ML12355A096

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Letter Dated July 13, 2012, from Richard L Holm, University of Illinois, to John Hickman, NRC, Regarding University of Illinois Response and Clarification to Orise Report of Independent Confirmatory Survey
ML12355A096
Person / Time
Site: University of Illinois
Issue date: 07/13/2012
From: Holm R
University of Illinois
To: John Hickman
NRC/FSME
References
5173-SR-01-0
Download: ML12355A096 (66)


Text

UNIVERSITY OF ILLINOIS AT URBANA-CLANIPAIGN Department of Nuclear, Plasma Richard L. Holm and Radiological Engineering Reactor Administrator 21", [albot Labotator 217-333-7755 H4 South Wnght Street Urbana, IL 61801-243 r-holmwjllinoistjdu Docket No. 50-151 License No. R-115 July 13, 2012 John B. Hickman USNRC MS T-8F5 Washington, DC 20555

SUBJECT:

University of Illinois Response and Clarification to ORISE Report: DCN 5173-SR-01-0 Mr. Hickman, Please find enclosed the University of Illinois Response and Clarification to ORISE Report DCN 5173-SR-01-0.

If there are any further questions please do not hesitate to contact me.

I declare under penalty of perjury that the foregoing is true and correct. Executed on July 13, 2012.

Sincerely, Richard L. Holm Reactor Administrator C: James Stubbins, Dept Head, Nuclear Plasma and Radiological Engineering rc!rphý,,u 2 1 -1 11",

- tai 2 17 3 :11 2 00t,

University of Illinois Response and Clarification to ORISE Report:

"Independent Confirmatory Survey of the Nuclear Research Laboratory at the University of Illinois Urbana-Champaign, Illinois" June 2012, DCN 5173-SR-01-0 The following is a response to issues identified in the Summary section 9, pages 13 and 14 of DCN 5173-SR-01-0:

"9.

SUMMARY

At NRC's request, ORA U conducted confirmatory survey activities within the NRL at the University during the week of May 7, 2012. The survey activities included visual inspections!

assessments, surface activity measurements, and volumetric concrete sampling activities.

During the course of the confirmatory activities, ORA U noted several issues with the survey-for-release activities performed at the University. Issues included inconsistencies with: survey unit classifications were not designated according to MARSSIM guidance; survey instrument calibrations were not representative of the ROCs: calculations for instrumentation detection capabilities did not align with the release criteria discussed in the licensee's survey guidance documents; total surface activity measurements were in excess of the release criteria; and Co-60 and Eu-152 concentrations in the confirmatory concrete samples were above their respective guidelines. "

.survey unit classifications were not designated according to MARSSIM guidance:"

The building clearance surveys were a MARSSIM "style" survey. This was not a final status survey and hence was not meant to meet the guidance in MARSSIM. No class I survey was mentioned in the U of I Building Clearance Survey Guidance document because the bioshield (the only *class I" area) was covered by a separate document (UI RX Guidance for Release of Bioshield) which specified 100% scan of the interior concrete surface. (See Attachment 1)

" "survey instrument calibrations were not representative of the ROCs;,"

C-14 was suggested as a calibration source for our surface scan instruments instead of Tc-99. C-14 is listed as a Radionuclide of Concern (ROC) only with respect to the Derived Concentration Guidance Limits (DCGLs) for the soil. The default NRC DCGLs were adopted in the Decommissioning Plan wholesale. C-14 is identified in the Site Charactization Report (2005) only with respect to graphite and not general building contamination. C-14 was not considered to be present in any quantity to be a surface contamination problem in comparison with Co-60 and Cs-137. Smear surveys were analyzed in an LSC and no indication of C-14 was present. The Tc-99 check source is

much more representative of the decay energy levels for Co-60 and Cs-137.

S"calculations for instrumentation detection capabilities did not align with the release criteria discussed in the licensee's survey guidance documents;"

The survey sheets upon which ORISE made this statement were not the completed sheets.

I am unsure how this occurred. The final sheets have been provided and show the Scan MDC below the surface scan release criteria in all cases. (See Attachment 2)

"total surface activity measurements were in excess of the release criteria;"

Several areas were identified by ORISE as having surface activity above the release criteria. All areas identified by ORISE were remediated and resurveyed to be less than the release criteria. The survey sheets showing the remediated areas and survey points have been provided. (See Attachment 3)

-Co-60 and Eu-152 concentrations in the confirmatory concrete samples were above their respective guidelines. "

ORISE identified four locations from biased samples that showed activity above the release criteria for concrete rubble that are based on a resulting dose of I mrem/yr. These areas were remediated and resampled. Offsite analysis verified that the areas were now below the release criteria. (See Attachment 4)

UI Rx Guidance for Release of Bioshield

Prepared by:

Reviewed by:

Approved by:

Guidance for release of Bioshield April 9, 2012 Chris Higgins Radiation Safety Officer Scott LaBuy LVI Project Manager Rich Holm University of Illinois Project Manager

Guidance Release of the Lower Bioshield

==

Introduction:==

Once the upper bioshield and Bulk Shielding Tank (BST) walls are segmented and removed, LVI/ENERCON will begin removal of the internal components of the reactor tank and drain the remaining water from the tank. The result will be an empty aluminum tank about 12 feet deep surrounded by high density concrete more than 7 feet thick in some locations. The bioshield is only 3 feet think on the side of the BST and there is direct access to the tank interior through the two thermal columns and the various beam ports.

With the water gone, the tank interior will be surveyed using hand-held and long-reach survey instruments as deemed necessary to maintain radiation doses ALARA. It will then be removed in sections using appropriate metal cutting techniques to expose the concrete behind the tank wall. A Radiation Work Permit (RWP) will define the necessary radiation protection methods to be used during the tank removal task.

Purpose:

Radiological surveys will initially be performed to assess surface activity, assess the potential for volumetric activation, and to support the planning of work to maintain doses ALARA. Additional decontamination support surveys will be used to evaluate the progress of the removal of activated concrete. Once site health physics personnel believe that all activated concrete has been removed, additional surveys will be performed to confirm that there is a low probability for additional activated or contaminated concrete above the rerelease criteria provided in Table 2.4 of the Decommissioning Plan. This guidance provides the methods for conducting surveys these confirmation Surveys and collecting concrete final confirmation samples from the interior surface of the reactor bioshield.

Applicability:

The guidance below applies to the reactor bioshield concrete walls, concrete making up the base and floor of the bioshield, and the concrete walls and floor of the pipe chase tunnel located below the bioshield. It also applies to metal components embedded within the bioshield wall. These include steel rebar, shadow shields and the beam tubes. Components removed from the bioshield such as beam tubes or shadow shields will be surveyed and released or managed as radioactive waste in accordance with material and equipment free-release procedures.

Release Criteria:

Concrete:

The inner concrete surfaces of the bioshield must conform with the release criteria previously established for detectable surface contamination as well as the volumetric criteria provided in Table 2-4 of the Decommissioning Plan (shown below).

TABLE 2-4 RELEASE CRITERION TRITIUM IN CONCRETE RUBBLE 95'b Percentile Dose Associated Radionuclide (mrem/yr per pQi 1 mreu/yr Release Critical Scenario Criftd= 5!i/z)"

Tritium 1.1 E-03 9.1 E+02 Leajbae-indjjia

-Iron-55 1.5-&05 6.7E+04 PCocessing oocre*e Cobalt-60 2.OE+00 5.0E-0I1 Road building I Nickel-63 1.5E-05 6.7E+04 Processing conicrete I Buropium-152 8.IEI.

I E+O0 Road Building Notes:.

a - The associated release criteria is the invemsc of the 95P percentile dose.

As previously discussed in separate documents including the Decommissioning Plan and a subsequent procedure outlining surface contamination release criteria for clean waste to be released from the NRL, there will be no radioactivity associated with licensed activities measureable on any material released from the NRL as clean waste.

This includes portions of the bioshield that will remain in place for final "clean" building demolition. For concrete surface surveys, the measurable limit criteria equate to about 2,500 dprm/100 cm2 total beta/gamma, about 350 dpm/100 cmr2 removable beta/gamma, about 16 dpm/100 cm 2 removable alpha, and about 200 dpm/100 cm2 removable tritium (actual values are dependent on the daily background values).

Shadow Shields, etc.:

Surface contamination release criteria for clean waste to be released from the NRL will apply to shadow shields and other embedded items removed from the bioshield during demolition. There will be no radioactivity associated with licensed activities measureable on any piece of material released from the NRL as clean waste. For surface surveys, the criteria equates to about 2,500 dpm/1 00 cm2 total beta/gamma, about 350 dpm/100 cm2 removable beta/gamma, about 16 dpm/100 cm2 removable alpha, and about 200 dpm/1 00 cm 2 removable tritium (actual values are dependent on the daily background values).

Perquisites:

RWPs-wi llbe prepared for removal ofthe alumihnum reactor tank, concrete.'and Oembddedeitem removals (.interior demoliition),. and interior surveys :and concrete sampling. RWPs will describe proper personnel protective equipment (PPE),

engineering controls, and dose monitoring.

Personnel entering the interiorspace of the bioshield will wear appropriate fall protectionequipment and recovery harnesses if accessing the area from above. If personnel access is by way of the largetherrnal column openinhg fall prqtectiod Will not be necessary.

Calibrated instruments capable of measudrng totalanbd.removable betafgamma are available and maintained in accordance with. ENERCON 'procedures. The University's liquid s-cintillatioh counter (LSC) is available for measuring remoVable H-3 contamination samples.

Sample contaihers and sampling equzipmentare available'fot collecting concrete samples of:50 to100 grams.

Procedure:

1. Cjoncrete blocks removed from the top of the reador showed occasionai low-level surface.contamination onmthe'surface against.the tank wail. Therefore, once.

the alumiunum tank is removed, the initial step Will be to perform a surface

decontamination on thejnterior concrete surface. While initial surface
decontamination will not remove activated 'material, it should 'remove surface cohtamination -that could be transfer to other surfaces, equipment, or personnel.
2. LVI ýwill use 'a Brokk robotic tool withaifttached demolition hammers-to rubblize the

,bioshield from the inside.-oUt Periodically demolition will stop for removal of the corncrete rubble. Concrete rubble will be containerized fordisposal As LLRW.

3. At a point when itis believed that most of.the activated concrete has been
removed, surface surveys of the interior will be performe dto assess additional gross' or targeted decontamination/demolifion.

a, Perform a 100 %/ scan of the, interior concrete sUrface using 2-inch by 2-inch sodium iodide (2x2Nal) gamma scintillation detectors. These detectors will allow'for the delineation of additional areas activated, above the release criteria that wil! require additional targeted removals.

b.,Micro Shield indicates 'that concrete with ýconcentrations of C-0,or Eu-15 2. at the criteriavprovided. inr Table 2-4 of t]e Decommissioning Plan, will resulthin an increase of about 1000 counts per mhinutte (cdprm),onb the 2x2.Z Nal detector.
c. Activated concrete samplescollelted in. 2005 indicated that the Co-60,and Eu-1 52 concentrations were approximately equal (on average)., However, because m0re than". one half-ife.ofG o-60 has:passed since 2065:and"dnly about one--half of an Eu-I 52^ hallf4ife, has passed.the Co-60 concentrations are expected to be about one-half of the Eu-I52' co.ncentratibn.s.

d.. Activated: concrete samples. from 2005: indicpate that Fe-55 is aboutfhalfof the:Co-60 con.centration*.. Due to, the differences'in lthe half-liveS, Fe-55 in, activated 'concrete is expected to be about one-quarter of the Co-60 activity. Given that the Table 2-4 -release criterion for Fe-55 is 10,000 times, the;criteria fo*r-Co-60, 2,2 Nal surveys ihdicating that the Co-60 and Eu-I 52, concentrationsarebelow the Table 2-4 criteria, the surveys will also be indica~ive of the Fe-55 activity concrete being well below.-the Table, 2-4 criteria. The maximum F-55 concentiration rýeported in 13 samplesý was

522,+/-69 -pCi/g.,(decayed to about 100 pC,ilg today-and more than..500.

times.less than the Table-2-4 criterio.m,)

e, Activated cobnredtesample..s from 2005 indicate that Ni-,63 is not present'in measureable amounts,. Thirteen of 13 concretesam-ples analyzed for Ni-63 indýicated that concentrations are :less,than the.-detection imit which Was Jess than 5 pCilg or moretthan 1.000 times le.ss than'.the'Table.2-4 release criterion.

f, Targeted decontaminnation/demolition'may include removing rebar or other

  • embedded items or:concrete rubbilization.
4. Repeat surveys with,2x2, Nal detectors and targeted remoivals until no. areas of activation are idenitified.

5., Once the 2x2-Nal surveys. indicate that activated concrete.and activated embedded itemshave been removed, a detailed, survey will ýbe:perform"ed using, a MARSSIM-based grid system. Thb survey will include a.100% scan of the intJe'rior of the bioshieid and.direct. static measurementsusihg 2x2.Nal de.tectors andsurvey instruments sensitive to beta/garmma, radiation (iý.e., Geiger-Mueller, gas proportionali, r beta scintillationAdetectors). Static measurement oIcatiodns willbe determined using a random-start grid. Removable;contamination smears Will :also be taken at static measurement ioc.*ations fo.r total beta, and H,3 analysis.

6. AlI2x-Nal measurements should be, indistinguishable from backgroundand beta survey measutements..should, be below the surface contamination releas.e criteria discussed above,
  • 7. Additional biased measurements will be taken on exposed r#ebar. These

-measuremerits will be noted on the survey form.

8. Gammaarindbeta/gamma surveys, together with prior characterization data, are sufficient to demhonstrate:compliance, with the volumetric'release criteria in Table 2-4 criteria and the surface conrtamination criteria. Therefore, :concrete sampling

will be limited to 6 samples collected from six different direct measurement locations. Each sample will be analyzed by an off-site laboratory by gamma spectroscopy for gamma-emitting isotopes including Co-60 and Eu-1 52 and by liquid scintillation counting for H-3, Fe-55, and Ni-63. Minimum detectable concentrations should be less than 50% of the Co-60 and Eu-I 52 criteria and less than 10% of the H-3, Fe-55, and Ni-63 criteria.

9. An additional 2 rebar samples will be collected from two separate locations that received direct survey measurements. These samples will be analyzed as described above. However, H-3 analysis is not required.

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7q TELEDYNE BROWN ENGINEERING, INC.

A Tdedyne Ts*tMn Compan 2508 Quality Lane Knoxville, TN 37931-3133 865-690-6819 Chris Higgins Enercon 4490 Old William Penn Highway Murrysville, PA 15668 Report of Analysis/Certificate of Conformance 05/01/2012 LIMS #:

L49994 Project ID#:

EN005-3EREGUOI-12 Received:

04/10/2012 Delivery Date:

05/10/2012 P.O.#A PER RECEIPT Release #:

SDG#:

This is to certify that Teledyne Brown Engineering - Environmental Services located at 2508 Quality Lane, Knoxville, Tennessee, 37931, has analyzed, tested and documented samples, as received by the laboratory, as specified in the applicable purchase order.

This also certifies that requirements of applicable codes, standards and specifications have been fully met and that any quality assurance documentation which verified conformance to the purchase order is on file and may be examined upon request.

I hereby certify that the above statements are true and correct.

Keith Jeter (I

Operations Manager Cross Reference Table Client ID Laboratory ID Station ID (if applicable)

SS-RRF-001 L49994-1 SS-RRF-002 L49994-2 SS-RRF-003 I

A9994-3 I

-L49994_4 7

I SS-RRF-004 I

SS-RRF-00 SS-RRF-006 L49994-5 L49994-L49994-7 SS-RRF-008 L49994-8 Page I of 24

7Rlk TELEDYNE BROWN ENGINEERING, INC.

ATWn Twhnowgu Cowpany 2508 Quality Lane Knoxville, TN 37931-3133 865-690-6819 Cross Reference Table Client 1)

Laboratozy ID Station ID (if applicable)

SS-RRF-M0 L49994-9 SS-RRF-010 L,49994-10 SS-RRF-0 I L49994-11 SS-RRF-012 L49994-12 SS-RRF-013 IA9994-13 SS-RRF-014 L49994-144 SS-RRF-015 LA9994-15 SS-LAF-001 L49994-16 SS-RCF-001 L49994-17 SS-BCT-W L49994-18 SS-BCT-NW L49994-19 SS-BCT-NE L49994-20 SS-BCT-E L49994-21 SS-WTF-001 L49994-22 SS-NFT-001 L49994-23 SS-NFr-002 L49994-24 SS-RRF-007 (DUPLICATE)

L49994-25 UI-BS-001 L49994-26 UI-BS-002 L49994-27 UI-BS-003 1 L49994-28 LU-BS-004 A942 UTI-BS-005 LA9994-30 Ul-BS-006 L49994-31 Ul-BSR-001

]

A9994-32 UI-BSR-002 L49994-33 Method Reference Numbers Matrix Analysis Method Reference IS GAMMA EPA 901.1 SD GAMMA EPA 901.1 This report shall not be reproduced or distributed except in its entirety.

Page 2 of 24

Report of Analysis TEFh E DmwE Report 12 ofAnl i

BROWN ENGINEERING, INC.

05/01/12 10:44 A Tole" Tachnotlag Company L49994 Enercon ENOOS-3EREGUOI-12 Sample ID: SS-RRF-001 Collect Start: 04/05/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/10/2012

% Moisture:

LIMS Number LA9994-1 OPF Activity I Uncertainty Run Aliquot AlIiquot Reference Count Count Count Radionuclide SOP#

Cone 2 Sigma MDC Units Volume Units Date Date Time Units Flag Values H-3__-003 2.61E+00 g

1.91 gwet 104/30/121 20 M-

-- -F---I Sample ID: SS-RRF-002 Collect Start: 04/05/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/10/2012

% Moisture:

LIMS Number IA9994-2 Sop#

Activity Uncertainty 1 F Run:

Aliquot Aliquot T Reference Count Count Count Radionuclide Cone 2 Sigma MDC UNits Volume Units Date Date Time Units Flag Values FF5 06

<206E+01 pCi/g 2.014 7 wet 104/05/12 12:001 0/7/1211800 Sec U

No W-3 2003 21E+00 pCi/g

[

1.99 g wet 04/30/12-20 M

U 2013 41E501 pCi/g" 2.0147 gwet1 04/27/1 45 M

U Sample ID: SS-RRF003 Collect Start: 04/05/2012 12:00 Matrix:

Soil (S)

Station:

Coiled Stop:

Volume:

==

Description:==

Receive Date: 04/10/2012

% Moisture:

LIMS Number. LA9994-3

  1. Activityn UncertaintY2 1g Run Aliquot Aliquotu 1 Reference I Count [ Count Count Radionuclide Cone 2 Si MDC units Volume Units Date Date Time units Flag Values H-3 12003

. J i.94.*+ i pCi/g 2.57 g wet 04/30/12f 20 M- -T=

UT*

Sample ID: SS-RRF-004 Collect Start: 04/05/2012 12:00 Matrix:

Soil (5)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/10/2012

% Moisture:

LIMS Number:

L49994-4 LIMp NActivity n

Uncertainty its

ý Run Aliquot Aliquot Reference Count Count Count Radionuclide SOP#

Cone 2 Sigma MDC Units Volume Units Date Date Time Units Flag Values 1"-3

____....3 2.38E+00 pCi/g f

1 gwet 04/30/121 20 Flag Values U

=

Compound/Analyte not detected (< MDC) or less than 3 signma No = Peak not identified in gamma spectrum

+

=

Activity concentration exceeds MDC and 3 sigma; peak ideatified(gamma only)

Yes = Peak identified in gamma spectrum U

=

Compoud/Anslye not detected. Peak not identified, but forced activity concentration exceeds MDC and 3 sigma High

=

Activity concentration exceeds customer reporting value

        • Unless o n

tle anlytical mutts Spec

=

MDC exceeds customer technical specification are related only to the samples tested in the condition they L

=

Low recovery ae received by the laboratory.

If 1-ugh recovery tl

=

HightccocryMDC

- Minimum Detectable Concentration Bolded text indicates reportable value.

Page 3 of 24

Report of Analysis 05/01/12 10:44 L49994 Enercon EN005-3EREGUOI-12 TELEWYNE 7

BROWN ENGINEERING, INC.

ATOM" TI n~dWogiqSCOuIm.VY Chris Higgins Flag Values II Compound/Analyte not detected (< MDC) or les than 3 sigma

+

=

Activity concentration exceeds MDC and 3 sigma; peak identified(gamnm only)

U*

Compound/Analytc not detccted. Peak not identified, but forced activity concentration cxcccds MDC and 3 sigma High

=

Activity concentration exceeds customer reporting value Spec

=

MIX exceeds customer technical specification L

=

Low recovcry H

=

High recovery Bolded text indicates reportable value.

Page 4 of 24 No

= Peak not identified in gamma spectrum Yes a Peak identified in gamma spectrum

        • Unless oducrwisc noted, the analytical results mpoted are related only to the samples tested in the condition they we received by the laborat".

MDC - Minimum Detectable Concentration

Report of Analysis 05/01/12 10:44 L49994 Enercon EN005-3EREGUOI-12 TELEDYNE SBROWN ENGINEERING, INC.

A Tetpy Toduatss Cwumi Chris Higgins Sample ID: SS-RRF-008 Collect Start: 04/05/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/10/2012

% Moisture:

LIMS Number:

IA9994-8 RAntivty o

ne rtDainty 1

Run Aliquot Aliquot I Reference Count Count [VCount Radionuclide SOP#

Cs2 MDC Units Volume Units Date Date Time Units Flag Values

-3 L[203 2.55E+O 1,

pCi/g

[]

1.961 gwet I

F04/30/12 20 [ M..

Sample ID: SS-RRF-009 Collect Start: 04/05/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/10/2012

% Moisturc:

IJMS Number:

L49994-9 R

Activity Uncertainty F

Run Aliquot Aliquot I Reference Count Count Radlonuulide SO Cone 2 Sigm.

MIUnDC U#

Volume Units Date Date Time Units Flag Values V-3 2.06E+00 pCi/g 2.42 Vgwet 04/30/121 20

[

M I] UI i

[Z Y Sampl ID: SSRRF010O Collect Start: 04105/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/10/2012

% Moisture:

LIMS Number LA9994-10 RaP Activity Uncertainty Run Aliquot Aliquot Reference Count Count Count Come 2 Sigma MDC Units N

Volume Units Date Date Time Units Flag Values H-3 272003

[

2_27+0_

6 pCi/g t7 2

i gwt

0.

04/30/121 20 1 M Sample ID: SS-RRF-011 Collect Start: 04/05/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/10/2012

% Moisture:

LIMS Number:

LA9994-11 Activity Uncertainty Run Aliquot Aliquot Reference Count Count Count Radiouuclide SOP#

Conc 2 Sigma MDC Units 0 n Volume Units Date Date Time Units Flag Values H-3 2_<

_224E+00

_pCi/g

___22

_g w

04/30/121 20 J M__[

Flag Values U

=

Ccsnpmd/Anal)4e not detected (< MC) or less than 3 sigma

+

Activity conentration ceeds MDC and 3 sigma; peak identified(gamma only)

U*

CompoumdAnalyte not detcted. Peak not identified, but forced activity concentratio exceeds MDC and 3 sigma High

=

Activity concentration exceeds customer reporting value Spec

=

MDC exceeds customer technical specification L

=

Low recovey H

=

High recovery Bolded text indicates reportable value.

Page 5 of 24 No

ý Peak not identified in gamma spectrum Yes = Peak identified in gamma spectrum

        • Unless oenise noted, dhe malytical results reported are related only to the samples testd in the condition they arc received by the laboratoy.

MDC - Minimum Detectable Concentration

Report of Analysis 05/01/12 10:44 IA9994 Enercon Chris Higgins EN005-3EREGUOI-12 J k TELEDYNE BROWN ENGINEERING, INC.

AT

%dTetwmqie Coairy Sample ID: SS-RRF-012 Collect Start: 04/05/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/10/2012

% Moisture:

LLMS Number-L49994-12 1

Activity Uncertainty I 1

i Runi Aliquot Aliquot Reference Count Count Count RadionuclideSON Coic 2 Sigma MDC Units U

Volume Units Date Date Time Units Flag Values

-3

-2003

-]

1E+

pCi/g gwe

_04/30/12 20_

I I

U-J Sample iD: SS-RRF-013 Collect Start: 04/05/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/1012012

% Moisture:

LIMS Number.

IA9994-13 SOT Activity I Uncertainty 1 1

Run Aliquot Aliquot Reference Count Count Count Radionuclide Conc 2 Sigma MI#

Units Volume Units Date Date Time Units Flag Values FE-55 2006 2.46E+01 pCi/g 2.0017 gwet 04/05/12 12:00 04/30/12 600 Sec U-No tl-3 2003

<_2.57E+00 pCi/g 1.94 g wet 04/30/12 20 M

U Nj-63 2013 4.5E-01 pCi/g 2.0017 gwet 04/27/12 45 M

U Sample ID: SS-RRF-014 Collect Start: 04/05/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/1012012

%Moisture:

LIMS Number:

IA9994-14

~Activity UncrtInty Ru1 CountT on on Radionuclide SO#

Cone 2 Sga MDC Units Volunie Units DtDae Time uis FagVle H-3

]2003 2.30E+O0 pCi/g

]

2.17 4 gwet

[

_[

"10

[-"-M4/30/121

___-i

- MJ 2

Sample ID: SS-RRF-OIS Collect Start: 04/05/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume;

==

Description:==

Receive Date: 04/10/2012

% Moisture:

LIMS Number.

L49994-15 7

E --

-i _

i Radionuclide 1--3

]

Activity Uncertainty SOP#

Conc 2 Sigma MDC 2003j 1.96E+00 1i Run Aliquot Aliquot Units Volume Units pCi/g....-

2.55 g

Reference count count count Date Date Time Units Ftag Values L --L-Flag Values U

Compound/Analytc not detected (< MDC) or less than 3 sigma

+

Activity concentration exceeds MDC and 3 sigmna peak idcatified(ganuna only)

U*

=

Compound/Analyte not detected. Peak not identified, but forced activity concentration exceeds MDC and 3 sigma High Activity concentration exceeds customer reporting value Spec

=

MDC cxcceds customer technical specification L

=

Low recovery H

High recovery Bolded text indicates reportable value.

Page 6 of 24 No = Peak not identified in gamma spectrum Yes = Peak identified in gamma spectrum

        • Unless otherwise notel, the analytical results repoted aw related only to the samples tested in the condition they an received by the laboratory.

MDC - Minimum Detectable Concentration

Report of Analysis 05/01112'10:.44 IA9994.

-Enercon Chris Higgins EN005-3EREGUOP-I2I BROWNENGINEERING. INC.

A Teae1, dmaoe~Cse Samplýe D:ý SS-LAF-001 Collect Stait 0*,o152ol2 12:00 Matfix: Soil (S) 1 Station:l Collcct Stop:

Volume:

==

Description:==

v ReceiveDate: "0410/2012

% Moisture:

LIMSNumber: L49994-16 Actvty Uncertainty

~Runj Moiot. jAliquot' *Reference Count Co6unt.

Countr

-Radidfnudideý SOP#

Cone I 2 Si*

'AI M units 9f Volume Units' Date

'Date jTime

-Units I Flag Values 1

2.0030 1

i 2.00E+o0 pCi/g 2.5

'Og:,t 05101M12 20 M,

U BET A2007 A

3.09E-O1 pCi/g 208.67 q.ge 04105/12-12:00.

04/212f12.

6124-Sec V

PO K-40 2007 t7.4E+60*

8.85E01 1

pCilg 208.67 g,'t' I04/05/12'!2f00 04/12/12/

6124"

-Sec

+

Ye MN954 2007 3.97F,-02.

pCi/g 208.67 j giw-t W4905112 12:00 04/12/121 6124

.Sec U

No CO-.58 2007 3.00E-42, pCilg 208.67

  • gwd. 04105/12-12:00, 04f112]

6124 ISeC

.U No.

FE-59

".2007 803E.02 pCilg 208.67 1 gwct:

04/05/12,12:00 '0412A2 6124 Sec U.

No CO-60,

-2007 3.65E-02 pCi/g 208.67 J gwet 04/05/12 12:00 04/12/12]:

61242 See U

No

,N-65,

-2007 8.30E-022 pCi.g j

208.67 igwet 04/05/12 12:00 04112112-6124*:

.See:

U No ZR795 207 6.21E-02 pCi/g

_ j 20.8.67 g

04/05/12 12p00 N04/-12/2 6124

Sec, U

RU-.03 32007 3.32&02 pC-i/g j

2,8.67 g

04/05112 12:001 04/12/12 6124

'Sec U

No RU-106 2007 3.30EAI :

pOi/i 208.67

  • g wet 04/05[12 12:00 04/12/12[

6124 j Sec U iN 1431

.2007 5.64F-0 pCi/k 20817 g~wet-10/5/2201411162 Sec U

Nol CS-134 200

2.

pCilg L

208.67

,g-wet 04/05(12 12'-00 04/121121

-6124.

Sec.

U 0N

ý1.J37 1,2007

<13.7.4E-02 pCi/

j 298.67 g~wet N 405/12 12:00104/12/126'4,1Sec, V

~ NO 13A-140' i 2007 l70-I pCi/g

__j208.67 gwet 04/05/12-12.00 [04/12/2 12 Sec

-U jNo.

CE.441 J 2007 4E:02 P

208.67.

g wet7 104105/12.12:00 04.1212 6124 "Sec U

N CIE-w1 2007

<l.99E.01 pCilg f

208:67 get.

04/05/1212:00 04.12I 6124;t.

Sec U

No WS-152-2007 8.77E-02.

pCi/g 208.67 g.Nyq 04105/12 12:00 W1O 2 /l 6124 Sec N.-

o S-.2261 12007 0<

6.6,-04",,

pCi/g 208.67 gwet 04/05/12.12:00 04/12/12.

6124.

Sec U

t es.

W-228.

2007 5,

025&02_". pCi/g 208.67 g.Wd W04/12: 12:00 04/12i1 t6124 Sec T-3,I1 2007 I<O 5_

02 i pCi/g

[

.20867 g.wet 04/05/12 12:00 04/12/12 6124 Sec T Ues U-235

-2007 2.;16EA, ]I pCiig

[

208:67 gwet 04105/1241200 04/12/12 6124 Sec' UNo U-238.

-2007 4<S E_-_,+00 I

pCi/g 1

208.67.

gct

.04105/12 12:00

'04/l212Uj 6124 1Sec j U j No flýg Values-U Co*poundiAnalyte not detected (< MDC) or less than-3.sigma.

+

Actvit*yoneenraiocxeeedMDC and3 sigma; peak idintried(gaumna only).

U Crf-ohind/AnaIlenot detetd. Peaknotidwntifled bid forced ativityconcentratin exceeds MDC arid 3sigma, high-Activity concentrml*on exceeds customerreporting valu.

Spec, AMDC iceds customer telnil specification L

Lo6wrecovery H

-=

tigh:rcovery Boldedtext indicates reportable'value.

Page? o.024 N1o =lPaknot idcnil~d iigarnsa~speefur Yes =Peak identified in gamma spectrum Onless 6tberwise ntited the anai)licalresylts reported*

are related only tothe samples-tested in the conditio Ithey

-Are received by the laboratiny..

MDiC-Minimum DetetableCOncetr-alion

Report of Analysis 05/01/12 10:44 L49994 AM TELEDYNE BROWN ENGINEERING, INC.

AT*Wdpw Tedwiolope Compeav Enercon Chris Higgins EN005-3EREGUOI-12 Sample ID: SS-RCF-O01 Collect Start: 04/05/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/10/2012

% Moisture:

LIMS Number.

IA9994-17 Radionuclide 7-3

-ý k FE-59 RU-103 RFU-4 tS-1_34 CE-lU4 VU-152 --

RA-226 U-2F35-SOP#

Activity Uncertainty Conc 2 Sigma 2003 2007 2007 6.4E+00 1.041+0 2007 20071 2007 2007 201 V7 2007 2007 2007 2007 2~007 2007 2007 2.70E-OI 7.255E-02 2007 3.55E-01 I.24E-01 MDC 1.94E+00 4.32F,01 Units pCLg pCi/g Ran Aliquot N

Volume 2.58 Aliquot Units g wet g wt Reference Date Count Date 05101112 04/U112 04/05/12 12:00 5.70E-02 4.68F-02 1i.21E-01

_i.iE_-02 i.SSE-42 9AO0E-02 1101g pCi/g

_pCi/g pCi/g pCi/g pCi/g pCi/g 199.99 199.99 199.99 199.99 199.99 199.99 199.99 199.99 199.99 g wet g wet g wet g wet g wet g wet g wet g wet g wet 04/05/12 12:00 04/05/12 12:00 04/05/12 12:00 04M05/12 12:00 04/05/12 12:00 04/05/12 12:00 04/05/12 12:00 04/12/12 04/12/12 04/12/12 04/12/12 04/12/12 04/12/12 04/12/1 j Count Time 20 60O E6000 6000 6O000 6000 6OO 6O000 4.70F,02 4.63E-01 8.46"~O 4.99F,2 4.7F) 2.23FeOl 7.23F,-02 2.79"1-l IM3E-01 IIJ4E-+00 2.79E.-01

_6.2E+00_

pCilg pCi/g 04/05/12 12:00 04/12112 04/05/12 12:00 04/12/12 i

i pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

_pCi/g PCI/g __

pCi/g 199.99 g wet 199.99 gwet 04/05/12 12:00 04/05/12 12:00 04/I 06411 199.99 1

gwet 04/05/12 12:00 04/1 199.99 g wct 04/05/12 12:00 04/I 199.99 g wet 04/05/12 12:00 04/1 199.99 g wet 04/05/12 12:00 04/1 199.99 g wet 04/05112 12:00 04/1 199.99 g wet 04/05/12 12:00 04/1 199.99 gwet 04/05/12 12:00 04/I 199.99 g wet 04/05/12 12:00 04/I 199.99 gwet 04/05/12 12.00 04/I 1999.99 gwet 04/05/12 12:00 04/1 12/12 2/12 12/12

.2/12

.2/12 2/12 2/12

.2/12 12/12 2/12 6000 6000 6000 6000 6000 6000 6000 6000 6000 6000 6000 6000 6000 6000 Count Units Flag Values s* -UNo Sec

+

Yes Sec U

NO Sec U

No Sc U

No Sec U

No Sec U

Sec U

No Sec U

No Sec U

No Sec U

No Sec U

No Sec U

No Sec U

No Sec U

No Sec U

No Sec U

No Sec U

Yes Sec

[

Yes Sec] +

Yes F-Flag Values U

=

Compound/Analyte not detected (< MDC) or less than 3 sigma

+

Activity concentration exeeds MDC and 3 sigma; peak ideatified(gamma only)

U*=

Conpmmod/Analyte not detected. Peak not identified, but forced activity concen*ration exceeds MDC and 3 sigma Iligh Activity concentration exceeds customer reporting value Spec

=

MDC exceds customer technical specification L

Low recovay II High recovery Bolded text Indicates reportable value.

Page8 of 24 No = Peak not identified in gamma spectrum Yes = Peak identified in gamma spectrum

        • Unless otherwise noted, the analytical results reported are related only to the uamples tested in the condition they are received by the laboratory.

MDC - Minimum Detectable Concentration

Report of Analysis 05/01/12 10:44 L49994 Enercon EN005-3ERFGUOI-12

,P11h TELEDYNE BROWN ENGINEERING, INC.

ATvId*aeT-chamqtesCmpany Chris Higgins Sample ID: SS-BCT-W Collect Start: 04/05/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/10/2012

% Moisture:

LIMS Number.

LA9994-1 8 Radionudide H-3 BiE-7 K-40___

WN-54

,"E-59 cX-60 ZN-65 zic-9 RU-103 RU-106 1-131 CS-134 CS-137 BA-140 CE-141I CE-144 EU-152 RA-226 Th-228 rH-232 U-235 SOP#

2003 2007 2007 2007 2YO07 2007 2007 2007 2007 2007 2007 2007 2007 2007 2007 2007 2007 2007 2007 2007

2007 2007 RO0 Activity Conc

&.77E+00 2.539-Ol 2.42F-01 Uncertainity 2 Sigma 9.82E-01 MDC 2.61E+00 4.4rE0 1.07F,01 6.61E-02 1.OSE-01 Units pCi/g pCi/g pCi/g pCi/g pCi/g pC/g pCi/g pcilg

-pCi/g pCi/g pCi/g pCi/g 7.90E-02 6.06F,02l

_2.51E-01 8.1 ZE-2 3.20E-01 1.2,7E-I 1.02E+00 6.55F-02 I.09B-01 3.04F,01 5

+000 Run Aliquot Aliquot Reference Count Volume Units Date Date 1.91 gwet 05/01/12 188.17 gwet--d 405/12 12:00 04/12/12 188.17 gwet 04/05/12 12:00 04/12/12 188.17 g wet 04/05/12 12:00 04/12/12 188.17 g wet 04/05/12 12-0'04/12/12 188.17 gwet 04/05/12 12:00 04/12/12 188.17 1 gwet 04/05/12 12:00 04/12/12 188.17 gwct 04/05/12 12:00 04/12/12 188.17 g wet 04/05/12 12:00 04/12/12 188.17 gwet 04/05/1212:00 04/12/12 188.17 gwet 04/05/12 12:00 04/12/12 188.17 g wet 04/05/12 12:00 04/12/12 188.17 gwct 04/05/12 12:00 04/12/12 188.17 gwet 04/05/12 12:00 04/12/12 188.17 g wet 04/05/12 12:00 04/12/12 188.17 g wet 04/05/12 12:00 04/12/12 188.17 gwct 04/05/12 12:00 04/12/12 188.17 gwet 04/05/12 12:00 04/12/12 188.17 gwct-04/05/12 12:00 04/12/12 188.17 g wet 04/05/12 12:00 04/12/12 188.17 g wet 04/05/12 12:00 04/12/12 188.17 gwet 04/05/12 12:00 04112/12 188.17 gWt 04/05/12 12:00 04/1I/V2 Count Time 20 6000 6000 6000 6000 6000 6000 6000 pCi/g pCi/g PCi/g pCi/g pCi/g pCi/g pCi/g pCi./g pCi/g 6000 6000 6000 6000 6000 6000 6Ow0 6000 6000 (6000 6000 6000 6000 6000 Count Units Flag Values M

U Sec U

No Sc

+

Yes SecU No Sec i

N Sec U

Scc U

No Sec U

No Sec U

No Sec U

No Sec U

No Scc U

No Sec U

No Sec U

No Sm-U No Scc U

No Sec U

No Sec U-Yes Sec

+

Yes Sec

+

Yes Scc U

No SecI No I J Flag Values U

=

Compound/Analyte at detected (< MD* or less tlum 3 sigma

+

=

Activity concentration exceeds MDC ad 3 sigma; pcok identifiefdamnma only)

U*

Compound/Analyte not detected. Peak not identified, but forced activity concentration exceeds MDC mad 3 sigma High

=

Activity conicntratio exceeds customer reporting value Spec

=

MDC exceeds customer technical specifiwation L

=

Low recoveay H

=

High recovery Bolded text indicates reportable value.

Page 9 of 24 No

= Peak not identified in gamnma spectrun Yes Pedak idatirwd in gamma spectrum

        • Unes otherwise noted, the malytical results reporied we related only to the samples tested in the condition they am received by the labotmtoy.

MDC - Minimum Detectable Concentration

Report of Analysis 05/01/12 10:44 L49994 Enercon Chris Higgins EN005-3EREGUOI-12 IftL TELEDYNE BROWN ENGINEERING, INC.

A TVlme Tschneo4oes Coany Sample ID: SS-BCT-NW Collect Start: 04/05/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/10/2012

% Moisture:

LIMS Number:

L49994-19

-- 7T

~.

t

~.

7 T

Radionudide H-3 SOP#

Activity Conc Uncertainty 2 Sigma Run N

MDCI Units pCi/g Aliquot Volume Aliquot Units Reference Count Count Count Date Date Time Units Flag Values

~T20031 1

2.26E+00 32IKO 2.21 BE-7 K-40 MN-5 CO-58 FE-59 CO-60 b4-65 2007 2007 2007 2007 6.01K+00 pCi/g pCi/g 189.44 189.44 g wet g wet g wet 04/05112 12:00 04/05/12 12:00 04/05112 12:00 05/01/12 04/12/12 04112/12 04112/12 20 6000 6000 60O0 M

Sec Sec Sec U

+

U 1.00E+00 No Yes No 4.15E.02 pCig 189.44 19.44 g wet 4.OOE-02 pCi/g g wet F

4-

-4 F

4 4

4..Z

~04/05/12 12:00 04/12/12 04/05/112 12:00 04112/12 60001 Sec LU No 2007 2007 4W07 9.40E.-02 5.05E-02 8.43E-02 939F-02 pCi/g pCi/g

-pell/

189.44 g wet 6000 Sec IU 189.44 g wet 104/05/12 12:00 04112/121 6000 Se U

189.44 4

4

-l I-ZR-95 2007 pCi/g 189.44 g wet 04/05112 12:00 gwet 104/05/12 12:00 gwet 04/05/12 12:00 04/12/12 04112/12 6000 6000 Sec Sec Sec U

U No No No No No RU-103 RU-106 CS-134 2007 2007 4.2 1E102 pCi/g pCi/g 189.44 3.47E-01 189.44 I

- g wet 04/05112 12:00 gwet 04/05/12 12:00 04/12/12 04/12/12 04/12/12 6000 6000 6000 2007 2007 7.25E-02 pCi/g pCi/9 A

F

+

189.44 Sec Scc Sec Sec U

U U

U 4.19E-02 A

I-

-+

189.44 189.44 gwet 04/05/12 12:00 g wet 04/05/12 12:00 CS-137 BA-140 CE-141 CE-144

EU-152 2007 2007

~20O7 2007 2 0-7 5.28E-02 pC0g 04112/12 04/12/12 04/12/12 6000 6000 No No No No 2.OOE-01 5.66E-02 pCi/g pCi/g 2.27E-01 1.09E-01 pCi/g pCi/g pdi/g pCi/g iRA-226 1TI1-228 2007 2007 9.07E-01 2-SOE-01 2.76E-O 5.7213-01 5.61E-02 9.771B-02 189.44 189.44 189.44 189.44

-189.44 189.44 189.44 189.44 189.44 g wet 04/05/12 12:00 g-- et 04/05/12 12:00 g wet 04/05/12 12:00 g net 04/05/12 12:00 F-A F

+zzr-F 4~

04/12/12 04/12/12 6000 Sec U

TH-232 1J.-235 Uf-238 2007 2007 2007 pCi/g g wet 04/05/12 12:00 g wet 04/05/12 12:00 g wet 04/05/12 12:00 g wet

04/05/12 12:00 g wet 104/05/12 12:00 04/12/12 04/12/12 04112/12 6000

_6000_

6000 6000 6000

~6000 No No 04112/121 6000 Sec I U Sec U

No Sec Sec Sec Sec Sec Sec U

+

+

+

U No Yes Yes Yes No No 2.39E-01 pCi/g pCi/g 04112/12 04/12/12

".52+00 Flag Values U

=

Compound/Analyte not detected (< MDC) or less than 3 sigma

+

=

Activity concentration cxceeds MDC and 3 sigma, peak idenlifled(gamma only)

U*

=

Compound/Anhlyte not detected. Peak not identified, but forced activity concentration exceeds MDC and 3 sigma High Activity concentration exceeds customer reporting value Spec

=

MWC exceeds customer technical specification L

Low recovery H

=

High recovery Bolded text indicates reportable value.

Page 10 of 24 No = Peak not identified in gamma spectrmn Yes = Peak identified in gamma spectnrm

        • Unless otherwise noted, the analytical results reported ae related only to the samples tested in the condition they we received by the laboratory.

MDC - Minimum Detectable Concentration

Report of Analysis 05101112 10:44:

L4999.4

Enercon.

ENOO5-3EREGIJL142 TELEDYNE 71 BROWN ENGINEERING 'INC.

'ATeled*a Tnhwhngls Conanp Chris Higgins Sa4m

SS-BCT-NES Collect Staxt:.04105/201212:00 Mgd: Si (S)
  • Staon:
Co~llct Stop:

Volume:.

==

Description:==

Receive Date:- 04/tq101201 osue LIMS Number: 1A999-20 1 Activity Uncetainty 1

Aliquot

-Reference Count Count-Count Radioqnuclideý Sol?

Cone ZSigrna MDC. j Units 0

Volume Units

-Date Date jTime.

Units [

FlagVaes FE-55-20 2.19E-i01.

pCikg 2.0025

.gWet-04105112:12-00' 04/30/12j 600 W:

Se W

~

o 113.

20031 2.92E40 0 pcg

/1.71 gwet 05101/12!

20 1

U NI763 2013 C

'4.56F01 pCi/gk 2.0025 gwet 104/27/12]

4 f5 M

U BE-7

'20071 4

.420 pCig.

j 18o.36 oet 0410511212:00 04/12/12 6000 Sec U [No*

K-40.

.2007 1 7.8sE+00 1 !-04fE-0 1

J pClg-180.36 gw' 04/05/1212:001 04112/12 6000

.-Sec

+

MN-54 2007 5.88E-02 pCi/g f

.180:36.

get 04105/12A2:00 04112/12

-6000' -J -Se U

No CO-58:

12 0 07 1 4.54E-02

pCilg:

18036 g wet 04105/1212:00

.04/12/12 6*000 Sc F-59'

'o2007-1J l-:09O01oJ pi 180.36 gwet

.04/05/1o.12*1.ý;'

01. 2/12 6000 o.Sec Uo, CO-60
2007 Jj 45&-02 ig

.!10.836, glvet J-04o0!/212:0 4/22 6000 Sec ZN-652

<1

_7 L3E-O1 J pCi/g

.180.36-gc;t 104105/12312:00

,04/12/12

.'6000 Sec U

7R-95, 2007 180

9.

2I pCilg

,180.36.

g2wt 104/051212:00 I04/12/12 "6000 Sec U

Nd' T00

.3.7F0

'04/12/12t 0415 RU-103.-

120071 1

5.27F&)2 pCifg 180.36 gwet

.04105/12112"00 j 04/12/1 6000 Se U

No RU-106 2007'1 432E-01 pCi0g 18036-gwct JW045112.12:00,1 04/12/12 6000 Sec:

UI INO 1-131

2007 J i 9.110F,02

.pCi'g_

18036.

gwet 0ý/05/1212.00.1._04.12/12 2 6000 Secr U

No CS-134.

20007 j j______J4S1E-02

-pCilg 4 8036' [gmwet

ý04I05/12_'1I200 104/12/212

6000 JSec; U

'No' CS-13?l 200T7' J

.7OF.02 I pCi/g' 180,36 g5 wet'

04/05/12.12-00

.04/12/1 6000 Secý.

U

ýNo IBA140 2007' 2 5Z8]-B01 i

pCi/g 180.36' gwet 104/05112,12:00

'04/12/12

'6000_':

See' U

"No; CF-141

-200-

.785F_02

.pCi/gf 18036-gwet

'04105112:12:00

.0412/1 60 Se U.

No-CE-144 207.<'3.21&-01 f

pCi/g 180.36'-

gwet..04/05/12 12:00 04/12/12 600 Sec U

N' iU-152 2007'-

463F.,-01 PCi/g

'180.36ý gkwt j.04/0/12.12:00.

0121 6000 Sec.

U RA-226 2007 1.<'"

1.1-E+00 PCiLg 180.36.

g vwet 104/05/12-12:00 04/12/1 6000 Sce U

jYes

-228 f 2007 2.03F-0I ICO9E-01

_-0_-0pcikg:

180.36.:

g:wet 104/05112,12:00

-04112]

6000 Sec 7

Yes U.-235 2007-

-3.l,-1

[

.pCi/g.

J8036"'

gwet

'04105/12 12:00

,60100 Sec U

,No U-238:

2007 l

6.06E+00

.pCilg 180.36-g wet J04/0512"12:00'0412/I 600ý0 Sec.

U W.4o

'FlagValues UI CompoundlAnalyre nor deitected (< MDC or less ihmn 3 sigma

+:

Activity concentrti"on exceeds M* and 31 s p

identifi!d(*gmma onl)

U.-

=

Cqmpoýn&.Analytc nordetected. Peak not identified, but Rtced actiity c6ncnltration excecds MDC and-3 sigma High Actiiitk

  • encemntiio cxe*" customer. reportigValue Spec'

.MDICcxmeds cimer technical sp*ification

L

=

Low recoVery*

Boldedltexttindicates reorita-le Ivalie.

e No =Pea.not identifited ingammaipem Yes' =-Peak'idicrtilied ingrm spectnun

  • 44ijaes oqrriisc noted, tihe ana~tcl results reported ae related onlyo the'samples tested in the condition they are received bythe laboratoy.

MDC -Mfinimum Detectable Concantration

Report of Analysis

.05011/ -10:-44 L49994 ERdneon ENOOS-73EREGUOI1_i2 A*r.

TELEDYNE

.BROWN ENGINEERING,,INC..

'A t&,"ITedclres Caunpiey

  • Chris Higgins

'Sample ID: SSmBCT-E Collect6Sta&t 04105/2012 12:00

.Marix:,Soil (S.

,Station:

CollecutStop:

Volume:

==

Description:==

ý RcceiveDate:'04/10=2012:

%'Moistur ULMS Numbe.

L49994-21 Activity lUncertainty ARimtj Aliquot Aliquot Reference Count Count Count

.Radioinuxide jSOP#.

Cone,

2 Sigma MDC Units Volume.

Unis J Date

, Date Time Units Flag Values, FE-55

<2006 I.65E-+0l pCi/g 2.0028 g*wt 10/12 12:080 04/30112

'43j

.-Sec'.

_U No H13.

21003.

2.38E400 pCitg 1:2.1 1 gwet 1 "

" I 05/01/12 20(

M U

N-63,

-2013 J 4.58&01o pCr/g 2.0028

  • gwet._

04/27/12

45.

M U

BE?7 2007 3.IE-0.

piClg 19261 J.gwet

'04/05/12,12:00:

04/1-2/12 6000 f _

uNo KAO:

2007 6.12E+00 1.04E+00 ICi/g 19Z61 r gwetr 04/05/1I22:00' 04/12/12 6000

Scc

+

"Ye MN-54 2007 2.84F_02, pCilg

192761 g wet 04/0512-1220 04/1211.2
6000, See U

-Wo CO-58 2007 3.76E-02 pg 192.61 I,g wet-04/05/12-12:00' 04/12/12 6000 I Sec U,

".No FE-59

.2007.

_<+

8.08E-02I pCi/g 1

92.61_

gwet 04/05112 12:00.

04/12.12 6000.-

Sec

1....

. No90 CO-60

ý2007 J 1.62E"O1 4.97E-02

.pCig 192.61 g wet 04/05/12 12:00.

04/12/12 6000

.Sec

+Yes 2ZN-65. pCi/g 1192-61' g

rWet 04/05/12,12:00

'04/12/12 6000' Sc U.

No ZR-95 2007 1 5566E-0Z P0/g 192.616 gwet; 04105/12,12:00 04112V12

6000,

.Se U

No RU-103 2007 [

3iSE-02 p-l/g 192-61 0

gwct 104/05/12.1200 04/1211,2 6000 "Sec

Uo RU-06 2Q07 2_

2,91E-01:

0 0Pi/g 1,92.61'

.g9.vet 04/05112.12:00.

041./12112 '60001

-Scc

-No 1-:131.

2007 1 F,0

_..23E-:02 pC0g4 192.61

.gwet-04/05/12.!2:00' 04/1V12 6000 Sec "U

i No S.-33.0 2007

3205-0Z pCrlg 192.61'
gviet

.04/05/12,12:00

,04/12/12 6000

'Sic U

NO CS437.

2007 53.E-02FM pCpi/g 192.611 gwet 104/05/-1212:00 04/12/12 6000:

S*c; U,

BA-140 2007 I_.71F-,01, pCig I'

19.61

g t

04/05/12 12:.00.

04112/12 6000 Sec.

..U

-.No CE4I41.

2007

_4.12&M, "pu*i~g 192.61 igwet

.04/05/1212.00, 04/2/12

6000 Secý O

No CE-144 2007 1.S5E-01 "pCi/g *

.192.61 gwet 04105(1212:00., 04,12/12t 6000 Sec U

-jo EU-152 2007 I

1.OSE-01

pCV/g

-192.61 gwet 04/05/12 12:00

.04/12/12 6000 Sac RA-226 2007

_C <

9.15E-"1 pCi/g 1."

192.616 g.v OV 0/05/1212:00

-04/12A-2 6000.

Sc

U' No T11-228 2007.

ISU1E.0 5.66E-0

_____pM/

192.611 6wt %1045f12 12:00,'. 04/12/12 6000 jScec

+

yes U-235 2007 1

t.85E pCi/g

-192.61, gwct 10410511212:001:04.1212, 6000-..

Sce U

jNo U7238; 2007 4.-74E+001 p Cilg J

192.61, g wet 104/05/1212:00 1.04/12/121 6'000 soc.

U o.

F14 Val&e U

CbmpmmundfAnaly1c riot detrted (<NMD) Qor-less than 3 gigma Activit.yconcenfltaiion.eeeds A'nd i3 sigimapeak identiie gamnma only)

U Corpwiud/Ana1)ie not dewtect.

Peak-not ideiitified,,but forced actiity conicnrai~on exceeds MDC and 31sga Hh Ativi'ty conCefliaiii xicceds~cusitoiiierepo 'igv owlu Spe I

M L-c ea 'customer tedtmicals'pciaion BH

-High ateo.

Bolded text indicates-rpodrtaible value.

t

20 4 "No 'mPeak.nt id *entificd igamma spectrum Yes:

Pe aik idititUci, in gamma spectrun U0-ýnkss othaviisc noted lhi analytica results reported areirlated only to tht samples tested in thconditioo they.

are received bi the'laborato.

MDC -Mintimum DetcctaibmiCocentration.

Report of Analysis 05101112 10:44 L49994 Enercon EN005-3EREGUOI-12

,I qmL TELEDYNE BROWN ENGINEERING, INC.

A Tdom TNemo Cami Chris Higgins Sample ID: SS-WTF-001 Collect Start: 04/05/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/10/2012

% Moisture:

LIMS Number:

IA9994-22 Radionuclide 130-7--

K-40 MN4-54

]FE-59 ZN-65 ZR-95 RiJ-103 RU-106-

.CS-137 EBIAý-14 1

EU152 RUA-'226 IU-238 Activity Uncertainty i

Run I Aliquot Aliquot Reference Count Count Count cone 2 Sigma hD lgVle SOF Coe Sima i

Nt Volume Units Date I

Date 71Tme Units FlgVle 2007

_.1_+5.47E.-O-pi/g 19-7.69 wct 104/05/12 12:00 2

04/12/12 -6000 S-c U-No 2007 S.*K126-04 )

20*-

ppCi/g 197.69 gwet w

04/05/12 12:00 W /1211 6000 e

I

+

Ye0 200 7.47..

.2 pCi/g 197.69 gwet

,104/05/12 12:00 04/12/121 6000

-Sec 1J No 2007 7.JsM..02 1 pCi/g 197.69 ge 04/05712 12:00 -04/12/12I 6000

-Sc UN 2007 I

1J4E-I_

__i/

197-.69 g*wet 104/05/1212:00 04/12/121 6000 Se-U No 2007 1.051E+0i 9.98E-02 pC

/g 19769 --

g-wet

-04/05/-12 12:00 04/12/12 6000 Sec

+-

2007 1<

.7SF-1i pci/g 197.69 g&wet 04/05/12 12:00 04/12/12i 6000 Se* c U

S2007 1.14E-O pCi/g i97.&69

-gwct+-

04/05/2 12:00

-04/12/i21

-6000 e--c U

-No 2-f--

27E-02 pCi/g B

197.6 gwet 04/05/12,12:00 04/12/12 6000 Sec U

No 2007 pCi/g 197.69 g.wet 04/05/12 12-00 04/12126000 Sec U

No 2007 OF-0" pCi/g 197.69 g wet 04J05/-12100

/12 6*0 Sec

.U No 7

2007

<j 67 02 pCi/g 197.69 gwet 04/05/12 12:00 04/12/12 6000 T

-No

_t 7_04-

<000

+-"

2007 17.239F0 pCi/g 197.69 g-wet 04/05/12 12:00 04/12/12 6000 Sec Jl No

-20077 1.93F-00 pCi/g 197.69 g wet 04/05/12_12:00 0,/12-i2 6

Sec No 9.21E-02 pCi/g 197.69 gwct-0/05/112.00 0412/12

-6000 Sec U.N 207 3.5-t pig197.69 g wet 04/05/ 2 12:00 04112/12 600 Sec U

N 2007 1.99E-O1 1~/

97.69 g wct 04/05/f2 12:00 0-4/21212 6000 Sec U

No 2067 19FI.2E0

~

/

197.69 g wet 04/05/12 12:00 04/12112j 6000 Sec Uý 7

Ye 2 0 211

- I 73 1 - 2pci/g

-197.69

-g w et - 04/ '035/1 +2 f12 00 04/1 112 6 000- -I S c +c y !

((2007

-[

3-.72E-0-1 pCi/g 197.69 gwet

/05/12 1200

/2 6000 Sec U

No 2007 !

.6019 pCi/g

- 197.69 gwet 6405/12 12.0o 04/12/12 6000 ec U

No l

Flag Values U

=

CompourdlAaalyte not detected (< MDC) or less than 3 sigma

+

=

Activity concentration exceeds MMX and 3 sigma; peak identified(ganm only)

U*

=

Compond/Analyte not detected. Peak not identified, but fbroed activity concentration exceeds MDC and 3 sigma High Activity concentration exceeds custmner reporting value Spec MDC exceeds customer technical specification L

=

low recovery H

H ttigh recovery Bolded text indicates reportable value.

Page 13 of 24 No = Peak not idenlified in gumn spectrum Yes Peak identified in gamma spectuam 0*** Unless otherwise noted, the analytical results reported ae redlated only to the samples tested in the condition they awe received by the laboratory, MDC - Minimum Detectable Concentration

Report of Analysis 05/01/12 10:44 149994 Enercon 7 *q.

TELEDYNE BROWN ENGINEERING, INC.

A ltatya Tsrmk*togs" ComwmN Chris Higgins EN005-3EREGUOI-12 Sample ID: SS-NFT-001 Collect Start: 04/05/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/1012012

% Moisture:

LIMS Numbcr:

L49994-23 Radionuclide BE-7 K-40 MN-54 CO-58 FE-59 CO-60

.ZN-65 ZR-95 RU-103 RtU-106 f-1-3-1 CS-134 CS-137 BA-4140 CE-141 CE-144 rEU-152 I*R*-226 TH-228 I1J-235

-Activity Uncertainty 2007 5.24F,+00 L171-',+00 2007

_<6.14E-02 2007 6.70E-02 2007

'9.1-01

-2007

<9.79E-02 2007 1.28E-01 2007-1.18E-01 2007 6.83E-02 207 6.%F,01 2007

<1.14K-1 6.841-02 2007-ý-

6.7s£02 2007W 3.43K-0l 007 9.95-02 020707 4.04K-01 20607 1 0--E.-01

-2007 1.32E+00 12007-7 2.24E-Cl 1.07E-i 2007 3.96&-01 20!07 8.Z3E+060

Unit, Pci/g PCi/g9 pCi/g pCi/g Pci/g PCi/g Pci/g pCi/g pCiJ/g PCi/g PCilg Rn Aliquot Alquot Volume Units 182.16 g wt-412J6 g__

e7 182.16 gwet 182.16 gwct 182.16 g-wet 1*2.16 g wet 182.16 gwet 182.16 gwet 182.16 g wet 182.16 gwet 182.16 gwet 1821.16 get 182.16 gwet 182.16 g wet 1-82.16 gjw-ct 182.16 g wet 182.16 g wet 182.16 wet 182.16 g wet 182.16 g wet 182.16 g wet Reference Count Date Date 04/05/12 12.00 0/2 0/05/12 12:o00

-4/12/12-04/05/12 12:00 0411I 2I2 04/05/12 12-00 04-12/12 04/05/12 12:00 04/12J1 04/05/12 12-00 04/12/U2 04/05/12 12:00 04/12/12 04/05/12 12:00 04/12-2 04/05/1 12:00- 04/12/12 04/0512

'20 o4/12,12 04/5/12 12-00 04/12/12 0/05/12 12:00

  • 4-121 2 04/W/2 12.:00 0412112 04/03/12 12:00 04/12/12 04/05/12 12:0 04/-1212 04/05/2 12:-00

-04/12/1212 04/05/12 12:00 -.04/1 2/12 f 04/05/12 12:00 04/12/121 04105/12 12:00 0I4/12/12 04/5/12-12:00 04/121 04/05/12 12:00 04/12/121 Count Time 6000 6000 6000 i0(

6000 6000 6000 6000 6000 60600 6000 6000

~~6000 6000 6000 6000 6000 600 Count Units Flag Values Sce U

No 2 Sec

+

Yes See U

No Sec U

No Sec u

No 4*.

S7 U

Se-c U

U No I S*e U

NO u4

-o Sec U

No see U

No see U

No Sec 7U No Sec U

No U

0 Sec U

No Sec e Yes Sec U

No See o

i Fag Values U

Conpound/Analytc not detected (< MDC) or less than 3 sigma

+

=

Activity concentration exceeds MDC and 3 sigma; peak identifed(ganuma only)

U*

Compownd/Analyte not detected. Peak not identified, but forced activity concentration exceeds MD)C and 3 sigma Iligh

=

Activity concentration exceeds customer reporting value Spec MC exceeds customer technical specification L

=

Low recovery H

=

Iligh recovery Boided text indicates reportable vaiue.

Page 14 of 24 No

= Peak not identified in gamma spectrun Yes = Peak identified in gamma spectrum

        • Unless otherwise noted, the aalytical results reported are related only to the samples tested in the condition they ae received by the laboratory.

MDC - Minimum l~nectable Concentration

Report of Analysis 05/01/12 10:44 1.49994 Encrcon EN005-3EREGUOI-12 IABRhWN ENGINEERING, INC.

A Tdospw TschncolqiW Comp" Chris Higgins Sample ID: SS-NFT-002 Station:

==

Description:==

LIMS Number:

IA9994-24 Collect Start: 04/05/2012 12:00 Collect Stop:

Receive Date: 04/10/2012 Matrix:

Soil Volume:

% Moisture:

(S) I So#IActivity Uncertainty IIRun Aliquot Aliquot Reference count count Count Radionuclide SOP#

Cone 2 Sigma i

MDC Units N

Volume Units Date Date Time Units

[BE7 2007 6.37E-01 Pai/g 158.6 g wet 04/05/12 12:00 b-4-/2/12 6000

-See LK-4o 2007 6-34E+00 1.34E8400 pCi1g 158.6 g wet 04/05/12 12:00O 04/12/12j 6000 SOe 4

2007

" 6J6.--

g I

158.6 I

gwwet _04/05/1 212:00 04/12/12, 6000 sec CO58 2007 8.48E-02 pCi/g

_158.6 g wd 04/05/12 12:00 -04/12/12' 6000 See FH-59.

2007 1.65E-01I pCi/g 158.6 g wet 04/05/12 12:00 04/12/12t 600 S

CO-0 207 47E01

.26-0

~ pi/g

58.

1 Wet 0405 12:0 4i/-12/112 600-0 See O-60.

2007 "1.9-9-6

/

-2 158.6 g wet 04/05/12 12:00 04/12/12; 6000 Sec ZN-65 2007

<1.69F101 pCi/g 1-581.6 g we

-04/05/12-l2-:00 04/12/12 6000 Sec ZRU-103 6

200 7

-3<

.6.E-02 pci/g 158.6 g wet 04/05/12 12:00 04/12/12 6000 sec R-103 2007

-~-

.7-I pig 186 ge 40/22000411260 c

1-131 2007 1_

1.148F.-O2 pCi/g 158.6 gwwet

/0/1212.:0 04/12/121 6000 Sec IcM.134 ZO..

20 4E-

,ig 158.6 g wet

-4/05/1_2 2-:.0 04/12/126000

_sec

'1-31 2007 i

1.76E-0I1.02-01..-

g.158.6 gwet 04/05/1212:00 04/12/12 6000 Sc I 2007

. 3.61 pg 158.6 w"I-2 wet_

005/12 12:000/2/12 00 Se jCE-41 2

7.1 pý2

  • -i 15.6 g wet 04/05/12 12:00 0W12/1
  • 6000 Sec
CE-144 2007 !

I 3.64E-01 pCi/g i

158.6 gwet 04/05/12 12.00 04112/12, 6000 S'

EU-152--

2007 2

i_3.

76-- 01 158.6

_g--w 9/-0 0

04/I2/h2 6000 --

Set

15.

gýwctý 04/05/2120

  1. Aý-6 102007 pCi/g I'158.6 gw-t 04/0

-12 12:00 04/12/12 6000 Sec E1141228 --

2007 1.67E-01 I

1.OO-01 pCi-g --

158.6 g.wet 0405/1212:00 04712/12 6000 Sec

'E142007~

/0 6-4.401 pCi-g 158.6 g wet 04/05/12 12:00 04/12/12 6000 Sec RU-238

_2-6 2007 1

9K93_+00 pCi/.

158.6 g wet _04/05112 12:0I 04/12/121 6000 _

U Flag Values U

=

Compound/Analyte not detected (< MM) or less tham 3 sigma

+

=

Activity concentration exceeds MDC and 3 sigma; peak idcntified(gpuua only)

U*

Compound/Analyte nat detected. Peak not identified, but forced activity concentration exceeds MDC and 3 sigma High

=

Activity concentration exceeds custwer reporting value Spec MIC exceeds custoame tedmical specilfeation L

=

Low recovery H

=

I ligh rcwovcry Bolded text indicates reportable value.

Page 15 of 24 No

= Peak not ientified in gamma spcctun Yes = Peak identified in gamma specltrm

        • Unless otherwise noted, the =alytical results repuled ar related only to the sunples tested m the condition they we rceived by the labatory.

MIX - Minimum Detcctable Concentration

Report of Analysis 05/01/12 10:44 L49994 Enercon EN005-3EREGUOI-12 TELEDYNE

'PI BROWN ENGINEERING, INC.

A Teledyne Technologies Compare Chris Higgins Flag Values U

=

Compound/Analyte not detected (< MX") or less than 3 sigma

+

=

Activity concentration excecds ML)C and 3 sigma; peak identified(gamma only)

U*

=

Compound/Analyte not detected. Peak not identified, but forced activity concentration exceeds MIC and 3 sigma High

=

Activity concentration exceeds customer rcpirting value Spec MDC exceeds customer technical specification I.

=

Low recovery if

=

Iligh recovery Holded text indicates reportable value.

Page 16 of24 No

= Peak not identified in gamma spectrum Yes = Peak identified in gamma spectrum

        • Unless otherwise noted, the analytical results reported are related only to the samples tested in the condition they are received by the laboratory.

MDC - Minimum lclectable Concentration

Report of Analysis 05/01/12 10:44 IA9994 Enercon EN005-3EREGUOI-i 2 rELEDYNE 3ROWN ENGINEERING, INC.

A TOWV TM**ine-Comp" Chris Higgins Sample ID: UI-BS-001 Collect Start: 04/05/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/10/2012

% Moisture:

LIMS Number-L49994-26 Radionuclide FE-55 M-54 C6o-58s FE-ý59 SO#Activity Uncertiy SOP#

Cne 2 Sigma MDC 2006 1.29E+01 Units pCi/g Run 2003 2013 2007 2007-7.33E+00 2007 2007 2007 2007 3.90E-01 1.11

-E+00 4.31E-02 5.10E-02 pCi/g pci/g pCi/g

-pCi/g pCi/g pCi/g Aliquot Aliquot Volume Units 2.0123 g wet 1.61 g wet 2.0123 g wet 196.77 g wet 196.77 g wet 196.77 g wet Reference Date 04/05/12 12:00 04/05/12 12:00 04/05/12 12:00 04/05/12 12:00 04 05 04 04 04 /30/12

/01/12 W2812

/12/12

/12/12

/-12-/l2

/12/12

/12112 Count Date Count 1me 600 20 45 6000 6000 6000 6000 6000 6-000--

6000 Count Units Sec M

M Sec Sc Sec Sec sec Sec Sec Sec Sec 196.77 gwet 104/05/12 12:00 04 196.77 gwet 04/0511212:00104 1.10O,011 ZN-65 2007 ZR1-95 2007 1.OIE-.01 1.05K-Ol 5.26F,02 pCi/g pCi/g pCi/g pCi/g Wilk~

pCi/g pCi/g---

196.77 g wet 04/05/12 12:00 196.77 T gwet 104/05/12 12:00 04 04 U

-V U

U

+

-U U

u U

U

-U U-

-U

-V RU-103 2007 RU-106 2007 1-131 2007 4.17E-01 7.80E-02 CS-134 CS-137 2007 2007 4.79-A-2 5.67E-02 2.18E-01 7.90E-02 BA-140 2007 CE-141 2007 CE-144 KU--1-5 2 2007 2007 2E7E-01 1.46"-01 pCi/g pCi1g pCi/g pCi/g pCi/g

~pCi/g pCi/g pci/g 196.77 196.77 196.77 196.77 196.77 196.77 196.77 196.77 196.77 196.77 g wet 04/05/1212:00 04/12/12 6000 gwet 04/05/12 12:00 04/12/12 6000 Flag Values No No Yes No No No No No No No No No No No No No No Yes

-No-

--ýNo g wet g wet g wet 04/05/12 12:00 04/05/12 12:00 04/05/12 1200 04/12/12 04/12/12 04/12/12 04/12/12 04/12/12 6000 6000 6000 60OO Sec Sec Sec Sec Sec RA-226 TH~i-228 U-235 U-238 g wet g wet g wet g wet g wet 04/05/12 12:00 04/05/12 i2:00 04/05/12 12:00 04/05/12 12:00 04/05/12 12:00 04/12/12 04/12/12 04/12/12 04/12/12 04/12/12 6000 6000 6000 See Sec Sec Smc Sec 2007 2007 2.37E-01 2007 2007 1.17E+00 8.04E-02 3.15"10 t6iwEo 196.77 196.77 196.77 g wet g wet g wet 04/05/12 12:00 04/05/12 12:00 04/05112 12:00 U

--U.

U

+

Uij 04112/121 6000 Sec 1-

-- 196.77 196.77 wet W---

05FI212:00 1 04/1ý/Iý 6000 See Flag Values U

=

CompoundJAnalyte not detected (< MDC) or less than 3 sigma

+

=

Activity concentration exceeds MDC and 3 sigma; peak idantified(gamma only)

U*

Compound/Anaiyt not detected. Peak not identified, but forced activity concentration exceeds MDC and 3 sigma High

=

Acvity cwcer" exceeds customer reporting value Spec

=

MDC exceeds cutonmer technical specificatio L

=

Low ecovey H

=

High recovery Bolded text indicates reportable value.

Page 17 of 24 No = Peak not identified in gamma spectrum Yes = Peak identified in gamma spectrum

        • Unless oherwise noted, the analytical results reported are related only to the samples tested in the condition dthy are received by the laboratory.

MDC - Minimum Dtectabl Concentration

Report of Analysis 05/01/12 10:44 L49994 Enercon EN005-3EREGUOI-12 TELEDYNE r

BROWN ENGINEERING, INC.

A lms Ted~aoes Ceipq Chris Higgins Sample ID:

UI-BS-002 Collect Start: 04/05V2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/10/2012

% Moisture:

LIMS Number:

L49994-27 Radionuclide H-3 M--63 MN-54 t6:-58 F&-59 CO-60

&£-65 ZR RU-10-3 R-U-406 1-131 CS--134 CS-437-BA-140 ME-14-1 ffE-1-i44-EU--152-RA-226 M1-228 rHi-232 U-235-SOP#

Activity Uncertainty Run!

Aliquot Aliquot Cone 2 Sigma MDC Units Volume Units Reference Count Count Date Date Time Count Units Flag Values 9.--

,.=~---

2006 2003 2013 2007 2007 2007 2007 2007 2007 1.25E+01 pCi/g 2.0072 g wet 104/05/12 12:00 1 04/30/12 600 pCi/g 1.73 05/0l/12j 20 2A9E+00

  • 458F,01

- pc 1

.02 42li2 1.73 2.0072 g wet g wet 05/tn/iý zu Sec M

M U

U UUii No No pCi/9 200.95 i 3.33F.41 7.33 r+-0 8.86E-01 pci/g 200.95 g wet g wet g wet 04/05/12 12:00 0C4/5/1212:i-0-0 04/12/124 6000 Sec 04112/121 6000 Sec

+

IYesI No 4.60E-02

.U1-4K-Cl2-1.15K-Cl 6.43E-02 MUMK-C pCi/g

--pCi/g pCi/g 200.95 200.95 200.95 200.95 200.95 04/05/12 12:00 g wet g wet gwet g wet 04/05/12 12:00 04/05/12 12:00 04/12/12 04/12/12 4/12/12 6000 60M 6000 Se I U Sec Sec Sec Sec U

U U

U No No No No 04/05/12 12:00 04/05/12 12:00 04/05/12 12.00 04/12/12 6000 04/12/12 6000-2007 2007 2007

--2007 2007 2007-2007 2007 2007 07 2007 2100-7 2007 2007 2007 7.55K-02 4.13K-C2 pCi/g pCi/g 200.95 200.95 g wet 04/12/121 6000 Sec I U No g wet 04/05/12 1200 04/12/12 pCi/g g wet 6000_

Sec S6000 Sec

<~

3.53E-01 7.35K-C2 3.60E-02 4.84K-02 2.12K-01 6.27E-C1 2.37K-01 pCi/g pCi/g pCi/g P019g pCi/g pCi/g 200.95 200.95 200.95 200.95 200.95 200.95 200.95 200.95 200.95 200.95 200.95 200.95 200.95 g wet g wet g wet 04/05/12 12:00 04/12/12 U

U U

04/05/12 12:00 04/12/121 60001 See 04/05/12 12:00-04/12/12 6000 Sec No No No No No No No No g wet g wet g wet 04/05/12 12:00 04/12/12 6000 04/05/12 12:00 04/12/12 6000 Sce Sec Sec U

U

-U U

04/05/12 12:U00 04/12/121 6000 I.OE-01K 7.60E-01 pCi/g pCi/g 3.60E-01 2.90K-01 5.5313-02 1.24E-01 pCi/g pCi/g pCi/g g wet g wet g wet g wet g wet g wet g wet

+--------------+-

04/05/12 12:00 04/05/12 12:00 04/05/12 12:00 04/121121 041~12112

-0/12-12 6000 6000 6000 600O 04/05/12 12:00 1 04/12/121 6000 Sec Sec Sec Sec Sec 04/05/12 12:00 04/12/121 6000 U

U

+

+

U U

No Yes Yes Yes No No 2.50K-Cl 5.ISE-+00 pCi/g 04/05/12 12:00 04/12/12 04/05/12 12:00 {04/12/12 Flag Values U

=

Compound/Analyte not detected (< MIX,) or less than 3 sigma

+

Activity concentration exceeds MDC and 3 sigma; peak identified(ganmm only)

U*

=

Compound/Analyte not detected. Peak not identified, but forced activity concentration exceeds MDC and 3 sigma High

=

Activity concentration exceeds customer reporting value Spec

=

MDC exceeds customer technical specification L

=

Lowrecovery H

=

High recovery Bolded text indicates reportable value.

Page 18 of 24 No l Peak not identified in gamma spectrum Yes = Peak identified in gamma spectrum

  • "" Unless otherwise noted, the analytical results merted are related only to the samples tested in the condition they ae received by the laboratory.

MDC - Minimum Detectable Concentration

Report of Analysis 05/01112 10:44 L49994 Enercon EN005-3EREGUOI-12 TEHEDYNE BROWN ENGINEERING, INC.

A T.4adyTkh-e" a~~Cuup" Chris Higgins Sample ID: UI-DS-003 Collect Start: 04/05/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: W410/2012

% moisture:

LIMS Number:

1,49994-28 Sample ID: UI-BS-003 Collcct Start: 04/05/2012 12.'00 Station:

Collect Stop:

==

Description:==

Receive Date: 04/10/2012 LIMS Numb:r:

1,49994-28 Radian 11-3

[Nl-63

ýBE-?

rFE-58 RU- 06 Kt1 34

ý E-141 1C11144 RA-226 TH-228

.TII-232 L-38 So I

Activity Uncertainty I

Run uclide Conc 2 Sigma MI)C Units

___2063 1.09E+01 pCig l

2003 2.31IE+00O pCi/g 2013 4.56-0*1 pCi/g 2007 3.93E-41 pCi/g

..... 2007 s.76E+00 7.84E-01 pci/g 2N07

< _E-02 pCig 2007

<4.51 0

pcJ g 2007 9.05*e-l2

  • i/g 4__ 0

-4 riý&

pCi/g 2007 L$IK-02 pCi/g j2007~

7.95"-02 pCi/g 2007 4.93E-02 pCi/g 20o07

i/g 2007 7.81E-02 pCi/g 2<67 4 4.,02 i pCi/gI 2007 5.09E-02 pCi/g

__- 0-0 6_07E-01 pCi/g 2007 fpffi/gL~o 2007 6E-o1 p-/g1 2007 1.2F-01 pCi/g 200-7

-&1871F01 pCi/g 2007 3.IoE-o0 6.5(0-02 pCi/g 2007 2S.4-1 9.63E,02-pi/g 0071 2.57E-01 pCi/g 2007 5.45E+0o 1 pCi/g Aliquot Aliquot Refeirence Count Volume Units Dote De 20116.

Wet 04105/12.12:00 04/30/12 216 g wet 400 5/01/2 2.0116

- gwet 04-/28/1 218.38 g wet 04/05/12 12:00 04/12/12 218.31

-gw-et 04/05/1212:00 011*/2 218.3-ggwet 04/05/12 12:00 04/12/121 218.38 gw-et 04/05/12 12:00 W-/12/12 218.38 g-wet 04/05/1212:00 04/12/121.

218.38 gwet 04/05/12 12:00 04/12/121 218.38 gwet 04/05/12 12:00 04/12/12 218.38 g wct 04/05/12 12:00 04/12/12 218.38 g wct 04/05/12 12:00 04/12/1I_

218.38 gwet

-C0/05/12 12:00 04112/12 218.38 g wet 04/05/12-12:0-04/12/12 218.38 g wet 04/05/12 12:00 041 2/I-2 218.38 g-wet 04/05/12 l2i.-- 04/12/12 218.38 g wct 04/05/12 12:00 04/12/1 218.38 g wet 04/03/12 12:00 04/12/12 218.38 g wct 104/05/12 12:00 04/12/12 218.38 g wet 04/05/12 12:00 04/12/12 21.38-gwt 0/5 1:0-0 04/'12/12 218.38 wet J04/05/12120 042/

21.3 g et-04/0 /12 12:00 604/12 /1 218.38 jg~wct 04/05/12 12:00 04/12/12 Count Count Time Units Flag Values

_09_

Sec U1i

_J0 20 M

Ui 45 M

U 6000 sac U

No 60o Sec Yes 6000 Sec U

No 6000 Sc U

No 6000 Sec U.

No 6000 Sec U

Not 6000 Sec U

No 600 Sec-No - 6000 S0c-U

~

No 6000 Sec U

No 60-00 Sec U

N 6

000 c

U No o ---

6000 Scc U

No woo- "sa-U-7--

-140-6000 ISci U

NO 6000 eL U

6000 5cc U

Ye 6 ooo-

-ScIU-u-

1 6000 SeclU Yes 60-00

~ v 6000 icc U

N Flag Values U

=

ConpouwdAnalye not detected (< MDC) or lks than 3 sigma

+

=

Activity concenratim exceeds MDC and 3 sigma; peak identified(gamma only)

Us

=

Cenmpound/Analyte not desected. Peak not identified, hut forced activity concentration exceeds MDC mad 3 sigma High

=

Acivity coucaiuiion exceeds custemer reporting value Spec

=

MDC exceeds custome technical specification L

=

Low recovery H

=

High recery Bolded text indicates reportable value.

Page 19 of 24 No = Peak not identified in gamma spectrum Yes - Peak identified in gamma spectrum

'*'* Unless otherwise noted, the analytical results reported are related only to the samples tested in the condition they art received by the laboratory.

MIC - Minimum Detabc Con*cntration

Report of Analysis 05101/12 10:44 L49994 Enercon EN005-3EREGUOI-12 W

TELEDYNE DROWN ENGINEERING, INC.

A TO44-T-.Anolooiw CeWpIy Chris Higgins Sample ID: UI-BS-004 Station:

==

Description:==

LIMS Number L49994-29 Collect Start: 04/05/2012 12:00 Collect Stop:

Receive Date: 04/10/2012 Matrix:

Soil Volume:

% Moisture:

(S)

S Activity Uacerteinty Radionuclide sop#

Cone 2 Sitpis FE-55 200 H-3 20-03 NI-63 2013 BE-7

".2007 K-40 2007 4.93E+O0 8.74E-01 MN-54 2007 CO-M-2007 FE-59 2007 co-660 i0_07 ZN-65 2<

ZR-95 2--i RU-103 2007 RUJ-1066 0 -

1-131 207-CS-134 2007 CS-137 2007 MDC 151K+01 M.556H0

-4."K-01 2.93F,0 2.52E-02 4.12F,02 7.10E-02

_3.53_F_02 7.57&-N s5s"zuVi 2.95K-In 2.85E-01 4_.99K-2_

7.74F,032

_3.3_2K-lU Run Aliquot

  1. I Volume Units pCi/g pCi/g pCi/g__

pCi/g pCi/g pCilg pCi/g pCi/g pCi/g-pCi/g 2.0106

.96 2.0106

_210.06 210.06 210.06 210.06 210.06 210.06 210.06 210.06 210.06 Aliquot Reference Units Date g wet 04/05/12 12:,00 g wet g Wet g wet 04/05/12 12.00 g-w_- OV/60112 12-00 g wet_

04/05/12 12:00 g we(

04/05/12 12:00 g wet 04/05/12 12:00 g wet 04/05/1212:00 g wet 04/05/12 12.00 g-wet M4-5/12 1*.00-gwet 04/05/12 12:00 g wet 04/05/12 12:00 g-wet 04/05112 12:00 g wet 04/05/12 12:00 gwet 04/05/12 12:00 g wet 04/05/12 12:00 g wet 04/05/12 12:00 g wet-04/5/12-12:060 g wet 04/05/12 12:00 g wet 04/05/12 12:00 g -weit "6/5/121-2-00 g wet 04/05/12 12:00 Count Count Count Date Time Units Flag Val 04/30/12 600 scc U

05m/01/1 20 _ M U.

04/28/12 45 M

U W1/2/12 6000 Sec U

  • iV-1 6(

-S.

+ - -!

04/1212 6000 Se

--U 04/12/12 6000 Sec U

04112/12 6000 Sec U__

04/12/12 6000 Sec U

04/12/12 60 ae I Uc -

U 04/12/1*

6000 SeeP U 04/121 60-0

-Sc

-UT- -

04/12/12 6000 Sec U

4/12/*12 6000 Sec_

U 04/12/12 6000-Sec U

04/12/12 6000 Sec U

04/12/

6000 Se 04/12/12 6000 See U

0 4/12t12 6000 5c U

04/12/12 6000 See U

-04/12112

_6000- Sec-U 04/12/12 6000 See

+

04/12/12 6000_

ec

+

0/-12/126000 Sec

-U

-U 04/i2/12j§ 600

_SceQ-r LBA-1406 k CE4-14

.EU-I 52 iRA-226 111-228

_tH-232 FU-235 LU-238 2 0 0 7 2007 2007

_TI 2007 2067 207 3E,-01

  • 6 64E-02 2007 2.14K"Ol 7.99E-02 2007 1.30K-e[l Pý1/g 3.44K-02 pCi/g 11.12"-I

-pCi/

4.63K-0l pCi/g pCi/g I pCi/g 4.36K4430 p~i/g 210.06 210.06 210.06 210.06 210.06 210.06 10.06 210.06

-- :0-~6-Rlag Values U

=

Compound/Analyte not detected (< MDC) or less th 3 sigma

+

Activity concentration exceeds MDC and 3 sigmr peak identified na only)

U*

=

Compound/Analyte not detected. Peak not identified, but forced activity concentration exceeds MDC and 3 signma High Activity concentration exceeds customer reporting value Spec

=

M eC exceeds customer technical specification L

=

Low recovery H

High recovery No - Peak not identified in pmmna spectrum Yes = Peak identified in gamma spectrum

        • Unless otherwise noted, the analytical results reoted we related only to the samples tested in the condition they re received by the laboratory.

MDC - Minimum Detectable Concentration Bolded text indicates reportable value.

Page 20 of 24

Report of Analysis 05/01112 10:44 LA9994 Enercon EN005-3EREGUOI-12 "L TELEDYNE 7

BROWN ENGINEERING, INC.

ATeWadvnTemW~swsCmu Chris Higgins Sample ID:

UI-BS-005 Collect Start 04/05/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/10/2012

% Moisture:

LIMS Number-L49994-30 soP#dActivity RaSdionuclide S

Conc

,FE.S 7

_2006 NI-63 2013 BE_7 2007oi K-.40

_2007 7.3569-D00 IM-54 2007 CO-SlI 2007 FE-59 j6_2007 CO-60 i667 ZN-65 200-7*-

iR-95 12007 RU-103 2007 RU-106 2007 1

2007 CS-134 2007 CS-137 7

BA-1440

__2007--

CF-141 2007 iCE-144 2007 EU-15-2 2007 RA-22 20 IRa-:

2067-TH-228 20 2.891-01O fU-235

<-2 U4 8

2007-

+

Uncertainty 2 Sigma KDC 1i.39E+01

-1.15600 4.54F,01 A A, ]F-n 1.21E40 6.28&-02 6.IIE-02 7.11E-02 1.230141

&6.42142 8.581-02 1.612-01 t.443 Units pCi/g pci/g pCi/g pCi/g pCii/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCil/g pCi/g

-pCi/g pCi/g pCi/g pCi/g pcW pCi/g-pCi/g-pCi/g Opoi/

Run Aliquot Aliquot Reference Count Count CAPmOt N#

Volume

[lnits Date Date Time Units Flag Values

-* 2.00 gwct-04/05/12 12:00 040_12--_600 Sec U

NoJ

.2.32 g we

  • 056/0/12l 20 M

U 2.008 g gwet_

04/28/12 45 M

U 177.82 g wet 04/05/12 12:00 04/12/12 6000 Sec 11 No

-177.82 gwet 104/05/2 12:00 04/12/12 *60 ec

-e-177.82 gwet

-04/05/12 12:00 04/12/12 6000 sec U

No 177.82 gwct 04/05/12 12:00 04/12/12 6000 Sec U i No j_ _

177.32 [ _gwet_04/0/!2 12:00}.!04/12/12_ 6000__ Sec r

_ ~No 177.32 9 wet 04/05/12 12:00 04/1211 6000 Sec U

No 177.32 gwet 04/05/12 12:00 04/12/12 6000 Sec U

No 177.82 g wet_

04/05/12 12:00 04/12/12 6000 Sec U

No 177.82 g wet 04/05/12 12:00 04/1V/12 6000 Scc U

No 177.-2 gw1et 04/05/12 12:00 04/12/12 6000 See I

No 177.82 gwet 04/05/12 12:00 04/12/12 6000 Sec U

No 177.82 g wet 04/05/12 12:00 04/12/121 6000 vie IUl No 177.82 g wet 04A05/1212:00 04/12/121 6000 USc No 177.82 gwet 04/05/12 02.-0 04lI2/121 6000 Se s

U No 177.s2 g-wet 04_05/i2 1 041/2 6000 Sec 177.82 gwet 04/05/12 12:00 04/12/12 6000 Sec U

No 177.2

__gwet

-0405/12-12:00

/ 1 6000 see Uf-177.82 g wt 04105/12-12:00 04/12/12 6000 Sec U

No

-177.82 gwt 04105/12-12-:00 04/12/12 6000 Sec

+6 Yeo 177.2 g wet -04/65/1.2 12:00 (04/-12/I2 606oof-e

-LNo 177.82 g wet 0401 2:-

04/112/1211-660 Sm 1+

N 8.42E-0:

Flag Values U

=

Compound/Anlle not detected (< MDC) or less than 3 sigma

+

=

Activity conentration exceeds MDC and 3 signm peak idenified(ganuns only)

Us

=

C"pndVAnuyte not detected. Peak not identified, but forced activity concentration exceeds MDC and 3 sigma lligh Activity concentration xceeds customer repoting value Spec MDC exceeds customer technical specification 11 Low recovery H

=

High recovery Bolded test indicates reportable value.

Page 21 of 24 No = Peak not ideitified in gamma spectrum Yes - Peak identified in gamma spectrum

        • Unless oterwise noted, the analytical results reported ae related only to the samples tested in the condition they Me received by the laboratory.

MDC - Minimum l)etctable Concentration

Report of Analysis 05/01/12 10:44 L49994 Enorcon EN005-3EREGUOI-12 W

TELEDYNE BROWN ENGINEERING, INC.

A TWu*hne Wiioou Coui Chris Higgins

.Start: 04/05/2012 12:00 Matrix:

Soil Volume:

% Moisture:

(S)

Aliquot Aliquot Reference Cout Volume Units Date Date 2.0051 g

gwet 04/05/12 12:00 04/30/12 2.37 gwct 05/01/12 2.0051 g wet.

-28/12 182.53 gwet 04/05/12 12:00 04/12/12 18 2-.53

_g wet 04/0'5-/12 12:00-0-4/12/1'2 12-g wet 04/5-/12 12:oo0 04/12/12 18_.53__ wet 0_405/12 1200 04/12/12

12. "53 g wet 0415/12 12:00 04/ 12/12 182.53

_gwet.

04105t12_12:00 6/I21-12 182.53 g w*t 045/12 12:00 W0412/12 182.53 gwet 0'6/5/12 12:0 04/1211_

182.53 w

04/05/12 12:00 04/12/12 182,53 gwct -041051i2 12:00 04/12/12 182.53 g wet 04/05/12_12:00 04/12/121 182.53 I g wct ___05/121200 04-12(121 l8.53

_gwct 0-4/05/1212:00 _04/12/121 182.53 gwet 04/0512 12:00 04/12/12 1

-2.53 gwet I 04105/1212:0-04/12/12" 182.53 gwet 045/12 12:W0 04/72/12

_182-.53 gc 40/21:0 0/21 182.53 g wet 04/05/12 12:00-04/12-112-1253 g wet 04/05/122:004112 182.53 g wet 104/05/1 12:00 04(1-/121 182.53 igwct 0*/0/12-12:00 104/1V12 12.53 gwct 04/0!/2 212:00 704[12/121 Count Count 1 Tune Units Flag Values 600 Sec U

No 20 M

U 45 M

U 6000 Se-U No 6000 Sec

+

Yes 6000 Sec u

No 6000 Sec U

No 6000

-Sect UF Nio 6000 SWc N

6000 Sec U

No 6000 Sec U

No 6000-Sec U

-No 6000 See U

No 6000 Sec U

No 6000 S-C U

No Xl Sec U

No 6000 i Se U

-No 6000 Sec U

No 6000 Sec U

Ye 6000 Sec

-+

Yes 6000 Sec

+

Yes 6000 Sec U

No 6000 Sec U

N I

Flag Values I)

Compouad/Analyte not detected (< MID) or less than 3 sigma

+

Activity concentration eacceds MDC and 3 sigma, peak idntifid(gaua only)

Us CompodWAnaytc not detected. Peak not identified, but forccd activity concentration exceeds MDC and 3 sigma High

=

Activity concentration eceeds custome reposting value Spec NDW exceeds customer technical specification L

=

Low recovery H

Iligh recovery No

= Peak not identified ia gamma spectrum Yes = Peak identificd in gauna spectrum

        • Unless otherwise noted, the analytical resuits reported ma related only to the snupls tested in the condition thdy arI

-ceiivmd by Dte laboratory.

MCDC - Minimum Detectable Concentration Boded text indicates reportable value.

Page 22 of 24

Report of Analysis 05/01/12 10:44 L49994 Enercon Chris Higgins ENO05-3EREGUOI-12 7j.L TELEMYNE q

BROWN ENGINEERING, INC.

A Tdudu T-khnoW9-Cwmnpy T

Flag Values U

=

Compound/Analyte not detected (< MDC) or less than 3 sigma

+

Activity coccnutaion exceeds MDC and 3 sigma; peak identified(gamma only) u*

Comaund/Anfyte not detected. Peak not identified, but forced activity concentration exceeds MDC and 3 sigma High

=

Activity concentration exceeds custmw porting value Spec

=

MDC exceeds customw technical specification

=

Low recovery H

fish recovery Boldled text indicates reportable value.

P 23 of24 No ý Peak not identified in gamma spectnun Yes = Peak identified in gamma spectrur

        • Unless otherwise noted, the analytical eults reported we related only to the sa*plcs tested in the cndition they ae received by the laboratory.

MDC - Mbinuan Detectable Concentration

Report of Analysis 05/01/12 10:44 L49994 Eamcon EN005-3EREGUOI-12 TELEDYNE P

BROWN ENGINEERING, INC.

A Tgsdml rhfchWlOO aOCmy Chris Higgins Sample ID: UI-BSR-002 Collect Start: 04/05/2012 12:00 Matrix:

Solids (SD)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 04/10/2012

% Moisture:

IIMS Number:

LA9994-33 Radionuclide

ýBE-7 K-40 MN-S4 CO-58 i-i-59 ZN-65 ZR-95 RUJ-103 RU-106 1-131 CS-134 CS-137 BA-140 CE-141 CE-144 SOP#

Activity Uncertainty Cone 2 Sigma MDC Units Run#

Aliquot Aliquot Reference Count Volume Units Date Date 2007 2007 2007 2007 2007 2OO7 2007 2007 2007 2007 2007 2007 2007 2007 2007 2007 2007 2007 2007-1.59E-01 7.13E-02 1.28-K411 7.2i1F,1 6.78E-02 7.661-02 1.20E-01 11.5-Z41 6.95F,02 6.871-01 1.13"1-

. 7AI-M02 6.79F,02 3.06F-01 9.411-02 2.411-01 1.47E44)i 1.32F,01 3.60F,01 6.7-8E+00 ptv/g-pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g KpCi/g p1/g__

pCi/g pKite pCi/g pCi/g pCi/g pCi/g pCi/g 67.14 67.14 67.14 67.14 67.14 67.14 67.14 67.14 67.14 67.14 67.14 67.14 67.14 67.14 67.14 67.14 67.14 67.14 g wet 04/05/12 12.M0 g wet 04/05/12 12.00 g wet 04/0541212:00<

g wet 04/05/1212-00 gwet 04/05/12 12:00 g wet 04/05/12 12:00 gwct 04/05/12 12:00 g wet 04/05/12 12:00 g wet 04/05112-12.00 g wet 04/05/12 12:00 g wet 04/05412 12:00 gwet 04/05/12 12:00 g wet 104/05/12 12:00 1wet 04/05/12 12:00 g wet 04/05/12 12:00 gwet 04/05/12 12:00 g wet 04/05/12 12:00 gwet 04/05/12 12:00 04/12/12 04/12112 04/12/12 4/12/12 04/12/12 04/12/12 04/12/12 04/12112 04/12112 04/12/12 04112/12 04/12/12 04/12/12 04/12112 04/12112 Count Time 6000 60 6000 600 6000 6000 6000 6000 6000 6O0 6000 6000 6000 6000 Count Units Flog Values Sec U

S

-c U

Yes Sec U

No

-U -

No Sec U

No Sec

+

Yes S§=

U No Sec U

No Sec U

No Sec U

No Sec

-U No Sec U

No Sec U

No Sec U

No Sec U

No Sec U

No Sec U

No Sec U

No Sec U

No-04/12/12 6000 EU-152 RA-226 T11-228 U-235 U-238 04/12112 04/12/12 67.14 67.14 67.14 g wet g wet 04/05/12 12:00 04/05/12 1200 04/05112 12:00 04/1112 W411-2/12 6000 6000 6000 6000 Flag Values U

=

Conpouud/Analyte not detced (< MDC) or less than 3 sigma

+

=

Activity concentration exceeds MDC and 3 sigma; peak identilied(gaunma only)

U*

=

Ccmnpotd/Analyte not detected. Peak not identified, but flrced atvity cancentrakio exceeds MDC and 3 sigma High Activity concentration exceeds customer reporting value Spec

=

MDC exceeds customer technical specification L

=

Low recovery H

=

High recovey Bolded text indicates reportable value.

Page 24 of 24 No

= Peak not identified in gammna spectrum Yes = Peak identified in gamma spectrum

        • Unles otbcrwisc noted, the analytical results rted ae reldated only to the samples tested in the condition they we received by the laboutoy.

MDC - Minimum Dctcctablc Cocemnration

I ( I Cl Q Ci Q m

Page:

I of 4

1R%

Project#: MLIC LVI 008 4

Name:

Chris Higgins I Rich Holm COC Number "': COC-UI-03 F.3 E

Stree:

190' M*RL 104 S Goodlwin AVE City/StalrLip:

Urbana. If. 61901-2902 Excellence-Every project. Every day.

Phone:

203-565-3272 ENERCON P.O.C:

Coey DeWitt 412-889-3124 e-mail.

4 Sample Analysis Requested (s (Fill in the number of containers for each test)

Project/Site Name:

University of Illinois e-mail:

1hr0,ihi:r h

aac.A'nl o.m

  • .1 1!

<-. P vaive Type (3) i Address:

190N MRL 104 S Goodwin AVE Urbana, IL 61801-2902 U

C m t Collected by (print/sign):

Chris Higgins C

Note: extra sample is eic s-ti

.required for sample Sample ID ZkQ-specific QC

/,'or postes - indicate start and stop date imee (um-dd-yy)

(Idani)

Q 1

SS-RRF-O01

/

04-05-12 i2:00 N

so Y

N I

X No drying or grinming SS-RRF-002 7

04-05-12 12:00 N

so Y

N I

X X

X No drying orgrindin SS-RRF-003 04-05-12 12:00 N

SO Y

N I

X No drying or grinding SS-RRF-004 si 04-05-12 12:00 N

SO Y

N I

X No drying or grinding SS-RRF-005 04-05-12 12:00 N

SO Y

N I

X No drying or grinding SS-RRF-M5 J

04-05.12 12:00 N

SO Y

N I

X X

X No drying or grinding SS-RRF-007 04-05-12 12:00 N

SO Y

N I

X X

X No drying or grinding SS-RRF-008

/

04-05-12 12:00 N

SO Y

N I

X No drying or grinding SS-RRF-009 04-05-12 12:00 N

SO Y

N I

X No drying or grinding SS-RRF-OI0 1

04-05-12 12:00 N

SO Y

N I

X No drying or grinding TAT RequestedL Normal:

X Rush:

Specify:

E-mail Results:

cs)

/

No Circle Deliverable: CofA I QCSummary I 1-vell / Level2 / Level 3 / Lcve14 Remarks: Normal TAT is defined as 30 days by Q233.

5SmLC o

Time Zone Egn Pacific central Other Mountain Chain or Custody Signatures Sample Shipping and Delivery Details R7R By(Signed)

Date Time i

ved by (signed)

Date Time Laboratory PM:

2 2

Airbill C 3

3 Airbill 0:

i.) t.

or mody Number -*S ;rocdq.

hor Lab Receivig Use Only 2.) QC Codes: N - Nonmal Sample, T1 Trip Ba* FD - Field Duplicate. £S Equaimea Blark. MS ý Matix Spike S

sli le, MSD Matix Spike Duapit G

Sampie, G - Grab, C - CoLmposile 3.) Prm*e*vati Type: HA - Hydrochlouic Acid, NI = Nitric Acid, Sit = Nodim Hydroxide. SA S*uifivic Acid, AA - Ascorbic Acid, LX - Hexame, ST Sodium Thiosufilne Woo pri rvotive is added - leave field blankh Cusiod'eal Intact?

4.) Nsiubi Codes: DW-Drinkbig Water GW-4Cqmodwatee. NW-Surface Wale. WW=Waste Water, W-Warer. ML -Misc Liquid, SG-Soid, Sfl-Sedimort SL.'Sludae. SS=Solid Waste 0-0dL V'iieer. P-wipe. iJ=Uirne, F-Fecal, N-Nasai YES N'O Cookr Temp:

5.) Sample Analysis Requeited Analytical meothd rquested (i.e, 82605, 601Ot7470A) aWd number ofoetainers provided for each (ue. 82608 -3, 60108 7470.4 - I).

Project#: MLIC LV008 Name:

Chris Higgins / Rich Holm COC Number "': COC-UI-03 F

3J E

Street:

190tN MRL 104 S Goodwin AVE Cproject.

Every day CityState/7zp:

Urbana. IL 61801.2902 Excellence-Every pPo:

203-565-3272 ENERCON P.O.C:

Corey DeWitt 412-889-3124 e-mail:

d Sample Analysis Requested (Fill in the numbcr of containers for each test)

Project/Site Name:

University of Illinois e-mail:

chrtsto1nhi IliŽgŽi)Lc3,lhj 11 I

<- Preservative Type (3)

Address:

19ON MRL 104 S Goodwin AVE Urbana, IL 61801-2902 U

C

.3 K

Comments Collected by (printisign):

Chris I iggins

_____1

~Note:

extra sample is

-Date Collected

'Time Collected z

eurdfrsml Sample ID isme 1tuaJy) QC cc, specific QC For cOmpomes-Idicare stoy and stop date

(-e-dd-yy)

(bai4 I

I I

I I

SS-RRF-OI I J,

04-05-12 12:00 N

SO Y

N I

X No drying or grinding SS-RRF-012 1

04-05-12 12:00 N

SO Y

N I

X No drying or grinding SS-RRF-013 1

04-05.12 12:00 N

SO Y

N I

X X

X No drying or grinding SS-RRF-014 1

04-05-12 12:00 N

SO Y

N I

X No drying or grinding SS-RRF-O15 J

04-05-12 12:00 N

SO Y

N I

X No drying or grinding SS-LAF-001 J

04-05-12 12:00 N

SO Y

N I

X X

No drying or grinding SS-RCF-001 04-05-12 12:00 N

SO Y

N I

X X

No drying or grinding 00N SS-BCT-W 04-05-12 12:00 N

SO Y

N I

X X I No drying or grinding SS-BCT-NW 04-05-12 12:00 N

SO Y

N 1

X X

No drying or grinding SS-BCT-NE 04-05-12 12:00 N

so Y

N I

X X

X X

No drying or grinding TAT Requested: Normal:

X Rush:

Specify:

E-mailResats:

( )

No Circle Deliverable: CofaA QC Summary / Level1 I Level2 / Level3 / Level4 Remarks: Normal TAT is defined as 30 days by Q233.

Sanmole Collection Time Zone Eastem Pacific Central Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Details y (Signed)

Date Time Rý by (signed)

Ti/

Laboratory PM:

I

%&_'~ <;P t

5ac-.

3

/

v

'~

s' Method ofShipmcm Date Shilpd 22 Airbill #:

3 3

I.I Chain ot Cusody Number - See Procedure For Lab Receiving Use Only 2.) QC Codes: N - Normal Sample. 3 = Trip Blsh. FD - Field Duplicate. ED - Equipment Blank MS - Marix Spike Sample. MSD - M0stx Spike Duplicate Sample. C-Grab, C Composite 3.) Prescrvatve Type: HA - Hydrochlorc Acid, NI-1 Nitric Acid. SH - Sodium Hydroxide. SA ýiSluic Acid, AA = Ascorbic Acid, lIX = Hexane, ST = Sodium "rioulia. Ifn preservaiwve is added = leave fiedd btmk Custody Seal Intact?

4.) M;a,,, Codes-DI-Drinking Waler, GW-G*...dwa.e..

SW-Su. rAe WSW.r,

-*Wa_,e water, W=Waser. ML-Misc Liquid. SO-Soil, SD-Sediment. S.-Sludge...- Solid Wsateý 0-Oil, F-Filter, P-Wipe, U, Urine, F-i*-eu, N-Nasal YE.S NO Cooler Tern 5.) Sample Analysis Requested Analytial metbod requested (i.e. 52603. 6010174"70A) and number of containers provided for each (ic 82608.-3, 60108;7470A. I).

Pap 3

of 4

Project #: MLIC LVI 008 Name:

Chris Higgins I Rich Holm COC Number "': COC-41-03

.3 E

Sir:et:

190N MRL 104 S GoodWn AVE City/State)Zip:

Urbana, IL 61801-2902 Excellence-Every project Every day.

Phone:

203-565-3272 ENERCON P.O.C:

Corey DeWitt 412-889-3124 e-mail:

cxk",i'., ci*.ca,?txa,-

Sample Analysis Requested (' (Fill in the number of containers for each test)

Project/Site Name:

University ofIllinois e-mail:

Jirq,.opihi a aLj.,

£ec.mi w

I I

I I

<-- Preservative Typc (3)

Address:

190N MRL 104 S Goodwin AVE Urbana. IL 61801-2902 Bn Collected by (print/sign):

Chris Higgins N

extra Co ampments I

~

.~Note:

extra sample is eo T required for sample

'Date Collected

  • Time cteaW zape*S**fcQ Sample ID (MIary)h

)

QC Code specific QC For compo*sies -indicate stai and stop dateime (m-dd-yy) 04-)

Madrnt' SS-BCT-E Y

04-05-12 12:00 N

SO Y

N I

X X

X X

No drying org rinding SS-WTF-001 04-05-12 12:00 N

SO Y

N I

X X

No drying or grinding SS-NrF-001 1

04-05-12 12:00 N

SO Y

N I

X X

No drying or grinding SS-NTF-002

/

04-05-12 12:00 N

SO Y

N I

X X

No drying or grinding SS-RRF-007 (Duplicate) 04-05-12 12:00 N

SO Y

N 1

X No drying or grinding UI-BS-001 04-05-12 12:00 N

SO Y

N I

X X

X X

No drying or grinding UI-BS-002 M

04-05-12 12:00 N

SO Y

N I

X X

X X

No drying or gnnding UI-BS-003 04-05-12 12:00 N

SO Y

N I

X X

X X

No drying or grinding

/1 J,

0051 12:0 N

so N

I___Ndiornn UI-BS-O04 0

04-05-12 12:00 N

SO Y

N I

X X

X X

No drying or grinding

,/

UI-BS-005 04-05-12 12:00 N

SO Y

N I

X X

X X

No drying or grinding TAT Requested: Normal:

X Rush:

Specify:

E-mailResuRIs:

y

/

No CircleDeliverable: CofA / QC Summary / Level I Level2 / Level3 / Level4 Remarks: Normal TAT is defined as 30 days by Q233.

sanie Collection Time Zon Eastern Pacific CaIL Other

_Mountain Chain of Custody ýi'patures Sample Shipping and Delivery Details Signd) ate Tim

~

b (ssae) ~Time ReMIigne)

Di Tire 31 Daw imeLaborator PM:

I 1-I 4

ý_ 1

,0b t

1 I

P, OvC MediodofShia t-iDate Shipp:

2 2

Aibill #:

3 3

.Airbill 0:

I.) ClaIm of Custody Num er =See Procedure IFor Lab Receving Use Only 2.) QC Codes: N = Normal Sample. Ta - Trip Blan, FD - Field Duplicate. [3N Equipmem Blank, MS = Matrix Spike Sample. MSD, Matrix Spike Doplicate Sam*e. G - Umrab.

C = Composite 3.) Preservatie Type: HA - Hy.&dorlc Acid. NI - Nitric Acid, SH - Sodium Hydroxide. SA - Sulfiwic Acid, AA - Axucit Acid, HX - Hexmw. ST Sodium Thimalfse. If an prelnativme is added = leae field blank Cuody Seal Intact?

4.) Matixi Codes DW-Drtisking Waters.

GW-Gromnsdwaier, SW-Stulact Water hW-Waste waiter. W-Waser. ML-Miac Liquid. SO-Sol SDeSdsmemt.

SL-Shudge. 555obid Wasic, (Y-61. F-Fulter. ?'-Wtpe. [J=Uie, F-Fera, N=N&Wn YES NO Cooler Temp:

3.) Sample Analysis Requested Aunlytical method requested (.e. 826011 6010 1/7476A) and aumber ofecmaineirs provided for etb (i.e. 142608 - 3, 6010&-7470A. -I).

Project #: MLIC LVI 008 Nam:

Chris Higgins / Rich Holm COC Number "': COC-UI-03 Street:

19ON MRL 104 S Goodwin AVE City/Stale/Zip:

Urbana, I. 61801.2902 Excellence-- Every project. Every day.

Phone:

203-565-3272 ENERCON P.O.C:

Corey DeWit 412-889-3124 e-mail:

4kv'u rrcrii,.a Sample Analysis Requested ( (Fill in the number ofcontainers for each test)

PrejWct/Sitc Name:

University of Illinois e-mail:

.4 1--

i, ( V--1 i 1 L--

Note-extra1------

<-- Preservative Type (3)

Address:

190N MRL 104 S Goodwin AVE Urbana, IL 61901-2902 SCm et Collected by (print/sign):

Chris Higgins No:etrsapei

  • T~

~I F

required for sample Sample ID (military)

QC C specific QC For campiwwies - indicate stalr and slop date time (sm-Y)l-yy (liw-)

Mr 43hfuQ UI-BS-006 17 04-05-12 12:00 N

SO Y

N I

X X

X X

No dying or grinding UI-BSR-001

"'04-05-12 12:00 N

Y N

I X_________

U1-BSR.002 0 4-052 12:00 N

Y N

I X

TAT Requested: Normal:

X Rush:

Specify:

E-mail Results:

(

I No Circle Deliverable: C ofA / QC Summary / Level I / Level 2 / Level 3 / Level 4 Remarks: Normal TAT is defined at 30 days by Q233.

Snamle Collection Time Zone Eastern Pacific Central Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Detail epiid sined)

Date Time Rt edl b~y (signed)

Date Time Laboratory PM:

1 I

Method-f Shipment:

, aeSbhip 2

2

-Airbill 3

3 Airbil 0:

L) Chain of Culody Number - See fteedu For Lab Receiving Use Only

2) QC Codes: N - Normal Sample. Ta - Tnp Bhmb. tFD - Field Duplicate, ED - Equipment Btlak, MS Matrix Spike Sample. MSD = Matrix Spike Duplicule Sample. G - CDrb, C - Composite 2.) Pieservative Type: HA = Hydroclori Acid. NI = Nilt Acid. SH - Sodium Hydroxide, SA - Sulfusic Acid, AA - Ascorbic Acid, 1X -=texas., ST - Sodium Thiesulfue, If no peservae is added - leave field blark Custod Seatl Intact?

4.) MVaim Codes: VWDW-O~iuSk Waler. GW=3rowidwaier, SW'Smufaee Water. WW-Waste Water. W-Walee, ML Mlfsc Liquid. SO-Soil, 5D-'5edimnusi SL=Stiud*. 5SS-Sotid Waste. O-Oil, F-Tiher, P-Wipe. tl-UJrne F-l'eeal, NmNasal YS Nvo Cooler Temp:

5.) Suvmle*A.ialysms Requestedrt Analytical method requ"ed (Le. 826011. 6I4011747OA) &ad nuanber of comamers provided foe each (i.e.

260H - 3, 60109 7470.4 - I).

04/10/12 13:05 Teledyne Brown Engineering SR/#:1SR3:099 Sample Receipt Verification/Variance Report SR #:

SR30991 Client:

Enercon Services, Inc.

Project #: EN005-3EREGUOI-12 LIMS #L49994 Initiated By:

JSIMMONS Init Date: 04/10/12 Receive Date:

04/10/12 Notification of Variance Person Notified:

Contacted By:

Notify Date:

Notify Method:

Notify Comment:

Client Response Person Responding:

Response Date:

Response Method:

Response Comment Criteria Yes No NA Comment 1 Shipping container custody seals present NA and intact.

2 Sample container custody seals present NA and intact.

3 Sample containers received in good y

condition 4

Chain of custody received with samples Y

5 All samples listed on chain of custody Y

received 6

Sample container labels present and y

legible.

7 Information on container labels y

correspond with chain of custody 8

Sample(s) properly preserved and in NA appropriate container(s) 9 Other (Describe)

NA For Hazardous Materials Only:

10 Paperwork shows TBE and shippers name, NA address and phone number 12 Paperwork shows sample quantity NA information

4W TELEDYNE W

BROWN ENGINEERING, INC.

A Tedf, e Tohmosogio Cmpany 2508 Quality Lane Knoxville, TN 37931-3133 865-690-6819 Chris Higgins Enercon 4490 Old William Penn Highway Murrysvillc, PA 15668 Report of Analysis/Certificate of Conformance 06/28/2012 LIMS #:

Project ID#:

Received:

Delivery Date:

P.O.#

Release #:

SDG#:

L50878 ENOOS-3EREGUOI-12 06/26/2012 06/28/2012 PER RECEIPT This is to certify that Teledyne Brown Engineering - Environmental Services located at 2508 Quality Lane, Knoxville, Tennessee, 37931, has analyzed, tested and documented samples, as received by the laboratory, as specified in the applicable purchase order.

This also certifies that requirements of applicable codes, standards and specifications have been fully met and that any quality assurance documentation which verified conformance to the purchase order is on file and may be examined upon request.

I hereby certify that the above statements are true and correct.

k~I/~ --.

Keith Jeter Operations Manager Clienti 1

__)

uI-BS.Fi-Ul-BS-F2 UI-BS-WW UI-B3S-NW Cross Reference Table Laboratory ID StationI applicable)

L50878-1

[ L50878-2 L50878-3 S L50878-4 Method Reference Numbers Knalysis Matrix Method Refrence S

GAMMA EPA 90 1.1 Page 1 of 6

qLW TELEDYNE BROWN ENGINEERING, INC.

A Teledyne Technrobes Company 2508 Quality Lane Knoxville, TN 37931-3133 865-690M6819 This report shall not be reproduced or distributed except in its entirety.

Page 2 of 6

Report of Analysis 06/28/12 09:42 L50878 Enercon EN005-3EREGUOI-! 2 APl qTELEDEYN BROWN ENGINEERING, INC.

A Tk* @usT-mobgtOmm ap Sample ID: UI-BS-FI Station:

==

Description:==

LIMS Number:

L50878-1 Collec Stairt: 06/25/2012 12:00 Collect Stop:

Receive Date: 06/26/2012 Matrix:

Soil Volume:

% Moisture:

(S)

B&-7 K-~40 ZN-65

,V-95 R/U-1-03 RU-106 1-131-CS--134-t§S-37 BA-140 CEi-4 1 Cfi-144 EU-152 T-228

[I1-132 I-235

-:238 Activity Uncertainty ActitCoy 2 Sigma MDC Units

-~2007 2.15F-01 PCi/g 2007 S.33E+0O 5.25E-01 pCi/g 2007 3.102 pCi/g-

-T

!s2.33E-02 pCi/g

-12007 T

S.42E-02 pýcilg 2007 ý pCi/g 2 0 07 T-6-

6.54F,02 pCi/-

2007+

14.73E-02 pCi/g 2007

.52E-0ipCi/-

2007 2.370E-OI pCi/g 2007 I

-m 2007

<.9

-- 2 pCi/g 2007 1.03..- 1 pCi/g 2007

_ _8<

3ASE-02 pCi/g pCi/g 2007 11.7&E-01 4.58E1 E-2 jC/

ý2007 1.SKO 4.33E-0 pCi/g

-~~~~~

07 219-1 861 2

pci/g 2007

i.,72&el-T pCi/g-

-207~

I 38+0

ý/

Run[

Aliquot Aliquot Reference 01 Volume Units Date Count Count CountI Date Time Units I 1

199.31 19931 199.31 I 193-31 199.31 199.31 199.31 199.31 I-993-1 199.31 199.31 199.31

- 199.31 199.31 199.31 199.31 19433 1 199.311 199.31 g dry 06125/12_12:00 06/27A2 i2982 Sec

-Ul g dry 06/25/1212:00 06/27/12!

12982 Sec

_*+

_I gdry 06/25/12 12:00 06/27/12 12982 Sec jitu~

__gdlTy 06/25/12 12:00 06/27/12 12982 Sec I

+ g dry 06/25/12 12:00 O6/27It12 12982 See U

gdry 06/25/12 12:00 06/27/12 12982 Sec U

g"i-d 0605/1291200 06/27/12 1 29 Se-UI2 g dry 06/25/12 12:00 06/27/12 12982 Sec gdry 06/25/121200 N027/12 12982 Sec UV g dry

ý06125/12 120 06/27/12 -

129k2 tSc U

gdry 06/25/12 12:00 06/27/12 12982 Smc g dry 06/25/12 12:00 06/27/121 12982V Sec U

g dry 06125/12 12:00 06-.--/12 128_S g ry 062v-fIE66 06/27/12 12982 Sc g dry 06/25/12 12:00 06/27/121 12982 Se U

g dry 06/21212:00 06/2/W12' 2982 S.c U

g dry 02 12:00 06/27/12 2122 Sec T g dry 06/25/12 12-00 106/27/12 12982 Sec j +

g dry 06/25/12 12:00 106/27/12 12982 Sec

-9gdz 06/25/1212MOO 6612f/121 _2982 Yes Yes%

No Flag Values U

=

U*

f Ut.s

=

hligh Spec

=

L

=

H

=

Bolded test CompoundiAnalyte not detected (< MC or less than 3 signm Activity conceatration exceeds MDC and 3 sigma pea identifled(gamma only)

CompoundAnalytc not detected. Peak not identified, but forced activity conntrdion exceeds MDC and 3 sigwm Activity conccntatio, exceeds customer reporting value MDC exceeds customer technical specification Low recovery Iligh recovery No =Peak not identified in gmmna spectrum Yes = Peak identified in gamma spectnum

... Unless otherwise noted. the analytical results repole re related only to the samples tested in the condition ihey are recived by the laboratory.

MIX - Minimum Detectable Concentration t indicates reportable value.

Page 3 of 6

Report of Analysis 06/28/12 09:42 L50878 Enercon EN005-3EREGUOI-12 Ajq111TELEDYNE BROWN ENGINEERING, INC.

A1I4U I *TIClfOt Conpayw Chris Higgins Sample ID: UI-BS-F2 Collect Start: 06/25/2012 12:00 Matrix:

Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 06/26/2012

% Moisture:

LIMS Number:

L50878-2 Radionucide SOP#

BE-7 2007 WK-40

.2007 MN-54 2007 634-5 2I 0-0-7 ftE-59 2007 C-60 2007-ZN-65 2007 ZR-95 i200 i0U-t03 2007 RU-16

.200W7 11-131 2007 CS-137

, 2007

[BA-I4O-007 CE-141 2007 EU-52 I2007 RA-226 2007-

[U-235 --

2007-U-238 12007 Activity IUncertainty Conc 2 Sigma MDC 2.32F-01 6.31E-t00 6.42E-01

~6.59E-02 1.60E-01 3.01E-02 6.19E-02 5.45E-O2 2.87"-2 3.04&-02 2.70F-02 2.59E-01 3.94E-02

<~_

1.13E-1

~

3.65-02

&.IOE.02 SJ39R0I0 4.68E-01l 2.47E-01 3.72E-02 I."9E01

-7.896-02ý T

1-.64-E-61ij

~

3-19E+00 Units

-pCi/g pCi/g

_-PCi/

pCi/g pCi/g9 pCi/g9 pug

_Pci/g, pCi/g pCi/g pCi/g

-- pCL/g pCi/g

-pC~iig pCig pCi/g Run Aliquot Aliquot Reference Count TCount Count I Volume Units Date Date Time Units Flag Values f 19227*~g dry 06125/12 12:00 06/27/12 12981.

sc U L No 192.27 1gdy 06_2511212:00 106/27M12 12981 Sec 4

NYes 192.7 gdry_

06W25/12 12'00 062/12 12981 Sec U

No 192.27 g-dry 06/25/12 12:00 0

06/27/12 12981 Sec

--U No 192.27 gdry 06/25112 12:00 06*27/12 12981 Sec U

No 192.27 g-dry 06/25/12 12:00 06/27/12 12981 Sec No 192.27 ig-dry 06/25/12 12:00_.06/27/12 12981 See U

No 192.27 9

gdy'06/25/12 12:001 06/27/12 12981 Sece U.

NONo 192.27_

gdry _-065/l-22.:00b 06/27/12

- 12981 i.Sec No 192.27-1 gdry 06025/12 12:00 06/27/12 12981 F Sec

-U No

  • 192.27 g dry 06/25/12_12:00-[

12_

12981 See

+.

No 192.27 1 gd, 06/25/12 12:00 *06/27/12 12981 Sec U

No P9-2.274 gdry 40"9125/12 2:00 06/27/1 1298 Sc

+

Ys 192.7 gdry 0409512 E200i0/71 128 Se UN 192.2ý7 g-dry 06/25/1 2

00Y6/2-7112 12981-

-Sec

-U N6o 192.27 gdciy 06/25/1212:00 06/27/12 12981 Sec U

I-No 192.27 06 125/ 12_ 42:00 06/2.7/12 12 81 Se e

+

J 192.27 g dry 06/25/12 12:00 06/27/12 12981 Se_

U --

Yes 1.0127 dry 06/25/12 12:00 1 06/27/12 12981 M SI

+

Yec

.. 192.27 g dry 06/25/12 12:00 06/27/12 12981/

Scc-

+

-1 SYe 192.27 g dry_06/25/12:1200 06127/12 129811 Sec U

No 192.271 gdry 06/25/12 12:00 06/27/12 12981 Sec

+U N

I L

Flag Values U

=

Compound/Anaile not detected (< MDC.) or less than 3 sigma

+

=

Activity concentration exceeds MDC and 3 sigma; peak identified(gamma only)

U*

=

Compound/AnalrC not detected. Peak not identified, but forced activity concentration exceeds MDC and 3 sigma High

=

Activity concentration exceeds customer reporting value Spec

=

MDC exceeds customer technical specification L

=

Low recery H

=

High recovery No = Peak not identified in gamma spectrum Ye

= Peak identified in gamma spectrum

        • Unless otherwise noted, the analytical results reported are rdated only to the samples tested in the condition they we received by the laboratory.

MDC - Minimum )etectable Concentration Bolded text indicates reportable value.

Page 4 of 6

Report of Analysis 06/28/12 09:42 L50878 Enercon TELEDYNE kBROWN ENGINEERING, INC.

A Taoym Tuhn*W" Comrpan Chris Higgins EN005-3EREGUOI-12 Sample ID: UI-BS-WW Collect Start: 06/25/2012 12:00 Matrix: Soil (S)

Station:

Collect Stop:

Volume:

==

Description:==

Receive Date: 06/26/2012

% Moisture:

LIMS Number:

L50878-3 Radionuclide 6 E iMN-54K CO-60 IRU-106 F1--131_

CS-137 ij Ba-140 CE-IM1 EU-l152 U-_2 j_5

"- 38 CcI A

I r

S U

IRu.n Aliquot Aliquot Reference 10P# Ac Unerai]

Units Volue Units Date Coa 2 Sim 120 1.9

-gr 0/5-12 12 T-2 2.88E-01 pCi/g I

201.96 g

dry 0&6 5/12 I.N04 F 2007 6.E-456004 7.34E pCiEi 2671.-

g dry 06/25/212 2007 3.74E-02 pC_/

201.96 g dry 06/25/1212:01 2007

< z 1

2 9 -E42 pCi/g 261.9_

i gy

-06/25/12 12:04 27 7X1-02 pCi/g 2 201.96 Igdry 06/25/12 12:04

  • 4I09 -0F

_c-

-a--

2007

-7 p:i/g 201.96 dry 06_25/12 12:0.

---*o*7v "f

1. 4-o-.o

- -i -

20.9 lV 1-11:a,2 2007 201.96 g dry -06/Z52 1204 200 5.69"E-02 pCi/g 201.96 g dry 06/25/12 12:04 20.9 g..

Jr-Ooi.l 1--2 1

i -02:

-2007 3.51E-02 pCi/g 201.96 gdry 06/25/1212:01 2007 pCi/g

-0 201.96 g dry 0625/12 120 Vý2007 4.02E,02 pCi/g9

- 1.6 g dry 06/25/1,2 12:0 r162007

_ 23.4-8F-02 8PCi-0" 201.96%

gdy 06/25/12 12:04 3.44E-2 p/

dry W25/12 12:04 2007 1.27E-01 pCi/g 201 96

-dry 6-/25/12 12:i S2007

~-J 3

pCi/g 201.96 gdsy 106/25/12 12"0.

P2007 42.301:O pCi/g 201.%

g dry 0.6/25/12 12.01 07 1.8 6.8

-01 I

,_ ~

200 l18+00 6.8E0lpCi/g 201.96 g dry 06/25/12 12.)

_20607-2394-F-,4 5.51E-02_

-Pai/g-~

20196 g dry 06/25/12 120) 2007 2.671:41 71 68E-02 pCi/g 201.96 gdiy 4 6/25/12 12:0 2007

~

2.56E41~pig 201.%

g dry 06/25/12 120) 2007

<j

.E-4600 pCi/g 20NO1:96

_g-dry 106/5/1-212:04(

Count Count Count Date Time Uniths Flag Values 6/27/ 12 12978T SecU-14-06_27/12 129782 Sec

+

Yes 0

06/27/12 12978 Sec U

No 06/27/12-12978 Se U

No' 06/71/12 12978 Sec U

-No

  • 7*---i*

f-u -

No --

106/27/12 12975 Sýec U_

IN 06/2-7/12 12978 Sec U Nmo 3027/12, 12978~ Sec UJ No 6~06/7/12 12978 e

i47t 0j6/27/1 2 12971 See Ui No1 3

06/27/12 12978 Sec U

-No 3

06/27/12I 12978 Sec U

I No 306/27/12 127icc U-o 6W 06271 2 i 129-78 Sec 4U

-No 306/27/121 129-78 Si-U No 06127/12 129784 Sec IU No 306/27/12{

12078+~c I

6

/ 7/~j1278 Soc

+

yes 06&27/121 12I9_78 1Sec

+

Yes.

F &ýW/i12 81 47-+/-1 Yest 306/27/12 12978 Sc 1-W 62711229_78i SwcUI7N-0 Flag Values U

Como*und/Analyte not detected (< MD) or less than 3 sigma

+

=

Activity wonentration exceeds MDC and 3 sigma; peak identified(gamma only)

U*

=

CompoundlAnalyte not dctected. Peak not identified, but forced activity concentration cxcecds MDC and 3 sigma High Activity concentration exceeds customer reporting value Spec MDC exceeds customer technical specification L

Low recovery H

High recovery Bolded text indicates reportable value.

Pagec5of 6 No = Peak not identified in gamnam spectrum Yes = Peak identified i gamma spectrum

      • Unless otherwise noted, t1e analytical results reported are related only to tie samples tested in the condition they ar received by the labonatory.

MDC - Minimumn Detectable Concentration

Report of Analysis 06/28/12 09:42 L50878 Enercon EN005-3EREGUOI-12 TELEDYNE JIM BROWN ENGINEERING, INC.

ATs~hme T~c-W-C-haiaCw Chris Higgins SI I

I_

T pCi/-g -_- -

182.09 g dry 06/25/12 00:00 pCi/g dr 06ý25/2_00:*00 pNi/g 182.09 gdry 106/25/1200.00 pCi/g 182.09 g cry LO6/2S/12 00:00 pCi/]

182.09 g-dry 06/25/1200:00

.209 g dry

!06/25/12 00:00 pcI/

gdr 06/25/12 00:00 pCi/g 182.09 g dry 06/25/12 00:00 1pCi/g

-82.09 gdry

!06/25/12 00:00 pCi/g

+

182.09 gdry 106/25/1200b00-p/g182.09 g-dry

-i66a 5/12 00:00

~ pii ~ -h 182.09 g dry b6/5/I2 00:00

~ p~r/g --

18.0 g

rn L--

pCi/g 182.09 gdry

[o6/25/12 00:00 pcvig 1 4-82.09 g-dy [06/2/12 00:00 pcP F: 182.09 gd dry

["

-/12 00:00 p ~-/

182.09 gdry_

06/25/12 00:00 pCi/g

~

182.09 g dry 06/25/.12 00:00 SpCi/g

_182.09 g dry 06/25/12 00:00 Flag Values U

=

Compound/Analyte not detected (< MDC) or less than 3 sigma

+

=

Activity concentration exceeds MDC and 3 sigma; peak identified(gamma only)

U

=

Compound/Analyte not detected. Peak not identified, but forced activity concentration e"ceeds MDC and 3 sigma High

=

Activity concentration exceeds customer reporting value Spec MI)C exceeds customer technical specification I.

Low recovery I!

=

High recovery Bolded text Indicates reportable value.

Page 6 of 6 No

- Peak not identified in gamma spectrum Yes = Peak identified in gamma spectrum 0*00 Unless otherwise noted, the analytical results reported ate related only to the samples tested in the condition they ae received by the l*antory.

MDC - Minimum Detectable Concentration

L ~c?~'

Page I

of I~

Project N: MLIC LVI 008 Nne:

Chris Higgins / Rich Holms COC Number...: COC-Ul-06 E

N E

Street:

190N MRL 104 S Goodwin AVE CityiStatctZip:

trbana, IL 61801-2902 Excellence--Every project. Every day.

Phone:

203-565-3272 W A 3c.

ENERCON P.O.C:

Corey DeWitt 412-889-3124 e-mail:

ý.tdsAitt a, cn.r,qt.gAmlj Sample Analysis Requested (' (Fill in the number of containers for each test)

Project/Site Name:

University of Illinois e-mail:

_hrt r

Ul

<- Preservative Type (3)

Address:

19ON MRL 104 S Goodwin AVE Urbana, IL 61801-2902 AuI 1

'a Comet SComments Collected by (print/sign):

Chris Higgins Note: extra sample is

'Daue Collected

  • Time Collected Sampeuiedfrleml Sample ID

'..111 Mrl 4

Q C specific QC h'ar composites - indicate start and stop date time (tm-d&yy)

(hmw) j UI-BS-FI 06-25-12 12:00 N

SO Y

N I

X UI-BS-F2 06-25-12 12:00 N

SO Y

N I

X U1-BS-WW 06-25-12 12:00 N

SO Y

N I

X UI-BS-NW 06-25-12 0:00 N

SO Y

N I

X TAT Requested Normal:

Rush:

X Specify:

ASAP F-mail Results:

Y*

/

No CircleDeliverable: C ofA QC Summary / Levelt / ILvel2 / Level3 / Levd4 Remarks:

1Samle Collection Time Zone Eastgn Pacific Central Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Details

)"

Date Time Received by (signed)

Date Time Laboatory PM:

I__________________________

1__________________________Method of Shi DaeShippd 2

2 Airbill #:

3 3

Airbill #:

1) i of Cu Number - Sele Prceue

]or Lab Receiving Use Only 2.) QC Codes-N - Normal Sample, -"B - Trip Blank, FD = Field Duplicate. EX - Equipment Bflak, MS - Matrix Spike Sample, MSD = Matrix Spike Duplicate Sample, G - Grab, C - Composite 3.) Preservadve Type: HA - Hydochloric Acid. NI - Nitric Acid SH - Sodium Hydroxide, SA = Sulfufic Acid. AA Ascorbic Acid, fix - tilcm, ST - Sodims Thiosltate, Btan preservative is added - leva field blank Custody Seal Intact?

4.) Multi, Codes: DW-Drinking water. GW Groundwater, gw-Surface water WW=Waste Water, W-Wuler, N4L-Misc Liquid, SO-Smd. SD-Sedime.u. SL-Slmidg, SS-Solid Waule, 0-0i. F-kilter, P--Wipe. VU4Jroe, F4ecai. N-Nasal YES NO Cooler lemp.,

5.) Sample Analysis Requested: Analytical method requested (i.c. $260B. 6S1011'/470A) and snumber of contain provided fot each (i.e. 8260B -3, 60108'7470A. I).

06/26/12 08:29 Teledyne Brown Engineering Sample Receipt Verification/Variance Report SR #:

SR31803 Client:

Enercon Services, Inc.

Project #: EN005-3EREGUOI-12 LIMS #L50878 Initiated By: JSIMMONS Init Date: 06/26/12 Receive Date:

06/26/12 Notification of Variance Person Notified:

Contacted By:

Notify Date:

Notify Method:

Notify Comment:

Client Response Person Responding:

Response Date:

Response Method:

Response Comment Criteria Yen No NA Comment 1

Shipping container custody seals present NA and intact.

2 Sample container custody seals present NA and intact.

3 Sample containers received in good Y

condition 4

Chain of custody received with samples Y

5 All samples listed on chain of custody Y

received 6

Sample container labels present and Y

legible.

7 Information on container labels Y

correspond with chain of custody 8

Sample(s) properly preserved and in NA appropriate container (s) 9 Other (Describe)

NA For Hazardous Materials Only:

10 Paperwork shows TBE and shippers name, NA address and phone number 11 Paperwork shows sample quantity NA information

Name Location SS-RRF-001 Rx Floor SS-RRF-002 Rx Floor SS-RRF-003 Rx Floor SS-RRF-004 Rx Floor SS-RRF-005 Rx Floor SS-RRF-006 Rx Floor SS-RRF-007 Rx Floor SS-RRF-008 Rx Floor SS-RRF-009 Rx Floor SS-RRF-010 Rx Floor SS-RRF-011 Rx Floor SS-RRF-012 Rx Floor SS-RRF-013 Rx Floor SS-RRF-014 Rx Floor SS-RRF-015 Rx Floor SS-LAF-001 Loading SS-RCF-001 Cage SS-BCT-W Beam SS-BCT-NW Beam SS-BCT-NE Beam SS-BCT-E Beam SS-WTF-001 Water Tank SS-NTF-001 N16 North SS-NTF-002 N16 South SS-RRF-007 (Duplicate)

UI-BS-001 Biosield UI-BS-002 Biosield Ul-BS-003 Biosield UI-BS-004 Biosield UI-BS-005 Biosield UI-BS-006 Blosield UI-BSR-001 Biosield Rebar UI-BSR-002 Biosield Rebar UJ-BS-FI Floor I MOO00 ORISE#5 UI-BS-F2 Floor 2 M0002 ORISE #7 UI-BS-WW West Wall M0008 ORISE #8 Eyebrow UI-BS-NW North Wall M0009 ORISE #20

4F

I 0

0 0

1'~>

5, 0

1" o

0 I..--

~43

~I I.

'I 1.1 t

I-I' 0?j S.