ML19095B355
| ML19095B355 | |
| Person / Time | |
|---|---|
| Site: | 07000371 |
| Issue date: | 03/01/2018 |
| From: | Cabrera Services |
| To: | NRC Region 1 |
| Shared Package | |
| ml051740240 | List:
|
| References | |
| Download: ML19095B355 (12) | |
Text
- G A M M A S P E C T R U M A N A L Y S I S *****
Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2120\\W6H-IMC-212 Report Generated On : 4/19/2017 10:37:06 AM Sample Title : W6H-IMC-2120-S-P-2 Sample Description :
Sample Identification : 2120-S-P-2 Sample Type :
Sample Geometry : Cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.500 keV Sample Size : 2.292E+002 GRAMS Sample Taken On : 3/17/2017 12:00:00 AM Acquisition Started : 3/28/2017 8:25:26 AM Live Time : 1800.0 seconds Real Time : 1800.3 seconds Dead Time : 0.02 %
Energy Calibration Used Done On : 3/24/2017 Efficiency Calibration Used Done On : 4/19/2017 Efficiency ID : H-IMC-2120-S-P-2
Peak Analysis Report 4/19/2017 10:37:06 AM Page 1
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Detector Name: 8566 Sample
Title:
W6H-IMC-2120-S-P-2 Peak Analysis Performed on: 4/19/2017 10:37:02 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 305-312 308.52 77.35 0.70 5.53E+001 20.98 6.27E+001 F 2 737-748 742.09 185.80 0.74 4.99E+001 17.32 4.20E+001 F 3 948-958 953.45 238.67 0.84 7.15E+001 21.49 5.78E+001 F 4 1173-1186 1179.06 295.11 1.05 4.02E+001 16.75 4.06E+001 F 5 1401-1413 1406.24 351.94 1.20 7.08E+001 19.44 2.86E+001 F 6 2425-2441 2433.77 608.97 1.78 5.48E+001 16.79 2.13E+001 F 7 5827-5850 5838.23 1460.58 2.66 1.39E+002 22.11 5.33E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma
Interference Corrected Activity Report 4/19/2017 10:37:06 AM Page 2
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Sample
Title:
W6H-IMC-2120-S-P-2 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL
.................... IDENTIFIED NUCLIDES....................
Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/GRAM) Uncertainty K-40 0.996 1460.82* 10.66 9.29523E+000 1.67383E+000 Pb-212 0.999 74.82 10.28 77.11* 17.10 2.81022E-001 1.20683E-001 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 2.02758E-001 6.88607E-002 300.09 3.30 BI-214 0.361 76.86* 0.55 8.81738E+000 3.79485E+000 79.29 0.91 89.26 0.11 89.81 0.21 273.80 0.13 348.92 0.10 386.78 0.29 388.89 0.40 405.72 0.17 454.79 0.29 469.77 0.13 609.32* 45.49 3.89661E-001 1.27824E-001 665.45 1.53 703.11 0.47 719.87 0.39 752.85 0.13 768.36 4.89 786.35 0.32 806.18 1.26 821.18 0.16 826.45 0.12 934.06 3.11 964.08 0.37 1051.96 0.31 1069.96 0.27 1120.29 14.92 1133.66 0.25 1155.21 1.63 1207.68 0.45 1238.11 5.83 1280.98 1.43 1303.75 0.11 1377.67 3.99
Interference Corrected Activity Report 4/19/2017 10:37:06 AM Page 3 Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/GRAM) Uncertainty BI-214 0.361 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1538.53 0.40 1543.34 0.30 1583.20 0.70 1594.75 0.27 1599.37 0.32 1661.27 1.05 1684.01 0.21 1729.59 2.88 1764.49 15.30 1838.36 0.35 1847.43 2.03 1873.16 0.21 1896.05 0.15 2118.51 1.16 2204.06 4.92 2293.38 0.31 2447.70 1.55 PB-214 0.999 74.82 5.80 77.11* 9.70 4.95410E-001 2.17375E-001 86.83 1.70 87.35 2.24 89.78 0.82 241.99 7.25 258.76 0.53 274.80 0.35 295.22* 18.42 3.32265E-001 1.48013E-001 351.93* 35.60 3.64062E-001 1.13267E-001 462.02 0.21 480.43 0.34 487.14 0.43 533.66 0.18 580.14 0.37 785.96 1.06 839.07 0.58 Ra-226 0.990 81.07 0.20 83.79 0.32 186.21* 3.64 1.36626E+000 5.28002E-001
- = Energy line found in the spectrum.
@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.500 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma
Interference Corrected Activity Report 4/19/2017 10:37:06 AM Page 4
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Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/GRAM) Uncertainty K-40 0.996 9.295232E+000 1.673826E+000 Pb-212 0.999 1.736557E-001 6.079287E-002 BI-214 0.361 3.864526E-001 1.277470E-001 PB-214 0.999 3.240302E-001 8.438809E-002 Ra-226 0.990 1.366260E+000 5.280018E-001
? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma
- U N I D E N T I F I E D P E A K S **********
Peak Locate Performed on: 4/19/2017 10:37:01 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.
No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified.
Nuclide MDA Report 4/19/2017 10:37:06 AM Page 5
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Detector Name: 8566 Sample Geometry: Cylinder Sample
Title:
W6H-IMC-2120-S-P-2 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM
+ K-40 1460.82* 10.66 9.549E-001 9.55E-001 9.295E+000 3.872E-00 CO-60 1173.23 99.85 2.147E-001 1.91E-001 1.047E-001 9.934E-00 1332.49 99.98 1.915E-001 2.052E-002 8.681E-00 CS-137 661.66 85.10 1.534E-001 1.53E-001 4.683E-002 7.114E-00 Pb-210 46.54 4.25 2.346E+000 2.35E+000 2.831E+000 1.117E+00 BI-212 288.20 0.34 1.921E+001 2.14E+000 -9.707E+000 9.007E+00 328.03 0.13 6.401E+001 1.427E+001 3.017E+00 452.98 0.36 2.683E+001 -1.661E+001 1.252E+00 727.33 6.67 2.142E+000 7.484E-001 9.933E-00 785.37 1.10 1.296E+001 -1.498E+000 5.972E+00 893.41 0.38 4.530E+001 2.289E+001 2.099E+00 952.12 0.17 1.029E+002 -1.445E+001 4.753E+00 1078.62 0.56 3.260E+001 -1.954E+001 1.499E+00 1512.70 0.29 5.087E+001 -1.166E+001 2.202E+00 1620.50 1.47 9.241E+000 -3.065E+000 3.903E+00
+ Pb-212 74.82 10.28 6.729E-001 1.17E-001 9.176E-001 3.247E-00 77.11* 17.10 2.159E-001 2.810E-001 1.011E-00 86.83 2.07 2.400E+000 1.322E+000 1.147E+00 87.35 3.97 1.225E+000 -8.212E-002 5.849E-00 89.78 1.46 3.104E+000 -2.487E-001 1.477E+00 115.18 0.60 6.183E+000 4.179E+000 2.912E+00 238.63* 43.60 1.169E-001 2.028E-001 5.461E-00 300.09 3.30 2.223E+000 -4.414E-001 1.048E+00
+ BI-214 76.86* 0.55 6.776E+000 1.87E-001 8.817E+000 3.172E+00 79.29 0.91 5.943E+000 -2.201E+000 2.844E+00 89.26 0.11 4.173E+001 2.977E+001 1.987E+00 89.81 0.21 2.158E+001 -1.729E+000 1.027E+00 273.80 0.13 5.222E+001 -1.820E+001 2.462E+00 348.92 0.10 1.024E+002 -1.220E+002 4.883E+00 386.78 0.29 2.655E+001 -1.213E+001 1.235E+00 388.89 0.40 2.019E+001 -6.928E+000 9.411E+00 405.72 0.17 5.443E+001 2.692E+001 2.551E+00 454.79 0.29 3.418E+001 1.539E+001 1.598E+00 469.77 0.13 7.875E+001 -2.067E+001 3.683E+00 609.32* 45.49 1.867E-001 3.897E-001 8.376E-00 665.45 1.53 8.201E+000 -3.948E+000 3.789E+00 703.11 0.47 3.005E+001 1.395E+001 1.396E+00 719.87 0.39 3.486E+001 1.940E+000 1.612E+00 752.85 0.13 1.114E+002 -3.387E+001 5.149E+00 768.36 4.89 3.250E+000 2.113E+000 1.513E+00 786.35 0.32 4.334E+001 -2.315E+001 1.992E+00 806.18 1.26 1.326E+001 8.887E+000 6.176E+00
Nuclide MDA Report 4/19/2017 10:37:06 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM
+ BI-214 821.18 0.16 9.241E+001 1.87E-001 -2.041E+001 4.259E+00 826.45 0.12 1.328E+002 1.347E+001 6.141E+00 934.06 3.11 5.163E+000 2.409E+000 2.371E+00 964.08 0.37 5.020E+001 4.073E+001 2.326E+00 1051.96 0.31 5.688E+001 4.281E-001 2.612E+00 1069.96 0.27 7.120E+001 7.374E+000 3.290E+00 1120.29 14.92 1.590E+000 1.102E+000 7.436E-00 1133.66 0.25 8.326E+001 2.518E+001 3.855E+00 1155.21 1.63 1.302E+001 3.937E+000 6.027E+00 1207.68 0.45 4.301E+001 -3.832E+001 1.969E+00 1238.11 5.83 4.032E+000 1.136E+000 1.873E+00 1280.98 1.43 1.303E+001 6.642E-001 5.918E+00 1303.75 0.11 1.536E+002 -3.012E+000 6.867E+00 1377.67 3.99 4.323E+000 -8.287E-001 1.932E+00 1385.31 0.79 2.303E+001 3.997E+000 1.035E+00 1401.52 1.33 1.619E+001 4.242E+000 7.399E+00 1407.99 2.39 8.586E+000 1.439E-001 3.904E+00 1509.21 2.13 7.523E+000 3.284E+000 3.296E+00 1538.53 0.40 4.199E+001 4.988E+000 1.846E+00 1543.34 0.30 5.794E+001 2.094E+001 2.563E+00 1583.20 0.70 2.603E+001 6.139E+000 1.155E+00 1594.75 0.27 6.770E+001 1.216E+001 2.995E+00 1599.37 0.32 5.207E+001 1.229E+001 2.282E+00 1661.27 1.05 1.327E+001 -4.952E-001 5.604E+00 1684.01 0.21 5.987E+001 -3.679E+001 2.483E+00 1729.59 2.88 5.603E+000 2.689E+000 2.412E+00 1764.49 15.30 1.431E+000 5.732E-001 6.411E-00 1838.36 0.35 3.974E+001 -1.653E+001 1.648E+00 1847.43 2.03 9.015E+000 1.762E+000 3.919E+00 1873.16 0.21 5.469E+001 -2.732E+001 2.170E+00 1896.05 0.15 1.141E+002 2.728E+000 4.885E+00
> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00
> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00
> 2293.38 0.31 0.000E+000 0.000E+000 0.000E+00
> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00
+ PB-214 74.82 5.80 1.193E+000 1.51E-001 1.626E+000 5.756E-00 77.11* 9.70 3.807E-001 4.954E-001 1.782E-00 86.83 1.70 2.923E+000 1.610E+000 1.396E+00 87.35 2.24 2.172E+000 -1.455E-001 1.037E+00 89.78 0.82 5.527E+000 -4.429E-001 2.631E+00 241.99 7.25 1.180E+000 -5.656E-001 5.667E-00 258.76 0.53 1.153E+001 4.477E+000 5.426E+00 274.80 0.35 1.821E+001 -9.382E+000 8.562E+00 295.22* 18.42 2.909E-001 3.323E-001 1.343E-00 351.93* 35.60 1.510E-001 3.641E-001 6.856E-00 462.02 0.21 5.066E+001 4.790E-001 2.377E+00 480.43 0.34 3.397E+001 1.620E+001 1.597E+00 487.14 0.43 2.564E+001 -6.211E+000 1.201E+00 533.66 0.18 6.465E+001 3.843E+001 3.021E+00 580.14 0.37 3.837E+001 6.866E+000 1.806E+00 785.96 1.06 1.294E+001 -4.536E+000 5.943E+00
Nuclide MDA Report 4/19/2017 10:37:06 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM
+ PB-214 839.07 0.58 2.628E+001 1.51E-001 -1.048E+001 1.212E+00
+ Ra-226 81.07 0.20 2.101E+001 9.98E-001 -2.800E+000 9.921E+00 83.79 0.32 1.368E+001 2.655E+000 6.494E+00 186.21* 3.64 9.980E-001 1.366E+000 4.619E-00 AC-228 89.96 1.90 5.298E+013 1.52E+013 -4.245E+012 2.521E+01 93.35 3.10 2.803E+013 -1.745E+013 1.324E+01 99.51 1.26 6.343E+013 -4.405E+012 2.983E+01 104.82 0.39 2.065E+014 -3.956E+013 9.717E+01 105.60 0.74 1.105E+014 1.337E+013 5.208E+01 108.58 0.28 2.984E+014 2.038E+014 1.407E+01 129.07 2.42 4.084E+013 3.498E+013 1.941E+01 145.85 0.16 5.836E+014 -2.615E+014 2.755E+01 153.98 0.72 1.333E+014 -5.925E+013 6.301E+01 191.35 0.12 8.947E+014 -8.296E+013 4.224E+01 199.41 0.31 3.978E+014 1.842E+014 1.888E+01 204.03 0.11 1.040E+015 -9.251E+014 4.912E+01 209.25 3.89 3.000E+013 4.392E+012 1.415E+01 214.85 0.76 1.481E+014 -1.232E+012 6.963E+01 270.24 3.46 4.407E+013 2.569E+013 2.082E+01 278.95 0.16 8.959E+014 -5.375E+014 4.209E+01 321.65 0.23 6.815E+014 -1.146E+015 3.186E+01 327.44 0.12 1.479E+015 9.893E+014 6.970E+01 328.00 2.95 6.027E+013 1.344E+013 2.840E+01 332.37 0.40 3.877E+014 -5.742E+014 1.809E+01 338.32 11.27 1.516E+013 -8.651E+011 7.110E+01 340.96 0.37 4.832E+014 2.238E+014 2.272E+01 409.46 1.92 1.127E+014 9.242E+013 5.297E+01 440.44 0.12 1.712E+015 1.384E+014 7.985E+01 463.00 4.40 5.371E+013 -1.038E+013 2.518E+01 478.33 0.21 1.219E+015 3.292E+014 5.729E+01 503.82 0.18 1.328E+015 -2.046E+015 6.201E+01 508.96 0.45 7.448E+014 9.704E+014 3.544E+01 523.13 0.10 2.474E+015 8.573E+014 1.156E+01 546.47 0.20 1.334E+015 6.810E+014 6.238E+01 562.50 0.87 3.000E+014 1.525E+013 1.397E+01 570.91 0.18 1.509E+015 5.364E+014 7.045E+01 572.14 0.15 1.835E+015 1.158E+015 8.566E+01 583.41 0.11 2.858E+015 3.301E+015 1.345E+01 674.75 2.10 1.419E+014 5.943E+013 6.584E+01 701.75 0.17 1.818E+015 1.165E+015 8.446E+01 707.41 0.16 1.944E+015 -2.145E+014 8.995E+01 726.86 0.62 5.075E+014 2.132E+014 2.351E+01 755.32 1.00 3.177E+014 -6.442E+013 1.469E+01 772.29 1.49 2.384E+014 -2.164E+013 1.110E+01 782.14 0.49 6.829E+014 1.561E+014 3.160E+01 794.95 4.25 7.911E+013 -2.961E+013 3.660E+01 830.49 0.54 6.306E+014 -3.575E+013 2.911E+01 835.71 1.61 2.186E+014 2.800E+013 1.012E+01 840.38 0.91 3.853E+014 1.172E+014 1.782E+01 904.20 0.77 4.909E+014 -5.725E+014 2.271E+01 911.20 25.80 1.660E+013 9.677E+012 7.747E+01
Nuclide MDA Report 4/19/2017 10:37:06 AM Page 8 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM) (pCi/GRAM AC-228 947.98 0.11 3.817E+015 1.52E+013 2.468E+015 1.770E+01 958.61 0.28 1.303E+015 -2.010E+014 5.982E+01 964.77 4.99 8.165E+013 4.343E+013 3.783E+01 968.97 15.80 2.697E+013 1.245E+013 1.254E+01 1033.25 0.20 1.875E+015 -7.839E+014 8.584E+01 1065.18 0.13 3.423E+015 1.858E+015 1.588E+01 1095.68 0.13 3.038E+015 -2.744E+015 1.390E+01 1110.61 0.28 1.684E+015 -9.225E+014 7.827E+01 1153.52 0.14 3.394E+015 1.380E+015 1.571E+01 1247.08 0.50 9.820E+014 7.584E+013 4.537E+01 1459.14 0.83 1.209E+015 3.041E+015 5.788E+01 1495.91 0.86 4.108E+014 -3.024E+013 1.800E+01 1501.57 0.46 7.901E+014 2.405E+014 3.474E+01 1557.11 0.18 1.947E+015 -3.131E+013 8.464E+01 1580.53 0.60 6.020E+014 -1.977E+014 2.628E+01 1588.20 3.22 1.421E+014 1.010E+014 6.389E+01 1625.06 0.25 1.236E+015 4.807E+014 5.257E+01 1630.63 1.51 2.172E+014 1.924E+012 9.301E+01 1638.28 0.47 7.254E+014 4.344E+013 3.123E+01 1666.52 0.18 1.811E+015 3.495E+013 7.705E+01 TH-230 67.67 0.38 1.242E+001 1.24E+001 1.322E+000 5.862E+00 PA-234 742.81 0.11 1.401E+002 2.09E+001 1.234E+001 6.510E+00 766.42 0.32 4.853E+001 -3.636E-001 2.254E+00 1001.03 0.84 2.089E+001 1.284E+001 9.619E+00 TH-234 63.29 3.70 1.386E+000 1.39E+000 -1.556E-001 6.548E-00 92.38 2.13 2.000E+000 1.803E+000 9.493E-00 92.80 2.10 1.926E+000 -4.947E-001 9.115E-00 112.81 0.21 1.768E+001 -9.013E+000 8.334E+00 U-234 53.20 0.12 4.241E+001 4.24E+001 -1.186E+001 1.972E+00 120.90 0.04 9.804E+001 7.125E+000 4.593E+00 U-235 72.70 0.12 4.807E+001 4.04E-001 -7.762E+001 2.301E+00 89.96 3.43 1.321E+000 -1.058E-001 6.285E-00 93.35 5.54 7.058E-001 -4.393E-001 3.334E-00 104.82 0.69 5.290E+000 -1.013E+000 2.490E+00 105.60 1.31 2.810E+000 3.399E-001 1.324E+00 108.58 0.50 7.519E+000 5.137E+000 3.547E+00 109.19 1.66 2.254E+000 4.106E-001 1.063E+00 140.76 0.20 2.050E+001 -3.468E+000 9.680E+00 143.76 10.96 4.041E-001 3.670E-001 1.916E-00 163.36 5.08 8.229E-001 -3.634E-001 3.872E-00 182.62 0.39 1.438E+001 -6.880E+000 6.849E+00 194.94 0.63 7.820E+000 -4.377E+000 3.688E+00 202.12 1.08 5.042E+000 1.716E+000 2.388E+00 205.32 5.02 1.019E+000 -8.288E-001 4.804E-00 221.39 0.12 4.409E+001 1.735E+001 2.072E+00
+ = Nuclide identified during the nuclide identification
- = Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
4/19/2017 10:37:06 LACE Lace v3.2.1 Page 1
- L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
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Analysis using Key Line Activities
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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2120\\W6H-IMC-212 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:
'^' Denotes Key Line energy
- All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/GRAM) %Uncert* [uncert]
K-40 1460.8 ^ 9.30E+000 18.007 Pb-212 77.1 2.81E-001 42.944 1.386[54.751] 1.58 -0.289 238.6 ^ 2.03E-001 33.962 1.000[48.030] [ 0.645]
4/19/17 10:37:06 LACE - Key Line Results Page 2 Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/GRAM) %Uncert* [uncert]
BI-214 76.9 8.82E+000 43.038 22.628[54.115] 9.66 -1.507 609.3 ^ 3.90E-001 32.804 1.000[46.392] [ 0.344]
PB-214 77.1 4.95E-001 43.878 1.361[53.789] 1.29 -0.228 295.2 3.32E-001 44.547 0.913[54.336] [ 0.437]
351.9 ^ 3.64E-001 31.112 1.000[43.999]
Ra-226 186.2 ^ 1.37E+000 38.646