ML19095B342

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W6H-IMC-2079-S-P-6

ML19095B342
Person / Time
Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
Shared Package
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References
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Text

• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2079\\W6H-IMC-207 Report Generated On : 5/1/2017 9:59:21 AM Sample Title : W6H-IMC-2079-S-P-6 Sample Description :

Sample Identification : 2079-S-P-6 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 2.524E+002 grams Sample Taken On : 3/17/2017 12:00:00 AM Acquisition Started : 3/31/2017 11:52:21 AM Live Time : 1800.0 seconds Real Time : 1800.3 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 3/24/2017 Efficiency Calibration Used Done On : 5/1/2017 Efficiency ID : H-IMC-2079-S-P-6

Peak Analysis Report 5/1/2017 9:59:21 AM Page 1

• • • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W6H-IMC-2079-S-P-6 Peak Analysis Performed on: 5/1/2017 9:59:17 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 182-191 186.00 46.70 0.55 3.50E+001 15.83 5.00E+001 M 2 295-313 299.74 75.15 0.68 8.97E+001 22.53 5.70E+001 m 3 295-313 308.45 77.33 0.69 5.36E+001 17.91 4.62E+001 F 4 947-957 953.67 238.73 0.65 3.38E+001 15.99 4.95E+001 F 5 5825-5848 5836.77 1460.22 2.73 1.32E+002 21.72 9.33E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/1/2017 9:59:21 AM Page 2

• • • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W6H-IMC-2079-S-P-6 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.944 1460.82* 10.66 8.63076E+000 1.59620E+000 Pb-210 0.996 46.54* 4.25 1.42680E+000 7.62465E-001 Pb-212 0.995 74.82* 10.28 7.66177E-001 2.46784E-001 77.11* 17.10 2.69347E-001 1.05092E-001 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 9.39221E-002 4.68443E-002 300.09 3.30

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/1/2017 9:59:21 AM Page 3

• • • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.944 8.630755E+000 1.596204E+000 Pb-210 0.996 1.426797E+000 7.624645E-001 Pb-212 0.995 1.417686E-001 4.215727E-002

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

• • • • • • • • • • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 5/1/2017 9:59:17 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified.

Nuclide MDA Report 5/1/2017 9:59:21 AM Page 4

• • • • • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W6H-IMC-2079-S-P-6 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 1.178E+000 1.18E+000 8.631E+000 5.009E-00 CO-60 1173.23 99.85 1.821E-001 1.58E-001 -1.113E-001 8.320E-00 1332.49 99.98 1.585E-001 -4.451E-002 7.050E-00 CS-137 661.66 85.10 1.553E-001 1.55E-001 4.847E-002 7.217E-00

+ Pb-210 46.54* 4.25 1.661E+000 1.66E+000 1.427E+000 7.754E-00 BI-212 288.20 0.34 1.960E+001 1.85E+000 6.353E+000 9.215E+00 328.03 0.13 6.205E+001 -2.130E+001 2.922E+00 452.98 0.36 2.821E+001 6.227E+000 1.324E+00 727.33 6.67 1.852E+000 -1.579E+000 8.500E-00 785.37 1.10 1.218E+001 3.745E+000 5.593E+00 893.41 0.38 4.240E+001 2.232E+000 1.957E+00 952.12 0.17 1.070E+002 -4.066E+000 4.968E+00 1078.62 0.56 2.911E+001 -9.802E+000 1.327E+00 1512.70 0.29 5.553E+001 3.532E+001 2.442E+00 1620.50 1.47 1.193E+001 3.719E+000 5.262E+00

+ Pb-212 74.82* 10.28 3.230E-001 1.07E-001 7.662E-001 1.500E-00 77.11* 17.10 1.726E-001 2.693E-001 7.950E-00 86.83 2.07 2.281E+000 7.012E-001 1.088E+00 87.35 3.97 1.154E+000 -3.647E-001 5.497E-00 89.78 1.46 2.962E+000 -1.500E+000 1.407E+00 115.18 0.60 6.081E+000 -1.392E+000 2.864E+00 238.63* 43.60 1.066E-001 9.392E-002 4.955E-00 300.09 3.30 2.177E+000 -2.208E+000 1.026E+00 BI-214 76.86 0.55 1.211E+001 3.18E-001 5.280E-002 5.839E+00 79.29 0.91 5.255E+000 -5.594E-001 2.501E+00 89.26 0.11 3.862E+001 1.813E+000 1.833E+00 89.81 0.21 2.059E+001 -1.043E+001 9.781E+00 273.80 0.13 5.141E+001 3.015E+001 2.424E+00 348.92 0.10 8.246E+001 6.232E+001 3.892E+00 386.78 0.29 2.886E+001 3.154E+000 1.352E+00 388.89 0.40 2.089E+001 -9.906E-001 9.777E+00 405.72 0.17 5.231E+001 3.450E+000 2.449E+00 454.79 0.29 3.415E+001 1.749E+001 1.598E+00 469.77 0.13 7.559E+001 -6.134E-001 3.530E+00 609.32 45.49 3.175E-001 1.218E-001 1.493E-00 665.45 1.53 8.464E+000 5.059E+000 3.927E+00 703.11 0.47 2.895E+001 9.533E+000 1.343E+00 719.87 0.39 3.052E+001 -4.180E+001 1.398E+00 752.85 0.13 1.100E+002 3.035E+000 5.091E+00 768.36 4.89 3.085E+000 1.156E+000 1.433E+00 786.35 0.32 3.920E+001 -2.230E+001 1.789E+00 806.18 1.26 1.088E+001 9.310E+000 4.996E+00

Nuclide MDA Report 5/1/2017 9:59:21 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram BI-214 821.18 0.16 9.481E+001 3.18E-001 3.119E+001 4.387E+00 826.45 0.12 1.265E+002 4.188E+001 5.833E+00 934.06 3.11 5.467E+000 4.173E+000 2.528E+00 964.08 0.37 5.318E+001 2.830E+000 2.479E+00 1051.96 0.31 5.507E+001 -1.320E+001 2.527E+00 1069.96 0.27 7.096E+001 6.691E+001 3.283E+00 1120.29 14.92 1.322E+000 -4.084E-001 6.107E-00 1133.66 0.25 7.858E+001 1.573E+001 3.627E+00 1155.21 1.63 1.217E+001 -8.510E+000 5.613E+00 1207.68 0.45 4.209E+001 -7.531E+000 1.927E+00 1238.11 5.83 3.247E+000 -9.568E-001 1.483E+00 1280.98 1.43 1.165E+001 -4.333E-001 5.237E+00 1303.75 0.11 1.558E+002 -7.369E+001 6.993E+00 1377.67 3.99 4.068E+000 6.542E-001 1.810E+00 1385.31 0.79 2.137E+001 4.516E+000 9.551E+00 1401.52 1.33 1.238E+001 -2.047E+000 5.507E+00 1407.99 2.39 6.764E+000 -3.754E-001 3.001E+00 1509.21 2.13 6.967E+000 1.289E+000 3.029E+00 1538.53 0.40 3.792E+001 -6.099E-001 1.649E+00 1543.34 0.30 4.848E+001 -1.245E+001 2.098E+00 1583.20 0.70 2.599E+001 1.925E+001 1.156E+00 1594.75 0.27 6.766E+001 3.598E+000 3.002E+00 1599.37 0.32 4.680E+001 -1.331E+001 2.025E+00 1661.27 1.05 1.051E+001 -1.669E+001 4.246E+00 1684.01 0.21 7.424E+001 1.236E+001 3.213E+00 1729.59 2.88 5.295E+000 2.953E-001 2.267E+00 1764.49 15.30 1.400E+000 7.574E-001 6.270E-00 1838.36 0.35 4.082E+001 -4.777E+000 1.710E+00 1847.43 2.03 5.577E+000 -2.531E+000 2.213E+00 1873.16 0.21 6.798E+001 -1.040E+001 2.847E+00 1896.05 0.15 8.903E+001 -4.150E+000 3.649E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2293.38 0.31 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00 PB-214 74.82 5.80 1.136E+000 2.55E-001 4.556E-001 5.473E-00 77.11 9.70 6.747E-001 4.440E-003 3.254E-00 86.83 1.70 2.777E+000 8.539E-001 1.324E+00 87.35 2.24 2.046E+000 -6.464E-001 9.743E-00 89.78 0.82 5.273E+000 -2.670E+000 2.505E+00 241.99 7.25 1.042E+000 -7.275E-001 4.979E-00 258.76 0.53 1.224E+001 3.745E+000 5.789E+00 274.80 0.35 1.851E+001 -1.603E+000 8.726E+00 295.22 18.42 3.989E-001 3.484E-002 1.885E-00 351.93 35.60 2.547E-001 3.221E-001 1.206E-00 462.02 0.21 4.190E+001 -4.579E+001 1.943E+00 480.43 0.34 2.903E+001 2.890E+000 1.352E+00 487.14 0.43 2.227E+001 -8.030E+000 1.035E+00 533.66 0.18 6.202E+001 -3.573E+000 2.894E+00 580.14 0.37 3.858E+001 3.220E+001 1.819E+00 785.96 1.06 1.183E+001 -6.730E+000 5.398E+00

Nuclide MDA Report 5/1/2017 9:59:21 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram PB-214 839.07 0.58 3.025E+001 2.55E-001 2.057E+001 1.413E+00 Ra-226 81.07 0.20 1.887E+001 1.53E+000 -6.386E+000 8.858E+00 83.79 0.32 1.389E+001 5.203E+000 6.601E+00 186.21 3.64 1.528E+000 9.015E-001 7.274E-00 AC-228 89.96 1.90 2.493E+017 7.05E+016 -1.262E+017 1.184E+01 93.35 3.10 1.487E+017 -1.947E+016 7.060E+01 99.51 1.26 2.996E+017 -2.929E+016 1.406E+01 104.82 0.39 8.490E+017 -9.241E+017 3.951E+01 105.60 0.74 4.802E+017 1.547E+017 2.246E+01 108.58 0.28 1.319E+018 -8.026E+017 6.183E+01 129.07 2.42 1.703E+017 5.785E+016 8.025E+01 145.85 0.16 2.684E+018 3.347E+017 1.263E+01 153.98 0.72 6.330E+017 2.753E+017 2.988E+01 191.35 0.12 4.305E+018 -1.136E+018 2.032E+01 199.41 0.31 1.788E+018 -2.428E+017 8.452E+01 204.03 0.11 4.955E+018 8.248E+017 2.338E+01 209.25 3.89 1.413E+017 2.805E+016 6.655E+01 214.85 0.76 7.669E+017 2.005E+017 3.619E+01 270.24 3.46 1.906E+017 -6.055E+016 8.943E+01 278.95 0.16 4.842E+018 2.076E+018 2.290E+01 321.65 0.23 3.526E+018 1.423E+018 1.656E+01 327.44 0.12 6.996E+018 -2.731E+018 3.293E+01 328.00 2.95 2.881E+017 -9.893E+016 1.357E+01 332.37 0.40 2.073E+018 -1.225E+018 9.740E+01 338.32 11.27 7.053E+016 -2.508E+015 3.300E+01 340.96 0.37 2.200E+018 1.467E+018 1.030E+01 409.46 1.92 4.997E+017 -3.301E+017 2.336E+01 440.44 0.12 8.091E+018 1.388E+018 3.767E+01 463.00 4.40 2.236E+017 -1.142E+017 1.038E+01 478.33 0.21 5.107E+018 -3.786E+017 2.378E+01 503.82 0.18 6.807E+018 -1.277E+019 3.191E+01 508.96 0.45 3.585E+018 3.306E+018 1.705E+01 523.13 0.10 1.154E+019 4.671E+018 5.378E+01 546.47 0.20 5.142E+018 -4.954E+018 2.362E+01 562.50 0.87 1.427E+018 5.525E+017 6.637E+01 570.91 0.18 6.925E+018 4.021E+018 3.221E+01 572.14 0.15 8.289E+018 -1.250E+018 3.850E+01 583.41 0.11 1.381E+019 1.146E+019 6.499E+01 674.75 2.10 5.870E+017 -3.118E+017 2.688E+01 701.75 0.17 8.349E+018 -1.168E+018 3.863E+01 707.41 0.16 9.877E+018 -8.546E+018 4.588E+01 726.86 0.62 2.230E+018 -1.495E+018 1.025E+01 755.32 1.00 1.589E+018 -1.403E+017 7.368E+01 772.29 1.49 1.051E+018 -1.066E+017 4.862E+01 782.14 0.49 2.956E+018 -2.469E+017 1.355E+01 794.95 4.25 3.537E+017 4.140E+016 1.626E+01 830.49 0.54 3.185E+018 1.517E+018 1.476E+01 835.71 1.61 1.065E+018 -7.905E+017 4.932E+01 840.38 0.91 2.170E+018 2.356E+018 1.015E+01 904.20 0.77 2.533E+018 3.269E+017 1.178E+01 911.20 25.80 7.958E+016 6.792E+016 3.713E+01

Nuclide MDA Report 5/1/2017 9:59:21 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram AC-228 947.98 0.11 1.747E+019 7.05E+016 5.541E+018 8.065E+01 958.61 0.28 7.222E+018 -1.385E+018 3.355E+01 964.77 4.99 4.266E+017 9.616E+016 1.988E+01 968.97 15.80 1.343E+017 7.367E+016 6.255E+01 1033.25 0.20 9.455E+018 2.359E+018 4.346E+01 1065.18 0.13 1.524E+019 5.009E+018 7.023E+01 1095.68 0.13 1.484E+019 6.954E+018 6.793E+01 1110.61 0.28 7.023E+018 -3.000E+018 3.225E+01 1153.52 0.14 1.565E+019 4.422E+018 7.218E+01 1247.08 0.50 4.606E+018 1.015E+018 2.123E+01 1459.14 0.83 5.718E+018 1.403E+019 2.735E+01 1495.91 0.86 1.577E+018 -1.056E+017 6.661E+01 1501.57 0.46 3.309E+018 3.114E+017 1.425E+01 1557.11 0.18 9.117E+018 -6.043E+017 3.945E+01 1580.53 0.60 2.824E+018 -1.612E+018 1.228E+01 1588.20 3.22 6.622E+017 6.375E+017 2.966E+01 1625.06 0.25 6.404E+018 -3.506E+018 2.757E+01 1630.63 1.51 1.085E+018 -1.033E+018 4.670E+01 1638.28 0.47 3.829E+018 2.166E+018 1.672E+01 1666.52 0.18 8.392E+018 4.817E+018 3.544E+01 TH-230 67.67 0.38 1.189E+001 1.19E+001 3.383E-001 5.600E+00 PA-234 742.81 0.11 1.478E+002 2.02E+001 6.117E+001 6.903E+00 766.42 0.32 4.865E+001 -1.023E+001 2.264E+00 1001.03 0.84 2.024E+001 9.846E+000 9.312E+00 TH-234 63.29 3.70 1.231E+000 1.23E+000 2.342E-001 5.773E-00 92.38 2.13 2.081E+000 2.426E+000 9.901E-00 92.80 2.10 2.061E+000 6.567E-001 9.800E-00 112.81 0.21 1.685E+001 4.494E+000 7.923E+00 U-234 53.20 0.12 4.897E+001 4.90E+001 -1.256E+001 2.301E+00 120.90 0.04 9.577E+001 -5.967E+001 4.485E+00 U-235 72.70 0.12 4.173E+001 3.69E-001 9.390E+000 1.985E+00 89.96 3.43 1.260E+000 -6.379E-001 5.985E-00 93.35 5.54 7.593E-001 -9.942E-002 3.604E-00 104.82 0.69 4.410E+000 -4.800E+000 2.052E+00 105.60 1.31 2.475E+000 7.972E-001 1.158E+00 108.58 0.50 6.737E+000 -4.101E+000 3.159E+00 109.19 1.66 2.078E+000 -6.915E-001 9.761E-00 140.76 0.20 1.892E+001 -1.609E+001 8.903E+00 143.76 10.96 3.690E-001 3.099E-001 1.742E-00 163.36 5.08 7.938E-001 4.709E-001 3.731E-00 182.62 0.39 1.380E+001 2.568E+000 6.565E+00 194.94 0.63 8.154E+000 4.814E+000 3.859E+00 202.12 1.08 4.697E+000 1.670E+000 2.218E+00 205.32 5.02 9.986E-001 -1.239E-001 4.708E-00 221.39 0.12 4.246E+001 -3.233E+000 1.993E+00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

5/1/2017 9:59:21 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2079\\W6H-IMC-207 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 8.63E+000 18.494 Pb-210 46.5 ^ 1.43E+000 53.439 Pb-212 74.8 7.66E-001 32.210 8.158[59.372] 7.79 -1.426 77.1 2.69E-001 39.017 2.868[63.324] [ 0.722]

238.6 ^ 9.39E-002 49.876 1.000[70.535]