ML20138P455
| ML20138P455 | |
| Person / Time | |
|---|---|
| Site: | Comanche Peak, 05000000 |
| Issue date: | 04/19/1984 |
| From: | Arnold J IMPERIAL PROFESSIONAL COATINGS |
| To: | |
| Shared Package | |
| ML20138M609 | List:
|
| References | |
| FOIA-85-59 759, NUDOCS 8511070165 | |
| Download: ML20138P455 (13) | |
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- TECHNICAL REPORT NUMBER 759 I. TITLE
! E1cometer Adhesion Tests l Nucac Concreta Costing Repair Systems 11S/1201/11S/1201
, Ils/1201/11/120L ,
1 FOR I Preparation for: Comanche Peak Nuclear Plant I Clan Rose, Texas i
) CUSTOMER i -
- i Submitted by
- Jerry Arno' "
l l Accepted by: i Approved:
Date: g///[/f SOUTitERN IMPERIAL COATINGS CORPOR ATION. INC.
P. O. Box 29077
- New Orleans Louiusna 70lM's
{ Plione: (504) 254 143.1 8511070165 051016
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Introduction:
Following the installation of the 11S/1201 concrete coating system.
_it sometimes becomes necessary to repair damaged areas or fill holidays in the original system. Also separate applications sometimes result in overlap of the newly applied coatings to -
adjacent, aged systema. The result is the application of Nutec 115 or 11 over previously applied and cured 1201 topcoat. The purpose of this adhesion teac is to demonstrate the validity of this practice.
Procedures: Concrete blocks measuring 2x4x2" were coated with the following
. systems:
A] Nutec 115 (10 mils)
. Nutec 1201 (3 mils)
Nucac 11S (10 mils)
Nutec 1201 (3 mils)
B] Nutec 115 (35 mils)
Nutec 1201 (16 mils)
, Nutec 11S (35 mils)
. Nutec 1201 (16 mils)
Cl Mutec 115 (10 mils)
Nutec 1201 (3 mils)
Nutec 11 (3 mils) v Nutec 1201 (3 mils)
D] Nutec 115 (35 mils)
Nutec 1201 (16 mils)
Mutec 11 (20 mils)
Nutec 1201 (16 mils)
The dry film thicknesses applied were selected to envelope the ,
thickness range actually applied at nuclear jobaites. For application and curing details refer to the attached panel preparation sheets.
Six adhesion tests were conducted on each system (two tests per concrete block) using an E1cometer adhesion teater.
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Ave. Mode of System PSI Tailure -
115 (10 mils)/1201 (3m11s)/115 (10 11s)/1201 (3 mils) 313 100% Concrete ils (35 mils)/1201 (16 ails)/115 (35 mils)/1201 (16a11s) 337 75% Concrete 25% 11S(1st Co4 ils (10 mils)/1201 (3 mils)/11 (3 mils)/1201 (3 mils) 325 85% Concrete 7% 115 8% Clue 115 (35 mils)/1201 (16 m11s)/11 (20 mils)/1201 (16 mils) 313 85% Concrete 15% 11S Conclusiones. All pulla exhibited concrete failure and surpeesed the minimum 200 PSI values required by ANSI N5.12.
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p f * 'i-; TEST FANEL FREFARATIO'N DATA - ll_,. . . e
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- 1. PRODUCT TO BE TESTED: htec IIS/htee 1201/hr c its/htec 1201 - .;
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.. 2. TYPE SUBSTRATE: concrete .
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- 3. SURFACE PREFARATION (Describe): All surfaces limhtiv virabrushed en r.=ava efflorescence and/or I l
laitance, followed by a 80 PS!.cnepressed air blow down. . I: , [ '
- 4. PRODUCT DATA: SAMPLE NO. (s) : -.
6151. 6152. 6153 ,
- . 3. DATE AND TIME CURING CONFOUNDED OR PRIMER AFFl.IED: N/A ,
t. AFFl.ICATION CONDITIONS THICKNESS TIME & DATE !. PRODUCT ' PRODUCT CODES . BATC11 # HETil0D , R/H(*F) 2R.ll. (ins.) APPLIED i I. COAT 1 Nutec ' IIS 4286/4287/4288 Squeegee 69/86 12.3 4/2/84 k 1 l' L. 2 Notec 1201 4284/4285 Spray 68/62 3s7 4/5/84 J r; E '4 3 Mutec IIS 4286/4287/4288 Squeegee 69/67 , 12.1 4/7/84 ' 4 4 Mutec 1201 4284/4285 SPray
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- TEST PROCEDURE: Eleometer f e_esion .
e , TEST PREFORHED BY: Imperial
- DATE SusHITTED: 4-17-84
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I REPORT WUHSER 759 APPROVED BY: - r l'
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TEST PANEL PREPARATI0N' DATA , i I. PRODUCT TO BE TESTED: Mutec IIS/Nutec' 1201/Nutec 11S/Nutec 1201 e FN
- 2. TYPE SUBSTRATE: concrete . ;8 All surfacen lightly wirehrushed to remove efflorescence and/or . .-
- 3. SURFACE PREPARATION (Describe):
Iaitance, followed by a 80 PSI compr,essed air blow down. ,
- 4. PRODUCT DATA: SAMPLE NO. (s) 6154, 6155. 6156
- 8
- 5. DATE AND TlHE CURING COHPOUNDED OR PRIMER APPL.IED: N/A PRODUCT APPLICATION CONDITIONS TilICKNESS TIME & DATE '
COAT PRODUCT CODES BATCil # HETilOD , R/H(*F) IR.H. (ine.) APPLIED Nutec 11S 5 9 "**E**
- 1 4286/4287/4288 69/86 37.5 4/2/84 .
2 Nutec 1201 ~ 4284/4285 S Pray 4.3 68/62 4/5/84 Nutec Squee[ee 69/67 11.2 4/7/84
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- AMBIENT TEMP. 6n - inn *F REL. IlUHIDITY 40 - so I HINIHUH CURE 8 DAYS PFST PROCEDURE: E1cometer Adhesion ; I 1' REST PREFORHED BY: 1.e,remi
- DATE SUBHITTED: 4/17/84 ,
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.PPROVED BY /y M N REPORT W1418ER 759 ,
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- 3. _
SURFACE PREPARATION (Describe): All surfaces 11ehtiv utrehr- ' ' to r =ve'effinr .r nr. - 'lar .,.. . laitence. folic:;;' by a 80 PSI comorJased air blau h. ,.
~
.4 d j
- 4. F3000CT BATA: SAMPLE NO. (s) 6157, 6158, 6159
- 5. DATE Alm TIME CURIIIG COMPOUBIDED OR PRIMER APPLIED: N/A PRODUCT APPL.ICATICII CONDITIONS THICENESS TIME & DATE COAT PRODUCT CODES BATCH # HETIIOD R/M(*F) IR.H. (ine.) APPLIED
- o. ,
1 Netec - 115 4286/4287/4288 Squeesee 69/86 . 12.2 4/2/84 -
~2 Notec 1201 4284/4285 Spray 68/62 .
4/5/84 3 IIntec 11 4290/4292/4293 Squeegee 69/67 , 4.5 4/7/g4 4* Notec 1201 4234/4235 Spray 74/74 3.5 4/9/g4 ;; tj r.; I. i
== .
' ~
A I) CMllIG COISITICIIS: AMBIEllT TEMP. 60 - 100 *P REL. IRGIIDITY 40 - 80 I MINIHL4t CURE 8- DAYS . FEST N r unc - rer = sam l <. 3' TEST FREPORMED BY 18Perial eDATE SUstflTTED: 4/17/84 ! I ; 1 --0 j WF30tED BY - REPORT NUMBER 759
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i~ . TEST PANEL PREFARATIOIl DATA . [t l 1t
,~
- i. 1. PRODUCT TO BE TESTED: Ihetac 1islmrac 12n1/ me., 11/ hrac 12nt -
t a -
' s ;I .2. TYPE SUSSTRATE: Concreta .
s
,. - 'sa I, ~ '
All surface. it.hriv wireb'uad to remove affiar. r
!l 3.
SURFACE PREPARATION (Describe): - - ya
'E
, Imitance, followed by a 80 PSI comerJ-- ' air hiau J - '
T ~ ll . - tc g .-u
- 4. PRODUCT DATA: SAMPLE NO. (s) 6160. 6161. 6162 -
; jl
. e ..
- 5. DATE AIS TIME CURIIIG CONFOUNDED OR PRIMER APPLIED: as/A 1
APFt.ICATION CONDITIONS TNIC300ESS TIME & DATE i PR060CT i COAT PRODUCT CODES BATCH # HETil0D , R/H(*F) 2R.M. (ine.) APPLIED I I Ilutec Ils 4286/4287/4288 - Squeegee 69/86 36.0 4/2/84 ,. I
.e
'I 2 Ihatec 1201 4284/4285 Spray 68/62 17.4 4/5/84 Ihstec 4290/4292/4293 Squeeg'ee 69/67 21.9 4/7/84 ). 3 II 4 Ihatec 1201 4284/4285 Spray 74/74 16.8 4/9/84 i' l! ..
. 1 l; -
i j jCURIIIC CONDITICIIS: AMBIENT TEMP. so .' n on *F REL. HIStIDITT 40 - 80 I HININIM CNRE 8 DAYS TEST PROCEDURE: mi,_rar * * .a t t+ .
- t
' rrial *DATE SUSHITTED: sit 71as -
l TEST PREPORMED BT ' ! d ;: # REPORT WIM8ER 759 v , F < lAPPDOWEDBY - i f* h j
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- TECHNICAL REPORT 1 . .
.'I .
NUMBER . .
~~
.353-41
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M r TES"I' FEDGRAM.TO EVAIRATZiDIA FII2M2fABCI'
. cF. ovms cm.:sc sTsTzus (CatacI.IIz/IsrEx:AO i
- Ra sEAVER val.I.Er tarI 2.
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STUEE AND WERSTER 3 G M ttad by: GEIAI.:1 E. A330Z3 N j Aymd o==: 20EEIr 1. THIct- ,y f g
= == = a.. n at N SCUIBERN DIFERIAI. COATINGS CORPORATION, INC. . .
- P Ce aos 29077,
- New Orla a. Lommaa 70189 Phams: (504) 254 1433 .
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- ] T41 TERT ynnanAnt TO ETALHAZE DEA FER20mfA33 l1 0F OTEEL&P CDAZZ3E ST5 Tiles (CA130LINE/ IMPERIAL)
. 7 3.IIATER VAZZZZ W ZZ Z !
.s
-;. . / INDEI i '
Sect 1os Fase
- IEIREBOC:205 l' . 1-1 f
*C SIDEE'& EEISTER. TEST SFICIMER FIEFAEAZIDE 2 3-12
.?5 PsocIDas .
' STW E 4rBERSTER TESE SPEC 2EEE FREFAEAZ:DK 13 - 115 M.- r DATA 3
* (EIC EADIATION/DIA FROCEDUEEE & . 116 - 111 .
4
- . . . EADIAZ:cs AED nak IEEULT5' 5 -
119 - 131. . 1CD . . 1-
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h.4. -% sccyr: Se purposer of this test was te eTainata the DBas perforsmane of t carbolins/ Imperial sized syscams for use at Beaver Yanny 1 - Beclear Flant. Systems to be tasted ars: ,
- _.. m -
A1: cz-n/191 i
, al cz-n/ist/1201 ; c1 cr-n/1201 . . ;. D] cz-n/1201/191-11 c1-n/us/11/1201 -.
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- MAfTERf1BWl g t
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-- Se above systems are possible overlap combinations at Beaver,,,,, ,,,,, - - , , . Ta12my 7"=11y os staal imbeds. Most staaL imbeds at the- , ; project arm. already ea=*=d with carbolina's c1-11 primer or r e
' c2-n topcoac with #191. sham the adjacent comarote is coated .
.I with Imperial's 113/n/1201 system. some of tha coated. imbeds.
are overlapped. , , Ther tase specimens were ,. . - : under the direc" .: :1-
- and webstae by. painters at the seaver Vaney Protest. The . ;, coated. -r- d- werer them. submittad. to Imperial. Imperial coordinated. the tasting activistas at CIEL. The sosk was . .' ?
V'
'- mathetized. by- Stone and.sebsters Purchase. Order i E24476 .
s * ' e , .=
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1- SUtafAIT.0F RESULTS:. , , _ 2 A n test g - ' - were. irradiated to 2.66.x 10 7 rada and tham-
' DBA tasted with anzimum temperature and pressura paraantars of
- j. ,
340*F anst 70 752G respectively. AD. penals perforand in accord-
' anos with the acceptaase critaria. of AESI M101.2.
~
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Fw'Me': I,t The test spesiaans wars fabricated, asuk coated at the Beaver 1 Yellay Esalaar 21 ant in Shippir.g;;.. Pa. Seation.I of,this .. , ~ ~ .5 report canzadas- the Stone and webster ,c c. for test speci-7 maay., = h . Tha specific penal preparation, data can be- ...n... m found la Sacsima 3'. It describes tha costing applicattaa personned by senart Faiattag under the servainance of Stona. :- 2.r-j
. and sebster geslity control. The coated spestaans ==== anosed
*! to cura and then. sera shipped to Imperial aa=M "Te. coordi- .
! antica of the tasting activistas was.perforand by T----d=1 ..
- thronsh its contract with SEL. Anchorization of this tasting -
program wee ande by' Stone and Webstar per Purchase O.r.~de.r -- . #E2,4476..
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_G w.v. M_ m-X. . . i rese program To avaluate DEL M Oc ovenia, coating systems. (carbo 11as/v----*-1). i '-. For Beagwz Valley Unit 2 . ], y - . Pasa 2 i , g gggg 7 emste 4 3333 ggbgitted to Oak E.1dge 4=e4rwi=1 I. abo-9 ratorias.Where- Wert esposed 20 a.Cumalative radiation. *
! dose of 2.64r r 10 rada and-than DBA tastad. Tha test was
$ designed to be subdestad to - tamperature and. pressure U
of 280*F a d 45 PSIG respectively. Boeuver. during the test . i . a sedden. surge in theos parameters resultad in a =-4=== s
. -_ r -- of 340*7 and 4. =-4==
pressure of 70 PSIG. Tha " " '
"y tamparature/ pressure spike- lasted, for only 1.5 minutes. T5e a
initial 28-hours of the DEA tasted were performed,in the mata-
. clave. The r===4=4=g.11 daye were conducted sa a constant '
t' ,.-p e chamber at- 130*7 and' 100Z EI. ,' - T- C- -- --
'l IISULTS: .
4 . 1; . The case results, section 5.. describe the.eand4e4= of tha 'a---t
- following, 'W_i=ttaa thee again an tha~end of DEA tasting.
~ -
i,* CDWCLU52 DES: . The- testad syscame met the acceptance critaria of ABII ET.12- - [! (.
.? .( radiaciar toleranca). and AEsr 310I.Z. CDEA t---<a9. Two-
- & defects-(unacceptabla.per AESI) were.notad.on penals 4-1-4-2 and 4-3-4-4 along the coacfag overlap area whers.the repair coating-sus tied. into the previsualy applied syntae. Some minor ==---=*d- uns oca---d==. at this incarface prior to j -h-4 ,,.mi og the panels.to OIEL. This n - rf= can ba 7 attributed to the taping method used to apply the repair coat -
3 ing and tha 1--eh of tian the tape was. alloemd to remaine on.
..- the panels 11 hem the spesiamas warm reenived by T.gerial
': / ther tape was still intaar aloes the edges of the 3.4. and 4A series. The tapias reemitad. La high millages along the tape-
",y
$ line solvest aserspuest, and azposed repair , .; . Some of the repair system began.to peal back a short distanca from
'I the tape.line shnathe tapa was removed. As a consequence of
.li ehamar observations, the staar defects.noted on peals 4-1-4-1 and. 4-3-4-6,. should be ignored g - -+ =117 since. the I d a 4 = =-
*j; four panels- 4-5-4-4, 4-1&-4-2A, 4 * * ' ' ' and. 4-5Ar4-4A., ezhthitad
; no-defects.
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.i Manufacturer: Isoortat Analyticai Chemistry Otvistas
' Gak Ridge National Laboratory-Date: October- 29, 1981
.d i "} ,
New Orleans, Louisiana f
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. . . .,,. - .. e.:-.
~
ST5 tdt IDENTIFICATION , x Steel panel Concrete bTock v
.i. CI-11/1201/191 ,
1 CI-u/1201- . j 9 1 D8A TEST
.i- . .. . . .. . e . ..;,
f ORNL Mastar Analytical Manual Method No. 2 0922. :- .. *-:"- 13U5. Log Book No. A9675 A10-8-1 . -- Sample.No. DBA chase Test results . 1,. . - - . ,
-je s- . . .c . . : . . :
~v Front: . Coatings intact,' ner defects.aftar' spray
- 3-1-3-E c ?..
. *j . one day. Blisters #6 , few, at coating - -
interphase and weld area at ens ef-tast r., Rear: Coatings intact no. defects. after
. one day. 811starr, #6 few., at coating'.
g; interphase and welt. Acaa_at. and..of. test. J.i. .' ~3-3-? ' spray
- Front: Coatings intact,. no defects. after- ' - - -
.; __ ane da2 Blisters, #6 few, atyeid area: 7'
.~- . o at end of test. - -
. Rearr Coatings intact, no defects after .
one day. 811 stars. #6 few,. insert area at and of tast. : e ..
.4 3-5-7-6 sprey* Front:
one day.. Coatings. intact, few..no defects area. after and , '. ~.
.~ .
. . Blisters,. 74 weld ~ -
.. ., . ... .. costing interphase at end of-tast.c -- - -
Rear Coatings. intact, no.,defectr'aTT * - ~-
.. / ,,
areas
.: s. . c
- Irradiated.
~
c Evaluated M . Approved . E -
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4- .- . .e .: . o
.g '4 Page 131. .- .> : s.
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- s. :
smount OF REstETS ---
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,T . .Ill C - M / u GI. lla Defacts - -- - - --
i, _ .... .
, 1/3 c-11/120I Mor Defacts . ... . . . .. .. .. . ,. '.j 2/1. c-u/us/u/uC1 #8m .
- 2/r c-n/us/u/uC1 -
#8u.
2/3 c-u/us/u/120r Tuir--
+.. .
3-1-3-2. c- u/1201 c-n/1201/191 M at coating interphase and weld are
. 3-3-3-4 c-u/120b c-n/1201/191. Mrveld area 2
3-5-3 c-u/I20I. c-n/1201/191 MF wald aras (front only) 4-1-4-2, C-II/19b C-11/191/1201 MinEf saijiiifattan at. coating interphas
.* , 4-3-4-A c-u/19L C-u/191/1201 One large'b1'ister ou 4-3 - -
. 5 . ..
. s. - 4-5-4-4 c-11/19 b C-11/191/1201 No Defacts. . . . . .. .
c-11/191. c-11/191/1201 "a. , 4-1A-4-2A No Defacts. - ( en. 4-34-4-4A c -11/19 b C-n/191/1201 No Def~ects : . ,
~ --
4-5A-4-4A c -11/191. C-n/191/1201. No Defacts . . 9 - - 1 , o , . . . .
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