ML19095B243

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Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W6H-IMC-0011-S-P-6
ML19095B243
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Site: 07000371
Issue date: 03/01/2018
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Download: ML19095B243 (8)
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          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0011\\W6H-IMC-001 Report Generated On : 3/10/2017 1:03:16 PM Sample Title : W6H-IMC-0011-S-P-6 Sample Description : UNC 2017 Sample Identification : IMC-0011-S-P-6 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 2.827E+002 GRAMS Sample Taken On : 2/28/2017 12:00:00 PM Acquisition Started : 3/10/2017 10:00:21 AM Live Time : 1800.0 seconds Real Time : 1800.7 seconds Dead Time : 0.04 %

Energy Calibration Used Done On : 3/9/2017 Efficiency Calibration Used Done On : 3/10/2017 Efficiency ID : H-IMC-0011-S-P-6

Peak Analysis Report 3/10/2017 1:03:16 PM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8381 Sample

Title:

W6H-IMC-0011-S-P-6 Peak Analysis Performed on: 3/10/2017 1:03:13 PM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 182-190 186.11 46.50 0.50 7.41E+001 19.87 4.28E+001 F 2 296-304 299.75 74.93 0.55 8.75E+001 21.33 4.05E+001 F 3 949-959 953.67 238.51 0.79 5.18E+001 18.02 4.13E+001 F 4 1403-1412 1406.94 351.89 0.80 3.33E+001 14.65 2.70E+001 F 5 5825-5848 5836.04 1459.81 2.04 1.74E+002 73.33 2.67E+001 F 6 7043-7060 7051.79 1763.93 1.83 1.99E+001 9.97 3.60E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 3/10/2017 1:03:16 PM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W6H-IMC-0011-S-P-6 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\GE UNC_b_112211.NLB

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/GRAM) Uncertainty PB-212 0.619 74.82* 10.28 6.75064E-001 2.17381E-001 77.11 17.10 87.35 3.97 238.63* 43.60 1.20540E-001 4.65409E-002 300.09 3.30 BI-214 0.214 609.32 45.49 665.45 1.53 768.36 4.89 806.18 1.26 934.22 3.17 1120.29 14.92 1155.60 1.66 1238.12 5.83 1280.98 1.43 1377.67 3.99 1401.52 1.33 1407.99 2.39 1509.21 2.13 1729.59 2.88 1764.49* 15.30 7.21023E-001 3.67064E-001 1847.43 2.03 PB-214 0.191 53.23 1.08 74.82* 5.80 1.19651E+000 3.93495E-001 77.11 9.70 87.09 3.41 241.99 7.25 295.22 18.42 351.93* 35.60 1.32490E-001 6.15216E-002 785.96 1.06

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 3/10/2017 1:03:16 PM Page 3

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/GRAM) Uncertainty PB-212 0.619 1.417296E-001 4.497730E-002 BI-214 0.214 7.210232E-001 3.670640E-001 PB-214 0.191 1.537948E-001 6.063924E-002

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 3/10/2017 1:03:13 PM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 1 46.50 4.1180E-002 26.81 F 5 1459.81 9.6551E-002 42.20 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 3/10/2017 1:03:16 PM Page 4

          • N U C L I D E M D A R E P O R T *****

Detector Name: 8381 Sample Geometry: cylinder Sample

Title:

W6H-IMC-0011-S-P-6 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\GE UNC_b_112211.NLB Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM K-40 1460.82 10.66 3.301E+000 3.30E+000 9.044E+000 1.590E+00 CO-60 1173.23 99.85 1.406E-001 1.38E-001 5.056E-002 6.487E-00 1332.49 99.98 1.378E-001 8.173E-002 6.289E-00 CS-137 661.66 85.10 1.223E-001 1.22E-001 1.835E-002 5.716E-00 BI-212 727.33 6.67 1.634E+000 1.63E+000 -3.453E-001 7.618E-00 785.37 1.10 1.135E+001 -1.312E-001 5.321E+00 1620.50 1.47 7.505E+000 1.778E+000 3.276E+00

+ PB-212 74.82* 10.28 3.121E-001 8.21E-002 6.751E-001 1.456E-00 77.11 17.10 2.393E-001 2.320E-001 1.135E-00 87.35 3.97 7.706E-001 -3.080E-001 3.604E-00 238.63* 43.60 8.209E-002 1.205E-001 3.790E-00 300.09 3.30 1.561E+000 -1.909E-001 7.301E-00

+ BI-214 609.32 45.49 2.467E-001 2.47E-001 1.839E-001 1.164E-00 665.45 1.53 6.779E+000 -2.172E+000 3.168E+00 768.36 4.89 2.525E+000 -1.239E+000 1.184E+00 806.18 1.26 1.042E+001 1.904E+000 4.895E+00 934.22 3.17 4.298E+000 -1.271E+000 2.006E+00 1120.29 14.92 9.709E-001 -2.280E-001 4.505E-00 1155.60 1.66 9.814E+000 6.840E+000 4.584E+00 1238.12 5.83 2.962E+000 1.838E+000 1.384E+00 1280.98 1.43 1.046E+001 3.226E+000 4.824E+00 1377.67 3.99 3.401E+000 5.700E-002 1.546E+00 1401.52 1.33 1.020E+001 -5.197E-001 4.631E+00 1407.99 2.39 5.687E+000 4.508E-001 2.582E+00 1509.21 2.13 5.959E+000 4.107E+000 2.669E+00 1729.59 2.88 4.652E+000 1.982E+000 2.069E+00 1764.49* 15.30 4.101E-001 7.210E-001 1.560E-00 1847.43 2.03 5.901E+000 -8.412E-001 2.565E+00

+ PB-214 53.23 1.08 3.415E+000 1.07E-001 1.686E+000 1.560E+00 74.82* 5.80 5.532E-001 1.197E+000 2.581E-00 77.11 9.70 4.219E-001 4.090E-001 2.001E-00 87.09 3.41 9.272E-001 -4.607E-001 4.346E-00 241.99 7.25 7.068E-001 0.000E+000 3.342E-00 295.22 18.42 3.192E-001 6.578E-002 1.507E-00 351.93* 35.60 1.069E-001 1.325E-001 4.807E-00 785.96 1.06 1.166E+001 -2.671E+000 5.462E+00 Ra-226 186.21 3.64 1.053E+000 1.05E+000 1.043E+000 4.948E-00 TH-228 240.80 3.97 1.523E+000 1.52E+000 4.121E-001 7.264E-00 TH-230 67.67 0.38 8.522E+000 8.52E+000 1.703E-001 3.954E+00 TH-232 129.07 2.45 8.743E-001 3.33E-001 -2.442E-002 3.975E-00 209.25 3.88 1.116E+000 -2.873E-001 5.259E-00 270.24 3.43 1.527E+000 1.134E+000 7.189E-00

Nuclide MDA Report 3/10/2017 1:03:16 PM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM TH-232 277.35 2.48 2.065E+000 3.33E-001 -1.957E+000 9.696E-00 327.99 3.06 1.844E+000 -3.301E-001 8.634E-00 338.32 11.30 5.606E-001 1.645E-001 2.639E-00 409.46 1.94 3.775E+000 7.954E-001 1.774E+00 463.01 4.44 1.669E+000 3.478E-001 7.791E-00 583.00 30.96 3.328E-001 1.408E-001 1.566E-00 755.32 1.01 1.056E+001 -2.097E+000 4.907E+00 772.29 1.50 8.995E+000 2.253E+000 4.240E+00 794.95 4.34 2.745E+000 -1.375E+000 1.281E+00 835.71 1.68 7.842E+000 4.531E+000 3.676E+00 860.30 4.32 3.026E+000 -6.704E-002 1.415E+00 911.21 26.60 5.574E-001 6.673E-002 2.621E-00 964.77 5.11 2.882E+000 7.289E-001 1.350E+00 968.97 16.20 8.833E-001 1.246E-001 4.130E-00 1588.21 3.27 4.044E+000 1.619E+000 1.811E+00 1630.63 1.60 6.119E+000 3.413E-001 2.620E+00 U-233 42.44 0.06 8.814E+001 8.81E+001 1.518E+000 3.996E+00 54.70 0.01 2.187E+002 -1.361E+002 9.854E+00 97.14 0.02 9.860E+001 -2.093E+001 4.495E+00 146.35 0.01 3.592E+002 3.960E+001 1.635E+00 164.51 0.01 3.669E+002 2.216E+002 1.672E+00 291.32 0.01 1.009E+003 -1.460E+003 4.733E+00 317.13 0.01 5.854E+002 -4.252E+002 2.728E+00 320.51 0.00 1.905E+003 1.413E+003 8.957E+00 U-234 53.20 0.12 2.987E+001 2.99E+001 1.475E+001 1.365E+00 120.90 0.04 6.065E+001 1.180E+000 2.793E+00 U-235 105.60 1.32 1.565E+000 6.82E-002 -1.063E-001 7.106E-00 109.16 1.54 1.497E+000 6.606E-001 6.868E-00 143.76 10.96 1.968E-001 -1.481E-001 8.925E-00 163.33 5.08 4.748E-001 -3.877E-002 2.164E-00 185.71 57.00 6.825E-002 7.665E-002 3.211E-00 202.11 1.08 3.269E+000 -2.015E+000 1.522E+00 205.31 5.01 7.931E-001 -1.720E-001 3.720E-00 U-238 63.29 3.70 1.108E+000 8.14E-001 8.624E-001 5.201E-00 92.60 4.23 8.136E-001 5.291E-001 3.839E-00 766.42 0.32 3.709E+001 -1.644E+000 1.735E+00 1001.03 0.84 1.585E+001 1.493E+000 7.360E+00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

3/10/2017 1:03:16 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0011\\W6H-IMC-001 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/GRAM) %Uncert* [uncert]

PB-212 74.8 6.75E-001 32.202 5.600[50.276] 8.13 -1.485 238.6 ^ 1.21E-001 38.610 1.000[54.603] [ 0.640]

BI-214 1764.5 7.21E-001 ******

PB-214 74.8 1.20E+000 32.887 9.031[56.901] 8.33 -1.421 351.9 ^ 1.32E-001 46.435 1.000[65.669] [ 0.561]

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