ML19095B358

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W6H-IMC-2120-S-P-3

ML19095B358
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Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
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References
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Text

• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2120\\W6H-IMC-212 Report Generated On : 4/19/2017 10:38:25 AM Sample Title : W6H-IMC-2120-S-P-3 Sample Description :

Sample Identification : 2120-S-P-3 Sample Type :

Sample Geometry : Cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.500 keV Sample Size : 2.315E+002 GRAMS Sample Taken On : 3/17/2017 12:00:00 AM Acquisition Started : 3/28/2017 10:12:49 AM Live Time : 1800.0 seconds Real Time : 1800.3 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 3/24/2017 Efficiency Calibration Used Done On : 4/19/2017 Efficiency ID : H-IMC-2120-S-P-3

Peak Analysis Report 4/19/2017 10:38:25 AM Page 1

• • • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W6H-IMC-2120-S-P-3 Peak Analysis Performed on: 4/19/2017 10:38:21 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts M 1 293-313 299.58 75.11 0.77 1.08E+002 25.14 7.85E+001 m 2 293-313 308.29 77.29 0.77 5.27E+001 19.06 6.49E+001 F 3 346-354 348.89 87.44 0.60 3.57E+001 15.96 4.20E+001 F 4 736-747 741.87 185.75 0.93 4.32E+001 17.03 3.75E+001 F 5 948-959 952.97 238.55 0.89 6.78E+001 20.91 5.70E+001 F 6 1175-1183 1179.32 295.17 0.71 2.07E+001 13.30 2.88E+001 F 7 5825-5851 5837.46 1460.39 2.59 1.67E+002 24.01 3.00E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 4/19/2017 10:38:25 AM Page 2

• • • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W6H-IMC-2120-S-P-3 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/GRAM) Uncertainty K-40 0.987 1460.82* 10.66 1.10321E+001 1.84379E+000 Pb-212 0.998 74.82* 10.28 9.30846E-001 2.86050E-001 77.11* 17.10 2.66238E-001 1.10286E-001 86.83 2.07 87.35* 3.97 7.28084E-001 3.56886E-001 89.78 1.46 115.18 0.60 238.63* 43.60 1.90613E-001 6.60666E-002 300.09 3.30 PB-214 0.270 74.82* 5.80 1.64984E+000 5.28053E-001 77.11* 9.70 4.69348E-001 1.98960E-001 86.83 1.70 87.35* 2.24 1.29040E+000 6.42041E-001 89.78 0.82 241.99 7.25 258.76 0.53 274.80 0.35 295.22* 18.42 1.69584E-001 1.12319E-001 351.93 35.60 462.02 0.21 480.43 0.34 487.14 0.43 533.66 0.18 580.14 0.37 785.96 1.06 839.07 0.58 Ra-226 0.987 81.07 0.20 83.79 0.32 186.21* 3.64 1.17407E+000 5.03832E-001

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.500 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 4/19/2017 10:38:25 AM Page 3

• • • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/GRAM) Uncertainty K-40 0.987 1.103212E+001 1.843794E+000 Pb-212 0.998 2.135658E-001 5.744026E-002 PB-214 0.270 2.069636E-001 9.890872E-002 Ra-226 0.987 1.174072E+000 5.038318E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

• • • • • • • • • • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 4/19/2017 10:38:21 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified.

Nuclide MDA Report 4/19/2017 10:38:25 AM Page 4

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Detector Name: 8566 Sample Geometry: Cylinder Sample

Title:

W6H-IMC-2120-S-P-3 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM

+ K-40 1460.82* 10.66 7.745E-001 7.74E-001 1.103E+001 2.978E-00 CO-60 1173.23 99.85 1.949E-001 1.60E-001 -1.614E-002 8.952E-00 1332.49 99.98 1.603E-001 -2.143E-002 7.133E-00 CS-137 661.66 85.10 1.571E-001 1.57E-001 -4.701E-002 7.304E-00 Pb-210 46.54 4.25 2.332E+000 2.33E+000 2.320E+000 1.111E+00 BI-212 288.20 0.34 1.916E+001 2.21E+000 9.188E-001 8.989E+00 328.03 0.13 5.974E+001 4.650E+001 2.805E+00 452.98 0.36 2.839E+001 1.011E+001 1.331E+00 727.33 6.67 2.211E+000 1.027E+000 1.028E+00 785.37 1.10 1.404E+001 2.227E+000 6.519E+00 893.41 0.38 4.127E+001 6.954E+000 1.899E+00 952.12 0.17 1.057E+002 5.620E+001 4.895E+00 1078.62 0.56 3.264E+001 -1.841E+001 1.502E+00 1512.70 0.29 6.390E+001 1.350E+001 2.856E+00 1620.50 1.47 1.089E+001 -4.088E-001 4.736E+00

+ Pb-212 74.82* 10.28 3.771E-001 1.18E-001 9.308E-001 1.769E-00 77.11* 17.10 2.032E-001 2.662E-001 9.478E-00 86.83 2.07 2.429E+000 -5.099E-001 1.161E+00 87.35* 3.97 7.427E-001 7.281E-001 3.438E-00 89.78 1.46 3.268E+000 -2.600E+000 1.560E+00 115.18 0.60 6.299E+000 2.283E+000 2.971E+00 238.63* 43.60 1.180E-001 1.906E-001 5.519E-00 300.09 3.30 2.314E+000 -1.918E+000 1.094E+00 BI-214 76.86 0.55 1.287E+001 3.30E-001 1.592E-001 6.221E+00 79.29 0.91 5.507E+000 -2.813E-001 2.627E+00 89.26 0.11 4.219E+001 -1.680E+001 2.011E+00 89.81 0.21 2.272E+001 -1.807E+001 1.084E+00 273.80 0.13 4.905E+001 1.532E+000 2.305E+00 348.92 0.10 9.350E+001 5.963E+001 4.441E+00 386.78 0.29 2.612E+001 9.918E+000 1.214E+00 388.89 0.40 1.818E+001 -1.289E+001 8.411E+00 405.72 0.17 5.396E+001 2.669E+001 2.529E+00 454.79 0.29 3.274E+001 6.784E-002 1.527E+00 469.77 0.13 6.754E+001 -6.861E+001 3.125E+00 609.32 45.49 3.301E-001 1.586E-001 1.555E-00 665.45 1.53 8.914E+000 1.663E+000 4.148E+00 703.11 0.47 2.978E+001 8.589E+000 1.383E+00 719.87 0.39 3.608E+001 -2.019E+001 1.674E+00 752.85 0.13 1.133E+002 -9.150E+001 5.251E+00 768.36 4.89 3.073E+000 -1.380E+000 1.426E+00 786.35 0.32 4.841E+001 3.016E+000 2.248E+00 806.18 1.26 1.101E+001 -9.897E+000 5.057E+00

Nuclide MDA Report 4/19/2017 10:38:25 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM BI-214 821.18 0.16 9.337E+001 3.30E-001 -5.294E+000 4.310E+00 826.45 0.12 1.292E+002 -7.327E+000 5.966E+00 934.06 3.11 6.106E+000 3.048E+000 2.844E+00 964.08 0.37 5.689E+001 5.074E+001 2.662E+00 1051.96 0.31 5.872E+001 2.535E+001 2.707E+00 1069.96 0.27 7.185E+001 -2.849E+000 3.325E+00 1120.29 14.92 1.411E+000 1.102E+000 6.544E-00 1133.66 0.25 7.412E+001 8.741E+000 3.401E+00 1155.21 1.63 1.301E+001 6.943E+000 6.028E+00 1207.68 0.45 4.679E+001 -1.086E+001 2.160E+00 1238.11 5.83 3.366E+000 1.715E+000 1.541E+00 1280.98 1.43 1.344E+001 -7.240E+000 6.125E+00 1303.75 0.11 1.805E+002 6.269E+001 8.217E+00 1377.67 3.99 4.876E+000 2.342E+000 2.211E+00 1385.31 0.79 2.204E+001 -7.215E+000 9.873E+00 1401.52 1.33 1.565E+001 1.460E+001 7.136E+00 1407.99 2.39 7.916E+000 1.901E+000 3.572E+00 1509.21 2.13 8.519E+000 2.762E+000 3.799E+00 1538.53 0.40 3.728E+001 1.174E+001 1.613E+00 1543.34 0.30 4.756E+001 1.302E+001 2.048E+00 1583.20 0.70 2.467E+001 2.039E+001 1.088E+00 1594.75 0.27 6.708E+001 3.455E+001 2.968E+00 1599.37 0.32 5.159E+001 -6.416E+000 2.261E+00 1661.27 1.05 1.315E+001 -3.170E+000 5.553E+00 1684.01 0.21 8.393E+001 5.403E+001 3.690E+00 1729.59 2.88 5.168E+000 2.094E+000 2.199E+00 1764.49 15.30 1.468E+000 8.764E-001 6.601E-00 1838.36 0.35 4.323E+001 1.576E+001 1.826E+00 1847.43 2.03 7.507E+000 -3.555E+000 3.170E+00 1873.16 0.21 5.828E+001 -3.885E+001 2.355E+00 1896.05 0.15 9.019E+001 -5.045E+001 3.697E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2293.38 0.31 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 6.684E-001 2.22E-001 1.650E+000 3.136E-00 77.11* 9.70 3.583E-001 4.693E-001 1.671E-00 86.83 1.70 2.958E+000 -6.209E-001 1.414E+00 87.35* 2.24 1.316E+000 1.290E+000 6.093E-00 89.78 0.82 5.819E+000 -4.629E+000 2.777E+00 241.99 7.25 1.153E+000 2.526E-001 5.535E-00 258.76 0.53 1.059E+001 1.197E+000 4.958E+00 274.80 0.35 1.795E+001 2.573E+000 8.441E+00 295.22* 18.42 2.218E-001 1.696E-001 9.981E-00 351.93 35.60 2.778E-001 1.681E-001 1.320E-00 462.02 0.21 4.347E+001 -1.567E+001 2.020E+00 480.43 0.34 2.916E+001 -1.568E+001 1.357E+00 487.14 0.43 2.290E+001 -1.300E+001 1.065E+00 533.66 0.18 5.911E+001 -3.719E+001 2.746E+00 580.14 0.37 3.548E+001 4.022E+001 1.662E+00 785.96 1.06 1.484E+001 4.496E+000 6.900E+00

Nuclide MDA Report 4/19/2017 10:38:25 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM

+ PB-214 839.07 0.58 2.727E+001 2.22E-001 6.923E+000 1.263E+00

+ Ra-226 81.07 0.20 1.909E+001 9.39E-001 -2.498E+001 8.967E+00 83.79 0.32 1.398E+001 1.252E+001 6.643E+00 186.21* 3.64 9.393E-001 1.174E+000 4.329E-00 AC-228 89.96 1.90 6.824E+013 1.65E+013 -5.428E+013 3.257E+01 93.35 3.10 3.933E+013 1.530E+013 1.873E+01 99.51 1.26 7.580E+013 -3.945E+012 3.561E+01 104.82 0.39 2.615E+014 2.249E+014 1.234E+01 105.60 0.74 1.378E+014 6.356E+013 6.502E+01 108.58 0.28 3.570E+014 -6.571E+013 1.683E+01 129.07 2.42 4.398E+013 1.144E+013 2.076E+01 145.85 0.16 7.085E+014 1.387E+014 3.345E+01 153.98 0.72 1.657E+014 8.837E+013 7.838E+01 191.35 0.12 1.081E+015 4.447E+014 5.100E+01 199.41 0.31 4.026E+014 -1.197E+014 1.891E+01 204.03 0.11 1.268E+015 1.229E+014 5.991E+01 209.25 3.89 3.801E+013 9.422E+012 1.798E+01 214.85 0.76 1.788E+014 -1.066E+014 8.399E+01 270.24 3.46 4.273E+013 -2.020E+013 1.990E+01 278.95 0.16 1.188E+015 5.600E+014 5.612E+01 321.65 0.23 8.432E+014 8.241E+014 3.947E+01 327.44 0.12 1.709E+015 1.391E+015 8.027E+01 328.00 2.95 6.882E+013 5.357E+013 3.231E+01 332.37 0.40 4.769E+014 -2.322E+013 2.227E+01 338.32 11.27 1.652E+013 9.866E+012 7.690E+01 340.96 0.37 5.310E+014 -2.973E+014 2.480E+01 409.46 1.92 1.246E+014 -3.617E+012 5.824E+01 440.44 0.12 2.150E+015 7.617E+014 1.005E+01 463.00 4.40 5.662E+013 -2.207E+013 2.628E+01 478.33 0.21 1.233E+015 -2.580E+014 5.725E+01 503.82 0.18 1.554E+015 -2.274E+015 7.235E+01 508.96 0.45 8.314E+014 7.278E+014 3.939E+01 523.13 0.10 2.630E+015 5.441E+013 1.217E+01 546.47 0.20 1.574E+015 5.248E+014 7.346E+01 562.50 0.87 3.692E+014 -6.704E+013 1.721E+01 570.91 0.18 1.698E+015 7.067E+014 7.881E+01 572.14 0.15 1.978E+015 -1.255E+015 9.153E+01 583.41 0.11 3.273E+015 1.842E+015 1.535E+01 674.75 2.10 1.749E+014 8.125E+013 8.126E+01 701.75 0.17 2.169E+015 7.144E+014 1.006E+01 707.41 0.16 2.460E+015 -3.901E+014 1.142E+01 726.86 0.62 6.362E+014 3.837E+014 2.955E+01 755.32 1.00 4.313E+014 4.236E+014 2.011E+01 772.29 1.49 2.976E+014 2.991E+013 1.389E+01 782.14 0.49 9.186E+014 2.366E+014 4.284E+01 794.95 4.25 9.334E+013 4.347E+012 4.309E+01 830.49 0.54 7.502E+014 -5.605E+014 3.457E+01 835.71 1.61 2.833E+014 1.990E+014 1.318E+01 840.38 0.91 4.544E+014 -3.901E+013 2.096E+01 904.20 0.77 5.681E+014 -7.763E+014 2.618E+01 911.20 25.80 1.867E+013 6.801E+012 8.665E+01

Nuclide MDA Report 4/19/2017 10:38:25 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM AC-228 947.98 0.11 4.087E+015 1.65E+013 9.328E+013 1.875E+01 958.61 0.28 1.677E+015 -1.266E+015 7.744E+01 964.77 4.99 1.110E+014 7.446E+013 5.185E+01 968.97 15.80 3.322E+013 1.388E+013 1.546E+01 1033.25 0.20 2.632E+015 1.119E+015 1.220E+01 1065.18 0.13 4.081E+015 8.502E+014 1.891E+01 1095.68 0.13 3.219E+015 -4.073E+015 1.453E+01 1110.61 0.28 1.976E+015 2.888E+014 9.162E+01 1153.52 0.14 3.893E+015 -1.146E+015 1.794E+01 1247.08 0.50 9.976E+014 2.152E+014 4.536E+01 1459.14 0.83 1.526E+015 3.775E+015 7.318E+01 1495.91 0.86 4.576E+014 -1.049E+014 1.980E+01 1501.57 0.46 1.003E+015 2.181E+014 4.440E+01 1557.11 0.18 1.984E+015 -6.074E+014 8.378E+01 1580.53 0.60 6.887E+014 -3.081E+014 2.980E+01 1588.20 3.22 1.664E+014 8.436E+013 7.453E+01 1625.06 0.25 1.808E+015 1.078E+015 7.922E+01 1630.63 1.51 3.216E+014 2.106E+014 1.419E+01 1638.28 0.47 8.794E+014 5.266E+013 3.786E+01 1666.52 0.18 2.109E+015 -9.382E+014 8.906E+01 TH-230 67.67 0.38 1.247E+001 1.25E+001 -4.625E+000 5.892E+00 PA-234 742.81 0.11 1.400E+002 1.83E+001 2.914E+001 6.508E+00 766.42 0.32 4.733E+001 -2.586E+001 2.196E+00 1001.03 0.84 1.826E+001 1.775E+000 8.315E+00 TH-234 63.29 3.70 1.432E+000 1.43E+000 -9.105E-001 6.777E-00 92.38 2.13 2.221E+000 3.079E+000 1.060E+00 92.80 2.10 2.162E+000 5.483E-001 1.030E+00 112.81 0.21 1.738E+001 -6.836E+000 8.184E+00 U-234 53.20 0.12 5.029E+001 5.03E+001 2.073E+001 2.367E+00 120.90 0.04 9.794E+001 -5.574E+001 4.591E+00 U-235 72.70 0.12 4.575E+001 3.64E-001 0.000E+000 2.185E+00 89.96 3.43 1.390E+000 -1.106E+000 6.635E-00 93.35 5.54 8.095E-001 3.149E-001 3.854E-00 104.82 0.69 5.476E+000 4.710E+000 2.584E+00 105.60 1.31 2.863E+000 1.321E+000 1.351E+00 108.58 0.50 7.354E+000 -1.353E+000 3.466E+00 109.19 1.66 2.192E+000 -8.626E-001 1.033E+00 140.76 0.20 1.816E+001 -1.090E+001 8.516E+00 143.76 10.96 3.639E-001 -3.748E-002 1.715E-00 163.36 5.08 8.642E-001 3.361E-001 4.080E-00 182.62 0.39 1.355E+001 9.079E-001 6.436E+00 194.94 0.63 7.639E+000 4.627E+000 3.599E+00 202.12 1.08 4.637E+000 1.555E+000 2.186E+00 205.32 5.02 1.051E+000 -1.868E-001 4.968E-00 221.39 0.12 4.774E+001 -8.485E+000 2.256E+00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

4/19/2017 10:38:25 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2120\\W6H-IMC-212 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/GRAM) %Uncert* [uncert]

K-40 1460.8 ^ 1.10E+001 16.713 Pb-212 74.8 9.31E-001 30.730 4.883[46.321] 5.49 -1.001 77.1 2.66E-001 41.424 1.397[54.011] [ 0.516]

87.3 7.28E-001 49.017 3.820[60.033]

238.6 ^ 1.91E-001 34.660 1.000[49.017]

PB-214 74.8 1.65E+000 ******

77.1 4.69E-001 ******

87.3 1.29E+000 ******

295.2 1.70E-001 ******

Ra-226 186.2 ^ 1.17E+000 42.913