ML19095B318

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W6H-IMC-2008-S-P-7

ML19095B318
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Issue date:	03/01/2018
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To:	NRC Region 1
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• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2008\\W6H-IMC-200 Report Generated On : 3/27/2017 1:48:39 PM Sample Title : W6H-IMC-2008-S-P-7 Sample Description :

Sample Identification : 2008-S-P-7 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 2.879E+002 grams Sample Taken On : 3/17/2017 12:00:00 AM Acquisition Started : 3/27/2017 12:51:52 PM Live Time : 1800.0 seconds Real Time : 1800.3 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 3/24/2017 Efficiency Calibration Used Done On : 3/27/2017 Efficiency ID : H-IMC-2008-S-P-8

Peak Analysis Report 3/27/2017 1:48:39 PM Page 1

• • • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W6H-IMC-2008-S-P-7 Peak Analysis Performed on: 3/27/2017 1:48:35 PM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts M 1 296-314 299.67 75.13 0.78 9.13E+001 25.67 9.75E+001 m 2 296-314 308.38 77.31 0.78 7.41E+001 23.30 1.05E+002 F 3 735-750 742.25 185.84 1.02 7.22E+001 20.93 6.00E+001 F 4 948-960 953.06 238.58 1.12 1.07E+002 24.35 5.36E+001 F 5 1174-1186 1179.38 295.19 0.93 2.84E+001 14.41 3.38E+001 F 6 1400- 1413 1406.13 351.91 1.01 5.81E+001 17.87 3.22E+001 F 7 5822-5849 5836.62 1460.18 2.71 1.80E+002 25.06 1.24E+001 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 3/27/2017 1:48:39 PM Page 2

• • • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W6H-IMC-2008-S-P-7 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.937 1460.82* 10.66 1.10921E+001 1.80622E+000 Pb-212 0.996 74.82* 10.28 7.47634E-001 2.58798E-001 77.11* 17.10 3.57112E-001 1.33346E-001 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 2.80408E-001 7.78183E-002 300.09 3.30 PB-214 0.854 74.82* 5.80 1.32512E+000 4.73773E-001 77.11* 9.70 6.29547E-001 2.41811E-001 86.83 1.70 87.35 2.24 89.78 0.82 241.99 7.25 258.76 0.53 274.80 0.35 295.22* 18.42 2.17024E-001 1.15405E-001 351.93* 35.60 2.75913E-001 9.40917E-002 462.02 0.21 480.43 0.34 487.14 0.43 533.66 0.18 580.14 0.37 785.96 1.06 839.07 0.58 Ra-226 0.981 81.07 0.20 83.79 0.32 186.21* 3.64 1.83557E+000 6.16253E-001

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 3/27/2017 1:48:39 PM Page 3

• • • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.937 1.109211E+001 1.806216E+000 Pb-212 0.996 2.848519E-001 6.585274E-002 PB-214 0.854 2.545483E-001 6.997354E-002 Ra-226 0.981 1.835573E+000 6.162528E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

• • • • • • • • • • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 3/27/2017 1:48:35 PM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified.

Nuclide MDA Report 3/27/2017 1:48:39 PM Page 4

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W6H-IMC-2008-S-P-7 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 1.306E+000 1.31E+000 1.109E+001 5.701E-00 CO-60 1173.23 99.85 1.734E-001 1.63E-001 -3.685E-002 7.931E-00 1332.49 99.98 1.634E-001 -1.212E-001 7.347E-00 CS-137 661.66 85.10 1.543E-001 1.54E-001 2.123E-002 7.202E-00 Pb-210 46.54 4.25 2.497E+000 2.50E+000 2.940E+000 1.194E+00 BI-212 288.20 0.34 1.810E+001 2.06E+000 3.266E-001 8.496E+00 328.03 0.13 5.639E+001 -1.132E+001 2.649E+00 452.98 0.36 2.411E+001 -1.156E+001 1.123E+00 727.33 6.67 2.061E+000 -9.042E-001 9.585E-00 785.37 1.10 1.149E+001 -1.033E+001 5.276E+00 893.41 0.38 3.961E+001 5.425E+000 1.827E+00 952.12 0.17 9.045E+001 1.000E+001 4.162E+00 1078.62 0.56 3.160E+001 2.408E+000 1.459E+00 1512.70 0.29 5.100E+001 1.359E+001 2.235E+00 1620.50 1.47 1.097E+001 6.867E+000 4.822E+00

+ Pb-212 74.82* 10.28 3.986E-001 1.10E-001 7.476E-001 1.882E-00 77.11* 17.10 2.423E-001 3.571E-001 1.146E-00 86.83 2.07 2.564E+000 4.842E-001 1.231E+00 87.35 3.97 1.298E+000 3.874E-002 6.228E-00 89.78 1.46 2.978E+000 -5.627E+000 1.419E+00 115.18 0.60 6.196E+000 -1.013E+000 2.930E+00 238.63* 43.60 1.095E-001 2.804E-001 5.122E-00 300.09 3.30 2.139E+000 3.693E-001 1.011E+00 BI-214 76.86 0.55 1.350E+001 3.16E-001 2.709E+001 6.544E+00 79.29 0.91 6.134E+000 2.382E-001 2.946E+00 89.26 0.11 4.057E+001 -9.356E+000 1.935E+00 89.81 0.21 2.070E+001 -3.911E+001 9.862E+00 273.80 0.13 5.074E+001 1.235E+001 2.399E+00 348.92 0.10 9.250E+001 -4.434E+001 4.407E+00 386.78 0.29 2.621E+001 -8.238E-001 1.225E+00 388.89 0.40 2.011E+001 1.085E+001 9.423E+00 405.72 0.17 4.811E+001 -1.047E+001 2.248E+00 454.79 0.29 3.182E+001 1.240E+001 1.488E+00 469.77 0.13 7.037E+001 -5.154E+001 3.284E+00 609.32 45.49 3.158E-001 2.793E-001 1.490E-00 665.45 1.53 9.037E+000 2.676E+000 4.231E+00 703.11 0.47 2.616E+001 -9.307E+000 1.209E+00 719.87 0.39 3.418E+001 -7.618E+000 1.588E+00 752.85 0.13 1.118E+002 1.820E+001 5.202E+00 768.36 4.89 2.911E+000 1.368E+000 1.352E+00 786.35 0.32 4.003E+001 -1.704E+001 1.840E+00 806.18 1.26 1.206E+001 -1.412E+000 5.613E+00

Nuclide MDA Report 3/27/2017 1:48:39 PM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram BI-214 821.18 0.16 8.365E+001 3.16E-001 -5.814E+000 3.849E+00 826.45 0.12 1.097E+002 -1.122E+002 5.023E+00 934.06 3.11 5.729E+000 4.109E+000 2.670E+00 964.08 0.37 5.158E+001 2.496E+001 2.409E+00 1051.96 0.31 5.077E+001 -4.345E+000 2.325E+00 1069.96 0.27 6.446E+001 -1.003E+001 2.973E+00 1120.29 14.92 1.407E+000 -1.268E-001 6.562E-00 1133.66 0.25 7.264E+001 -6.140E+001 3.348E+00 1155.21 1.63 1.301E+001 5.661E+000 6.060E+00 1207.68 0.45 4.395E+001 5.245E+000 2.030E+00 1238.11 5.83 3.891E+000 2.784E+000 1.814E+00 1280.98 1.43 1.250E+001 -3.878E+000 5.697E+00 1303.75 0.11 1.884E+002 1.527E+002 8.666E+00 1377.67 3.99 4.337E+000 5.814E-001 1.957E+00 1385.31 0.79 2.291E+001 -1.881E+001 1.039E+00 1401.52 1.33 1.510E+001 1.146E+001 6.906E+00 1407.99 2.39 7.128E+000 -1.723E+000 3.205E+00 1509.21 2.13 7.105E+000 9.848E-001 3.124E+00 1538.53 0.40 3.243E+001 -5.743E+000 1.389E+00 1543.34 0.30 3.601E+001 -2.534E+001 1.493E+00 1583.20 0.70 2.726E+001 -6.485E+000 1.228E+00 1594.75 0.27 7.008E+001 -1.473E+001 3.145E+00 1599.37 0.32 4.917E+001 -3.773E+000 2.162E+00 1661.27 1.05 1.367E+001 -8.418E-001 5.884E+00 1684.01 0.21 6.541E+001 -7.645E+000 2.800E+00 1729.59 2.88 4.985E+000 2.211E+000 2.134E+00 1764.49 15.30 1.219E+000 5.100E-001 5.410E-00 1838.36 0.35 4.341E+001 1.084E+001 1.858E+00 1847.43 2.03 7.263E+000 -2.903E+000 3.090E+00 1873.16 0.21 6.093E+001 1.594E+001 2.527E+00 1896.05 0.15 1.222E+002 5.191E+001 5.354E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2293.38 0.31 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 7.064E-001 1.50E-001 1.325E+000 3.336E-00 77.11* 9.70 4.272E-001 6.295E-001 2.021E-00 86.83 1.70 3.122E+000 5.896E-001 1.499E+00 87.35 2.24 2.300E+000 6.866E-002 1.104E+00 89.78 0.82 5.303E+000 -1.002E+001 2.526E+00 241.99 7.25 1.184E+000 1.699E-001 5.703E-00 258.76 0.53 1.108E+001 2.165E+000 5.223E+00 274.80 0.35 1.828E+001 -7.353E+000 8.638E+00 295.22* 18.42 2.427E-001 2.170E-001 1.110E-00 351.93* 35.60 1.503E-001 2.759E-001 6.873E-00 462.02 0.21 4.794E+001 2.649E+001 2.253E+00 480.43 0.34 3.069E+001 2.903E-001 1.440E+00 487.14 0.43 2.400E+001 -8.729E-001 1.125E+00 533.66 0.18 5.600E+001 -1.204E+001 2.604E+00 580.14 0.37 3.697E+001 3.847E+001 1.744E+00 785.96 1.06 1.208E+001 -6.451E+000 5.553E+00

Nuclide MDA Report 3/27/2017 1:48:39 PM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 839.07 0.58 2.450E+001 1.50E-001 3.672E+000 1.131E+00

+ Ra-226 81.07 0.20 2.289E+001 1.19E+000 -5.299E+000 1.090E+00 83.79 0.32 1.639E+001 1.481E+001 7.868E+00 186.21* 3.64 1.191E+000 1.836E+000 5.612E-00 PA-234 742.81 0.11 1.263E+002 1.83E+001 -1.115E+001 5.857E+00 766.42 0.32 4.337E+001 -7.556E-001 2.009E+00 1001.03 0.84 1.828E+001 -9.845E-001 8.380E+00 TH-234 63.29 3.70 1.538E+000 1.54E+000 1.598E+000 7.323E-00 92.38 2.13 2.216E+000 1.539E+000 1.060E+00 92.80 2.10 2.225E+000 1.200E+000 1.064E+00 112.81 0.21 1.706E+001 -2.284E+000 8.052E+00 U-234 53.20 0.12 4.804E+001 4.80E+001 1.942E+000 2.259E+00 120.90 0.04 1.008E+002 1.837E+001 4.753E+00 U-235 72.70 0.12 5.082E+001 4.01E-001 -2.813E+001 2.443E+00 89.96 3.43 1.267E+000 -2.393E+000 6.034E-00 93.35 5.54 8.519E-001 7.457E-001 4.076E-00 104.82 0.69 5.469E+000 -2.510E+000 2.589E+00 105.60 1.31 2.921E+000 2.625E-001 1.385E+00 108.58 0.50 7.287E+000 -3.756E+000 3.444E+00 109.19 1.66 2.122E+000 -2.973E+000 1.001E+00 140.76 0.20 2.222E+001 2.691E+000 1.058E+00 143.76 10.96 4.006E-001 7.392E-002 1.905E-00 163.36 5.08 8.210E-001 -2.084E-001 3.879E-00 182.62 0.39 1.501E+001 -2.226E+000 7.189E+00 194.94 0.63 7.918E+000 -6.688E+000 3.753E+00 202.12 1.08 4.895E+000 -1.053E+000 2.323E+00 205.32 5.02 1.001E+000 -1.469E+000 4.734E-00 221.39 0.12 4.685E+001 2.038E+000 2.220E+00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

3/27/2017 1:48:39 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2008\\W6H-IMC-200 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 1.11E+001 16.284 Pb-212 74.8 7.48E-001 34.616 2.666[44.367] 3.05 -0.559 77.1 3.57E-001 37.340 1.274[46.524] [ 0.443]

238.6 ^ 2.80E-001 27.752 1.000[39.247]

PB-214 74.8 1.33E+000 35.753 4.803[49.409] 5.00 -0.876 77.1 6.30E-001 38.410 2.282[51.364] [ 0.355]

295.2 2.17E-001 53.176 0.787[63.171]

351.9 ^ 2.76E-001 34.102 1.000[48.227]

Ra-226 186.2 ^ 1.84E+000 33.573