ML19095B362

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W6H-IMC-2120-S-P-4

ML19095B362
Person / Time
Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
Shared Package
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References
Download: ML19095B362 (10)

Text

• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2120\\W6H-IMC-212 Report Generated On : 4/19/2017 10:40:34 AM Sample Title : W6H-IMC-2120-S-P-4 Sample Description :

Sample Identification : 2120-S-P-4 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.500 keV Sample Size : 2.354E+002 grams Sample Taken On : 3/17/2017 12:00:00 AM Acquisition Started : 3/29/2017 10:38:50 AM Live Time : 1800.0 seconds Real Time : 1800.3 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 3/24/2017 Efficiency Calibration Used Done On : 4/19/2017 Efficiency ID : H-IMC-2120-S-P-4

Peak Analysis Report 4/19/2017 10:40:34 AM Page 1

• • • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W6H-IMC-2120-S-P-4 Peak Analysis Performed on: 4/19/2017 10:40:30 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 178-191 186.22 46.75 0.87 6.85E+001 20.23 5.13E+001 M 2 296-314 299.99 75.21 0.73 8.64E+001 22.60 5.70E+001 m 3 296-314 308.74 77.40 0.74 5.68E+001 19.35 6.33E+001 F 4 737-752 742.31 185.86 0.83 4.79E+001 18.06 6.20E+001 F 5 946-960 952.94 238.55 0.81 8.49E+001 20.95 4.88E+001 F 6 5826-5850 5838.42 1460.63 2.36 1.54E+002 23.70 8.33E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 4/19/2017 10:40:34 AM Page 2

• • • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W6H-IMC-2120-S-P-4 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.997 1460.82* 10.66 1.07456E+001 1.88574E+000 Pb-210 0.997 46.54* 4.25 2.82379E+000 1.15510E+000 Pb-212 0.997 74.82* 10.28 7.65884E-001 2.52974E-001 77.11* 17.10 2.96884E-001 1.17402E-001 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 2.49617E-001 7.31864E-002 300.09 3.30 Ra-226 0.992 81.07 0.20 83.79 0.32 186.21* 3.64 1.36173E+000 5.62377E-001

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.500 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 4/19/2017 10:40:34 AM Page 3

• • • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.997 1.074559E+001 1.885741E+000 Pb-210 0.997 2.823786E+000 1.155101E+000 Pb-212 0.997 2.914417E-001 6.031582E-002 Ra-226 0.992 1.361733E+000 5.623773E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

• • • • • • • • • • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 4/19/2017 10:40:30 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified.

Nuclide MDA Report 4/19/2017 10:40:34 AM Page 4

• • • • • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W6H-IMC-2120-S-P-4 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 1.210E+000 1.21E+000 1.075E+001 5.107E-00 CO-60 1173.23 99.85 2.137E-001 2.08E-001 3.126E-002 9.849E-00 1332.49 99.98 2.080E-001 6.689E-002 9.470E-00 CS-137 661.66 85.10 1.584E-001 1.58E-001 -4.201E-002 7.339E-00

+ Pb-210 46.54* 4.25 1.885E+000 1.88E+000 2.824E+000 8.867E-00 BI-212 288.20 0.34 2.042E+001 2.48E+000 -1.882E+001 9.589E+00 328.03 0.13 6.579E+001 -3.741E+001 3.098E+00 452.98 0.36 3.048E+001 8.661E+000 1.432E+00 727.33 6.67 2.479E+000 5.695E-001 1.158E+00 785.37 1.10 1.439E+001 -4.513E+000 6.667E+00 893.41 0.38 4.800E+001 -3.746E+000 2.227E+00 952.12 0.17 1.052E+002 4.102E+001 4.852E+00 1078.62 0.56 3.215E+001 -3.796E+000 1.471E+00 1512.70 0.29 5.920E+001 8.205E+000 2.603E+00 1620.50 1.47 1.242E+001 3.412E+000 5.461E+00

+ Pb-212 74.82* 10.28 3.353E-001 1.22E-001 7.659E-001 1.557E-00 77.11* 17.10 2.076E-001 2.969E-001 9.671E-00 86.83 2.07 2.434E+000 2.033E-002 1.162E+00 87.35 3.97 1.238E+000 -3.596E-001 5.904E-00 89.78 1.46 3.211E+000 0.000E+000 1.528E+00 115.18 0.60 5.968E+000 -1.005E+000 2.799E+00 238.63* 43.60 1.224E-001 2.496E-001 5.724E-00 300.09 3.30 2.319E+000 -2.120E+000 1.094E+00 BI-214 76.86 0.55 1.266E+001 3.34E-001 2.305E+001 6.105E+00 79.29 0.91 5.972E+000 1.002E+000 2.855E+00 89.26 0.11 4.254E+001 1.515E+001 2.025E+00 89.81 0.21 2.232E+001 0.000E+000 1.062E+00 273.80 0.13 5.192E+001 -3.206E+000 2.441E+00 348.92 0.10 9.122E+001 8.238E+001 4.316E+00 386.78 0.29 2.843E+001 -7.119E+000 1.325E+00 388.89 0.40 1.988E+001 -1.088E+001 9.229E+00 405.72 0.17 5.406E+001 -6.667E+000 2.526E+00 454.79 0.29 3.648E+001 -1.266E+001 1.708E+00 469.77 0.13 7.913E+001 -6.463E+001 3.692E+00 609.32 45.49 3.336E-001 2.534E-001 1.568E-00 665.45 1.53 8.693E+000 -3.631E+000 4.022E+00 703.11 0.47 3.103E+001 -5.858E-002 1.441E+00 719.87 0.39 3.790E+001 -4.242E+001 1.758E+00 752.85 0.13 1.289E+002 6.547E+001 6.006E+00 768.36 4.89 3.510E+000 1.063E+000 1.638E+00 786.35 0.32 5.169E+001 1.565E+001 2.403E+00 806.18 1.26 1.252E+001 -3.807E+000 5.787E+00

Nuclide MDA Report 4/19/2017 10:40:34 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram BI-214 821.18 0.16 1.026E+002 3.34E-001 -3.219E+001 4.755E+00 826.45 0.12 1.345E+002 -5.363E+001 6.206E+00 934.06 3.11 5.321E+000 -8.328E-001 2.442E+00 964.08 0.37 4.709E+001 7.355E+000 2.163E+00 1051.96 0.31 5.864E+001 1.138E+001 2.691E+00 1069.96 0.27 6.697E+001 2.397E+001 3.067E+00 1120.29 14.92 1.532E+000 7.142E-001 7.125E-00 1133.66 0.25 8.525E+001 -5.991E+001 3.942E+00 1155.21 1.63 1.192E+001 -7.790E+000 5.458E+00 1207.68 0.45 4.781E+001 5.669E+000 2.202E+00 1238.11 5.83 3.776E+000 3.768E+000 1.739E+00 1280.98 1.43 1.517E+001 4.847E+000 6.960E+00 1303.75 0.11 1.631E+002 -1.884E+001 7.307E+00 1377.67 3.99 5.274E+000 2.818E+000 2.398E+00 1385.31 0.79 2.361E+001 -3.374E+000 1.059E+00 1401.52 1.33 1.446E+001 -3.497E+000 6.503E+00 1407.99 2.39 9.071E+000 7.151E+000 4.130E+00 1509.21 2.13 8.426E+000 3.166E+000 3.728E+00 1538.53 0.40 3.251E+001 -4.877E+000 1.361E+00 1543.34 0.30 4.282E+001 -1.627E+001 1.793E+00 1583.20 0.70 2.536E+001 3.013E+000 1.115E+00 1594.75 0.27 7.214E+001 -8.007E+000 3.201E+00 1599.37 0.32 6.085E+001 -2.370E+001 2.707E+00 1661.27 1.05 1.193E+001 -1.700E+001 4.890E+00 1684.01 0.21 7.409E+001 3.326E+001 3.172E+00 1729.59 2.88 6.217E+000 -9.749E-001 2.703E+00 1764.49 15.30 1.466E+000 9.600E-001 6.552E-00 1838.36 0.35 5.090E+001 1.489E+001 2.191E+00 1847.43 2.03 8.229E+000 -3.290E+000 3.501E+00 1873.16 0.21 5.226E+001 6.527E-001 2.025E+00 1896.05 0.15 1.147E+002 4.521E+001 4.879E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2293.38 0.31 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00 PB-214 74.82 5.80 1.155E+000 2.66E-001 2.970E-001 5.563E-00 77.11 9.70 7.095E-001 4.616E-002 3.423E-00 86.83 1.70 2.964E+000 2.475E-002 1.415E+00 87.35 2.24 2.194E+000 -6.372E-001 1.046E+00 89.78 0.82 5.717E+000 0.000E+000 2.721E+00 241.99 7.25 1.256E+000 2.844E-001 6.039E-00 258.76 0.53 1.241E+001 4.045E+000 5.854E+00 274.80 0.35 1.825E+001 -5.800E+000 8.567E+00 295.22 18.42 4.307E-001 4.294E-002 2.037E-00 351.93 35.60 2.665E-001 1.761E-001 1.260E-00 462.02 0.21 5.267E+001 2.092E+001 2.472E+00 480.43 0.34 3.592E+001 1.116E+001 1.690E+00 487.14 0.43 2.458E+001 -5.425E+000 1.145E+00 533.66 0.18 6.301E+001 -1.355E+001 2.930E+00 580.14 0.37 3.927E+001 4.676E+001 1.846E+00 785.96 1.06 1.560E+001 6.202E+000 7.250E+00

Nuclide MDA Report 4/19/2017 10:40:34 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram PB-214 839.07 0.58 2.575E+001 2.66E-001 -1.276E+001 1.181E+00

+ Ra-226 81.07 0.20 2.066E+001 1.35E+000 -4.433E+000 9.729E+00 83.79 0.32 1.448E+001 1.045E+001 6.881E+00 186.21* 3.64 1.351E+000 1.362E+000 6.372E-00 AC-228 89.96 1.90 1.053E+015 3.10E+014 0.000E+000 5.011E+01 93.35 3.10 6.433E+014 1.020E+014 3.063E+01 99.51 1.26 1.292E+015 -5.515E+013 6.086E+01 104.82 0.39 4.139E+015 1.095E+015 1.949E+01 105.60 0.74 2.123E+015 -7.334E+014 9.981E+01 108.58 0.28 5.708E+015 -2.517E+015 2.687E+01 129.07 2.42 6.982E+014 3.762E+014 3.290E+01 145.85 0.16 1.215E+016 3.168E+015 5.754E+01 153.98 0.72 2.484E+015 -3.636E+014 1.169E+01 191.35 0.12 1.701E+016 -1.193E+015 8.011E+01 199.41 0.31 7.295E+015 -7.594E+014 3.447E+01 204.03 0.11 1.958E+016 -1.540E+015 9.217E+01 209.25 3.89 6.267E+014 3.030E+014 2.965E+01 214.85 0.76 3.082E+015 -2.127E+014 1.452E+01 270.24 3.46 8.404E+014 7.496E+013 3.961E+01 278.95 0.16 1.681E+016 -6.813E+015 7.865E+01 321.65 0.23 1.489E+016 3.755E+015 7.004E+01 327.44 0.12 2.996E+016 8.459E+015 1.413E+01 328.00 2.95 1.190E+015 -6.767E+014 5.604E+01 332.37 0.40 8.851E+015 -3.915E+015 4.167E+01 338.32 11.27 3.096E+014 -1.381E+013 1.455E+01 340.96 0.37 9.479E+015 -6.379E+014 4.452E+01 409.46 1.92 1.907E+015 -1.329E+015 8.864E+01 440.44 0.12 3.587E+016 -1.616E+016 1.678E+01 463.00 4.40 1.073E+015 1.294E+014 5.031E+01 478.33 0.21 2.488E+016 1.606E+016 1.172E+01 503.82 0.18 2.482E+016 -4.229E+016 1.153E+01 508.96 0.45 1.444E+016 1.545E+016 6.862E+01 523.13 0.10 4.702E+016 8.765E+015 2.190E+01 546.47 0.20 2.423E+016 2.882E+015 1.125E+01 562.50 0.87 6.387E+015 1.676E+015 2.988E+01 570.91 0.18 2.974E+016 2.034E+016 1.387E+01 572.14 0.15 3.374E+016 -2.046E+016 1.566E+01 583.41 0.11 5.461E+016 4.214E+016 2.563E+01 674.75 2.10 3.042E+015 5.997E+014 1.419E+01 701.75 0.17 3.488E+016 -1.669E+016 1.615E+01 707.41 0.16 4.156E+016 -3.325E+016 1.933E+01 726.86 0.62 1.161E+016 6.329E+015 5.432E+01 755.32 1.00 7.012E+015 -2.388E+015 3.266E+01 772.29 1.49 4.945E+015 4.148E+015 2.308E+01 782.14 0.49 1.414E+016 5.114E+014 6.561E+01 794.95 4.25 1.730E+015 2.058E+014 8.062E+01 830.49 0.54 1.250E+016 4.140E+015 5.766E+01 835.71 1.61 3.922E+015 -7.672E+014 1.798E+01 840.38 0.91 7.204E+015 -1.502E+015 3.312E+01 904.20 0.77 1.105E+016 -1.698E+016 5.160E+01 911.20 25.80 3.631E+014 2.117E+014 1.705E+01

Nuclide MDA Report 4/19/2017 10:40:34 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram AC-228 947.98 0.11 7.311E+016 3.10E+014 3.850E+015 3.378E+01 958.61 0.28 2.373E+016 -1.840E+016 1.080E+01 964.77 4.99 1.456E+015 3.323E+013 6.679E+01 968.97 15.80 4.513E+014 7.900E+013 2.066E+01 1033.25 0.20 3.962E+016 1.511E+016 1.823E+01 1065.18 0.13 5.801E+016 -1.336E+016 2.653E+01 1095.68 0.13 6.562E+016 -5.985E+014 3.022E+01 1110.61 0.28 3.236E+016 -9.483E+015 1.499E+01 1153.52 0.14 6.492E+016 4.181E+015 2.995E+01 1247.08 0.50 1.734E+016 -1.381E+016 7.921E+01 1459.14 0.83 2.515E+016 6.768E+016 1.206E+01 1495.91 0.86 8.643E+015 2.945E+015 3.813E+01 1501.57 0.46 1.658E+016 -1.646E+015 7.337E+01 1557.11 0.18 3.667E+016 2.823E+015 1.579E+01 1580.53 0.60 1.173E+016 1.980E+015 5.098E+01 1588.20 3.22 2.490E+015 2.942E+013 1.102E+01 1625.06 0.25 3.064E+016 8.418E+015 1.347E+01 1630.63 1.51 4.930E+015 -8.608E+014 2.152E+01 1638.28 0.47 1.243E+016 -1.094E+016 5.207E+01 1666.52 0.18 3.005E+016 -2.001E+014 1.232E+01 TH-230 67.67 0.38 1.380E+001 1.38E+001 5.248E+000 6.546E+00 PA-234 742.81 0.11 1.448E+002 2.26E+001 -4.920E+000 6.721E+00 766.42 0.32 5.405E+001 1.637E+001 2.523E+00 1001.03 0.84 2.262E+001 6.869E+000 1.045E+00 TH-234 63.29 3.70 1.585E+000 1.59E+000 5.021E-001 7.534E-00 92.38 2.13 2.290E+000 2.169E+000 1.092E+00 92.80 2.10 2.251E+000 7.455E-001 1.072E+00 112.81 0.21 1.658E+001 -4.009E+000 7.764E+00 U-234 53.20 0.12 4.943E+001 4.94E+001 2.602E+001 2.320E+00 120.90 0.04 1.069E+002 -4.596E+001 5.025E+00 U-235 72.70 0.12 4.280E+001 4.02E-001 -1.844E+001 2.035E+00 89.96 3.43 1.366E+000 0.000E+000 6.501E-00 93.35 5.54 8.431E-001 1.337E-001 4.015E-00 104.82 0.69 5.520E+000 1.461E+000 2.600E+00 105.60 1.31 2.809E+000 -9.703E-001 1.321E+00 108.58 0.50 7.487E+000 -3.302E+000 3.524E+00 109.19 1.66 2.231E+000 -9.052E-001 1.050E+00 140.76 0.20 2.121E+001 -1.038E+001 1.002E+00 143.76 10.96 4.021E-001 -2.435E-001 1.902E-00 163.36 5.08 8.091E-001 9.525E-002 3.794E-00 182.62 0.39 1.495E+001 -1.570E+000 7.123E+00 194.94 0.63 8.228E+000 2.768E+000 3.883E+00 202.12 1.08 4.821E+000 -1.446E+000 2.272E+00 205.32 5.02 1.034E+000 -6.249E-001 4.870E-00 221.39 0.12 4.774E+001 1.141E+001 2.250E+00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

4/19/2017 10:40:34 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2120\\W6H-IMC-212 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 1.07E+001 17.549 Pb-210 46.5 ^ 2.82E+000 40.906 Pb-212 74.8 7.66E-001 33.030 3.068[44.166] 3.40 -0.623 77.1 2.97E-001 39.545 1.189[49.228] [ 0.461]

238.6 ^ 2.50E-001 29.319 1.000[41.464]

Ra-226 186.2 ^ 1.36E+000 41.299