ML19095B338

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Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W6H-IMC-2079-S-P-5
ML19095B338
Person / Time
Site: 07000371
Issue date: 03/01/2018
From:
Cabrera Services
To:
NRC Region 1
Shared Package
ml051740240 List: ... further results
References
Download: ML19095B338 (10)
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Text

          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2079\\W6H-IMC-207 Report Generated On : 5/1/2017 9:58:10 AM Sample Title : W6H-IMC-2079-S-P-5 Sample Description :

Sample Identification : 2079-S-P-5 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 2.732E+002 grams Sample Taken On : 3/17/2017 12:00:00 AM Acquisition Started : 3/31/2017 11:12:35 AM Live Time : 1800.0 seconds Real Time : 1800.3 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 3/24/2017 Efficiency Calibration Used Done On : 5/1/2017 Efficiency ID : H-IMC-2079-S-P-5

Peak Analysis Report 5/1/2017 9:58:10 AM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W6H-IMC-2079-S-P-5 Peak Analysis Performed on: 5/1/2017 9:58:05 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts M 1 296-314 299.20 75.01 0.65 6.46E+001 20.78 5.95E+001 m 2 296-314 308.73 77.40 0.65 4.48E+001 17.94 6.32E+001 F 3 346-354 348.48 87.34 0.49 2.03E+001 12.51 3.45E+001 F 4 738-750 741.97 185.77 0.56 3.38E+001 15.04 5.04E+001 F 5 944-960 952.65 238.47 1.21 6.51E+001 20.91 5.95E+001 F 6 1400- 1411 1405.20 351.68 0.96 2.74E+001 14.07 2.64E+001 F 7 5825-5850 5836.79 1460.22 2.63 1.48E+002 22.78 5.78E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/1/2017 9:58:10 AM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W6H-IMC-2079-S-P-5 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.945 1460.82* 10.66 9.01128E+000 1.58155E+000 Pb-212 0.994 74.82* 10.28 5.30075E-001 2.01232E-001 77.11* 17.10 2.15465E-001 9.66247E-002 86.83 2.07 87.35* 3.97 3.92499E-001 2.54411E-001 89.78 1.46 115.18 0.60 238.63* 43.60 1.69361E-001 6.06809E-002 300.09 3.30 PB-214 0.661 74.82* 5.80 9.39512E-001 3.66438E-001 77.11* 9.70 3.79841E-001 1.73737E-001 86.83 1.70 87.35* 2.24 6.95634E-001 4.54793E-001 89.78 0.82 241.99 7.25 258.76 0.53 274.80 0.35 295.22 18.42 351.93* 35.60 1.28963E-001 6.88887E-002 462.02 0.21 480.43 0.34 487.14 0.43 533.66 0.18 580.14 0.37 785.96 1.06 839.07 0.58 Ra-226 0.973 81.07 0.20 83.79 0.32 186.21* 3.64 8.53533E-001 4.06385E-001

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/1/2017 9:58:10 AM Page 3

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.945 9.011281E+000 1.581554E+000 Pb-212 0.994 1.831014E-001 5.037906E-002 PB-214 0.661 1.389205E-001 6.433264E-002 Ra-226 0.973 8.535327E-001 4.063854E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 5/1/2017 9:58:05 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified.

Nuclide MDA Report 5/1/2017 9:58:10 AM Page 4

          • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W6H-IMC-2079-S-P-5 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 9.150E-001 9.15E-001 9.011E+000 3.754E-00 CO-60 1173.23 99.85 1.888E-001 1.79E-001 1.216E-002 8.708E-00 1332.49 99.98 1.794E-001 3.074E-002 8.158E-00 CS-137 661.66 85.10 1.427E-001 1.43E-001 -2.694E-004 6.624E-00 Pb-210 46.54 4.25 2.204E+000 2.20E+000 1.772E+000 1.047E+00 BI-212 288.20 0.34 1.697E+001 2.01E+000 -3.321E+000 7.939E+00 328.03 0.13 5.623E+001 -1.870E+001 2.643E+00 452.98 0.36 2.458E+001 -8.033E-001 1.147E+00 727.33 6.67 2.007E+000 -4.472E-001 9.322E-00 785.37 1.10 1.207E+001 -5.669E+000 5.571E+00 893.41 0.38 3.954E+001 -1.553E+001 1.825E+00 952.12 0.17 8.568E+001 -4.597E+001 3.927E+00 1078.62 0.56 2.941E+001 3.376E+000 1.351E+00 1512.70 0.29 4.770E+001 2.596E+001 2.074E+00 1620.50 1.47 9.403E+000 -1.341E+000 4.048E+00

+ Pb-212 74.82* 10.28 3.167E-001 1.24E-001 5.301E-001 1.472E-00 77.11* 17.10 1.910E-001 2.155E-001 8.900E-00 86.83 2.07 2.219E+000 3.717E-001 1.059E+00 87.35* 3.97 6.429E-001 3.925E-001 2.953E-00 89.78 1.46 2.929E+000 -1.854E+000 1.394E+00 115.18 0.60 6.196E+000 1.956E+000 2.931E+00 238.63* 43.60 1.238E-001 1.694E-001 5.840E-00 300.09 3.30 1.921E+000 -1.487E+000 9.022E-00 BI-214 76.86 0.55 1.110E+001 2.85E-001 1.794E+001 5.345E+00 79.29 0.91 5.172E+000 1.354E+000 2.465E+00 89.26 0.11 3.883E+001 1.175E+001 1.848E+00 89.81 0.21 2.036E+001 -1.289E+001 9.693E+00 273.80 0.13 4.843E+001 4.153E+000 2.285E+00 348.92 0.10 7.795E+001 -5.307E+001 3.681E+00 386.78 0.29 2.684E+001 -2.324E+000 1.257E+00 388.89 0.40 1.981E+001 1.715E+000 9.276E+00 405.72 0.17 4.254E+001 -3.216E+001 1.971E+00 454.79 0.29 3.046E+001 3.384E+000 1.421E+00 469.77 0.13 6.563E+001 5.736E+000 3.049E+00 609.32 45.49 2.848E-001 -4.878E-003 1.336E-00 665.45 1.53 7.704E+000 2.678E+000 3.567E+00 703.11 0.47 2.442E+001 -1.111E+001 1.124E+00 719.87 0.39 3.128E+001 -4.034E+001 1.444E+00 752.85 0.13 1.071E+002 6.675E+000 4.974E+00 768.36 4.89 3.058E+000 2.782E+000 1.427E+00 786.35 0.32 4.276E+001 5.476E+000 1.979E+00 806.18 1.26 9.928E+000 -1.307E+001 4.551E+00

Nuclide MDA Report 5/1/2017 9:58:10 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram BI-214 821.18 0.16 8.440E+001 2.85E-001 -9.756E+000 3.890E+00 826.45 0.12 1.168E+002 6.029E+001 5.384E+00 934.06 3.11 5.051E+000 4.306E+000 2.333E+00 964.08 0.37 4.810E+001 2.754E+001 2.237E+00 1051.96 0.31 5.560E+001 1.689E+001 2.569E+00 1069.96 0.27 6.121E+001 1.527E+001 2.814E+00 1120.29 14.92 1.265E+000 6.462E-001 5.857E-00 1133.66 0.25 6.667E+001 3.553E+001 3.053E+00 1155.21 1.63 1.176E+001 3.264E+000 5.441E+00 1207.68 0.45 4.422E+001 3.087E+001 2.046E+00 1238.11 5.83 3.233E+000 -3.130E-001 1.486E+00 1280.98 1.43 1.281E+001 2.017E-001 5.860E+00 1303.75 0.11 1.547E+002 -6.585E+001 6.992E+00 1377.67 3.99 4.008E+000 -6.002E-001 1.795E+00 1385.31 0.79 2.231E+001 1.256E+001 1.010E+00 1401.52 1.33 1.080E+001 1.931E+000 4.763E+00 1407.99 2.39 6.022E+000 1.019E-001 2.657E+00 1509.21 2.13 6.291E+000 8.861E-001 2.722E+00 1538.53 0.40 3.204E+001 8.511E-001 1.372E+00 1543.34 0.30 4.220E+001 9.716E+000 1.807E+00 1583.20 0.70 2.266E+001 -1.150E+001 9.995E+00 1594.75 0.27 6.021E+001 -1.892E+000 2.656E+00 1599.37 0.32 4.613E+001 -8.056E+000 2.014E+00 1661.27 1.05 1.207E+001 -4.504E-001 5.098E+00 1684.01 0.21 5.446E+001 1.528E+001 2.259E+00 1729.59 2.88 4.359E+000 -1.465E+000 1.826E+00 1764.49 15.30 1.179E+000 6.366E-001 5.215E-00 1838.36 0.35 4.582E+001 1.526E+001 1.983E+00 1847.43 2.03 7.706E+000 -2.077E+000 3.318E+00 1873.16 0.21 7.140E+001 1.631E+001 3.057E+00 1896.05 0.15 1.038E+002 -1.874E+001 4.442E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2293.38 0.31 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 5.613E-001 1.31E-001 9.395E-001 2.610E-00 77.11* 9.70 3.368E-001 3.798E-001 1.569E-00 86.83 1.70 2.701E+000 4.526E-001 1.290E+00 87.35* 2.24 1.139E+000 6.956E-001 5.234E-00 89.78 0.82 5.216E+000 -3.300E+000 2.483E+00 241.99 7.25 9.886E-001 2.579E-001 4.728E-00 258.76 0.53 1.024E+001 -6.584E+000 4.807E+00 274.80 0.35 1.708E+001 -9.420E+000 8.045E+00 295.22 18.42 3.365E-001 -1.443E-001 1.580E-00 351.93* 35.60 1.308E-001 1.290E-001 5.903E-00 462.02 0.21 3.919E+001 -3.203E+001 1.817E+00 480.43 0.34 2.589E+001 5.634E+000 1.201E+00 487.14 0.43 2.180E+001 1.365E+000 1.016E+00 533.66 0.18 5.095E+001 1.288E+001 2.354E+00 580.14 0.37 3.275E+001 1.142E+001 1.534E+00 785.96 1.06 1.267E+001 -1.652E+000 5.854E+00

Nuclide MDA Report 5/1/2017 9:58:10 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 839.07 0.58 2.282E+001 1.31E-001 2.012E+000 1.048E+00

+ Ra-226 81.07 0.20 1.805E+001 1.02E+000 -1.018E+001 8.472E+00 83.79 0.32 1.391E+001 1.733E+001 6.625E+00 186.21* 3.64 1.024E+000 8.535E-001 4.776E-00 AC-228 89.96 1.90 2.288E+017 6.44E+016 -1.448E+017 1.089E+01 93.35 3.10 1.410E+017 -1.253E+017 6.716E+01 99.51 1.26 2.733E+017 -5.860E+016 1.286E+01 104.82 0.39 8.634E+017 4.787E+016 4.058E+01 105.60 0.74 4.651E+017 1.816E+017 2.189E+01 108.58 0.28 1.242E+018 -8.971E+017 5.848E+01 129.07 2.42 1.328E+017 -7.211E+016 6.213E+01 145.85 0.16 2.411E+018 -8.913E+016 1.136E+01 153.98 0.72 5.196E+017 3.151E+016 2.443E+01 191.35 0.12 3.754E+018 4.275E+017 1.772E+01 199.41 0.31 1.558E+018 5.841E+017 7.368E+01 204.03 0.11 4.466E+018 -3.538E+018 2.111E+01 209.25 3.89 1.343E+017 -3.336E+016 6.359E+01 214.85 0.76 6.714E+017 -2.628E+017 3.170E+01 270.24 3.46 1.753E+017 1.016E+017 8.258E+01 278.95 0.16 4.134E+018 1.469E+018 1.953E+01 321.65 0.23 2.784E+018 -3.162E+018 1.299E+01 327.44 0.12 5.980E+018 9.231E+017 2.812E+01 328.00 2.95 2.423E+017 -8.061E+016 1.139E+01 332.37 0.40 1.912E+018 7.835E+017 9.015E+01 338.32 11.27 6.439E+016 -2.107E+016 3.023E+01 340.96 0.37 2.006E+018 6.934E+017 9.424E+01 409.46 1.92 3.878E+017 -2.397E+017 1.798E+01 440.44 0.12 7.231E+018 1.919E+018 3.374E+01 463.00 4.40 1.973E+017 -5.345E+016 9.164E+01 478.33 0.21 4.011E+018 -5.257E+017 1.853E+01 503.82 0.18 4.814E+018 -5.436E+018 2.222E+01 508.96 0.45 2.627E+018 1.836E+018 1.238E+01 523.13 0.10 9.861E+018 3.551E+018 4.591E+01 546.47 0.20 5.202E+018 2.014E+018 2.419E+01 562.50 0.87 1.188E+018 5.589E+017 5.510E+01 570.91 0.18 5.036E+018 -6.199E+017 2.308E+01 572.14 0.15 6.326E+018 2.638E+018 2.908E+01 583.41 0.11 1.164E+019 8.634E+018 5.470E+01 674.75 2.10 5.583E+017 3.505E+017 2.577E+01 701.75 0.17 6.766E+018 -1.069E+018 3.113E+01 707.41 0.16 8.625E+018 4.599E+018 4.009E+01 726.86 0.62 2.230E+018 2.302E+017 1.037E+01 755.32 1.00 1.388E+018 3.196E+017 6.438E+01 772.29 1.49 9.269E+017 5.068E+016 4.291E+01 782.14 0.49 2.560E+018 -7.876E+017 1.173E+01 794.95 4.25 3.535E+017 -8.407E+016 1.644E+01 830.49 0.54 2.535E+018 9.128E+017 1.166E+01 835.71 1.61 8.462E+017 3.745E+017 3.890E+01 840.38 0.91 1.457E+018 -1.217E+017 6.677E+01 904.20 0.77 2.192E+018 -1.495E+018 1.019E+01 911.20 25.80 7.445E+016 7.249E+016 3.493E+01

Nuclide MDA Report 5/1/2017 9:58:10 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram AC-228 947.98 0.11 1.408E+019 6.44E+016 -4.097E+018 6.460E+01 958.61 0.28 5.382E+018 -4.402E+017 2.469E+01 964.77 4.99 3.581E+017 2.368E+017 1.665E+01 968.97 15.80 1.161E+017 1.040E+017 5.410E+01 1033.25 0.20 8.428E+018 -7.002E+017 3.884E+01 1065.18 0.13 1.209E+019 -1.499E+019 5.531E+01 1095.68 0.13 1.159E+019 -2.869E+018 5.253E+01 1110.61 0.28 5.667E+018 -2.296E+018 2.586E+01 1153.52 0.14 1.326E+019 -7.282E+018 6.108E+01 1247.08 0.50 3.040E+018 -2.897E+018 1.364E+01 1459.14 0.83 5.163E+018 1.220E+019 2.474E+01 1495.91 0.86 1.667E+018 8.686E+016 7.275E+01 1501.57 0.46 3.126E+018 -3.829E+017 1.365E+01 1557.11 0.18 6.520E+018 -3.978E+018 2.731E+01 1580.53 0.60 2.640E+018 -1.490E+018 1.161E+01 1588.20 3.22 5.060E+017 1.578E+017 2.232E+01 1625.06 0.25 6.211E+018 2.585E+018 2.721E+01 1630.63 1.51 1.130E+018 3.925E+017 5.000E+01 1638.28 0.47 3.305E+018 1.258E+018 1.443E+01 1666.52 0.18 7.243E+018 -2.703E+017 3.059E+01 TH-230 67.67 0.38 1.146E+001 1.15E+001 -4.483E-001 5.397E+00 PA-234 742.81 0.11 1.281E+002 1.94E+001 -3.766E+001 5.949E+00 766.42 0.32 4.574E+001 1.702E+001 2.130E+00 1001.03 0.84 1.943E+001 -6.986E+000 8.963E+00 TH-234 63.29 3.70 1.344E+000 1.34E+000 1.196E+000 6.353E-00 92.38 2.13 2.210E+000 3.263E+000 1.057E+00 92.80 2.10 2.186E+000 1.518E+000 1.045E+00 112.81 0.21 1.731E+001 4.490E+000 8.180E+00 U-234 53.20 0.12 4.812E+001 4.81E+001 -5.158E+000 2.262E+00 120.90 0.04 9.171E+001 -2.173E+001 4.299E+00 U-235 72.70 0.12 4.521E+001 3.61E-001 -7.697E+000 2.163E+00 89.96 3.43 1.246E+000 -7.884E-001 5.931E-00 93.35 5.54 7.755E-001 -6.895E-001 3.695E-00 104.82 0.69 4.833E+000 2.679E-001 2.271E+00 105.60 1.31 2.583E+000 1.008E+000 1.216E+00 108.58 0.50 6.836E+000 -4.939E+000 3.220E+00 109.19 1.66 2.081E+000 -1.230E+000 9.807E-00 140.76 0.20 1.970E+001 -2.530E+000 9.323E+00 143.76 10.96 3.612E-001 3.585E-002 1.709E-00 163.36 5.08 7.598E-001 -2.320E-001 3.575E-00 182.62 0.39 1.316E+001 -9.512E+000 6.267E+00 194.94 0.63 7.418E+000 -9.272E-001 3.504E+00 202.12 1.08 4.662E+000 -6.364E-001 2.208E+00 205.32 5.02 1.003E+000 2.328E-001 4.746E-00 221.39 0.12 4.078E+001 5.620E-001 1.917E+00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

5/1/2017 9:58:10 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
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Analysis using Key Line Activities

===================================================

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2079\\W6H-IMC-207 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 9.01E+000 17.551 Pb-212 74.8 5.30E-001 37.963 3.130[52.201] 3.71 -0.679 77.1 2.15E-001 44.845 1.272[57.400] [ 0.546]

87.3 3.92E-001 64.818 2.318[74.062]

238.6 ^ 1.69E-001 35.829 1.000[50.670]

PB-214 74.8 9.40E-001 39.003 7.285[66.141] 6.20 -1.057 77.1 3.80E-001 45.739 2.945[70.324] [ 0.574]

87.3 6.96E-001 65.378 5.394[84.426]

351.9 ^ 1.29E-001 53.418 1.000[75.544]

Ra-226 186.2 ^ 8.54E-001 47.612

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