ML19095B374

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W6H-IMC-2120-S-P-8

ML19095B374
Person / Time
Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
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References
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Text

• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2120\\W6H-IMC-212 Report Generated On : 4/19/2017 10:44:22 AM Sample Title : W6H-IMC-2120-S-P-8 Sample Description :

Sample Identification : 2120-S-P-8 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.500 keV Sample Size : 2.579E+002 grams Sample Taken On : 3/17/2017 12:00:00 AM Acquisition Started : 3/30/2017 8:02:26 AM Live Time : 1800.0 seconds Real Time : 1800.3 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 3/24/2017 Efficiency Calibration Used Done On : 4/19/2017 Efficiency ID : H-IMC-2120-S-P-8

Peak Analysis Report 4/19/2017 10:44:22 AM Page 1

• • • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W6H-IMC-2120-S-P-8 Peak Analysis Performed on: 4/19/2017 10:44:17 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts M 1 294-315 299.69 75.14 0.71 7.06E+001 23.54 1.03E+002 m 2 294-315 308.67 77.38 0.71 6.17E+001 21.17 7.70E+001 F 3 737-746 742.37 185.87 0.83 5.47E+001 18.53 3.50E+001 F 4 946-960 953.72 238.74 1.05 7.64E+001 21.53 5.81E+001 F 5 1175-1184 1178.57 294.99 0.75 2.25E+001 13.52 3.30E+001 F 6 1398-1411 1405.36 351.72 0.93 4.76E+001 17.06 4.06E+001 F 7 5825-5850 5837.10 1460.30 2.36 1.52E+002 23.52 5.78E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 4/19/2017 10:44:22 AM Page 2

• • • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W6H-IMC-2120-S-P-8 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.981 1460.82* 10.66 9.11939E+000 1.60867E+000 Pb-212 0.998 74.82* 10.28 5.71934E-001 2.22878E-001 77.11* 17.10 2.93774E-001 1.16872E-001 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 1.96799E-001 6.36230E-002 300.09 3.30 PB-214 0.997 74.82* 5.80 1.01370E+000 4.05311E-001 77.11* 9.70 5.17890E-001 2.11241E-001 86.83 1.70 87.35 2.24 89.78 0.82 241.99 7.25 258.76 0.53 274.80 0.35 295.22* 18.42 1.68407E-001 1.04737E-001 351.93* 35.60 2.21423E-001 8.57799E-002 462.02 0.21 480.43 0.34 487.14 0.43 533.66 0.18 580.14 0.37 785.96 1.06 839.07 0.58 Ra-226 0.993 81.07 0.20 83.79 0.32 186.21* 3.64 1.36595E+000 5.17469E-001

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.500 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 4/19/2017 10:44:22 AM Page 3

• • • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.981 9.119393E+000 1.608669E+000 Pb-212 0.998 2.077902E-001 5.490612E-002 PB-214 0.997 2.068877E-001 6.336285E-002 Ra-226 0.993 1.365945E+000 5.174691E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

• • • • • • • • • • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 4/19/2017 10:44:17 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified.

Nuclide MDA Report 4/19/2017 10:44:22 AM Page 4

• • • • • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W6H-IMC-2120-S-P-8 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 9.027E-001 9.03E-001 9.119E+000 3.703E-00 CO-60 1173.23 99.85 1.825E-001 1.59E-001 -1.205E-001 8.406E-00 1332.49 99.98 1.594E-001 5.304E-002 7.169E-00 CS-137 661.66 85.10 1.419E-001 1.42E-001 4.094E-002 6.594E-00 Pb-210 46.54 4.25 2.568E+000 2.57E+000 3.536E+000 1.230E+00 BI-212 288.20 0.34 1.815E+001 2.15E+000 -3.362E+000 8.535E+00 328.03 0.13 5.832E+001 2.711E+001 2.749E+00 452.98 0.36 2.393E+001 -4.016E+000 1.116E+00 727.33 6.67 2.147E+000 1.765E+000 1.003E+00 785.37 1.10 1.224E+001 -2.122E+000 5.663E+00 893.41 0.38 3.429E+001 -1.990E+001 1.565E+00 952.12 0.17 9.597E+001 -1.154E+001 4.447E+00 1078.62 0.56 3.223E+001 6.716E+000 1.493E+00 1512.70 0.29 5.897E+001 6.055E+000 2.641E+00 1620.50 1.47 9.868E+000 3.386E+000 4.290E+00

+ Pb-212 74.82* 10.28 4.041E-001 1.17E-001 5.719E-001 1.911E-00 77.11* 17.10 2.072E-001 2.938E-001 9.717E-00 86.83 2.07 2.469E+000 2.040E+000 1.185E+00 87.35 3.97 1.201E+000 -8.219E-001 5.746E-00 89.78 1.46 2.948E+000 -5.139E+000 1.405E+00 115.18 0.60 5.383E+000 1.222E+000 2.526E+00 238.63* 43.60 1.166E-001 1.968E-001 5.479E-00 300.09 3.30 1.974E+000 -6.388E-001 9.294E-00 BI-214 76.86 0.55 1.251E+001 2.93E-001 2.127E+001 6.050E+00 79.29 0.91 5.899E+000 5.001E-001 2.830E+00 89.26 0.11 4.133E+001 1.914E+001 1.974E+00 89.81 0.21 2.049E+001 -3.573E+001 9.764E+00 273.80 0.13 4.811E+001 5.106E+000 2.270E+00 348.92 0.10 9.457E+001 1.153E+001 4.515E+00 386.78 0.29 2.459E+001 -1.141E+001 1.146E+00 388.89 0.40 1.881E+001 -7.829E+000 8.783E+00 405.72 0.17 4.547E+001 6.263E+000 2.119E+00 454.79 0.29 3.133E+001 -4.889E+000 1.466E+00 469.77 0.13 6.883E+001 -9.771E+000 3.212E+00 609.32 45.49 2.927E-001 6.419E-002 1.377E-00 665.45 1.53 8.115E+000 2.910E+000 3.776E+00 703.11 0.47 2.459E+001 -2.147E+001 1.133E+00 719.87 0.39 3.468E+001 -3.368E+001 1.616E+00 752.85 0.13 1.132E+002 4.192E+001 5.281E+00 768.36 4.89 2.772E+000 8.406E-001 1.285E+00 786.35 0.32 4.331E+001 8.894E+000 2.008E+00 806.18 1.26 1.131E+001 8.096E+000 5.248E+00

Nuclide MDA Report 4/19/2017 10:44:22 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram BI-214 821.18 0.16 7.994E+001 2.93E-001 4.212E+001 3.671E+00 826.45 0.12 1.106E+002 -1.237E+002 5.081E+00 934.06 3.11 4.937E+000 4.108E+000 2.279E+00 964.08 0.37 4.890E+001 3.207E+001 2.279E+00 1051.96 0.31 5.279E+001 -4.815E-001 2.431E+00 1069.96 0.27 5.780E+001 -2.417E+001 2.647E+00 1120.29 14.92 1.121E+000 3.923E-001 5.143E-00 1133.66 0.25 6.268E+001 -1.215E+001 2.857E+00 1155.21 1.63 1.051E+001 -1.200E+000 4.824E+00 1207.68 0.45 4.122E+001 -1.346E+001 1.898E+00 1238.11 5.83 3.475E+000 2.417E+000 1.609E+00 1280.98 1.43 1.218E+001 8.754E+000 5.554E+00 1303.75 0.11 1.615E+002 3.248E+001 7.343E+00 1377.67 3.99 3.883E+000 2.005E+000 1.735E+00 1385.31 0.79 1.962E+001 4.146E+000 8.768E+00 1401.52 1.33 1.246E+001 3.887E+000 5.601E+00 1407.99 2.39 6.830E+000 1.910E+000 3.066E+00 1509.21 2.13 8.012E+000 -3.257E-001 3.589E+00 1538.53 0.40 3.161E+001 8.396E-001 1.353E+00 1543.34 0.30 4.163E+001 1.106E+000 1.782E+00 1583.20 0.70 2.286E+001 -6.644E+000 1.012E+00 1594.75 0.27 6.076E+001 1.091E+001 2.688E+00 1599.37 0.32 4.294E+001 4.626E+000 1.858E+00 1661.27 1.05 1.085E+001 6.153E-001 4.498E+00 1684.01 0.21 6.597E+001 7.958E+000 2.840E+00 1729.59 2.88 5.027E+000 3.354E+000 2.164E+00 1764.49 15.30 1.284E+000 8.752E-001 5.752E-00 1838.36 0.35 4.075E+001 -8.089E+000 1.734E+00 1847.43 2.03 8.317E+000 1.970E+000 3.631E+00 1873.16 0.21 6.786E+001 -1.646E+001 2.887E+00 1896.05 0.15 8.627E+001 1.631E+000 3.578E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2293.38 0.31 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 7.162E-001 1.64E-001 1.014E+000 3.387E-00 77.11* 9.70 3.653E-001 5.179E-001 1.713E-00 86.83 1.70 3.007E+000 2.484E+000 1.443E+00 87.35 2.24 2.129E+000 -1.457E+000 1.018E+00 89.78 0.82 5.249E+000 -9.151E+000 2.501E+00 241.99 7.25 1.051E+000 2.000E-001 5.044E-00 258.76 0.53 1.075E+001 1.667E+000 5.068E+00 274.80 0.35 1.732E+001 -9.746E+000 8.172E+00 295.22* 18.42 2.207E-001 1.684E-001 1.002E-00 351.93* 35.60 1.637E-001 2.214E-001 7.555E-00 462.02 0.21 4.582E+001 4.333E-001 2.150E+00 480.43 0.34 3.055E+001 1.862E+001 1.435E+00 487.14 0.43 2.105E+001 -2.606E+001 9.795E+00 533.66 0.18 5.212E+001 -2.025E+001 2.415E+00 580.14 0.37 3.192E+001 2.105E+001 1.494E+00 785.96 1.06 1.307E+001 2.684E+000 6.059E+00

Nuclide MDA Report 4/19/2017 10:44:22 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 839.07 0.58 2.479E+001 1.64E-001 1.123E+001 1.148E+00

+ Ra-226 81.07 0.20 2.153E+001 7.97E-001 6.979E+000 1.022E+00 83.79 0.32 1.440E+001 -7.592E-001 6.876E+00 186.21* 3.64 7.969E-001 1.366E+000 3.646E-00 AC-228 89.96 1.90 1.077E+016 3.03E+015 -1.878E+016 5.133E+01 93.35 3.10 6.522E+015 3.752E+015 3.107E+01 99.51 1.26 1.358E+016 5.377E+015 6.415E+01 104.82 0.39 4.341E+016 -3.455E+016 2.051E+01 105.60 0.74 2.341E+016 -3.345E+015 1.107E+01 108.58 0.28 6.041E+016 -8.219E+014 2.854E+01 129.07 2.42 7.389E+015 -1.833E+014 3.496E+01 145.85 0.16 1.275E+017 8.130E+016 6.055E+01 153.98 0.72 2.719E+016 8.086E+015 1.288E+01 191.35 0.12 1.787E+017 1.798E+015 8.450E+01 199.41 0.31 7.177E+016 -1.650E+016 3.392E+01 204.03 0.11 2.056E+017 2.806E+016 9.720E+01 209.25 3.89 5.757E+015 4.890E+014 2.713E+01 214.85 0.76 2.820E+016 -5.120E+015 1.323E+01 270.24 3.46 7.935E+015 -1.932E+015 3.732E+01 278.95 0.16 1.948E+017 5.786E+016 9.213E+01 321.65 0.23 1.349E+017 -5.720E+016 6.317E+01 327.44 0.12 2.856E+017 1.433E+017 1.346E+01 328.00 2.95 1.176E+016 5.466E+015 5.544E+01 332.37 0.40 8.657E+016 2.786E+015 4.077E+01 338.32 11.27 3.029E+015 1.813E+015 1.423E+01 340.96 0.37 8.837E+016 -6.411E+016 4.138E+01 409.46 1.92 1.992E+016 -4.334E+015 9.307E+01 440.44 0.12 3.388E+017 5.156E+016 1.582E+01 463.00 4.40 1.065E+016 5.775E+014 5.003E+01 478.33 0.21 2.399E+017 1.505E+017 1.129E+01 503.82 0.18 2.660E+017 -5.154E+017 1.245E+01 508.96 0.45 1.447E+017 2.081E+017 6.887E+01 523.13 0.10 4.308E+017 4.341E+016 1.997E+01 546.47 0.20 2.530E+017 1.597E+017 1.181E+01 562.50 0.87 6.422E+016 2.508E+016 3.011E+01 570.91 0.18 2.940E+017 2.183E+017 1.373E+01 572.14 0.15 3.449E+017 5.874E+016 1.607E+01 583.41 0.11 5.220E+017 4.287E+017 2.448E+01 674.75 2.10 2.650E+016 -1.107E+016 1.226E+01 701.75 0.17 3.427E+017 2.283E+017 1.589E+01 707.41 0.16 3.789E+017 -3.107E+016 1.754E+01 726.86 0.62 1.106E+017 1.023E+017 5.171E+01 755.32 1.00 6.717E+016 6.342E+015 3.128E+01 772.29 1.49 4.497E+016 4.345E+016 2.090E+01 782.14 0.49 1.330E+017 -1.922E+016 6.158E+01 794.95 4.25 1.619E+016 -2.768E+015 7.526E+01 830.49 0.54 1.337E+017 8.132E+016 6.217E+01 835.71 1.61 4.330E+016 2.161E+016 2.008E+01 840.38 0.91 7.368E+016 1.301E+016 3.404E+01 904.20 0.77 1.130E+017 -6.826E+016 5.296E+01 911.20 25.80 3.578E+015 3.279E+015 1.683E+01

Nuclide MDA Report 4/19/2017 10:44:22 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram AC-228 947.98 0.11 7.234E+017 3.03E+015 1.644E+017 3.349E+01 958.61 0.28 2.884E+017 -2.930E+016 1.340E+01 964.77 4.99 1.666E+016 6.959E+015 7.752E+01 968.97 15.80 5.158E+015 2.730E+015 2.396E+01 1033.25 0.20 3.217E+017 6.815E+016 1.456E+01 1065.18 0.13 5.101E+017 -6.370E+016 2.313E+01 1095.68 0.13 5.194E+017 -5.631E+017 2.347E+01 1110.61 0.28 3.031E+017 -5.220E+016 1.402E+01 1153.52 0.14 5.741E+017 -2.390E+017 2.629E+01 1247.08 0.50 1.666E+017 -1.745E+017 7.612E+01 1459.14 0.83 2.427E+017 5.752E+017 1.164E+01 1495.91 0.86 8.099E+016 1.123E+016 3.561E+01 1501.57 0.46 1.660E+017 -5.264E+016 7.385E+01 1557.11 0.18 3.633E+017 -2.408E+016 1.572E+01 1580.53 0.60 1.188E+017 -1.176E+016 5.207E+01 1588.20 3.22 2.591E+016 1.236E+016 1.158E+01 1625.06 0.25 2.866E+017 1.193E+017 1.256E+01 1630.63 1.51 4.979E+016 2.243E+016 2.189E+01 1638.28 0.47 1.394E+017 -7.634E+016 6.003E+01 1666.52 0.18 3.045E+017 1.727E+016 1.263E+01 TH-230 67.67 0.38 1.267E+001 1.27E+001 -9.191E+000 6.008E+00 PA-234 742.81 0.11 1.284E+002 1.88E+001 6.604E+001 5.971E+00 766.42 0.32 4.196E+001 2.294E+000 1.943E+00 1001.03 0.84 1.880E+001 7.647E+000 8.656E+00 TH-234 63.29 3.70 1.594E+000 1.59E+000 1.935E+000 7.607E-00 92.38 2.13 2.102E+000 2.163E+000 1.004E+00 92.80 2.10 2.048E+000 1.025E+000 9.760E-00 112.81 0.21 1.534E+001 -6.805E+000 7.200E+00 U-234 53.20 0.12 5.224E+001 5.22E+001 4.084E+001 2.469E+00 120.90 0.04 9.181E+001 -1.729E+001 4.307E+00 U-235 72.70 0.12 4.993E+001 3.62E-001 1.879E+001 2.400E+00 89.96 3.43 1.254E+000 -2.186E+000 5.974E-00 93.35 5.54 7.669E-001 4.412E-001 3.654E-00 104.82 0.69 5.193E+000 -4.133E+000 2.453E+00 105.60 1.31 2.778E+000 -3.970E-001 1.314E+00 108.58 0.50 7.109E+000 -9.672E-002 3.358E+00 109.19 1.66 2.162E+000 8.959E-001 1.022E+00 140.76 0.20 1.948E+001 -4.908E+000 9.220E+00 143.76 10.96 3.620E-001 -3.191E-002 1.714E-00 163.36 5.08 7.596E-001 -2.479E-001 3.576E-00 182.62 0.39 1.387E+001 -8.112E+000 6.622E+00 194.94 0.63 7.194E+000 -4.229E+000 3.394E+00 202.12 1.08 4.570E+000 -1.573E-001 2.163E+00 205.32 5.02 9.600E-001 -5.461E-001 4.535E-00 221.39 0.12 4.230E+001 2.145E+001 1.995E+00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

4/19/2017 10:44:23 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2120\\W6H-IMC-212 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 9.12E+000 17.640 Pb-212 74.8 5.72E-001 38.969 2.906[50.634] 3.57 -0.654 77.1 2.94E-001 39.783 1.493[51.262] [ 0.508]

238.6 ^ 1.97E-001 32.329 1.000[45.720]

PB-214 74.8 1.01E+000 39.983 4.578[55.673] 4.93 -0.866 77.1 5.18E-001 40.789 2.339[56.254] [ 0.401]

295.2 1.68E-001 62.193 0.761[73.272]

351.9 ^ 2.21E-001 38.740 1.000[54.787]

Ra-226 186.2 ^ 1.37E+000 37.884