ML20080P561

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Change 2 to Procedure CP/O/A/8100/05, Chemistry Procedure for Determination of Chloride (Manual Method)
ML20080P561
Person / Time
Site: Catawba  
Issue date: 12/03/1982
From: Chaust R, Mcafee C, Tuckman M
DUKE POWER CO.
To:
Shared Package
ML20080P419 List:
References
CP-O-A-8100-05, CP-O-A-8100-5, NUDOCS 8402220583
Download: ML20080P561 (2)


Text

(

', Form SPD-1003-2 a

s DUKE POWER COMPANY (1)

ID No: CP/0/A/8100/05 PROCEDURE MAJOR CHANGE Change No:_

2 PROCESS RECORD Permanent / N W N (2)

STATION:

Catawba (3) PROCEDURE TITLE: Chemistrv Procedure for the Determination of Chloride (Mnnuni Method)

(4)

SECTION(S) 0F PROCEDURE AFFECTED: 3.1 and 3.2 (5) DESCRIPTION OF CHANGE:

(Attach additional pages, if necessary.)

See Attachment (6) REASON FOR CHANGE:

Procedure Improvement (7) PREPARED BY:

/M DATE:

(8)

SAFETY EVALUATION This change:

Yes No y

Represents a change to the station or procedures as described X in the FSAR, or a test or experiment not described in the FSI Yes No Requires a change to the station Technical Specifications?

Yes No X Involves an unreviewed safety question?

If the answer to any of the above is "Yes", attach a detailed explanation.

As appropriate attach a completed " Nuclear Safety Evaluation Check List" form.

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By:

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_ Date:

DATE:

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(9)

REVIEWED Y:

Cross-Disciplinary Review By:

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(10) TEMPORARY APPROVAL (IF NECESSARY):

By:

(SRO) Date:

By:

Date:

4 DATE:

I1 (11) APPROVED BY:

(12) MISCELLANEOUS:

l Reviewed / Approved By:

Date:

Reviewed / Approved By:_

Date:

(13) Page 1 of 2

8402220583 840215 PDR ADOCK 05000413 E

PDR Rev 14 9/20/77 l

Attachment I CP/0/A/8100/05 Change Section 3.1 to read:

Ferric, Nitrate, (10%)

Dissolve 100.0 1 0.1 g of reagent grade Ferric Nitrate (Fe (NO )3 9H 3

2 in 120 + 1 ml of domineralized water. Add 750 + 1 ml of concentrated Nitric Icid (HNO, sp. gr. 1.42).

Dilute to 1000 i 1 al with demineralized 3

water. This solution is stable indefinitely.

Change Section 3.2 te read:

Mercuric Thiocyanate, (0.3%)

Dissolve 0.750 1 0.001 gofMercuricThiocyanate(Hg(CNS)2)in25011al of reagent grade methanol (CH 0H). Allow to stand for at least 24 hours2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br />.

3 Filter & store in an amber reagent bottle. Do not use if more than 4. weeks

'old.

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