ML19095B303

From kanterella
Jump to navigation Jump to search
Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W6H-IMC-2008-S-P-2
ML19095B303
Person / Time
Site: 07000371
Issue date: 03/01/2018
From:
Cabrera Services
To:
NRC Region 1
Shared Package
ml051740240 List: ... further results
References
Download: ML19095B303 (9)
v • d • e


Text

          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2008\\W6H-IMC-200 Report Generated On : 3/27/2017 10:34:04 AM Sample Title : W6H-IMC-2008-S-P-2 Sample Description :

Sample Identification : 2008-S-P-2 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 3.110E+002 grams Sample Taken On : 3/17/2017 12:00:00 AM Acquisition Started : 3/27/2017 9:53:03 AM Live Time : 1800.0 seconds Real Time : 1800.4 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 3/24/2017 Efficiency Calibration Used Done On : 3/27/2017 Efficiency ID : H-IMC-2008-S-P-2

Peak Analysis Report 3/27/2017 10:34:04 AM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W6H-IMC-2008-S-P-2 Peak Analysis Performed on: 3/27/2017 10:34:00 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 182-191 186.91 46.93 0.30 3.57E+001 15.92 6.50E+001 M 2 295-315 299.81 75.17 0.59 7.32E+001 24.11 1.19E+002 m 3 295-315 308.79 77.41 0.60 7.26E+001 22.20 8.33E+001 F 4 732-749 742.06 185.80 0.95 6.91E+001 20.44 6.98E+001 F 5 945-960 953.40 238.66 1.08 1.18E+002 25.06 5.60E+001 F 6 1175-1184 1179.59 295.24 1.04 4.07E+001 15.98 2.40E+001 F 7 2028-2049 2040.00 510.47 1.71 8.12E+001 29.97 3.30E+001 F 8 5824-5850 5836.64 1460.19 2.61 2.08E+002 20.02 9.00E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 3/27/2017 10:34:04 AM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W6H-IMC-2008-S-P-2 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.938 1460.82* 10.66 1.03959E+001 1.33485E+000 Pb-210 0.976 46.54* 4.25 1.22191E+000 6.44620E-001 Pb-212 0.994 74.82* 10.28 5.04562E-001 1.94960E-001 77.11* 17.10 2.93971E-001 1.07649E-001 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 2.54581E-001 6.74903E-002 300.09 3.30 PB-214 0.408 74.82* 5.80 8.94292E-001 3.54694E-001 77.11* 9.70 5.18238E-001 1.95424E-001 86.83 1.70 87.35 2.24 89.78 0.82 241.99 7.25 258.76 0.53 274.80 0.35 295.22* 18.42 2.56023E-001 1.08171E-001 351.93 35.60 462.02 0.21 480.43 0.34 487.14 0.43 533.66 0.18 580.14 0.37 785.96 1.06 839.07 0.58 Ra-226 0.976 81.07 0.20 83.79 0.32 186.21* 3.64 1.44939E+000 4.93714E-001

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 3/27/2017 10:34:04 AM Page 3

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.938 1.039595E+001 1.334853E+000 Pb-210 0.976 1.221906E+000 6.446203E-001 Pb-212 0.994 2.396000E-001 5.762508E-002 PB-214 0.408 2.339104E-001 9.548989E-002 Ra-226 0.976 1.449391E+000 4.937140E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 3/27/2017 10:34:00 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 7 510.47 4.5107E-002 36.92 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 3/27/2017 10:34:04 AM Page 4

          • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W6H-IMC-2008-S-P-2 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 9.141E-001 9.14E-001 1.040E+001 3.895E-00 CO-60 1173.23 99.85 1.595E-001 9.93E-002 7.407E-002 7.374E-00 1332.49 99.98 9.934E-002 -9.136E-002 4.299E-00 CS-137 661.66 85.10 1.362E-001 1.36E-001 3.375E-002 6.388E-00

+ Pb-210 46.54* 4.25 1.575E+000 1.57E+000 1.222E+000 7.410E-00 BI-212 288.20 0.34 1.603E+001 1.90E+000 1.643E+000 7.562E+00 328.03 0.13 4.518E+001 -2.785E+001 2.120E+00 452.98 0.36 2.180E+001 1.501E+001 1.022E+00 727.33 6.67 1.899E+000 4.987E-001 8.911E-00 785.37 1.10 1.125E+001 3.664E+000 5.246E+00 893.41 0.38 3.317E+001 -1.094E+001 1.533E+00 952.12 0.17 7.870E+001 -1.397E+001 3.641E+00 1078.62 0.56 2.666E+001 -8.107E+000 1.234E+00 1512.70 0.29 2.841E+001 -8.410E-001 1.165E+00 1620.50 1.47 8.905E+000 -5.378E+000 3.916E+00

+ Pb-212 74.82* 10.28 3.692E-001 9.79E-002 5.046E-001 1.753E-00 77.11* 17.10 1.830E-001 2.940E-001 8.601E-00 86.83 2.07 2.151E+000 1.091E-001 1.034E+00 87.35 3.97 1.119E+000 -3.405E-001 5.374E-00 89.78 1.46 2.912E+000 -2.854E+000 1.397E+00 115.18 0.60 5.170E+000 4.467E-001 2.445E+00 238.63* 43.60 9.792E-002 2.546E-001 4.604E-00 300.09 3.30 1.714E+000 -2.482E+000 8.087E-00 BI-214 76.86 0.55 1.142E+001 2.64E-001 2.208E+001 5.537E+00 79.29 0.91 5.417E+000 -2.251E-001 2.607E+00 89.26 0.11 3.884E+001 1.333E+001 1.864E+00 89.81 0.21 2.024E+001 -1.984E+001 9.712E+00 273.80 0.13 3.929E+001 -2.516E+000 1.851E+00 348.92 0.10 7.262E+001 9.254E+001 3.452E+00 386.78 0.29 2.204E+001 -6.281E+000 1.032E+00 388.89 0.40 1.627E+001 1.034E+000 7.615E+00 405.72 0.17 4.556E+001 4.868E+001 2.149E+00 454.79 0.29 2.516E+001 -1.206E+001 1.174E+00 469.77 0.13 6.111E+001 -5.092E+000 2.863E+00 609.32 45.49 2.641E-001 9.388E-002 1.248E-00 665.45 1.53 6.984E+000 -3.287E+000 3.257E+00 703.11 0.47 2.246E+001 3.943E+000 1.043E+00 719.87 0.39 2.765E+001 -3.252E+001 1.284E+00 752.85 0.13 9.453E+001 1.000E+000 4.411E+00 768.36 4.89 2.537E+000 7.686E-001 1.184E+00 786.35 0.32 3.794E+001 -4.442E+000 1.766E+00 806.18 1.26 8.962E+000 -3.919E+000 4.140E+00

Nuclide MDA Report 3/27/2017 10:34:04 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram BI-214 821.18 0.16 8.023E+001 2.64E-001 4.076E+001 3.740E+00 826.45 0.12 9.336E+001 -3.973E+001 4.292E+00 934.06 3.11 4.731E+000 -9.176E-002 2.207E+00 964.08 0.37 4.169E+001 1.929E+001 1.946E+00 1051.96 0.31 4.269E+001 -3.173E+001 1.961E+00 1069.96 0.27 5.441E+001 3.189E+000 2.517E+00 1120.29 14.92 1.094E+000 5.940E-001 5.084E-00 1133.66 0.25 5.670E+001 8.322E+000 2.604E+00 1155.21 1.63 9.675E+000 6.504E-001 4.477E+00 1207.68 0.45 4.006E+001 6.835E+000 1.867E+00 1238.11 5.83 2.821E+000 -9.407E-002 1.303E+00 1280.98 1.43 9.764E+000 1.659E+000 4.433E+00 1303.75 0.11 1.382E+002 4.513E+000 6.299E+00 1377.67 3.99 3.684E+000 1.311E+000 1.670E+00 1385.31 0.79 1.835E+001 -6.377E+000 8.307E+00 1401.52 1.33 1.021E+001 -2.896E+000 4.581E+00 1407.99 2.39 5.886E+000 4.428E+000 2.652E+00 1509.21 2.13 4.079E+000 -1.771E+000 1.692E+00 1538.53 0.40 2.438E+001 -7.463E+000 1.029E+00 1543.34 0.30 3.591E+001 1.690E+001 1.546E+00 1583.20 0.70 1.727E+001 -2.566E+000 7.539E+00 1594.75 0.27 5.173E+001 4.522E+001 2.295E+00 1599.37 0.32 3.792E+001 -6.622E+000 1.655E+00 1661.27 1.05 1.110E+001 1.338E+000 4.778E+00 1684.01 0.21 5.847E+001 1.227E+001 2.542E+00 1729.59 2.88 4.047E+000 1.795E+000 1.732E+00 1764.49 15.30 1.324E+000 1.347E+000 6.061E-00 1838.36 0.35 3.260E+001 -1.778E+000 1.377E+00 1847.43 2.03 5.416E+000 -6.338E-001 2.268E+00 1873.16 0.21 6.072E+001 2.852E+001 2.614E+00 1896.05 0.15 9.915E+001 7.700E+001 4.345E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2293.38 0.31 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 6.544E-001 1.60E-001 8.943E-001 3.106E-00 77.11* 9.70 3.226E-001 5.182E-001 1.516E-00 86.83 1.70 2.620E+000 1.329E-001 1.259E+00 87.35 2.24 1.983E+000 -6.034E-001 9.525E-00 89.78 0.82 5.185E+000 -5.081E+000 2.487E+00 241.99 7.25 9.894E-001 -2.285E-001 4.769E-00 258.76 0.53 9.195E+000 -4.363E+000 4.339E+00 274.80 0.35 1.337E+001 -1.366E+001 6.276E+00 295.22* 18.42 1.603E-001 2.560E-001 7.163E-00 351.93 35.60 2.124E-001 2.650E-001 1.010E-00 462.02 0.21 3.877E+001 8.045E+000 1.821E+00 480.43 0.34 2.555E+001 7.786E+000 1.200E+00 487.14 0.43 1.877E+001 -7.889E-001 8.775E+00 533.66 0.18 4.716E+001 6.988E+000 2.198E+00 580.14 0.37 3.151E+001 3.000E+001 1.491E+00 785.96 1.06 1.145E+001 -1.341E+000 5.328E+00

Nuclide MDA Report 3/27/2017 10:34:04 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 839.07 0.58 2.192E+001 1.60E-001 5.092E+000 1.020E+00

+ Ra-226 81.07 0.20 1.887E+001 1.10E+000 -3.080E+000 8.971E+00 83.79 0.32 1.246E+001 1.218E+001 5.953E+00 186.21* 3.64 1.095E+000 1.449E+000 5.192E-00 U-234 53.20 0.12 4.421E+001 4.42E+001 -2.004E+001 2.087E+00 120.90 0.04 8.985E+001 -1.414E+001 4.253E+00 U-235 72.70 0.12 4.420E+001 3.34E-001 1.582E+001 2.127E+00 89.96 3.43 1.239E+000 -1.214E+000 5.942E-00 93.35 5.54 7.033E-001 1.019E-001 3.363E-00 104.82 0.69 4.533E+000 2.239E-001 2.145E+00 105.60 1.31 2.380E+000 -3.745E-001 1.126E+00 108.58 0.50 6.628E+000 -1.960E+000 3.148E+00 109.19 1.66 1.973E+000 6.151E-003 9.366E-00 140.76 0.20 1.690E+001 -2.110E+001 8.011E+00 143.76 10.96 3.338E-001 3.579E-002 1.588E-00 163.36 5.08 7.153E-001 -2.651E-001 3.390E-00 182.62 0.39 1.203E+001 -1.111E+000 5.756E+00 194.94 0.63 6.689E+000 1.617E+000 3.175E+00 202.12 1.08 4.016E+000 -2.036E+000 1.906E+00 205.32 5.02 8.752E-001 -4.438E-001 4.153E-00 221.39 0.12 3.823E+001 -5.219E+000 1.811E+00 U-238 63.29 3.70 1.307E+000 9.74E-001 1.189E-001 6.222E-00 92.60 4.23 9.735E-001 3.122E-001 4.666E-00 766.42 0.32 3.925E+001 3.091E+001 1.834E+00 1001.03 0.84 1.615E+001 2.861E+000 7.455E+00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

3/27/2017 10:34:04 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
===================================================

Analysis using Key Line Activities

===================================================

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2008\\W6H-IMC-200 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 1.04E+001 12.840 Pb-210 46.5 ^ 1.22E+000 52.755 Pb-212 74.8 5.05E-001 38.640 1.982[46.859] 1.97 -0.360 77.1 2.94E-001 36.619 1.155[45.208] [ 0.434]

238.6 ^ 2.55E-001 26.510 1.000[37.491]

PB-214 74.8 8.94E-001 ******

77.1 5.18E-001 ******

295.2 2.56E-001 ******

Ra-226 186.2 ^ 1.45E+000 34.064

Retrieved from "https://kanterella.com/w/index.php?title=ML19095B303&oldid=4932748"