ML19095B300

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Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W6H-IMC-2008-S-P-1
ML19095B300
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Site: 07000371
Issue date: 03/01/2018
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Cabrera Services
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NRC Region 1
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Download: ML19095B300 (9)
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          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2008\\W6H-IMC-200 Report Generated On : 3/27/2017 10:32:40 AM Sample Title : W6H-IMC-2008-S-P-1 Sample Description :

Sample Identification : 2008-S-P-1 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 2.074E+002 grams Sample Taken On : 3/17/2017 12:00:00 AM Acquisition Started : 3/27/2017 9:02:57 AM Live Time : 1800.0 seconds Real Time : 1800.3 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 3/24/2017 Efficiency Calibration Used Done On : 3/27/2017 Efficiency ID : H-IMC-2008-S-P-1

Peak Analysis Report 3/27/2017 10:32:40 AM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W6H-IMC-2008-S-P-1 Peak Analysis Performed on: 3/27/2017 10:32:37 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 180- 192 186.65 46.86 0.75 5.75E+001 19.57 6.50E+001 M 2 295-313 300.02 75.22 0.62 7.17E+001 22.54 7.77E+001 m 3 295-313 308.37 77.31 0.63 4.62E+001 18.24 6.96E+001 F 4 738-748 742.19 185.83 0.90 4.33E+001 18.95 5.64E+001 F 5 946-959 953.10 238.59 0.77 6.17E+001 19.51 6.13E+001 F 6 1401-1411 1405.98 351.87 1.04 2.80E+001 13.70 1.98E+001 F 7 5827-5851 5838.91 1460.76 2.17 1.72E+002 25.63 1.39E+001 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 3/27/2017 10:32:41 AM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W6H-IMC-2008-S-P-1 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.999 1460.82* 10.66 1.37868E+001 2.36452E+000 Pb-210 0.984 46.54* 4.25 3.05371E+000 1.35081E+000 Pb-212 0.995 74.82* 10.28 7.77469E-001 2.90354E-001 77.11* 17.10 2.94835E-001 1.30670E-001 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 2.12056E-001 7.50353E-002 300.09 3.30 PB-214 0.664 74.82* 5.80 1.37800E+000 5.29190E-001 77.11* 9.70 5.19761E-001 2.35061E-001 86.83 1.70 87.35 2.24 89.78 0.82 241.99 7.25 258.76 0.53 274.80 0.35 295.22 18.42 351.93* 35.60 1.74015E-001 8.89434E-002 462.02 0.21 480.43 0.34 487.14 0.43 533.66 0.18 580.14 0.37 785.96 1.06 839.07 0.58 Ra-226 0.980 81.07 0.20 83.79 0.32 186.21* 3.64 1.44567E+000 6.77845E-001

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 3/27/2017 10:32:41 AM Page 3

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.999 1.378685E+001 2.364516E+000 Pb-210 0.984 3.053706E+000 1.350811E+000 Pb-212 0.995 2.287144E-001 6.473003E-002 PB-214 0.664 1.872164E-001 8.369225E-002 Ra-226 0.980 1.445670E+000 6.778449E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 3/27/2017 10:32:37 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified.

Nuclide MDA Report 3/27/2017 10:32:41 AM Page 4

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W6H-IMC-2008-S-P-1 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 Full NLB.NL Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 1.735E+000 1.73E+000 1.379E+001 7.589E-00 CO-60 1173.23 99.85 2.510E-001 1.78E-001 -8.539E-002 1.159E-00 1332.49 99.98 1.778E-001 -1.720E-001 7.817E-00 CS-137 661.66 85.10 2.043E-001 2.04E-001 4.264E-003 9.544E-00

+ Pb-210 46.54* 4.25 2.651E+000 2.65E+000 3.054E+000 1.254E+00 BI-212 288.20 0.34 2.211E+001 2.69E+000 -3.689E+000 1.033E+00 328.03 0.13 6.573E+001 -6.173E+001 3.064E+00 452.98 0.36 3.524E+001 2.014E+001 1.655E+00 727.33 6.67 2.690E+000 -1.180E+000 1.251E+00 785.37 1.10 1.708E+001 -2.224E+000 7.927E+00 893.41 0.38 5.265E+001 4.489E+001 2.432E+00 952.12 0.17 1.180E+002 2.500E+001 5.428E+00 1078.62 0.56 3.796E+001 -3.117E+001 1.740E+00 1512.70 0.29 7.293E+001 1.855E+001 3.236E+00 1620.50 1.47 1.561E+001 1.149E+001 6.945E+00

+ Pb-212 74.82* 10.28 4.741E-001 1.56E-001 7.775E-001 2.224E-00 77.11* 17.10 2.650E-001 2.948E-001 1.239E-00 86.83 2.07 2.918E+000 1.427E+000 1.392E+00 87.35 3.97 1.498E+000 -3.454E-001 7.143E-00 89.78 1.46 3.946E+000 -3.267E+000 1.880E+00 115.18 0.60 6.709E+000 -2.668E+000 3.134E+00 238.63* 43.60 1.562E-001 2.121E-001 7.343E-00 300.09 3.30 2.866E+000 -2.788E+000 1.356E+00 BI-214 76.86 0.55 1.557E+001 3.60E-001 -5.363E-001 7.515E+00 79.29 0.91 7.254E+000 4.728E-001 3.467E+00 89.26 0.11 5.121E+001 -1.830E+000 2.437E+00 89.81 0.21 2.743E+001 -2.271E+001 1.307E+00 273.80 0.13 6.427E+001 2.340E+001 3.032E+00 348.92 0.10 1.039E+002 -3.925E+001 4.909E+00 386.78 0.29 3.428E+001 -1.641E+001 1.602E+00 388.89 0.40 2.564E+001 -1.835E+000 1.199E+00 405.72 0.17 6.543E+001 1.324E+001 3.066E+00 454.79 0.29 4.348E+001 6.204E+000 2.039E+00 469.77 0.13 8.522E+001 3.028E+000 3.954E+00 609.32 45.49 3.597E-001 -2.146E-003 1.682E-00 665.45 1.53 1.134E+001 5.558E+000 5.292E+00 703.11 0.47 3.595E+001 2.864E+001 1.669E+00 719.87 0.39 4.426E+001 -1.521E+001 2.055E+00 752.85 0.13 1.228E+002 -6.405E+000 5.633E+00 768.36 4.89 3.706E+000 2.212E+000 1.718E+00 786.35 0.32 5.982E+001 1.245E+001 2.781E+00 806.18 1.26 1.609E+001 2.303E+000 7.501E+00

Nuclide MDA Report 3/27/2017 10:32:41 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram BI-214 821.18 0.16 1.256E+002 3.60E-001 -1.471E+001 5.847E+00 826.45 0.12 1.712E+002 3.563E+001 7.959E+00 934.06 3.11 6.281E+000 8.821E-001 2.888E+00 964.08 0.37 6.345E+001 -3.071E+000 2.951E+00 1051.96 0.31 7.128E+001 2.343E+001 3.285E+00 1069.96 0.27 7.640E+001 -3.473E+001 3.494E+00 1120.29 14.92 1.821E+000 8.324E-001 8.489E-00 1133.66 0.25 9.187E+001 -8.826E+001 4.223E+00 1155.21 1.63 1.645E+001 -8.556E-001 7.644E+00 1207.68 0.45 5.110E+001 -3.539E+001 2.337E+00 1238.11 5.83 4.174E+000 8.336E-001 1.915E+00 1280.98 1.43 1.748E+001 -1.862E+000 8.020E+00 1303.75 0.11 2.188E+002 1.520E+002 9.960E+00 1377.67 3.99 4.891E+000 5.993E-001 2.170E+00 1385.31 0.79 2.623E+001 5.543E+000 1.172E+00 1401.52 1.33 1.550E+001 2.719E+000 6.911E+00 1407.99 2.39 8.301E+000 8.253E-001 3.683E+00 1509.21 2.13 1.071E+001 7.240E+000 4.797E+00 1538.53 0.40 4.072E+001 1.609E+001 1.732E+00 1543.34 0.30 6.472E+001 1.626E+001 2.836E+00 1583.20 0.70 2.845E+001 -1.278E+001 1.247E+00 1594.75 0.27 7.159E+001 -2.994E+001 3.112E+00 1599.37 0.32 6.084E+001 3.441E+001 2.656E+00 1661.27 1.05 2.101E+001 4.386E+000 9.267E+00 1684.01 0.21 9.382E+001 -2.852E+001 4.079E+00 1729.59 2.88 6.009E+000 -2.846E+000 2.538E+00 1764.49 15.30 1.654E+000 5.552E-001 7.375E-00 1838.36 0.35 3.938E+001 -6.172E+001 1.562E+00 1847.43 2.03 9.086E+000 3.312E+000 3.837E+00 1873.16 0.21 9.415E+001 4.076E+001 4.031E+00 1896.05 0.15 1.507E+002 1.090E+002 6.549E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2293.38 0.31 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 8.403E-001 1.49E-001 1.378E+000 3.942E-00 77.11* 9.70 4.672E-001 5.198E-001 2.184E-00 86.83 1.70 3.553E+000 1.737E+000 1.696E+00 87.35 2.24 2.654E+000 -6.122E-001 1.266E+00 89.78 0.82 7.025E+000 -5.817E+000 3.347E+00 241.99 7.25 1.432E+000 5.239E-002 6.877E-00 258.76 0.53 1.375E+001 -3.996E+000 6.465E+00 274.80 0.35 2.231E+001 4.598E+000 1.050E+00 295.22 18.42 5.073E-001 3.017E-001 2.401E-00 351.93* 35.60 1.488E-001 1.740E-001 6.597E-00 462.02 0.21 5.863E+001 2.884E+001 2.744E+00 480.43 0.34 3.445E+001 5.236E+000 1.599E+00 487.14 0.43 2.726E+001 -5.705E+000 1.266E+00 533.66 0.18 7.595E+001 3.242E+001 3.542E+00 580.14 0.37 4.658E+001 3.568E+001 2.193E+00 785.96 1.06 1.776E+001 -4.025E+000 8.247E+00

Nuclide MDA Report 3/27/2017 10:32:41 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 839.07 0.58 3.400E+001 1.49E-001 -1.197E+001 1.578E+00

+ Ra-226 81.07 0.20 2.729E+001 1.36E+000 2.516E+000 1.291E+00 83.79 0.32 1.709E+001 -3.798E+000 8.111E+00 186.21* 3.64 1.360E+000 1.446E+000 6.350E-00 U-234 53.20 0.12 6.208E+001 6.21E+001 1.016E+001 2.912E+00 120.90 0.04 1.235E+002 1.191E+001 5.794E+00 U-235 72.70 0.12 5.939E+001 4.75E-001 4.303E+001 2.840E+00 89.96 3.43 1.678E+000 -1.390E+000 7.996E-00 93.35 5.54 9.678E-001 3.041E-001 4.597E-00 104.82 0.69 6.606E+000 1.205E+000 3.111E+00 105.60 1.31 3.453E+000 3.458E-001 1.626E+00 108.58 0.50 9.041E+000 -5.820E-001 4.258E+00 109.19 1.66 2.752E+000 -5.844E-002 1.297E+00 140.76 0.20 2.460E+001 -2.398E+001 1.160E+00 143.76 10.96 4.752E-001 -5.093E-002 2.248E-00 163.36 5.08 1.042E+000 3.941E-001 4.911E-00 182.62 0.39 1.864E+001 -1.356E+001 8.902E+00 194.94 0.63 9.317E+000 -1.050E+000 4.388E+00 202.12 1.08 5.827E+000 2.506E+000 2.751E+00 205.32 5.02 1.288E+000 -6.084E-001 6.088E-00 221.39 0.12 5.324E+001 1.989E+001 2.502E+00 U-238 63.29 3.70 1.888E+000 1.30E+000 1.027E+000 8.952E-00 92.60 4.23 1.300E+000 5.402E-001 6.182E-00 766.42 0.32 5.510E+001 1.259E+001 2.549E+00 1001.03 0.84 2.488E+001 -3.576E+000 1.145E+00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

3/27/2017 10:32:41 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
===================================================

Analysis using Key Line Activities

===================================================

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2008\\W6H-IMC-200 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 1.38E+001 17.151 Pb-210 46.5 ^ 3.05E+000 44.235 Pb-212 74.8 7.77E-001 37.346 3.666[51.447] 4.18 -0.766 77.1 2.95E-001 44.320 1.390[56.712] [ 0.549]

238.6 ^ 2.12E-001 35.385 1.000[50.041]

PB-214 74.8 1.38E+000 38.403 7.919[63.932] 6.22 -1.062 77.1 5.20E-001 45.225 2.987[68.248] [ 0.561]

351.9 ^ 1.74E-001 51.112 1.000[72.284]

Ra-226 186.2 ^ 1.45E+000 46.888

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