ML19095B324

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W6H-IMC-2079-S-P-1

ML19095B324
Person / Time
Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
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References
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Text

• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2079\\W6H-IMC-207 Report Generated On : 5/1/2017 9:45:07 AM Sample Title : W6H-IMC-2079-S-P-1 Sample Description :

Sample Identification : 2079-S-P-1 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 2.737E+002 grams Sample Taken On : 3/23/2017 12:00:00 AM Acquisition Started : 3/30/2017 1:08:09 PM Live Time : 1800.0 seconds Real Time : 1800.3 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 3/24/2017 Efficiency Calibration Used Done On : 5/1/2017 Efficiency ID : H-IMC-2079-S-P-1

Peak Analysis Report 5/1/2017 9:45:07 AM Page 1

• • • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W6H-IMC-2079-S-P-1 Peak Analysis Performed on: 5/1/2017 9:45:02 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts M 1 295-312 299.81 75.17 0.66 6.09E+001 20.60 7.11E+001 m 2 295-312 308.16 77.26 0.67 5.59E+001 19.46 6.39E+001 F 3 737-749 741.80 185.73 0.68 4.01E+001 16.96 5.85E+001 F 4 948-957 953.24 238.62 0.83 6.33E+001 19.47 3.75E+001 F 5 1175-1184 1179.23 295.15 0.67 1.62E+001 12.07 2.30E+001 F 6 1400- 1412 1406.59 352.03 0.98 3.00E+001 14.62 3.12E+001 F 7 5826-5849 5837.56 1460.42 2.47 1.41E+002 22.48 5.33E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/1/2017 9:45:07 AM Page 2

• • • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W6H-IMC-2079-S-P-1 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.974 1460.82* 10.66 8.57168E+000 1.54572E+000 Pb-212 0.997 74.82* 10.28 4.98580E-001 1.96264E-001 77.11* 17.10 2.69428E-001 1.08297E-001 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 1.64627E-001 5.69588E-002 300.09 3.30 PB-214 0.998 74.82* 5.80 8.83691E-001 3.56734E-001 77.11* 9.70 4.74972E-001 1.95645E-001 86.83 1.70 87.35 2.24 89.78 0.82 241.99 7.25 258.76 0.53 274.80 0.35 295.22* 18.42 1.22896E-001 9.35113E-002 351.93* 35.60 1.41187E-001 7.18627E-002 462.02 0.21 480.43 0.34 487.14 0.43 533.66 0.18 580.14 0.37 785.96 1.06 839.07 0.58 Ra-226 0.968 81.07 0.20 83.79 0.32 186.21* 3.64 1.01199E+000 4.60694E-001

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/1/2017 9:45:07 AM Page 3

• • • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.974 8.571676E+000 1.545721E+000 Pb-212 0.997 1.848424E-001 4.936105E-002 PB-214 0.998 1.458591E-001 5.467358E-002 Ra-226 0.968 1.011986E+000 4.606944E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

• • • • • • • • • • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 5/1/2017 9:45:02 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified.

Nuclide MDA Report 5/1/2017 9:45:07 AM Page 4

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W6H-IMC-2079-S-P-1 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 8.676E-001 8.68E-001 8.572E+000 3.518E-00 CO-60 1173.23 99.85 1.768E-001 1.38E-001 -4.069E-002 8.112E-00 1332.49 99.98 1.377E-001 -5.923E-002 6.073E-00 CS-137 661.66 85.10 1.458E-001 1.46E-001 8.684E-002 6.783E-00 Pb-210 46.54 4.25 2.318E+000 2.32E+000 1.649E+000 1.104E+00 BI-212 288.20 0.34 1.728E+001 1.94E+000 -1.144E+001 8.093E+00 328.03 0.13 5.863E+001 2.615E+001 2.763E+00 452.98 0.36 2.276E+001 1.404E+000 1.057E+00 727.33 6.67 1.938E+000 7.880E-002 8.981E-00 785.37 1.10 1.412E+001 -1.317E+000 6.600E+00 893.41 0.38 4.093E+001 1.535E+001 1.895E+00 952.12 0.17 8.928E+001 -8.061E+001 4.108E+00 1078.62 0.56 2.602E+001 -2.321E+000 1.182E+00 1512.70 0.29 4.477E+001 2.987E+001 1.927E+00 1620.50 1.47 1.108E+001 1.553E+000 4.886E+00

+ Pb-212 74.82* 10.28 3.430E-001 8.56E-002 4.986E-001 1.604E-00 77.11* 17.10 1.922E-001 2.694E-001 8.960E-00 86.83 2.07 2.181E+000 3.156E-001 1.040E+00 87.35 3.97 1.127E+000 -9.654E-003 5.372E-00 89.78 1.46 2.753E+000 -1.376E+000 1.306E+00 115.18 0.60 5.810E+000 3.187E+000 2.738E+00 238.63* 43.60 8.565E-002 1.646E-001 3.931E-00 300.09 3.30 1.873E+000 -1.028E+000 8.783E-00 BI-214 76.86 0.55 1.157E+001 2.83E-001 0.000E+000 5.579E+00 79.29 0.91 5.586E+000 -7.579E-001 2.672E+00 89.26 0.11 3.692E+001 -7.252E+000 1.753E+00 89.81 0.21 1.914E+001 -9.564E+000 9.082E+00 273.80 0.13 4.836E+001 -1.467E+001 2.281E+00 348.92 0.10 8.078E+001 -9.417E+000 3.823E+00 386.78 0.29 2.504E+001 5.330E+000 1.167E+00 388.89 0.40 1.927E+001 -5.276E+000 9.008E+00 405.72 0.17 4.856E+001 -2.417E+000 2.272E+00 454.79 0.29 2.841E+001 1.715E+001 1.319E+00 469.77 0.13 6.657E+001 9.164E+000 3.096E+00 609.32 45.49 2.827E-001 2.565E-001 1.326E-00 665.45 1.53 7.890E+000 -3.049E+000 3.661E+00 703.11 0.47 2.630E+001 4.314E+000 1.218E+00 719.87 0.39 3.483E+001 1.151E+001 1.622E+00 752.85 0.13 1.078E+002 1.022E+002 5.010E+00 768.36 4.89 3.053E+000 2.229E+000 1.424E+00 786.35 0.32 4.935E+001 6.393E+000 2.308E+00 806.18 1.26 1.116E+001 5.054E+000 5.166E+00

Nuclide MDA Report 5/1/2017 9:45:07 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram BI-214 821.18 0.16 8.830E+001 2.83E-001 2.435E+000 4.085E+00 826.45 0.12 1.200E+002 2.119E+001 5.545E+00 934.06 3.11 5.135E+000 1.315E-001 2.376E+00 964.08 0.37 4.454E+001 1.209E+001 2.059E+00 1051.96 0.31 5.552E+001 1.686E+001 2.565E+00 1069.96 0.27 5.783E+001 3.857E+001 2.645E+00 1120.29 14.92 1.348E+000 -2.632E-001 6.273E-00 1133.66 0.25 6.881E+001 -5.697E+000 3.160E+00 1155.21 1.63 1.109E+001 3.785E+000 5.109E+00 1207.68 0.45 3.381E+001 -4.361E+001 1.526E+00 1238.11 5.83 3.054E+000 1.857E+000 1.397E+00 1280.98 1.43 1.118E+001 -8.054E+000 5.045E+00 1303.75 0.11 1.613E+002 6.574E+001 7.321E+00 1377.67 3.99 4.278E+000 1.686E+000 1.930E+00 1385.31 0.79 2.093E+001 7.354E-001 9.412E+00 1401.52 1.33 1.239E+001 3.465E+000 5.562E+00 1407.99 2.39 6.415E+000 1.860E+000 2.854E+00 1509.21 2.13 5.203E+000 -6.765E-001 2.179E+00 1538.53 0.40 3.199E+001 -1.869E+001 1.370E+00 1543.34 0.30 4.060E+001 -9.700E+000 1.727E+00 1583.20 0.70 2.509E+001 9.840E-001 1.121E+00 1594.75 0.27 6.912E+001 1.642E+001 3.102E+00 1599.37 0.32 4.850E+001 -2.929E+001 2.133E+00 1661.27 1.05 1.153E+001 1.315E+000 4.829E+00 1684.01 0.21 6.451E+001 -3.187E+001 2.762E+00 1729.59 2.88 4.916E+000 3.134E+000 2.105E+00 1764.49 15.30 1.150E+000 5.855E-001 5.075E-00 1838.36 0.35 4.125E+001 8.414E+000 1.755E+00 1847.43 2.03 6.581E+000 2.113E+000 2.756E+00 1873.16 0.21 6.311E+001 4.923E+000 2.643E+00 1896.05 0.15 9.171E+001 7.154E+000 3.841E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2293.38 0.31 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 6.080E-001 1.44E-001 8.837E-001 2.844E-00 77.11* 9.70 3.389E-001 4.750E-001 1.579E-00 86.83 1.70 2.655E+000 3.843E-001 1.267E+00 87.35 2.24 1.997E+000 -1.711E-002 9.520E-00 89.78 0.82 4.902E+000 -2.450E+000 2.326E+00 241.99 7.25 1.004E+000 -1.395E+000 4.807E-00 258.76 0.53 1.046E+001 -2.076E+000 4.918E+00 274.80 0.35 1.732E+001 -2.635E+000 8.167E+00 295.22* 18.42 1.896E-001 1.229E-001 8.456E-00 351.93* 35.60 1.439E-001 1.412E-001 6.558E-00 462.02 0.21 3.946E+001 -1.656E+001 1.830E+00 480.43 0.34 3.053E+001 3.330E+000 1.433E+00 487.14 0.43 2.359E+001 -3.271E+000 1.106E+00 533.66 0.18 5.536E+001 -7.025E+000 2.575E+00 580.14 0.37 3.058E+001 -1.901E+000 1.426E+00 785.96 1.06 1.449E+001 -5.965E+000 6.766E+00

Nuclide MDA Report 5/1/2017 9:45:07 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 839.07 0.58 2.396E+001 1.44E-001 2.939E+000 1.105E+00

+ Ra-226 81.07 0.20 2.040E+001 1.10E+000 -5.356E+000 9.650E+00 83.79 0.32 1.300E+001 6.862E-001 6.172E+00 186.21* 3.64 1.096E+000 1.012E+000 5.139E-00 AC-228 89.96 1.90 1.598E+009 4.65E+008 -7.985E+008 7.582E+00 93.35 3.10 9.555E+008 4.834E+008 4.531E+00 99.51 1.26 1.995E+009 -5.898E+007 9.375E+00 104.82 0.39 6.516E+009 2.961E+009 3.066E+00 105.60 0.74 3.376E+009 4.742E+008 1.587E+00 108.58 0.28 8.504E+009 3.461E+009 3.984E+00 129.07 2.42 1.136E+009 9.350E+008 5.362E+00 145.85 0.16 1.685E+010 -6.000E+009 7.913E+00 153.98 0.72 4.167E+009 -1.148E+009 1.968E+00 191.35 0.12 2.758E+010 1.031E+010 1.301E+01 199.41 0.31 1.073E+010 -1.687E+009 5.049E+00 204.03 0.11 3.314E+010 -1.175E+010 1.567E+01 209.25 3.89 9.790E+008 2.426E+008 4.629E+00 214.85 0.76 5.006E+009 4.850E+009 2.364E+00 270.24 3.46 1.342E+009 -2.903E+008 6.330E+00 278.95 0.16 2.825E+010 -7.289E+009 1.328E+01 321.65 0.23 2.220E+010 -1.606E+010 1.041E+01 327.44 0.12 4.608E+010 1.370E+010 2.171E+01 328.00 2.95 1.878E+009 8.373E+008 8.849E+00 332.37 0.40 1.306E+010 -1.431E+010 6.126E+00 338.32 11.27 4.833E+008 5.390E+007 2.271E+00 340.96 0.37 1.488E+010 3.983E+009 6.992E+00 409.46 1.92 3.427E+009 2.567E+009 1.609E+00 440.44 0.12 5.132E+010 -6.623E+009 2.387E+01 463.00 4.40 1.487E+009 4.669E+008 6.915E+00 478.33 0.21 3.526E+010 -5.502E+009 1.650E+01 503.82 0.18 3.923E+010 -4.995E+010 1.825E+01 508.96 0.45 2.150E+010 2.514E+010 1.019E+01 523.13 0.10 7.316E+010 -3.719E+010 3.406E+01 546.47 0.20 3.612E+010 6.973E+009 1.671E+01 562.50 0.87 9.800E+009 -2.310E+009 4.579E+00 570.91 0.18 4.242E+010 2.759E+010 1.966E+01 572.14 0.15 4.978E+010 1.748E+009 2.300E+01 583.41 0.11 8.438E+010 7.802E+010 3.958E+01 674.75 2.10 4.063E+009 -2.365E+009 1.873E+00 701.75 0.17 5.553E+010 3.383E+009 2.576E+01 707.41 0.16 5.981E+010 -8.322E+009 2.765E+01 726.86 0.62 1.562E+010 -1.281E+009 7.230E+00 755.32 1.00 9.401E+009 -1.137E+010 4.329E+00 772.29 1.49 7.170E+009 6.311E+008 3.331E+00 782.14 0.49 2.299E+010 -2.087E+009 1.070E+01 794.95 4.25 2.623E+009 -1.363E+009 1.220E+00 830.49 0.54 1.802E+010 -1.160E+010 8.259E+00 835.71 1.61 6.900E+009 3.967E+009 3.197E+00 840.38 0.91 1.173E+010 -6.651E+008 5.416E+00 904.20 0.77 1.494E+010 -1.364E+010 6.904E+00 911.20 25.80 4.653E+008 1.856E+008 2.156E+00

Nuclide MDA Report 5/1/2017 9:45:07 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram AC-228 947.98 0.11 1.163E+011 4.65E+008 4.828E+010 5.383E+01 958.61 0.28 4.205E+010 3.205E+010 1.938E+01 964.77 4.99 2.441E+009 3.643E+008 1.128E+00 968.97 15.80 7.448E+008 2.527E+008 3.430E+00 1033.25 0.20 6.609E+010 3.139E+010 3.060E+01 1065.18 0.13 8.314E+010 -7.414E+009 3.775E+01 1095.68 0.13 1.045E+011 7.958E+009 4.822E+01 1110.61 0.28 4.646E+010 -5.653E+010 2.139E+01 1153.52 0.14 9.539E+010 -4.074E+010 4.381E+01 1247.08 0.50 2.441E+010 2.933E+009 1.105E+01 1459.14 0.83 3.747E+010 9.020E+010 1.794E+01 1495.91 0.86 1.167E+010 5.961E+009 5.048E+00 1501.57 0.46 2.048E+010 9.066E+008 8.767E+00 1557.11 0.18 5.056E+010 -4.354E+009 2.135E+01 1580.53 0.60 1.755E+010 -2.792E+010 7.595E+00 1588.20 3.22 4.241E+009 1.506E+009 1.899E+00 1625.06 0.25 4.838E+010 1.508E+010 2.134E+01 1630.63 1.51 7.600E+009 4.298E+009 3.318E+00 1638.28 0.47 1.825E+010 -8.947E+009 7.569E+00 1666.52 0.18 4.894E+010 2.776E+009 2.030E+01 TH-230 67.67 0.38 1.192E+001 1.19E+001 3.828E+000 5.627E+00 PA-234 742.81 0.11 1.172E+002 1.88E+001 -1.078E+002 5.404E+00 766.42 0.32 4.567E+001 2.968E+001 2.126E+00 1001.03 0.84 1.883E+001 -4.685E+000 8.665E+00 TH-234 63.29 3.70 1.337E+000 1.34E+000 -3.802E-001 6.317E-00 92.38 2.13 1.876E+000 1.198E+000 8.904E-00 92.80 2.10 1.900E+000 5.889E-001 9.019E-00 112.81 0.21 1.549E+001 -8.212E+000 7.271E+00 U-234 53.20 0.12 4.351E+001 4.35E+001 2.009E+001 2.031E+00 120.90 0.04 9.160E+001 1.482E+001 4.293E+00 U-235 72.70 0.12 4.093E+001 3.10E-001 -1.802E+000 1.949E+00 89.96 3.43 1.171E+000 -5.852E-001 5.557E-00 93.35 5.54 7.074E-001 3.579E-001 3.354E-00 104.82 0.69 4.908E+000 2.230E+000 2.309E+00 105.60 1.31 2.523E+000 3.544E-001 1.186E+00 108.58 0.50 6.301E+000 2.564E+000 2.952E+00 109.19 1.66 1.813E+000 -3.825E-001 8.467E-00 140.76 0.20 1.849E+001 3.353E+000 8.721E+00 143.76 10.96 3.098E-001 -1.718E-001 1.452E-00 163.36 5.08 7.833E-001 2.813E-001 3.692E-00 182.62 0.39 1.360E+001 2.614E+000 6.487E+00 194.94 0.63 6.739E+000 -9.070E-001 3.165E+00 202.12 1.08 4.594E+000 3.041E+000 2.174E+00 205.32 5.02 9.968E-001 -7.420E-002 4.717E-00 221.39 0.12 4.003E+001 -2.817E+001 1.880E+00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

5/1/2017 9:45:07 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2079\\W6H-IMC-207 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 8.57E+000 18.033 Pb-212 74.8 4.99E-001 39.365 3.029[52.408] 3.89 -0.711 77.1 2.69E-001 40.195 1.637[53.035] [ 0.537]

238.6 ^ 1.65E-001 34.599 1.000[48.930]

PB-214 74.8 8.84E-001 40.369 6.259[64.964] 6.16 -1.072 77.1 4.75E-001 41.191 3.364[65.478] [ 0.496]

295.2 1.23E-001 76.090 0.870[91.544]

351.9 ^ 1.41E-001 50.899 1.000[71.982]

Ra-226 186.2 ^ 1.01E+000 45.524