ML19095B368

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W6H-IMC-2120-S-P-6

ML19095B368
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Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
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Text

• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2120\\W6H-IMC-212 Report Generated On : 4/19/2017 10:42:30 AM Sample Title : W6H-IMC-2120-S-P-6 Sample Description :

Sample Identification : 2120-S-P-6 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.500 keV Sample Size : 2.522E+002 grams Sample Taken On : 3/17/2017 12:00:00 AM Acquisition Started : 3/29/2017 12:34:20 PM Live Time : 1800.0 seconds Real Time : 1800.3 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 3/24/2017 Efficiency Calibration Used Done On : 4/19/2017 Efficiency ID : H-IMC-2120-S-P-6

Peak Analysis Report 4/19/2017 10:42:30 AM Page 1

• • • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W6H-IMC-2120-S-P-6 Peak Analysis Performed on: 4/19/2017 10:42:25 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 179-192 185.93 46.68 0.73 6.52E+001 20.05 6.53E+001 M 2 287-314 291.13 73.00 0.67 3.44E+001 17.26 7.09E+001 m 3 287-314 299.58 75.11 0.68 1.06E+002 24.37 6.42E+001 m 4 287-314 308.58 77.36 0.69 6.78E+001 20.04 5.68E+001 F 5 356-363 360.36 90.31 0.26 2.43E+001 20.80 4.80E+001 F 6 736-749 742.41 185.88 1.06 8.38E+001 22.73 5.95E+001 F 7 947-958 953.13 238.59 0.89 9.34E+001 23.35 5.70E+001 F 8 1173-1185 1179.46 295.21 0.77 2.88E+001 13.45 2.86E+001 F 9 1400- 1422 1405.41 351.73 0.79 3.51E+001 15.30 5.75E+001 F 10 5826-5851 5837.09 1460.30 2.49 1.45E+002 23.26 1.59E+001 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 4/19/2017 10:42:30 AM Page 2

• • • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W6H-IMC-2120-S-P-6 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.981 1460.82* 10.66 9.46610E+000 1.71939E+000 Pb-210 0.999 46.54* 4.25 2.66556E+000 1.11458E+000 Pb-212 0.998 74.82* 10.28 9.04892E-001 2.76934E-001 77.11* 17.10 3.40734E-001 1.21880E-001 86.83 2.07 87.35 3.97 89.78* 1.46 1.32351E+000 1.16325E+000 115.18 0.60 238.63* 43.60 2.59440E-001 7.67851E-002 300.09 3.30 PB-214 0.854 74.82* 5.80 1.60384E+000 5.11388E-001 77.11* 9.70 6.00675E-001 2.21562E-001 86.83 1.70 87.35 2.24 89.78* 0.82 2.35649E+000 2.08122E+000 241.99 7.25 258.76 0.53 274.80 0.35 295.22* 18.42 2.33841E-001 1.15043E-001 351.93* 35.60 1.76429E-001 8.12369E-002 462.02 0.21 480.43 0.34 487.14 0.43 533.66 0.18 580.14 0.37 785.96 1.06 839.07 0.58 Ra-226 0.993 81.07 0.20 83.79 0.32 186.21* 3.64 2.25227E+000 7.20401E-001

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.500 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 4/19/2017 10:42:30 AM Page 3

• • • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.981 9.466100E+000 1.719389E+000 Pb-210 0.999 2.665560E+000 1.114580E+000 Pb-212 0.998 2.808098E-001 6.395169E-002 PB-214 0.854 2.045292E-001 6.389179E-002 Ra-226 0.993 2.252267E+000 7.204014E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

• • • • • • • • • • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 4/19/2017 10:42:25 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide M 2 73.00 1.9085E-002 50.26 Tol. U-235 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 4/19/2017 10:42:30 AM Page 4

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W6H-IMC-2120-S-P-6 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 1.516E+000 1.52E+000 9.466E+000 6.695E-00 CO-60 1173.23 99.85 2.066E-001 1.55E-001 1.131E-001 9.544E-00 1332.49 99.98 1.553E-001 -1.443E-001 6.888E-00 CS-137 661.66 85.10 1.759E-001 1.76E-001 3.984E-002 8.250E-00

+ Pb-210 46.54* 4.25 2.094E+000 2.09E+000 2.666E+000 9.918E-00 BI-212 288.20 0.34 1.961E+001 2.30E+000 6.357E+000 9.221E+00 328.03 0.13 6.209E+001 1.599E+001 2.924E+00 452.98 0.36 2.719E+001 -4.244E+000 1.272E+00 727.33 6.67 2.301E+000 2.821E-002 1.074E+00 785.37 1.10 1.192E+001 -3.669E+000 5.466E+00 893.41 0.38 4.243E+001 1.641E+001 1.959E+00 952.12 0.17 9.401E+001 4.953E+000 4.318E+00 1078.62 0.56 3.160E+001 3.626E+000 1.451E+00 1512.70 0.29 4.660E+001 2.063E+000 1.995E+00 1620.50 1.47 8.653E+000 -3.520E+000 3.624E+00

+ Pb-212 74.82* 10.28 3.418E-001 1.17E-001 9.049E-001 1.593E-00 77.11* 17.10 1.899E-001 3.407E-001 8.816E-00 86.83 2.07 2.844E+000 4.079E+000 1.369E+00 87.35 3.97 1.454E+000 1.156E+000 6.995E-00 89.78* 1.46 2.043E+000 1.324E+000 9.479E-00 115.18 0.60 5.986E+000 7.181E-001 2.817E+00 238.63* 43.60 1.166E-001 2.594E-001 5.456E-00 300.09 3.30 2.244E+000 1.841E-001 1.060E+00 BI-214 76.86 0.55 1.314E+001 3.41E-001 3.001E+001 6.354E+00 79.29 0.91 5.861E+000 9.017E-001 2.804E+00 89.26 0.11 4.971E+001 1.052E+001 2.387E+00 89.81 0.21 2.573E+001 -1.327E+001 1.235E+00 273.80 0.13 5.066E+001 -9.948E+000 2.387E+00 348.92 0.10 9.061E+001 -4.083E+001 4.299E+00 386.78 0.29 2.739E+001 -7.185E+000 1.279E+00 388.89 0.40 2.063E+001 -1.487E-001 9.647E+00 405.72 0.17 5.560E+001 2.059E+001 2.613E+00 454.79 0.29 3.373E+001 7.645E+000 1.577E+00 469.77 0.13 7.024E+001 -1.903E+001 3.263E+00 609.32 45.49 3.414E-001 3.240E-001 1.613E-00 665.45 1.53 9.826E+000 2.983E+000 4.608E+00 703.11 0.47 2.921E+001 2.536E+000 1.356E+00 719.87 0.39 3.796E+001 -1.236E+001 1.769E+00 752.85 0.13 1.140E+002 -4.013E+001 5.287E+00 768.36 4.89 3.161E+000 1.399E+000 1.471E+00 786.35 0.32 4.202E+001 -4.238E+001 1.930E+00 806.18 1.26 1.041E+001 -3.932E+000 4.761E+00

Nuclide MDA Report 4/19/2017 10:42:30 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram BI-214 821.18 0.16 1.006E+002 3.41E-001 7.812E+001 4.676E+00 826.45 0.12 1.301E+002 -6.597E+001 6.017E+00 934.06 3.11 5.807E+000 3.448E+000 2.698E+00 964.08 0.37 5.124E+001 4.657E+001 2.382E+00 1051.96 0.31 5.689E+001 -2.201E+000 2.618E+00 1069.96 0.27 6.643E+001 -1.653E+001 3.057E+00 1120.29 14.92 1.347E+000 2.322E-001 6.232E-00 1133.66 0.25 8.365E+001 5.684E+001 3.881E+00 1155.21 1.63 1.206E+001 -1.019E+001 5.558E+00 1207.68 0.45 4.260E+001 1.376E+001 1.953E+00 1238.11 5.83 3.948E+000 -9.251E-001 1.834E+00 1280.98 1.43 1.258E+001 -7.371E+000 5.706E+00 1303.75 0.11 1.712E+002 2.360E+001 7.763E+00 1377.67 3.99 4.679E+000 1.982E+000 2.115E+00 1385.31 0.79 2.178E+001 -7.128E+000 9.755E+00 1401.52 1.33 1.335E+001 3.732E+000 5.991E+00 1407.99 2.39 7.942E+000 3.208E+000 3.590E+00 1509.21 2.13 5.860E+000 -3.925E-001 2.475E+00 1538.53 0.40 3.321E+001 -7.935E+000 1.413E+00 1543.34 0.30 4.852E+001 1.528E+001 2.099E+00 1583.20 0.70 2.321E+001 1.767E+000 1.017E+00 1594.75 0.27 6.627E+001 3.413E+001 2.932E+00 1599.37 0.32 4.826E+001 7.373E+000 2.098E+00 1661.27 1.05 1.243E+001 -1.230E+000 5.204E+00 1684.01 0.21 6.953E+001 -8.126E+000 2.977E+00 1729.59 2.88 4.691E+000 -3.631E+000 1.965E+00 1764.49 15.30 1.498E+000 1.171E+000 6.758E-00 1838.36 0.35 4.776E+001 -3.077E+001 2.056E+00 1847.43 2.03 8.294E+000 2.427E+000 3.571E+00 1873.16 0.21 6.803E+001 5.307E+000 2.849E+00 1896.05 0.15 9.887E+001 -1.513E+001 4.141E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2293.38 0.31 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 6.058E-001 2.38E-001 1.604E+000 2.824E-00 77.11* 9.70 3.348E-001 6.007E-001 1.554E-00 86.83 1.70 3.463E+000 4.967E+000 1.667E+00 87.35 2.24 2.577E+000 2.048E+000 1.240E+00 89.78* 0.82 3.638E+000 2.356E+000 1.688E+00 241.99 7.25 1.206E+000 -5.862E-001 5.802E-00 258.76 0.53 1.124E+001 -3.501E+000 5.288E+00 274.80 0.35 1.824E+001 -3.991E+000 8.588E+00 295.22* 18.42 2.383E-001 2.338E-001 1.082E-00 351.93* 35.60 2.417E-001 1.764E-001 1.141E-00 462.02 0.21 4.433E+001 5.634E-001 2.064E+00 480.43 0.34 3.115E+001 1.280E+001 1.458E+00 487.14 0.43 2.400E+001 -6.185E+000 1.121E+00 533.66 0.18 5.702E+001 5.107E-001 2.643E+00 580.14 0.37 3.304E+001 1.101E+001 1.542E+00 785.96 1.06 1.268E+001 -8.616E+000 5.823E+00

Nuclide MDA Report 4/19/2017 10:42:30 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 839.07 0.58 2.525E+001 2.38E-001 -9.054E+000 1.163E+00

+ Ra-226 81.07 0.20 2.146E+001 1.20E+000 2.555E+000 1.015E+00 83.79 0.32 1.609E+001 1.181E+001 7.701E+00 186.21* 3.64 1.204E+000 2.252E+000 5.658E-00 AC-228 89.96 1.90 1.508E+015 3.83E+014 -7.777E+014 7.237E+01 93.35 3.10 8.116E+014 3.210E+014 3.876E+01 99.51 1.26 1.525E+015 -9.817E+013 7.182E+01 104.82 0.39 5.304E+015 -1.053E+015 2.510E+01 105.60 0.74 2.882E+015 1.109E+015 1.366E+01 108.58 0.28 7.454E+015 -2.859E+015 3.529E+01 129.07 2.42 8.860E+014 5.033E+013 4.193E+01 145.85 0.16 1.531E+016 -5.637E+014 7.272E+01 153.98 0.72 3.269E+015 -9.520E+014 1.549E+01 191.35 0.12 2.174E+016 -1.101E+016 1.029E+01 199.41 0.31 8.893E+015 2.395E+015 4.211E+01 204.03 0.11 2.549E+016 3.245E+015 1.207E+01 209.25 3.89 7.331E+014 -1.909E+014 3.467E+01 214.85 0.76 3.713E+015 4.133E+014 1.752E+01 270.24 3.46 9.005E+014 -2.471E+014 4.219E+01 278.95 0.16 2.235E+016 1.463E+016 1.054E+01 321.65 0.23 1.813E+016 -6.318E+015 8.544E+01 327.44 0.12 3.442E+016 1.469E+016 1.622E+01 328.00 2.95 1.395E+015 3.593E+014 6.571E+01 332.37 0.40 1.032E+016 -4.813E+015 4.858E+01 338.32 11.27 3.832E+014 1.214E+014 1.806E+01 340.96 0.37 1.174E+016 4.362E+015 5.532E+01 409.46 1.92 2.452E+015 -1.029E+015 1.147E+01 440.44 0.12 3.674E+016 -4.481E+015 1.702E+01 463.00 4.40 1.135E+015 -8.417E+013 5.286E+01 478.33 0.21 2.582E+016 -8.800E+015 1.206E+01 503.82 0.18 3.042E+016 -8.659E+016 1.418E+01 508.96 0.45 1.710E+016 1.583E+016 8.130E+01 523.13 0.10 5.504E+016 -2.798E+016 2.563E+01 546.47 0.20 2.905E+016 -1.124E+016 1.351E+01 562.50 0.87 8.442E+015 2.363E+015 3.980E+01 570.91 0.18 3.480E+016 -1.514E+016 1.623E+01 572.14 0.15 4.202E+016 -7.629E+015 1.958E+01 583.41 0.11 6.118E+016 2.828E+016 2.863E+01 674.75 2.10 3.236E+015 -1.845E+015 1.498E+01 701.75 0.17 4.078E+016 2.947E+015 1.888E+01 707.41 0.16 5.221E+016 2.633E+016 2.441E+01 726.86 0.62 1.303E+016 -2.413E+015 6.080E+01 755.32 1.00 7.760E+015 3.294E+015 3.600E+01 772.29 1.49 5.616E+015 1.184E+015 2.616E+01 782.14 0.49 1.494E+016 -7.457E+015 6.874E+01 794.95 4.25 2.067E+015 2.252E+015 9.644E+01 830.49 0.54 1.475E+016 -5.405E+015 6.808E+01 835.71 1.61 4.684E+015 2.982E+015 2.151E+01 840.38 0.91 8.677E+015 -1.003E+015 3.999E+01 904.20 0.77 1.148E+016 -1.960E+016 5.311E+01 911.20 25.80 3.880E+014 1.515E+014 1.812E+01

Nuclide MDA Report 4/19/2017 10:42:30 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram AC-228 947.98 0.11 8.051E+016 3.83E+014 -1.814E+016 3.701E+01 958.61 0.28 2.980E+016 -2.292E+014 1.366E+01 964.77 4.99 1.973E+015 2.112E+015 9.167E+01 968.97 15.80 6.206E+014 2.583E+014 2.881E+01 1033.25 0.20 4.719E+016 -8.780E+015 2.175E+01 1065.18 0.13 7.083E+016 -2.226E+016 3.253E+01 1095.68 0.13 7.017E+016 -7.434E+016 3.206E+01 1110.61 0.28 4.147E+016 1.293E+016 1.935E+01 1153.52 0.14 7.650E+016 -5.083E+016 3.532E+01 1247.08 0.50 2.252E+016 4.834E+014 1.039E+01 1459.14 0.83 2.956E+016 7.861E+016 1.418E+01 1495.91 0.86 8.542E+015 2.436E+015 3.678E+01 1501.57 0.46 1.371E+016 -1.097E+016 5.740E+01 1557.11 0.18 4.276E+016 3.292E+015 1.841E+01 1580.53 0.60 1.285E+016 -6.598E+015 5.534E+01 1588.20 3.22 2.967E+015 2.106E+015 1.316E+01 1625.06 0.25 3.101E+016 1.857E+015 1.335E+01 1630.63 1.51 5.423E+015 -3.670E+015 2.347E+01 1638.28 0.47 1.854E+016 7.056E+015 8.095E+01 1666.52 0.18 4.064E+016 -1.516E+015 1.716E+01 TH-230 67.67 0.38 1.330E+001 1.33E+001 -7.234E+000 6.304E+00 PA-234 742.81 0.11 1.395E+002 2.17E+001 -8.565E+001 6.488E+00 766.42 0.32 4.831E+001 6.680E+000 2.247E+00 1001.03 0.84 2.165E+001 9.778E+000 1.002E+00 TH-234 63.29 3.70 1.612E+000 1.61E+000 1.387E+000 7.682E-00 92.38 2.13 2.471E+000 9.636E-001 1.185E+00 92.80 2.10 2.478E+000 1.527E+000 1.188E+00 112.81 0.21 1.740E+001 -1.786E+000 8.202E+00 U-234 53.20 0.12 4.785E+001 4.78E+001 -1.457E+000 2.244E+00 120.90 0.04 1.088E+002 -8.129E+000 5.138E+00 U-235 72.70 0.12 4.881E+001 4.02E-001 6.387E+000 2.339E+00 89.96 3.43 1.575E+000 -8.123E-001 7.559E-00 93.35 5.54 8.562E-001 3.387E-001 4.089E-00 104.82 0.69 5.694E+000 -1.130E+000 2.694E+00 105.60 1.31 3.069E+000 1.182E+000 1.455E+00 108.58 0.50 7.871E+000 -3.019E+000 3.726E+00 109.19 1.66 2.318E+000 -1.143E+000 1.096E+00 140.76 0.20 2.108E+001 4.594E+000 9.983E+00 143.76 10.96 4.018E-001 5.040E-002 1.906E-00 163.36 5.08 8.672E-001 2.202E-001 4.098E-00 182.62 0.39 1.547E+001 -7.368E+000 7.401E+00 194.94 0.63 8.550E+000 4.252E+000 4.057E+00 202.12 1.08 4.923E+000 2.288E+000 2.331E+00 205.32 5.02 1.054E+000 -4.275E-001 4.984E-00 221.39 0.12 4.420E+001 -1.390E+001 2.080E+00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

4/19/2017 10:42:30 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2120\\W6H-IMC-212 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 9.47E+000 18.164 Pb-210 46.5 ^ 2.67E+000 41.814 Pb-212 74.8 9.05E-001 30.604 3.488[42.574] 4.21 -0.767 77.1 3.41E-001 35.770 1.313[46.427] [ 0.453]

89.8 1.32E+000 87.892 5.101[92.741]

238.6 ^ 2.59E-001 29.596 1.000[41.856]

PB-214 74.8 1.60E+000 31.885 9.091[56.007] 7.05 -1.195 77.1 6.01E-001 36.886 3.405[58.997] [ 0.419]

89.8 2.36E+000 88.319 13.357[99.601]

295.2 2.34E-001 49.197 1.325[67.383]

351.9 ^ 1.76E-001 46.045 1.000[65.118]

Ra-226 186.2 ^ 2.25E+000 31.986