.806[70.321]

351.9 ^ 1.88E-001 41.350 1.000[58.478]

Ra-226 186.2 ^ 1.50E+000 36.404 TH-232 63.8 ^ 9.15E+000 61.607 TH-234 63.3 ^ 6.50E-001 64.425