ML19095B349

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W6H-IMC-2079-S-P-8

ML19095B349
Person / Time
Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
Shared Package
ml051740240	List: ML19095A013 ML19095A014 ML19095A016 ML19095A017 ML19095A018 ML19095A019 ML19095A020 ML19095A021 ML19095A022 ML19095A023 ML19095A024 ML19095A025 ML19095A030 ML19095A034 ML19095A035 ML19095A036 ML19095A037 ML19095A038 ML19095A040 ML19095A042 ML19095A043 ML19095A045 ML19095A046 ML19095A048 ML19095A049 ML19095A051 ML19095A052 ML19095A055 ML19095A056 ML19095A060 ML19095A061 ML19095A063 ML19095A064 ML19095A067 ML19095A069 ML19095A198 ML19095A200 ML19095A201 ML19095A204 ML19095A205 ML19095A206 ML19095A268 ML19095A269 ML19095A319 ML19095A321 ML19095A322 ML19095A324 ML19095A325 ML19095A326 ML19095A328 ... further results
References
Download: ML19095B349 (11)

Text

• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2079\\W6H-IMC-207 Report Generated On : 5/1/2017 10:01:09 AM Sample Title : W6H-IMC-2079-S-P-8 Sample Description :

Sample Identification : 2079-S-P-8 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 2.861E+002 grams Sample Taken On : 3/17/2017 12:00:00 AM Acquisition Started : 3/31/2017 2:02:31 PM Live Time : 1800.0 seconds Real Time : 1800.3 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 3/24/2017 Efficiency Calibration Used Done On : 5/1/2017 Efficiency ID : H-IMC-2079-S-P-8

Peak Analysis Report 5/1/2017 10:01:09 AM Page 1

• • • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W6H-IMC-2079-S-P-8 Peak Analysis Performed on: 5/1/2017 10:01:05 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 179-190 186.09 46.72 0.77 6.04E+001 18.74 4.00E+001 M 2 295-316 299.87 75.18 0.63 5.88E+001 20.46 6.86E+001 m 3 295-316 308.91 77.44 0.64 4.83E+001 17.52 4.57E+001 F 4 365-377 370.23 92.78 1.04 5.00E+001 18.11 4.12E+001 F 5 949-958 953.02 238.57 0.85 5.81E+001 19.48 4.50E+001 F 6 1400- 1410 1405.09 351.65 1.05 2.91E+001 14.44 2.42E+001 F 7 5824-5851 5836.72 1460.21 3.13 1.51E+002 22.40 9.33E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/1/2017 10:01:09 AM Page 2

• • • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W6H-IMC-2079-S-P-8 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.941 1460.82* 10.66 9.36266E+000 1.60009E+000 Pb-210 0.995 46.54* 4.25 2.45316E+000 1.03067E+000 Pb-212 0.993 74.82* 10.28 4.88728E-001 1.96612E-001 77.11* 17.10 2.36197E-001 9.79303E-002 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 1.53882E-001 5.70962E-002 300.09 3.30 PB-214 0.658 74.82* 5.80 8.66228E-001 3.56993E-001 77.11* 9.70 4.16388E-001 1.76663E-001 86.83 1.70 87.35 2.24 89.78 0.82 241.99 7.25 258.76 0.53 274.80 0.35 295.22 18.42 351.93* 35.60 1.39411E-001 7.21945E-002 462.02 0.21 480.43 0.34 487.14 0.43 533.66 0.18 580.14 0.37 785.96 1.06 839.07 0.58 TH-234 0.330 63.29 3.70 92.38 2.13 92.80* 2.10 1.81588E+000 8.21148E-001 112.81 0.21 U-235 0.507 72.70 0.12 89.96 3.43 93.35* 5.54 6.88328E-001 2.85551E-001 104.82 0.69 105.60 1.31 108.58 0.50 109.19 1.66 140.76 0.20 143.76 10.96 163.36 5.08 182.62 0.39

Interference Corrected Activity Report 5/1/2017 10:01:09 AM Page 3 Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty U-235 0.507 194.94 0.63 202.12 1.08 205.32 5.02 221.39 0.12

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/1/2017 10:01:09 AM Page 4

• • • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.941 9.362665E+000 1.600090E+000 Pb-210 0.995 2.453160E+000 1.030670E+000 Pb-212 0.993 1.678092E-001 4.903705E-002 PB-214 0.658 1.519902E-001 6.719017E-002

? TH-234 0.330 1.815875E+000 8.211482E-001

? U-235 0.507 6.883281E-001 2.855511E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

• • • • • • • • • • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 5/1/2017 10:01:05 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified.

Nuclide MDA Report 5/1/2017 10:01:09 AM Page 5

• • • • • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W6H-IMC-2079-S-P-8 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 1.163E+000 1.16E+000 9.363E+000 4.977E-00 CO-60 1173.23 99.85 1.688E-001 1.65E-001 -5.374E-002 7.694E-00 1332.49 99.98 1.650E-001 -5.591E-002 7.418E-00 CS-137 661.66 85.10 1.291E-001 1.29E-001 1.373E-003 5.934E-00

+ Pb-210 46.54* 4.25 1.574E+000 1.57E+000 2.453E+000 7.319E-00 BI-212 288.20 0.34 1.806E+001 2.11E+000 2.226E+000 8.471E+00 328.03 0.13 5.251E+001 -4.126E+001 2.454E+00 452.98 0.36 2.504E+001 -2.179E+001 1.169E+00 727.33 6.67 2.111E+000 1.341E-001 9.829E-00 785.37 1.10 1.207E+001 -2.667E+000 5.564E+00 893.41 0.38 3.318E+001 -5.324E+001 1.505E+00 952.12 0.17 9.576E+001 -2.269E+001 4.424E+00 1078.62 0.56 3.217E+001 1.620E+001 1.486E+00 1512.70 0.29 5.522E+001 1.200E+001 2.443E+00 1620.50 1.47 1.158E+001 7.907E+000 5.123E+00

+ Pb-212 74.82* 10.28 3.430E-001 9.49E-002 4.887E-001 1.602E-00 77.11* 17.10 1.669E-001 2.362E-001 7.684E-00 86.83 2.07 2.211E+000 6.798E-001 1.054E+00 87.35 3.97 1.115E+000 -7.856E-001 5.309E-00 89.78 1.46 2.708E+000 9.243E-001 1.283E+00 115.18 0.60 5.728E+000 1.047E+000 2.694E+00 238.63* 43.60 9.492E-002 1.539E-001 4.387E-00 300.09 3.30 2.098E+000 -9.432E-001 9.894E-00 BI-214 76.86 0.55 1.118E+001 2.70E-001 1.467E+001 5.380E+00 79.29 0.91 5.200E+000 9.065E-002 2.477E+00 89.26 0.11 3.619E+001 2.482E+001 1.714E+00 89.81 0.21 1.883E+001 6.425E+000 8.918E+00 273.80 0.13 4.830E+001 2.248E+001 2.276E+00 348.92 0.10 7.784E+001 6.186E+001 3.672E+00 386.78 0.29 2.663E+001 -2.559E+000 1.245E+00 388.89 0.40 1.926E+001 -1.558E+000 8.990E+00 405.72 0.17 4.823E+001 -7.163E+000 2.253E+00 454.79 0.29 3.233E+001 -7.663E+000 1.513E+00 469.77 0.13 5.886E+001 -6.663E+001 2.706E+00 609.32 45.49 2.705E-001 1.707E-001 1.263E-00 665.45 1.53 8.058E+000 1.212E+000 3.738E+00 703.11 0.47 2.686E+001 -7.920E+000 1.244E+00 719.87 0.39 3.530E+001 -1.130E+001 1.643E+00 752.85 0.13 1.093E+002 1.733E+001 5.073E+00 768.36 4.89 3.051E+000 2.046E+000 1.422E+00 786.35 0.32 3.995E+001 -4.468E+001 1.835E+00 806.18 1.26 1.179E+001 7.344E-001 5.472E+00

Nuclide MDA Report 5/1/2017 10:01:09 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram BI-214 821.18 0.16 8.524E+001 2.70E-001 5.686E+000 3.925E+00 826.45 0.12 1.106E+002 -7.551E+001 5.066E+00 934.06 3.11 5.384E+000 -1.705E+000 2.496E+00 964.08 0.37 5.479E+001 2.224E+001 2.568E+00 1051.96 0.31 5.235E+001 1.583E+001 2.402E+00 1069.96 0.27 6.864E+001 2.093E+001 3.180E+00 1120.29 14.92 1.335E+000 9.349E-001 6.196E-00 1133.66 0.25 6.879E+001 -1.005E+001 3.153E+00 1155.21 1.63 1.013E+001 -7.031E-001 4.619E+00 1207.68 0.45 4.089E+001 -9.410E+000 1.876E+00 1238.11 5.83 3.498E+000 1.818E+000 1.616E+00 1280.98 1.43 1.211E+001 2.058E+000 5.499E+00 1303.75 0.11 1.799E+002 6.718E+001 8.237E+00 1377.67 3.99 4.015E+000 9.361E-001 1.795E+00 1385.31 0.79 2.029E+001 1.326E+000 9.069E+00 1401.52 1.33 1.430E+001 5.591E+000 6.500E+00 1407.99 2.39 7.758E+000 3.579E+000 3.517E+00 1509.21 2.13 7.827E+000 1.081E+000 3.482E+00 1538.53 0.40 3.702E+001 -1.216E+001 1.616E+00 1543.34 0.30 4.602E+001 -2.059E+001 1.991E+00 1583.20 0.70 2.144E+001 4.526E+000 9.358E+00 1594.75 0.27 5.539E+001 -1.262E+001 2.408E+00 1599.37 0.32 4.442E+001 4.784E+000 1.922E+00 1661.27 1.05 1.232E+001 -5.480E+000 5.202E+00 1684.01 0.21 6.824E+001 3.310E+001 2.938E+00 1729.59 2.88 5.024E+000 2.229E+000 2.151E+00 1764.49 15.30 1.060E+000 5.805E-001 4.608E-00 1838.36 0.35 4.049E+001 6.275E+000 1.710E+00 1847.43 2.03 7.598E+000 4.238E-001 3.253E+00 1873.16 0.21 7.541E+001 2.051E+001 3.247E+00 1896.05 0.15 1.096E+002 -3.516E+001 4.718E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2293.38 0.31 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 6.079E-001 1.25E-001 8.662E-001 2.840E-00 77.11* 9.70 2.942E-001 4.164E-001 1.355E-00 86.83 1.70 2.692E+000 8.278E-001 1.284E+00 87.35 2.24 1.976E+000 -1.392E+000 9.409E-00 89.78 0.82 4.822E+000 1.646E+000 2.284E+00 241.99 7.25 1.043E+000 -1.756E-001 4.999E-00 258.76 0.53 1.135E+001 -2.351E-002 5.359E+00 274.80 0.35 1.673E+001 2.836E+000 7.860E+00 295.22 18.42 3.696E-001 1.237E-002 1.743E-00 351.93* 35.60 1.254E-001 1.394E-001 5.623E-00 462.02 0.21 4.497E+001 3.219E+001 2.103E+00 480.43 0.34 2.807E+001 -5.448E+000 1.308E+00 487.14 0.43 2.254E+001 -1.270E+001 1.052E+00 533.66 0.18 5.518E+001 2.334E+001 2.562E+00 580.14 0.37 3.317E+001 1.087E+001 1.554E+00 785.96 1.06 1.206E+001 -1.348E+001 5.537E+00

Nuclide MDA Report 5/1/2017 10:01:09 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 839.07 0.58 2.715E+001 1.25E-001 1.907E+001 1.263E+00 Ra-226 81.07 0.20 1.855E+001 1.50E+000 -5.652E+000 8.713E+00 83.79 0.32 1.373E+001 1.174E+001 6.533E+00 186.21 3.64 1.496E+000 1.602E+000 7.134E-00 AC-228 89.96 1.90 2.911E+017 9.23E+016 9.934E+016 1.379E+01 93.35 3.10 1.800E+017 1.031E+017 8.537E+01 99.51 1.26 3.738E+017 2.682E+017 1.756E+01 104.82 0.39 1.180E+018 -1.429E+017 5.539E+01 105.60 0.74 6.471E+017 3.481E+017 3.045E+01 108.58 0.28 1.633E+018 -5.219E+017 7.660E+01 129.07 2.42 2.132E+017 -2.163E+017 1.006E+01 145.85 0.16 3.286E+018 4.099E+017 1.547E+01 153.98 0.72 7.435E+017 5.092E+017 3.500E+01 191.35 0.12 5.358E+018 1.809E+018 2.532E+01 199.41 0.31 2.046E+018 8.836E+017 9.636E+01 204.03 0.11 5.801E+018 4.561E+017 2.730E+01 209.25 3.89 1.611E+017 -6.382E+016 7.553E+01 214.85 0.76 8.735E+017 5.545E+017 4.105E+01 270.24 3.46 2.558E+017 7.009E+016 1.207E+01 278.95 0.16 5.058E+018 2.823E+017 2.370E+01 321.65 0.23 4.192E+018 1.348E+018 1.966E+01 327.44 0.12 7.945E+018 -1.016E+018 3.723E+01 328.00 2.95 3.114E+017 -2.447E+017 1.455E+01 332.37 0.40 2.164E+018 -1.802E+018 1.006E+01 338.32 11.27 9.232E+016 8.550E+016 4.340E+01 340.96 0.37 2.762E+018 1.222E+018 1.296E+01 409.46 1.92 6.242E+017 4.543E+017 2.923E+01 440.44 0.12 1.021E+019 -3.567E+018 4.766E+01 463.00 4.40 2.958E+017 8.944E+016 1.381E+01 478.33 0.21 6.167E+018 3.159E+018 2.870E+01 503.82 0.18 8.383E+018 -5.343E+018 3.932E+01 508.96 0.45 4.231E+018 5.534E+018 2.010E+01 523.13 0.10 1.286E+019 6.151E+017 5.953E+01 546.47 0.20 7.008E+018 4.708E+017 3.249E+01 562.50 0.87 1.681E+018 4.928E+017 7.799E+01 570.91 0.18 8.157E+018 -5.434E+016 3.784E+01 572.14 0.15 1.016E+019 7.269E+017 4.723E+01 583.41 0.11 1.496E+019 4.280E+018 6.987E+01 674.75 2.10 8.194E+017 -1.428E+017 3.796E+01 701.75 0.17 1.033E+019 -1.799E+018 4.785E+01 707.41 0.16 1.210E+019 -1.574E+017 5.625E+01 726.86 0.62 3.224E+018 1.494E+018 1.503E+01 755.32 1.00 1.865E+018 0.000E+000 8.623E+01 772.29 1.49 1.334E+018 -7.290E+017 6.191E+01 782.14 0.49 4.008E+018 2.527E+018 1.854E+01 794.95 4.25 4.684E+017 7.225E+016 2.169E+01 830.49 0.54 3.665E+018 -1.079E+018 1.691E+01 835.71 1.61 1.317E+018 2.704E+017 6.104E+01 840.38 0.91 2.380E+018 1.483E+017 1.105E+01 904.20 0.77 3.435E+018 7.316E+017 1.610E+01 911.20 25.80 1.070E+017 -1.994E+016 5.026E+01

Nuclide MDA Report 5/1/2017 10:01:09 AM Page 8 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram AC-228 947.98 0.11 2.141E+019 9.23E+016 -9.397E+017 9.893E+01 958.61 0.28 8.628E+018 -2.141E+018 4.003E+01 964.77 4.99 5.682E+017 4.768E+017 2.666E+01 968.97 15.80 1.746E+017 1.306E+017 8.175E+01 1033.25 0.20 1.060E+019 4.124E+018 4.838E+01 1065.18 0.13 1.813E+019 3.107E+018 8.341E+01 1095.68 0.13 2.171E+019 1.166E+019 1.010E+01 1110.61 0.28 9.467E+018 -8.179E+017 4.386E+01 1153.52 0.14 1.643E+019 -5.842E+018 7.479E+01 1247.08 0.50 5.587E+018 -1.312E+018 2.575E+01 1459.14 0.83 7.248E+018 1.838E+019 3.474E+01 1495.91 0.86 2.523E+018 1.268E+018 1.113E+01 1501.57 0.46 5.442E+018 1.521E+018 2.442E+01 1557.11 0.18 1.139E+019 6.134E+018 4.950E+01 1580.53 0.60 3.217E+018 2.477E+017 1.385E+01 1588.20 3.22 6.937E+017 6.868E+016 3.050E+01 1625.06 0.25 9.571E+018 6.794E+018 4.247E+01 1630.63 1.51 1.399E+018 4.798E+017 6.080E+01 1638.28 0.47 3.792E+018 -2.117E+018 1.602E+01 1666.52 0.18 1.137E+019 -2.773E+018 4.897E+01 TH-230 67.67 0.38 1.300E+001 1.30E+001 7.072E+000 6.163E+00 PA-234 742.81 0.11 1.347E+002 1.90E+001 1.000E+002 6.273E+00 766.42 0.32 4.558E+001 9.486E+000 2.119E+00 1001.03 0.84 1.904E+001 -7.375E+000 8.754E+00

+ TH-234 63.29 3.70 1.570E+000 1.46E+000 6.062E-001 7.476E-00 92.38 2.13 2.013E+000 1.846E+000 9.582E-00 92.80* 2.10 1.462E+000 1.816E+000 6.820E-00 112.81 0.21 1.530E+001 -1.014E+001 7.168E+00 U-234 53.20 0.12 4.496E+001 4.50E+001 -3.960E+000 2.102E+00 120.90 0.04 9.384E+001 -2.614E+001 4.400E+00

+ U-235 72.70 0.12 4.345E+001 3.50E-001 2.564E+000 2.073E+00 89.96 3.43 1.152E+000 3.931E-001 5.456E-00 93.35* 5.54 5.543E-001 6.883E-001 2.585E-00 104.82 0.69 4.801E+000 -5.811E-001 2.253E+00 105.60 1.31 2.612E+000 1.405E+000 1.229E+00 108.58 0.50 6.533E+000 -2.088E+000 3.065E+00 109.19 1.66 1.932E+000 -9.361E-001 9.052E-00 140.76 0.20 1.912E+001 -7.770E+000 9.024E+00 143.76 10.96 3.504E-001 2.142E-001 1.654E-00 163.36 5.08 8.416E-001 4.720E-001 3.980E-00 182.62 0.39 1.310E+001 -5.741E+000 6.231E+00 194.94 0.63 7.511E+000 5.776E-001 3.547E+00 202.12 1.08 4.148E+000 -2.810E+000 1.949E+00 205.32 5.02 9.736E-001 7.661E-001 4.595E-00 221.39 0.12 4.008E+001 -1.601E+000 1.880E+00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

5/1/2017 10:01:09 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2079\\W6H-IMC-207 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 9.36E+000 17.090 Pb-210 46.5 ^ 2.45E+000 42.014 Pb-212 74.8 4.89E-001 40.229 3.176[54.728] 3.87 -0.708 77.1 2.36E-001 41.461 1.535[55.639] [ 0.571]

238.6 ^ 1.54E-001 37.104 1.000[52.473]

PB-214 74.8 8.66E-001 41.212 6.213[66.183] 5.64 -0.963 77.1 4.16E-001 42.428 2.987[66.946] [ 0.568]

351.9 ^ 1.39E-001 51.785 1.000[73.235]

TH-234 92.8 1.82E+000 ******

U-235 93.3 6.88E-001 ******