ML19095B332

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Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W6H-IMC-2079-S-P-3
ML19095B332
Person / Time
Site: 07000371
Issue date: 03/01/2018
From:
Cabrera Services
To:
NRC Region 1
Shared Package
ml051740240 List: ... further results
References
Download: ML19095B332 (10)
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Text

          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2079\\W6H-IMC-207 Report Generated On : 5/1/2017 9:49:07 AM Sample Title : W6H-IMC-2079-S-P-3 Sample Description :

Sample Identification : 2079-S-P-3 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 2.805E+002 grams Sample Taken On : 3/17/2017 12:00:00 AM Acquisition Started : 3/31/2017 9:48:53 AM Live Time : 1800.0 seconds Real Time : 1800.3 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 3/24/2017 Efficiency Calibration Used Done On : 5/1/2017 Efficiency ID : H-IMC-2079-S-P-3

Peak Analysis Report 5/1/2017 9:49:07 AM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W6H-IMC-2079-S-P-3 Peak Analysis Performed on: 5/1/2017 9:49:04 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 179-193 186.51 46.83 1.01 5.67E+001 19.35 5.25E+001 M 2 294-316 300.24 75.27 0.74 6.25E+001 21.01 7.71E+001 m 3 294-316 308.65 77.38 0.74 6.16E+001 19.47 5.46E+001 F 4 949-959 953.49 238.68 0.93 5.41E+001 18.29 3.71E+001 F 5 1400- 1411 1405.54 351.76 0.85 3.38E+001 14.49 2.76E+001 F 6 5825-5849 5837.06 1460.29 2.32 1.49E+002 23.89 1.39E+001 F 7 7047-7062 7055.16 1764.99 0.62 9.37E+000 2.56 1.60E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/1/2017 9:49:07 AM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W6H-IMC-2079-S-P-3 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.956 1460.82* 10.66 9.38538E+000 1.70533E+000 Pb-210 0.987 46.54* 4.25 2.29959E+000 1.01913E+000 Pb-212 0.993 74.82* 10.28 5.24238E-001 2.05571E-001 77.11* 17.10 3.04306E-001 1.14070E-001 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 1.45676E-001 5.44224E-002 300.09 3.30 PB-214 0.662 74.82* 5.80 9.29167E-001 3.73721E-001 77.11* 9.70 5.36458E-001 2.06810E-001 86.83 1.70 87.35 2.24 89.78 0.82 241.99 7.25 258.76 0.53 274.80 0.35 295.22 18.42 351.93* 35.60 1.64731E-001 7.46755E-002 462.02 0.21 480.43 0.34 487.14 0.43 533.66 0.18 580.14 0.37 785.96 1.06 839.07 0.58

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/1/2017 9:49:07 AM Page 3

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.956 9.385375E+000 1.705327E+000 Pb-210 0.987 2.299593E+000 1.019135E+000 Pb-212 0.993 1.694441E-001 4.849907E-002 PB-214 0.662 1.901047E-001 6.992667E-002

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 5/1/2017 9:49:04 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 7 1764.99 5.2083E-003 27.31 Tol. BI-214 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 5/1/2017 9:49:08 AM Page 4

          • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W6H-IMC-2079-S-P-3 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 1.366E+000 1.37E+000 9.385E+000 5.976E-00 CO-60 1173.23 99.85 1.941E-001 1.53E-001 4.979E-002 8.948E-00 1332.49 99.98 1.532E-001 -6.559E-002 6.816E-00 CS-137 661.66 85.10 1.406E-001 1.41E-001 -1.419E-001 6.498E-00

+ Pb-210 46.54* 4.25 1.919E+000 1.92E+000 2.300E+000 9.047E-00 BI-212 288.20 0.34 2.033E+001 2.08E+000 8.841E+000 9.600E+00 328.03 0.13 5.787E+001 -7.098E+000 2.719E+00 452.98 0.36 2.667E+001 2.273E+001 1.249E+00 727.33 6.67 2.082E+000 -2.729E-001 9.671E-00 785.37 1.10 1.240E+001 -3.651E+000 5.721E+00 893.41 0.38 3.517E+001 -1.870E+001 1.601E+00 952.12 0.17 8.166E+001 -2.925E+001 3.713E+00 1078.62 0.56 3.021E+001 -6.896E-001 1.386E+00 1512.70 0.29 5.622E+001 -5.579E+000 2.488E+00 1620.50 1.47 1.009E+001 3.064E+000 4.365E+00

+ Pb-212 74.82* 10.28 3.655E-001 9.05E-002 5.242E-001 1.714E-00 77.11* 17.10 1.833E-001 3.043E-001 8.495E-00 86.83 2.07 2.259E+000 9.362E-001 1.078E+00 87.35 3.97 1.124E+000 -6.757E-001 5.352E-00 89.78 1.46 2.823E+000 -2.966E+000 1.339E+00 115.18 0.60 5.709E+000 4.096E+000 2.682E+00 238.63* 43.60 9.052E-002 1.457E-001 4.162E-00 300.09 3.30 2.100E+000 -2.653E+000 9.894E-00 BI-214 76.86 0.55 1.182E+001 2.84E-001 2.122E+001 5.697E+00 79.29 0.91 5.573E+000 9.164E-002 2.663E+00 89.26 0.11 3.801E+001 0.000E+000 1.804E+00 89.81 0.21 1.963E+001 -2.062E+001 9.310E+00 273.80 0.13 4.934E+001 2.389E+001 2.325E+00 348.92 0.10 8.668E+001 -1.076E+001 4.110E+00 386.78 0.29 2.779E+001 1.444E+001 1.301E+00 388.89 0.40 1.944E+001 -7.391E+000 9.071E+00 405.72 0.17 4.251E+001 3.820E+000 1.964E+00 454.79 0.29 3.222E+001 -2.143E+000 1.506E+00 469.77 0.13 7.473E+001 -1.337E+000 3.495E+00 609.32 45.49 2.845E-001 1.062E-001 1.331E-00 665.45 1.53 8.785E+000 -4.681E-001 4.097E+00 703.11 0.47 2.481E+001 -1.803E+001 1.140E+00 719.87 0.39 3.394E+001 -8.278E+000 1.572E+00 752.85 0.13 1.130E+002 -4.071E+001 5.250E+00 768.36 4.89 2.737E+000 -1.947E+000 1.262E+00 786.35 0.32 4.235E+001 -3.164E+001 1.952E+00 806.18 1.26 1.097E+001 -2.423E+000 5.056E+00

Nuclide MDA Report 5/1/2017 9:49:08 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram BI-214 821.18 0.16 8.672E+001 2.84E-001 -1.266E+001 3.994E+00 826.45 0.12 1.200E+002 -3.028E+001 5.528E+00 934.06 3.11 5.095E+000 2.293E+000 2.348E+00 964.08 0.37 5.610E+001 6.822E+001 2.631E+00 1051.96 0.31 5.028E+001 -2.088E+001 2.294E+00 1069.96 0.27 6.422E+001 1.100E+001 2.955E+00 1120.29 14.92 1.290E+000 4.623E-001 5.965E-00 1133.66 0.25 7.079E+001 -8.079E+000 3.248E+00 1155.21 1.63 1.264E+001 3.452E+000 5.863E+00 1207.68 0.45 3.461E+001 -3.167E+000 1.559E+00 1238.11 5.83 3.528E+000 1.750E-001 1.629E+00 1280.98 1.43 1.181E+001 5.236E+000 5.338E+00 1303.75 0.11 1.607E+002 -2.850E+001 7.262E+00 1377.67 3.99 5.210E+000 3.099E+000 2.388E+00 1385.31 0.79 2.573E+001 1.652E+001 1.177E+00 1401.52 1.33 1.244E+001 -8.266E+000 5.560E+00 1407.99 2.39 7.067E+000 2.751E+000 3.165E+00 1509.21 2.13 7.639E+000 2.870E+000 3.380E+00 1538.53 0.40 3.557E+001 -1.591E+001 1.539E+00 1543.34 0.30 4.538E+001 3.494E+000 1.954E+00 1583.20 0.70 2.241E+001 1.348E+001 9.822E+00 1594.75 0.27 5.801E+001 -2.086E+001 2.532E+00 1599.37 0.32 4.232E+001 -1.736E+001 1.812E+00 1661.27 1.05 1.576E+001 7.128E+000 6.906E+00 1684.01 0.21 6.948E+001 8.381E+000 2.991E+00 1729.59 2.88 5.116E+000 2.854E-001 2.190E+00 1764.49 15.30 1.197E+000 4.193E-001 5.281E-00 1838.36 0.35 3.944E+001 -4.615E+000 1.652E+00 1847.43 2.03 5.796E+000 -5.343E-001 2.342E+00 1873.16 0.21 5.167E+001 -2.582E+001 2.050E+00 1896.05 0.15 9.978E+001 3.523E+001 4.214E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2293.38 0.31 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 6.479E-001 1.38E-001 9.292E-001 3.038E-00 77.11* 9.70 3.231E-001 5.365E-001 1.498E-00 86.83 1.70 2.751E+000 1.140E+000 1.312E+00 87.35 2.24 1.992E+000 -1.197E+000 9.485E-00 89.78 0.82 5.027E+000 -5.282E+000 2.385E+00 241.99 7.25 1.004E+000 -6.154E-002 4.799E-00 258.76 0.53 1.107E+001 -1.935E+000 5.214E+00 274.80 0.35 1.767E+001 1.141E+001 8.321E+00 295.22 18.42 3.922E-001 1.610E-001 1.855E-00 351.93* 35.60 1.382E-001 1.647E-001 6.249E-00 462.02 0.21 4.388E+001 -1.109E+001 2.046E+00 480.43 0.34 2.936E+001 -1.734E+001 1.371E+00 487.14 0.43 2.292E+001 4.479E+000 1.069E+00 533.66 0.18 6.050E+001 2.336E+001 2.824E+00 580.14 0.37 3.395E+001 2.073E+001 1.591E+00 785.96 1.06 1.265E+001 -1.395E+001 5.827E+00

Nuclide MDA Report 5/1/2017 9:49:08 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 839.07 0.58 2.342E+001 1.38E-001 6.568E+000 1.075E+00 Ra-226 81.07 0.20 1.918E+001 1.56E+000 -1.283E+001 9.022E+00 83.79 0.32 1.358E+001 8.802E+000 6.454E+00 186.21 3.64 1.560E+000 1.931E+000 7.446E-00 AC-228 89.96 1.90 1.884E+017 6.05E+016 -1.980E+017 8.938E+01 93.35 3.10 1.173E+017 6.158E+016 5.575E+01 99.51 1.26 2.337E+017 2.272E+016 1.098E+01 104.82 0.39 7.811E+017 1.910E+017 3.678E+01 105.60 0.74 4.138E+017 2.116E+017 1.949E+01 108.58 0.28 1.110E+018 2.698E+017 5.235E+01 129.07 2.42 1.336E+017 6.181E+016 6.302E+01 145.85 0.16 2.104E+018 1.123E+017 9.914E+01 153.98 0.72 4.480E+017 -3.601E+017 2.103E+01 191.35 0.12 3.265E+018 -5.834E+017 1.540E+01 199.41 0.31 1.401E+018 5.261E+017 6.632E+01 204.03 0.11 3.851E+018 1.081E+018 1.818E+01 209.25 3.89 1.149E+017 8.110E+016 5.429E+01 214.85 0.76 5.959E+017 1.527E+015 2.814E+01 270.24 3.46 1.465E+017 -7.749E+016 6.876E+01 278.95 0.16 3.231E+018 -1.633E+018 1.515E+01 321.65 0.23 2.531E+018 0.000E+000 1.183E+01 327.44 0.12 5.199E+018 4.665E+017 2.442E+01 328.00 2.95 2.131E+017 -2.614E+016 1.001E+01 332.37 0.40 1.647E+018 -3.554E+017 7.756E+01 338.32 11.27 6.051E+016 0.000E+000 2.852E+01 340.96 0.37 1.743E+018 -1.978E+017 8.181E+01 409.46 1.92 3.374E+017 -1.476E+016 1.562E+01 440.44 0.12 6.535E+018 4.741E+018 3.054E+01 463.00 4.40 1.828E+017 -9.807E+016 8.522E+01 478.33 0.21 4.180E+018 -1.438E+018 1.955E+01 503.82 0.18 5.388E+018 -9.205E+018 2.530E+01 508.96 0.45 2.784E+018 3.363E+018 1.325E+01 523.13 0.10 8.260E+018 -3.718E+018 3.830E+01 546.47 0.20 5.146E+018 -3.271E+017 2.412E+01 562.50 0.87 1.079E+018 -1.627E+017 5.013E+01 570.91 0.18 5.151E+018 -3.432E+016 2.390E+01 572.14 0.15 6.367E+018 -3.339E+017 2.958E+01 583.41 0.11 9.705E+018 7.074E+018 4.541E+01 674.75 2.10 5.601E+017 1.443E+017 2.611E+01 701.75 0.17 6.411E+018 -1.490E+018 2.966E+01 707.41 0.16 6.316E+018 -5.469E+018 2.889E+01 726.86 0.62 1.946E+018 -7.652E+016 9.038E+01 755.32 1.00 1.251E+018 2.295E+017 5.809E+01 772.29 1.49 8.218E+017 -3.643E+017 3.805E+01 782.14 0.49 2.642E+018 1.646E+017 1.227E+01 794.95 4.25 2.959E+017 1.341E+017 1.370E+01 830.49 0.54 2.248E+018 -3.976E+017 1.034E+01 835.71 1.61 7.504E+017 6.387E+015 3.450E+01 840.38 0.91 1.362E+018 9.597E+017 6.272E+01 904.20 0.77 1.803E+018 -1.975E+018 8.335E+01 911.20 25.80 6.402E+016 3.306E+016 2.997E+01

Nuclide MDA Report 5/1/2017 9:49:08 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram AC-228 947.98 0.11 1.178E+019 6.05E+016 6.223E+018 5.378E+01 958.61 0.28 5.407E+018 0.000E+000 2.507E+01 964.77 4.99 3.569E+017 3.495E+017 1.674E+01 968.97 15.80 1.096E+017 7.993E+016 5.131E+01 1033.25 0.20 6.943E+018 2.485E+018 3.179E+01 1065.18 0.13 1.192E+019 6.925E+018 5.501E+01 1095.68 0.13 1.261E+019 -2.479E+018 5.826E+01 1110.61 0.28 5.270E+018 -6.335E+018 2.416E+01 1153.52 0.14 1.300E+019 3.864E+018 6.033E+01 1247.08 0.50 3.462E+018 -6.315E+017 1.593E+01 1459.14 0.83 4.774E+018 1.196E+019 2.292E+01 1495.91 0.86 1.306E+018 -9.754E+017 5.592E+01 1501.57 0.46 2.618E+018 3.688E+017 1.133E+01 1557.11 0.18 5.511E+018 -3.879E+018 2.285E+01 1580.53 0.60 2.034E+018 -6.439E+017 8.758E+01 1588.20 3.22 4.277E+017 1.780E+017 1.874E+01 1625.06 0.25 5.220E+018 7.976E+017 2.269E+01 1630.63 1.51 7.432E+017 -4.148E+017 3.139E+01 1638.28 0.47 2.497E+018 9.712E+017 1.062E+01 1666.52 0.18 7.192E+018 -1.753E+018 3.096E+01 TH-230 67.67 0.38 1.273E+001 1.27E+001 6.261E-001 6.026E+00 PA-234 742.81 0.11 1.489E+002 1.90E+001 1.309E+002 6.972E+00 766.42 0.32 4.215E+001 -3.619E+000 1.944E+00 1001.03 0.84 1.897E+001 -1.894E+001 8.704E+00 TH-234 63.29 3.70 1.468E+000 1.47E+000 1.024E+000 6.963E-00 92.38 2.13 2.023E+000 2.558E+000 9.625E-00 92.80 2.10 2.042E+000 1.654E+000 9.712E-00 112.81 0.21 1.662E+001 -3.185E+000 7.824E+00 U-234 53.20 0.12 4.554E+001 4.55E+001 1.865E+001 2.130E+00 120.90 0.04 1.002E+002 1.830E+001 4.715E+00 U-235 72.70 0.12 4.200E+001 3.57E-001 -2.713E+000 2.000E+00 89.96 3.43 1.201E+000 -1.262E+000 5.697E-00 93.35 5.54 7.554E-001 3.964E-001 3.589E-00 104.82 0.69 5.117E+000 1.251E+000 2.409E+00 105.60 1.31 2.689E+000 1.375E+000 1.266E+00 108.58 0.50 7.154E+000 1.738E+000 3.373E+00 109.19 1.66 2.053E+000 -9.334E-001 9.650E-00 140.76 0.20 2.113E+001 -2.511E-001 1.002E+00 143.76 10.96 3.574E-001 -2.840E-001 1.687E-00 163.36 5.08 6.782E-001 -3.658E-001 3.160E-00 182.62 0.39 1.374E+001 6.911E-001 6.546E+00 194.94 0.63 7.774E+000 -4.888E-001 3.675E+00 202.12 1.08 4.537E+000 -8.573E-001 2.142E+00 205.32 5.02 9.441E-001 -5.938E-001 4.443E-00 221.39 0.12 4.309E+001 4.299E+000 2.029E+00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

5/1/2017 9:49:08 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2079\\W6H-IMC-207 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 9.39E+000 18.170 Pb-210 46.5 ^ 2.30E+000 44.318 Pb-212 74.8 5.24E-001 39.213 3.599[54.160] 4.84 -0.885 77.1 3.04E-001 37.485 2.089[52.922] [ 0.568]

238.6 ^ 1.46E-001 37.358 1.000[52.833]

PB-214 74.8 9.29E-001 40.221 5.641[60.603] 5.57 -0.952 77.1 5.36E-001 38.551 3.257[59.508] [ 0.501]

351.9 ^ 1.65E-001 45.332 1.000[64.109]

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