ML19095B322

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W6H-IMC-2008-S-P-8

ML19095B322
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Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
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• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2008\\W6H-IMC-200 Report Generated On : 3/27/2017 2:32:17 PM Sample Title : W6H-IMC-2008-S-P-8 Sample Description :

Sample Identification : 2008-S-P-8 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 2.808E+002 grams Sample Taken On : 3/17/2017 12:00:00 AM Acquisition Started : 3/27/2017 1:44:27 PM Live Time : 1800.0 seconds Real Time : 1800.4 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 3/24/2017 Efficiency Calibration Used Done On : 3/27/2017 Efficiency ID : H-IMC-2008-S-P-8

Peak Analysis Report 3/27/2017 2:32:17 PM Page 1

• • • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W6H-IMC-2008-S-P-8 Peak Analysis Performed on: 3/27/2017 2:32:13 PM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 181-192 186.19 46.75 0.63 6.62E+001 21.34 8.80E+001 M 2 286-315 291.02 72.97 0.76 2.98E+001 17.05 7.43E+001 m 3 286-315 299.56 75.11 0.77 1.16E+002 25.40 7.77E+001 m 4 286-315 308.26 77.28 0.77 9.72E+001 23.58 6.70E+001 F 5 735-749 741.82 185.73 1.04 6.56E+001 20.43 5.63E+001 F 6 946-956 952.65 238.47 0.80 8.53E+001 22.35 5.36E+001 F 7 1174-1187 1178.99 295.09 0.97 4.04E+001 16.00 3.64E+001 F 8 1401-1412 1405.39 351.73 0.98 6.93E+001 19.07 2.76E+001 F 9 2425-2441 2432.93 608.76 1.63 5.78E+001 32.92 2.27E+001 F 10 3865-3878 3872.21 968.79 1.26 2.28E+001 12.16 1.58E+001 F 11 5826-5849 5837.77 1460.47 2.41 2.07E+002 26.89 2.67E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 3/27/2017 2:32:17 PM Page 2

• • • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W6H-IMC-2008-S-P-8 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.980 1460.82* 10.66 1.30534E+001 2.02613E+000 Pb-210 0.993 46.54* 4.25 2.69250E+000 1.15585E+000 Pb-212 0.995 74.82* 10.28 9.77072E-001 2.90531E-001 77.11* 17.10 4.80695E-001 1.51511E-001 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 2.29339E-001 7.02256E-002 300.09 3.30 BI-214 0.255 76.86* 0.55 1.50824E+001 4.77312E+000 79.29 0.91 89.26 0.11 89.81 0.21 273.80 0.13 348.92 0.10 386.78 0.29 388.89 0.40 405.72 0.17 454.79 0.29 469.77 0.13 609.32* 45.49 3.89346E-001 2.26286E-001 665.45 1.53 703.11 0.47 719.87 0.39 752.85 0.13 768.36 4.89 786.35 0.32 806.18 1.26 821.18 0.16 826.45 0.12 934.06 3.11 964.08 0.37 1051.96 0.31 1069.96 0.27 1120.29 14.92 1133.66 0.25 1155.21 1.63 1207.68 0.45 1238.11 5.83 1280.98 1.43 1303.75 0.11

Interference Corrected Activity Report 3/27/2017 2:32:17 PM Page 3 Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty BI-214 0.255 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1538.53 0.40 1543.34 0.30 1583.20 0.70 1594.75 0.27 1599.37 0.32 1661.27 1.05 1684.01 0.21 1729.59 2.88 1764.49 15.30 1838.36 0.35 1847.43 2.03 1873.16 0.21 1896.05 0.15 2118.51 1.16 2204.06 4.92 2293.38 0.31 2447.70 1.55 PB-214 0.851 74.82* 5.80 1.73178E+000 5.37748E-001 77.11* 9.70 8.47411E-001 2.77779E-001 86.83 1.70 87.35 2.24 89.78 0.82 241.99 7.25 258.76 0.53 274.80 0.35 295.22* 18.42 3.17165E-001 1.35051E-001 351.93* 35.60 3.37294E-001 1.05261E-001 462.02 0.21 480.43 0.34 487.14 0.43 533.66 0.18 580.14 0.37 785.96 1.06 839.07 0.58 Ra-226 0.969 81.07 0.20 83.79 0.32 186.21* 3.64 1.71082E+000 6.06188E-001

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 3/27/2017 2:32:17 PM Page 4

• • • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.980 1.305343E+001 2.026133E+000 Pb-210 0.993 2.692504E+000 1.155845E+000 Pb-212 0.995 2.613012E-001 6.272815E-002 BI-214 0.255 3.897513E-001 2.260674E-001 PB-214 0.851 3.550297E-001 7.922655E-002 Ra-226 0.969 1.710823E+000 6.061883E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

• • • • • • • • • • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 3/27/2017 2:32:13 PM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide M 2 72.97 1.6556E-002 57.21 Tol. U-235 F 10 968.79 1.2675E-002 53.32 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 3/27/2017 2:32:17 PM Page 5

• • • • • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W6H-IMC-2008-S-P-8 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 6.877E-001 6.88E-001 1.305E+001 2.586E-00 CO-60 1173.23 99.85 1.937E-001 1.86E-001 -5.702E-002 8.927E-00 1332.49 99.98 1.859E-001 -8.067E-002 8.453E-00 CS-137 661.66 85.10 1.549E-001 1.55E-001 -6.865E-002 7.214E-00

+ Pb-210 46.54* 4.25 2.286E+000 2.29E+000 2.693E+000 1.088E+00 BI-212 288.20 0.34 2.012E+001 2.59E+000 -1.273E+001 9.492E+00 328.03 0.13 6.318E+001 1.934E+001 2.985E+00 452.98 0.36 2.579E+001 -3.845E+000 1.205E+00 727.33 6.67 2.595E+000 2.018E+000 1.223E+00 785.37 1.10 1.426E+001 -6.662E+000 6.651E+00 893.41 0.38 4.935E+001 4.832E+001 2.310E+00 952.12 0.17 1.017E+002 1.880E+001 4.717E+00 1078.62 0.56 3.389E+001 7.061E+000 1.570E+00 1512.70 0.29 5.362E+001 2.521E+001 2.358E+00 1620.50 1.47 9.429E+000 2.059E+000 4.037E+00

+ Pb-212 74.82* 10.28 3.674E-001 1.07E-001 9.771E-001 1.723E-00 77.11* 17.10 2.017E-001 4.807E-001 9.414E-00 86.83 2.07 2.672E+000 1.699E+000 1.284E+00 87.35 3.97 1.367E+000 -5.759E-001 6.566E-00 89.78 1.46 3.561E+000 -2.804E+000 1.708E+00 115.18 0.60 6.665E+000 7.189E+000 3.160E+00 238.63* 43.60 1.071E-001 2.293E-001 4.993E-00 300.09 3.30 2.314E+000 2.584E-001 1.097E+00

+ BI-214 76.86* 0.55 6.327E+000 1.82E-001 1.508E+001 2.954E+00 79.29 0.91 6.452E+000 -2.748E-001 3.102E+00 89.26 0.11 4.856E+001 4.938E+001 2.332E+00 89.81 0.21 2.476E+001 -1.949E+001 1.188E+00 273.80 0.13 5.056E+001 6.386E+000 2.386E+00 348.92 0.10 9.962E+001 -1.504E+002 4.757E+00 386.78 0.29 2.723E+001 -1.637E+001 1.274E+00 388.89 0.40 2.162E+001 1.851E+001 1.016E+00 405.72 0.17 5.761E+001 3.077E+001 2.719E+00 454.79 0.29 3.175E+001 -1.038E+000 1.482E+00 469.77 0.13 7.941E+001 1.648E+001 3.730E+00 609.32* 45.49 1.821E-001 3.893E-001 8.195E-00 665.45 1.53 9.442E+000 2.665E+000 4.426E+00 703.11 0.47 3.065E+001 1.066E+001 1.432E+00 719.87 0.39 3.800E+001 -1.378E+001 1.776E+00 752.85 0.13 1.074E+002 3.795E+001 4.971E+00 768.36 4.89 3.124E+000 7.322E-001 1.456E+00 786.35 0.32 5.124E+001 2.183E+000 2.397E+00 806.18 1.26 1.074E+001 -3.054E+000 4.943E+00

Nuclide MDA Report 3/27/2017 2:32:17 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ BI-214 821.18 0.16 9.410E+001 1.82E-001 -8.309E+000 4.363E+00 826.45 0.12 1.356E+002 4.425E+001 6.307E+00 934.06 3.11 5.744E+000 6.084E+000 2.673E+00 964.08 0.37 5.605E+001 1.505E+001 2.628E+00 1051.96 0.31 5.605E+001 -1.620E+001 2.583E+00 1069.96 0.27 6.858E+001 -2.719E+000 3.173E+00 1120.29 14.92 1.368E+000 1.659E-001 6.356E-00 1133.66 0.25 7.942E+001 -2.327E+001 3.680E+00 1155.21 1.63 1.187E+001 1.094E+000 5.479E+00 1207.68 0.45 4.158E+001 -2.887E+001 1.908E+00 1238.11 5.83 3.591E+000 1.162E+000 1.660E+00 1280.98 1.43 1.345E+001 -3.766E+000 6.157E+00 1303.75 0.11 1.744E+002 8.540E+001 7.947E+00 1377.67 3.99 4.904E+000 -1.780E-002 2.236E+00 1385.31 0.79 2.281E+001 3.192E+000 1.031E+00 1401.52 1.33 1.493E+001 1.210E+001 6.803E+00 1407.99 2.39 7.778E+000 -4.727E+000 3.521E+00 1509.21 2.13 6.529E+000 9.196E-001 2.825E+00 1538.53 0.40 2.653E+001 -1.472E+001 1.087E+00 1543.34 0.30 3.494E+001 -1.551E+000 1.432E+00 1583.20 0.70 1.993E+001 -6.308E+000 8.580E+00 1594.75 0.27 6.669E+001 1.692E+001 2.966E+00 1599.37 0.32 5.397E+001 -5.990E+000 2.395E+00 1661.27 1.05 1.401E+001 -8.631E-001 6.033E+00 1684.01 0.21 5.025E+001 -2.922E+001 2.030E+00 1729.59 2.88 5.289E+000 2.539E+000 2.277E+00 1764.49 15.30 1.467E+000 9.912E-001 6.630E-00 1838.36 0.35 3.751E+001 -6.975E+000 1.556E+00 1847.43 2.03 6.842E+000 3.695E+000 2.866E+00 1873.16 0.21 5.913E+001 -4.823E+001 2.424E+00 1896.05 0.15 9.536E+001 -1.459E+001 3.994E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2293.38 0.31 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 6.511E-001 1.38E-001 1.732E+000 3.054E-00 77.11* 9.70 3.555E-001 8.474E-001 1.660E-00 86.83 1.70 3.253E+000 2.069E+000 1.564E+00 87.35 2.24 2.423E+000 -1.021E+000 1.164E+00 89.78 0.82 6.341E+000 -4.993E+000 3.042E+00 241.99 7.25 1.221E+000 -2.066E+000 5.884E-00 258.76 0.53 1.100E+001 3.008E+000 5.180E+00 274.80 0.35 1.820E+001 -4.167E-001 8.590E+00 295.22* 18.42 2.625E-001 3.172E-001 1.206E-00 351.93* 35.60 1.380E-001 3.373E-001 6.243E-00 462.02 0.21 4.598E+001 1.517E+001 2.152E+00 480.43 0.34 3.293E+001 1.089E+001 1.550E+00 487.14 0.43 2.400E+001 7.065E-001 1.123E+00 533.66 0.18 6.002E+001 3.198E+001 2.801E+00 580.14 0.37 3.753E+001 2.011E+001 1.770E+00 785.96 1.06 1.546E+001 6.588E-001 7.232E+00

Nuclide MDA Report 3/27/2017 2:32:17 PM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 839.07 0.58 2.716E+001 1.38E-001 -2.798E+000 1.262E+00

+ Ra-226 81.07 0.20 2.009E+001 1.16E+000 -1.943E+001 9.477E+00 83.79 0.32 1.398E+001 3.693E+000 6.654E+00 186.21* 3.64 1.161E+000 1.711E+000 5.452E-00 PA-234 742.81 0.11 1.306E+002 2.09E+001 -7.956E+000 6.059E+00 766.42 0.32 4.522E+001 -2.032E+001 2.098E+00 1001.03 0.84 2.091E+001 -4.939E+000 9.676E+00 TH-234 63.29 3.70 1.588E+000 1.59E+000 3.750E-001 7.563E-00 92.38 2.13 2.349E+000 2.267E+000 1.126E+00 92.80 2.10 2.341E+000 1.175E+000 1.121E+00 112.81 0.21 1.964E+001 3.243E+000 9.334E+00 U-234 53.20 0.12 5.245E+001 5.25E+001 1.502E+001 2.476E+00 120.90 0.04 1.060E+002 1.720E+001 5.004E+00 U-235 72.70 0.12 5.066E+001 4.03E-001 -1.479E+000 2.433E+00 89.96 3.43 1.515E+000 -1.193E+000 7.267E-00 93.35 5.54 8.506E-001 -1.390E-001 4.065E-00 104.82 0.69 5.379E+000 1.508E+000 2.540E+00 105.60 1.31 2.798E+000 6.727E-002 1.321E+00 108.58 0.50 7.846E+000 3.021E+000 3.719E+00 109.19 1.66 2.383E+000 1.001E+000 1.130E+00 140.76 0.20 2.188E+001 2.107E+000 1.040E+00 143.76 10.96 4.031E-001 1.543E-001 1.915E-00 163.36 5.08 8.338E-001 1.923E-002 3.937E-00 182.62 0.39 1.518E+001 -6.005E+000 7.264E+00 194.94 0.63 8.084E+000 -5.314E+000 3.831E+00 202.12 1.08 4.958E+000 3.403E-001 2.352E+00 205.32 5.02 1.012E+000 -6.777E-001 4.783E-00 221.39 0.12 4.594E+001 -7.198E+000 2.171E+00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

3/27/2017 2:32:17 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

===================================================

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2008\\W6H-IMC-200 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 1.31E+001 15.522 Pb-210 46.5 ^ 2.69E+000 42.928 Pb-212 74.8 9.77E-001 29.735 4.260[42.683] 5.34 -0.977 77.1 4.81E-001 31.519 2.096[43.944] [ 0.463]

238.6 ^ 2.29E-001 30.621 1.000[43.305]

3/27/17 2:32:17 LACE - Key Line Results Page 2 Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

BI-214 76.9 1.51E+001 31.647 38.738[66.177] 11.33 -1.766 609.3 ^ 3.89E-001 58.119 1.000[82.193] [ 0.510]

PB-214 74.8 1.73E+000 31.052 5.134[44.024] 5.17 -0.896 77.1 8.47E-001 32.780 2.512[45.259] [ 0.316]

295.2 3.17E-001 42.581 0.940[52.792]

351.9 ^ 3.37E-001 31.207 1.000[44.134]

Ra-226 186.2 ^ 1.71E+000 35.433