ML19095B365

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W6H-IMC-2120-S-P-5

ML19095B365
Person / Time
Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
Shared Package
ml051740240	List: ML19095A013 ML19095A014 ML19095A016 ML19095A017 ML19095A018 ML19095A019 ML19095A020 ML19095A021 ML19095A022 ML19095A023 ML19095A024 ML19095A025 ML19095A030 ML19095A034 ML19095A035 ML19095A036 ML19095A037 ML19095A038 ML19095A040 ML19095A042 ML19095A043 ML19095A045 ML19095A046 ML19095A048 ML19095A049 ML19095A051 ML19095A052 ML19095A055 ML19095A056 ML19095A060 ML19095A061 ML19095A063 ML19095A064 ML19095A067 ML19095A069 ML19095A198 ML19095A200 ML19095A201 ML19095A204 ML19095A205 ML19095A206 ML19095A268 ML19095A269 ML19095A319 ML19095A321 ML19095A322 ML19095A324 ML19095A325 ML19095A326 ML19095A328 ... further results
References
Download: ML19095B365 (10)

Text

• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2120\\W6H-IMC-212 Report Generated On : 4/19/2017 10:41:26 AM Sample Title : W6H-IMC-2120-S-P-5 Sample Description :

Sample Identification : 2120-S-P-5 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.500 keV Sample Size : 2.803E+002 grams Sample Taken On : 3/17/2017 12:00:00 AM Acquisition Started : 3/29/2017 12:02:34 PM Live Time : 1800.0 seconds Real Time : 1800.4 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 3/24/2017 Efficiency Calibration Used Done On : 4/19/2017 Efficiency ID : H-IMC-2120-S-P-5

Peak Analysis Report 4/19/2017 10:41:26 AM Page 1

• • • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W6H-IMC-2120-S-P-5 Peak Analysis Performed on: 4/19/2017 10:41:22 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 182-191 186.16 46.74 0.63 5.91E+001 19.74 6.00E+001 M 2 295-313 299.67 75.13 0.74 8.03E+001 24.63 1.16E+002 m 3 295-313 308.31 77.29 0.75 9.01E+001 23.66 8.15E+001 F 4 737-749 742.37 185.87 0.93 4.97E+001 19.33 6.01E+001 F 5 949-959 953.22 238.61 0.98 1.13E+002 24.27 4.26E+001 F 6 1172-1184 1178.54 294.98 1.01 3.55E+001 14.74 2.34E+001 F 7 1399-1411 1405.67 351.79 1.06 3.13E+001 15.23 3.25E+001 F 8 2031-2049 2040.05 510.48 1.68 5.01E+001 17.28 3.33E+001 F 9 5825-5851 5837.68 1460.45 2.52 1.86E+002 25.72 1.20E+001 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 4/19/2017 10:41:26 AM Page 2

• • • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W6H-IMC-2120-S-P-5 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.990 1460.82* 10.66 1.17194E+001 1.90534E+000 Pb-210 0.997 46.54* 4.25 2.40496E+000 1.05363E+000 Pb-212 0.999 74.82* 10.28 6.74650E-001 2.47749E-001 77.11* 17.10 4.45515E-001 1.47454E-001 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 3.03365E-001 8.11640E-002 300.09 3.30 PB-214 0.998 74.82* 5.80 1.19576E+000 4.51959E-001 77.11* 9.70 7.85393E-001 2.69390E-001 86.83 1.70 87.35 2.24 89.78 0.82 241.99 7.25 258.76 0.53 274.80 0.35 295.22* 18.42 2.78494E-001 1.23706E-001 351.93* 35.60 1.52879E-001 7.75970E-002 462.02 0.21 480.43 0.34 487.14 0.43 533.66 0.18 580.14 0.37 785.96 1.06 839.07 0.58 Ra-226 0.993 81.07 0.20 83.79 0.32 186.21* 3.64 1.29677E+000 5.50247E-001

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.500 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 4/19/2017 10:41:26 AM Page 3

• • • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.990 1.171940E+001 1.905345E+000 Pb-210 0.997 2.404958E+000 1.053628E+000 Pb-212 0.999 3.296877E-001 6.880852E-002 PB-214 0.998 1.981613E-001 6.377990E-002 Ra-226 0.993 1.296774E+000 5.502469E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

• • • • • • • • • • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 4/19/2017 10:41:22 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 8 510.48 2.7857E-002 34.47 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 4/19/2017 10:41:26 AM Page 4

• • • • • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W6H-IMC-2120-S-P-5 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 1.308E+000 1.31E+000 1.172E+001 5.687E-00 CO-60 1173.23 99.85 2.351E-001 1.79E-001 1.203E-001 1.100E-00 1332.49 99.98 1.787E-001 3.574E-002 8.090E-00 CS-137 661.66 85.10 1.651E-001 1.65E-001 3.215E-002 7.725E-00

+ Pb-210 46.54* 4.25 1.805E+000 1.80E+000 2.405E+000 8.473E-00 BI-212 288.20 0.34 2.025E+001 2.39E+000 1.673E+001 9.555E+00 328.03 0.13 6.417E+001 5.488E+001 3.034E+00 452.98 0.36 2.475E+001 -1.827E+001 1.153E+00 727.33 6.67 2.392E+000 4.370E-001 1.122E+00 785.37 1.10 1.322E+001 6.596E+000 6.128E+00 893.41 0.38 4.614E+001 -8.980E+000 2.149E+00 952.12 0.17 1.093E+002 -3.594E+000 5.097E+00 1078.62 0.56 3.424E+001 1.455E+001 1.587E+00 1512.70 0.29 5.869E+001 2.592E+001 2.611E+00 1620.50 1.47 1.009E+001 -4.850E+000 4.367E+00

+ Pb-212 74.82* 10.28 4.443E-001 9.65E-002 6.746E-001 2.108E-00 77.11* 17.10 2.212E-001 4.455E-001 1.039E-00 86.83 2.07 2.668E+000 2.733E+000 1.282E+00 87.35 3.97 1.342E+000 -3.876E-001 6.441E-00 89.78 1.46 3.369E+000 -7.860E+000 1.612E+00 115.18 0.60 6.389E+000 3.970E+000 3.022E+00 238.63* 43.60 9.650E-002 3.034E-001 4.460E-00 300.09 3.30 2.079E+000 -6.691E-001 9.790E-00 BI-214 76.86 0.55 1.373E+001 3.43E-001 0.000E+000 6.656E+00 79.29 0.91 6.354E+000 5.500E-001 3.053E+00 89.26 0.11 4.570E+001 2.489E+000 2.189E+00 89.81 0.21 2.342E+001 -5.464E+001 1.121E+00 273.80 0.13 4.911E+001 -5.514E+001 2.314E+00 348.92 0.10 8.709E+001 -1.325E+000 4.130E+00 386.78 0.29 2.917E+001 -4.424E+000 1.371E+00 388.89 0.40 2.065E+001 -8.404E+000 9.675E+00 405.72 0.17 4.973E+001 1.374E+001 2.325E+00 454.79 0.29 3.289E+001 1.085E+001 1.539E+00 469.77 0.13 7.953E+001 1.041E+001 3.735E+00 609.32 45.49 3.430E-001 2.918E-001 1.624E-00 665.45 1.53 8.977E+000 9.211E-001 4.193E+00 703.11 0.47 2.535E+001 1.356E+001 1.166E+00 719.87 0.39 3.675E+001 -2.485E+001 1.713E+00 752.85 0.13 1.148E+002 -3.486E+001 5.342E+00 768.36 4.89 3.036E+000 -1.293E+000 1.412E+00 786.35 0.32 4.518E+001 -7.872E-001 2.093E+00 806.18 1.26 1.119E+001 -1.790E+000 5.166E+00

Nuclide MDA Report 4/19/2017 10:41:26 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram BI-214 821.18 0.16 9.183E+001 3.43E-001 2.533E+000 4.249E+00 826.45 0.12 1.358E+002 -6.761E+000 6.317E+00 934.06 3.11 5.098E+000 -5.998E-001 2.350E+00 964.08 0.37 5.614E+001 1.064E+001 2.632E+00 1051.96 0.31 6.188E+001 4.786E+001 2.874E+00 1069.96 0.27 6.683E+001 2.534E+001 3.085E+00 1120.29 14.92 1.392E+000 -5.838E-001 6.474E-00 1133.66 0.25 7.886E+001 -2.547E+001 3.651E+00 1155.21 1.63 1.095E+001 -4.170E+000 5.020E+00 1207.68 0.45 4.513E+001 -9.110E+000 2.085E+00 1238.11 5.83 4.249E+000 1.001E+000 1.989E+00 1280.98 1.43 1.267E+001 -2.934E+000 5.769E+00 1303.75 0.11 1.533E+002 -4.562E+001 6.894E+00 1377.67 3.99 4.722E+000 1.239E+000 2.144E+00 1385.31 0.79 1.948E+001 -7.115E+000 8.641E+00 1401.52 1.33 1.397E+001 4.231E+000 6.323E+00 1407.99 2.39 7.559E+000 3.842E+000 3.411E+00 1509.21 2.13 7.473E+000 -2.294E+000 3.296E+00 1538.53 0.40 3.873E+001 3.008E+001 1.697E+00 1543.34 0.30 4.968E+001 -7.380E+000 2.169E+00 1583.20 0.70 2.754E+001 1.981E+001 1.239E+00 1594.75 0.27 6.543E+001 -7.261E+000 2.903E+00 1599.37 0.32 4.663E+001 -1.750E+000 2.027E+00 1661.27 1.05 1.449E+001 7.528E+000 6.271E+00 1684.01 0.21 4.678E+001 -4.550E+001 1.856E+00 1729.59 2.88 5.470E+000 2.815E+000 2.367E+00 1764.49 15.30 1.401E+000 1.217E+000 6.300E-00 1838.36 0.35 4.614E+001 1.350E+001 1.986E+00 1847.43 2.03 8.012E+000 8.431E-001 3.450E+00 1873.16 0.21 8.852E+001 1.025E+001 3.893E+00 1896.05 0.15 9.094E+001 1.719E+000 3.771E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2293.38 0.31 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 7.875E-001 1.52E-001 1.196E+000 3.736E-00 77.11* 9.70 3.899E-001 7.854E-001 1.832E-00 86.83 1.70 3.249E+000 3.328E+000 1.562E+00 87.35 2.24 2.378E+000 -6.870E-001 1.142E+00 89.78 0.82 5.999E+000 -1.399E+001 2.871E+00 241.99 7.25 1.260E+000 3.571E-001 6.076E-00 258.76 0.53 1.160E+001 4.661E+000 5.477E+00 274.80 0.35 1.777E+001 -5.842E+000 8.373E+00 295.22* 18.42 2.108E-001 2.785E-001 9.477E-00 351.93* 35.60 1.520E-001 1.529E-001 6.939E-00 462.02 0.21 4.453E+001 9.734E+000 2.079E+00 480.43 0.34 3.152E+001 1.007E+001 1.479E+00 487.14 0.43 2.210E+001 -1.576E+001 1.029E+00 533.66 0.18 5.235E+001 -2.869E+001 2.417E+00 580.14 0.37 3.662E+001 -1.580E+000 1.724E+00 785.96 1.06 1.375E+001 4.170E+000 6.375E+00

Nuclide MDA Report 4/19/2017 10:41:26 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 839.07 0.58 2.677E+001 1.52E-001 -1.630E+000 1.242E+00

+ Ra-226 81.07 0.20 2.145E+001 1.15E+000 -3.416E+000 1.016E+00 83.79 0.32 1.487E+001 -1.287E+000 7.100E+00 186.21* 3.64 1.150E+000 1.297E+000 5.396E-00 AC-228 89.96 1.90 1.293E+015 4.00E+014 -3.016E+015 6.186E+01 93.35 3.10 8.156E+014 4.908E+014 3.910E+01 99.51 1.26 1.470E+015 -1.658E+014 6.944E+01 104.82 0.39 5.423E+015 3.780E+015 2.580E+01 105.60 0.74 2.919E+015 2.102E+015 1.390E+01 108.58 0.28 7.270E+015 -2.249E+014 3.452E+01 129.07 2.42 7.911E+014 -2.008E+014 3.738E+01 145.85 0.16 1.424E+016 3.746E+015 6.773E+01 153.98 0.72 2.942E+015 1.076E+015 1.393E+01 191.35 0.12 2.119E+016 -2.714E+015 1.006E+01 199.41 0.31 8.912E+015 4.698E+015 4.241E+01 204.03 0.11 2.330E+016 -6.961E+015 1.103E+01 209.25 3.89 7.176E+014 3.322E+014 3.407E+01 214.85 0.76 3.697E+015 -2.108E+015 1.753E+01 270.24 3.46 9.328E+014 3.634E+013 4.405E+01 278.95 0.16 2.082E+016 1.084E+016 9.832E+01 321.65 0.23 1.594E+016 -1.801E+016 7.499E+01 327.44 0.12 3.349E+016 1.979E+016 1.584E+01 328.00 2.95 1.359E+015 1.162E+015 6.423E+01 332.37 0.40 9.968E+015 -1.431E+016 4.707E+01 338.32 11.27 4.045E+014 4.065E+014 1.922E+01 340.96 0.37 1.167E+016 1.707E+015 5.527E+01 409.46 1.92 2.309E+015 7.745E+014 1.083E+01 440.44 0.12 3.656E+016 -5.908E+015 1.705E+01 463.00 4.40 1.089E+015 -7.243E+013 5.090E+01 478.33 0.21 2.587E+016 1.037E+016 1.216E+01 503.82 0.18 2.914E+016 -2.526E+016 1.363E+01 508.96 0.45 1.525E+016 7.884E+015 7.240E+01 523.13 0.10 4.985E+016 1.245E+016 2.320E+01 546.47 0.20 2.829E+016 1.026E+015 1.322E+01 562.50 0.87 6.638E+015 3.580E+015 3.099E+01 570.91 0.18 2.938E+016 -1.875E+016 1.362E+01 572.14 0.15 3.603E+016 3.361E+015 1.672E+01 583.41 0.11 6.166E+016 2.845E+016 2.904E+01 674.75 2.10 3.291E+015 1.072E+015 1.537E+01 701.75 0.17 3.450E+016 -2.034E+015 1.587E+01 707.41 0.16 3.958E+016 -2.288E+015 1.824E+01 726.86 0.62 1.277E+016 4.108E+015 5.990E+01 755.32 1.00 7.420E+015 -6.736E+014 3.455E+01 772.29 1.49 5.084E+015 1.892E+015 2.367E+01 782.14 0.49 1.568E+016 8.407E+015 7.299E+01 794.95 4.25 1.746E+015 5.717E+014 8.101E+01 830.49 0.54 1.500E+016 1.416E+015 6.983E+01 835.71 1.61 5.208E+015 4.271E+015 2.430E+01 840.38 0.91 8.290E+015 -6.435E+015 3.836E+01 904.20 0.77 1.210E+016 -2.259E+016 5.657E+01 911.20 25.80 3.998E+014 3.116E+014 1.882E+01

Nuclide MDA Report 4/19/2017 10:41:26 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram AC-228 947.98 0.11 8.665E+016 4.00E+014 1.749E+016 4.037E+01 958.61 0.28 3.313E+016 3.813E+015 1.543E+01 964.77 4.99 2.090E+015 8.548E+014 9.813E+01 968.97 15.80 6.665E+014 5.943E+014 3.130E+01 1033.25 0.20 4.301E+016 2.299E+016 1.982E+01 1065.18 0.13 6.315E+016 -5.186E+016 2.894E+01 1095.68 0.13 6.238E+016 8.021E+015 2.843E+01 1110.61 0.28 3.196E+016 -3.177E+016 1.472E+01 1153.52 0.14 6.701E+016 6.051E+015 3.083E+01 1247.08 0.50 2.428E+016 1.277E+016 1.134E+01 1459.14 0.83 2.953E+016 8.173E+016 1.422E+01 1495.91 0.86 8.273E+015 3.016E+015 3.597E+01 1501.57 0.46 1.681E+016 -4.576E+014 7.390E+01 1557.11 0.18 4.259E+016 1.665E+016 1.859E+01 1580.53 0.60 1.443E+016 -1.201E+015 6.403E+01 1588.20 3.22 2.971E+015 2.479E+015 1.333E+01 1625.06 0.25 3.252E+016 2.608E+016 1.430E+01 1630.63 1.51 5.087E+015 2.713E+015 2.211E+01 1638.28 0.47 1.379E+016 -1.452E+015 5.825E+01 1666.52 0.18 3.699E+016 -8.918E+015 1.562E+01 TH-230 67.67 0.38 1.334E+001 1.33E+001 3.381E+000 6.329E+00 PA-234 742.81 0.11 1.361E+002 1.68E+001 -7.943E+001 6.334E+00 766.42 0.32 4.784E+001 -1.190E+001 2.229E+00 1001.03 0.84 1.677E+001 -8.268E+000 7.602E+00 TH-234 63.29 3.70 1.685E+000 1.69E+000 4.354E-001 8.049E-00 92.38 2.13 2.457E+000 2.632E+000 1.179E+00 92.80 2.10 2.482E+000 3.272E+000 1.191E+00 112.81 0.21 1.913E+001 1.317E+001 9.077E+00 U-234 53.20 0.12 5.473E+001 5.47E+001 1.249E+001 2.590E+00 120.90 0.04 1.024E+002 -1.066E+001 4.825E+00 U-235 72.70 0.12 5.033E+001 4.04E-001 -4.070E+000 2.417E+00 89.96 3.43 1.433E+000 -3.343E+000 6.858E-00 93.35 5.54 9.134E-001 5.496E-001 4.379E-00 104.82 0.69 6.179E+000 4.307E+000 2.940E+00 105.60 1.31 3.300E+000 2.376E+000 1.572E+00 108.58 0.50 8.148E+000 -2.520E-001 3.869E+00 109.19 1.66 2.376E+000 -1.663E+000 1.126E+00 140.76 0.20 2.088E+001 -1.653E+001 9.894E+00 143.76 10.96 4.036E-001 -7.681E-002 1.918E-00 163.36 5.08 8.429E-001 5.350E-002 3.983E-00 182.62 0.39 1.511E+001 -3.608E+000 7.231E+00 194.94 0.63 8.726E+000 -6.456E-001 4.151E+00 202.12 1.08 5.025E+000 -5.875E-002 2.386E+00 205.32 5.02 1.055E+000 2.561E-002 4.999E-00 221.39 0.12 4.749E+001 -2.430E+001 2.248E+00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

4/19/2017 10:41:26 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2120\\W6H-IMC-212 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 1.17E+001 16.258 Pb-210 46.5 ^ 2.40E+000 43.811 Pb-212 74.8 6.75E-001 36.723 2.224[45.435] 2.79 -0.511 77.1 4.46E-001 33.097 1.469[42.559] [ 0.428]

238.6 ^ 3.03E-001 26.755 1.000[37.837]

PB-214 74.8 1.20E+000 37.797 7.822[63.284] 6.51 -1.076 77.1 7.85E-001 34.300 5.137[61.260] [ 0.457]

295.2 2.78E-001 44.420 1.822[67.449]

351.9 ^ 1.53E-001 50.757 1.000[71.781]

Ra-226 186.2 ^ 1.30E+000 42.432