ML070120546

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Final Status Survey Final Report Phase III, Rev 1, Appendix A4 Survey Unit Release Record 9527-0003, East Mountain Side
ML070120546
Person / Time
Site: Haddam Neck File:Connecticut Yankee Atomic Power Co icon.png
Issue date: 09/18/2006
From:
Yankee Atomic Electric Co
To:
NRC/FSME
References
9527-0003, CY-06-128
Download: ML070120546 (138)


Text

EAST MOUNTAIN SIDE SURVEY UNIT 9527-0003 RELEASE RECORD Revision 1 TABLE OF CONTENTS

1. SURVEY UNIT DESCRIPTION...........................................................3 2. CLASSIFICATI ON BASIS....................................................................3 3. DATA QUALITY OB JECTIVES (DQO)..............................................5 4. SURVEY DESIGN.................................................................................8 5. SURVEY IMP LEMENTATION..........................................................11 6. SURVEY RESULTS............................................................................12 7. QUALITY CONTROL.........................................................................16 8. INVESTIGATIONS AND RESULTS.................................................17 9. REMEDIATION AND RESULTS.......................................................17 10. CHANGES FROM THE FINAL STATUS SURVEY PLAN.............17 11. DATA QUALITY ASSESSMENT (DQA)..........................................18 12. ANOMALIES.......................................................................................18 13. CONCLUSION.....................................................................................18 14. ATTACHMENTS.................................................................................19 14.1 Attachment 1 - Figures (7 pages including cover) 14.2 Attachment 2 - Sample and Sta tistical Data (111 pages including covers)

EAST MOUNTAIN SIDE SURVEY UNIT 9527-0003 RELEASE RECORD Revision 1 3 1. SURVEY UNIT DESCRIPTION Survey Unit 9527-0003 (East Mountain Side) is designated as Final Status Survey (FSS) Class 2 and consists of 8,200 m 2 (2.03 acres) of uninhabited open land located approximately 0.16 miles from the reference coordinate system benchmark used at Haddam Neck Plant (HNP) (see Attachment 1, Figure 1). The survey unit is bounded by an unpaved road on the north (called north as oriented with the north to south flow of the Connecticut River) side, a fence to the east and south, and a partial fence to the west. The survey unit comprises wooded terrain with some steep rock ledge and rock outcroppings within the interior. The soil of this survey unit meets the requirements for unrestricted release as a Class 2 survey unit under the criteria and requirements of the HNP License Termination Plan (LTP). The reference coordinates associated with this survey uni t are E014 through E022 by S067 through S076 (refer to License Termination Plan (LTP) Section 5.4.4). The reference coordinates provide the maximum dimensions of a rectangle containing this survey unit. Some areas contained in this rectangle may not be part of this survey unit. The boundary of the survey unit was defined using a Global Positioning System (GPS).

2. CLASSIFICATION BASIS The survey unit was classified in accordance with Procedure RPM 5.1-10, "Survey Unit Classification." The historical information, scoping analyses and characterization results provided sufficient data to designate Survey Unit 9527-0003 as Class 2 in September 2005.

The "Classification Basis Summary" conducted for Survey Unit 9527-0003 consisted of:

a) A review of the 10CFR50.75 (g) (1) database, b) A review of the "Initial Characterization Report" and the "Historic Site Assessment (HSA) Supplement,"

c) Historic and current survey records review, d) Visual inspections and a "walkdown."

A review of the 10CFR50.75 (g) (1) database report identifies six (6) documents associated with or relating to this survey area.

a) Event PIR 80-37: Contamination was documented to be present in an area outside the restricted area. Small areas of low-level contamination were found on the facility grounds through routine survey in a normally non-radioactive area. The ar eas were cleaned up in 1980.

EAST MOUNTAIN SIDE SURVEY UNIT 9527-0003 RELEASE RECORD Revision 1 4 b) Radiological Assessment Branch (RAB) memo NE-83-RA-1374 (September 1983): Results of a contamination survey outside the southeast RCA boundary has identified plant related activity in an adjacent survey area to 9527. According to the memo the source could have been the events described by PIR 80-37.

c) Adverse Condition Report ACR 97-0994: Soil sample analysis identified plant related radioactivity on hillside east of plant (in another survey unit of 9527).

d) Scoping Survey Report 1998: Results of scoping samples performed for decommissioning characterization data. Cesium-137 was the predominate radionuclide found in this survey unit during the scoping survey. No other plant-related radionuclides were identified in this survey unit.

e) Event CR 05-0244: Tank farm material with low-level fixed contamination was found on the East Mountain Side in another survey unit of 9527. The single piece of tent material was found in Survey Unit 9527-0005 along the fence and about five hundred fifty (550) feet from

the nearest boundary of 9527-0003.

f) Memo ISC 05-045: Periodic surveillance following final status survey. Surveillance is required periodically by the LTP to ensure the radiological condition does not significantly change from the FSS results. The memo documents no negative change in the radiological status. A review of the "Initial and Supplemental C haracterization Reports" as well as the previous "Classification Basis Summaries" provided no additional information pertinent to classification. Characterization was performed by Site Closure personnel in April 2005 to determine existing conditions and obtain radiological data for Final Status Survey (FSS). The reported concentrations of Cs-137 found in the soil were statistically consistent with those concentrations in wooded areas determined from off-site locations as documented by Health Physics Technical Support Document (TSD) BCY-HP-0063, "

Background Cs-137 Concentration in Soil." The average concentration was 0.653 pCi/g which was slightly lower than expected; however, one (1) sample reported Cs-137 at a concentration of 1.18 pCi/g. The basic statistical quantities (i.e., mean, standard deviation, median) for Cs-137 and Co-60 are provided in Table 1.

EAST MOUNTAIN SIDE SURVEY UNIT 9527-0003 RELEASE RECORD Revision 1 5 Table 1 - Basic Statistical Quantities for Cs-137 and Co-60 from the Characterization Survey Parameter Cs-137 (pCi/g)

Co-60 (pCi/g) Minimum Value: 3.11E-01 -6.84E-03 Maximum Value: 1.18E+00 1.29E-01 Mean: 6.53E-01 2.17E-02 Median: 6.46E-01 1.28E-02 Standard Deviation: 2.52E-01 3.29E-02 The FSS Engineer performed a visual inspection and walkdown during September 2005 to assess the physical condition of the survey unit, evaluate access points and travel paths and identify potentially hazardous conditions.

The final designation was Class 2 based on historical information (HSA Supplement and LTP Table 2.10 and 2.11B) and characterization survey data which resulted in the expectation that no FSS sample would be reported in a concentration that that would exceed the LTP criteria.

3. DATA QUALITY OBJECTIVES (DQO) FSS design and planning used the Data Quality Objective (DQO) process as described by the LTP, Procedure RPM 5.1-11, "Preparation of Final Status Survey Plan," and the "Multi-Agency Radiation Survey and Site Investigation Manual" (MARSSIM). A summary of the main features of the DQO process are provided herein. The DQO process incorporated hypothesis testing and probabilistic sampling distributions to control decision errors during data analysis. Hypothesis testing is a process based on the scientific method that compares a baseline condition to an alternate condition. The baseline condition is technically known as the null hypothesis. Hypothesis testing rests on the premise that the null hypothesis is true and that sufficient evidence must be provided for rejection. In designing the survey plan, the underlying assumption, or null hypothesis was that residual activity in the survey unit exceeded the release criteria. Rejection of the null hypothesis would satisfy the release criteria objective of the FSS. Probabilistic sampling is a preferred method to select a sample so that each item in the population being studied has a known likelihood of being included in the sample. Probabilistic sampling might include simple random sampling where every sample has the same chance of being included, or systematic random sampling where samples are arranged in some order and a random starting point is selected. The primary objective of the Final Status Survey Plan (FSSP) was to demonstrate that the level of residual radioactivity in Survey Unit 9527-0003 did not exceed the release criteria specified in the LTP and that the potential dose from residual radioactivity is As Low As Reasonably Achievable (ALARA).

EAST MOUNTAIN SIDE SURVEY UNIT 9527-0003 RELEASE RECORD Revision 1 6 A fundamental precursor to survey design is to establish a relationship between the release criteria and some measurable quantity. This is done through the development of Derived Concentration Guideline Values (DCGLs). The DCGLs represent average levels of radioactivity above background levels and are presented in terms of surface or mass activity concentrations. Chapter 6 of the LTP describes in detail the modeling used to develop the DCGLs for soil (called Base Case Soil DCGL), existing groundwater radioactivity and additional future groundwater radioactivity from building basements and footings. The DCGLs presented in Chapter 6 of the LTP were developed for exposures from three (3) components, that is, residual radioactivity in soil, existing groundwater radioactivity, and future groundwater radioactivity from the burial of concrete foundations or footings from site buildings containing residual radioactivity. Equation 1 shows the mathematical relationship between the three (3) com ponents and the total dose.

Equation 1:

H Total=H Soil + H Existing GW

+ HFuture GW The total dose under the LTP criteria is 25 mrem/yr TEDE from all three components. The allowable total dose under the Connecticut Department of Environmental Protection (CTDEP) radiological remediation standard for Connecticut Yankee (CY) is 19 mrem/yr TEDE. To satisfy both the LTP and CY CTDEP criteria, the dose from soil must be reduced when using the existing and future groundwater dose values discussed above. This survey unit is affected by existing groundwater (reference CY memo ISC 06-024 and the Final Status Survey Final Report Phase III). The dose contribution from existing groundwater is bounded at 2 mrem/yr TEDE based on field data. This survey unit is not considered impacted by future groundwater radioactive contamination, as there are no concrete foundations or footings containing residual radioactive material within the groundwater saturated zone in the area (reference CY memo ISC 06-024). The dose contribution from future groundwater, the third dose component, is therefore 0 mrem/yr TEDE.

Equation 2:

19 mrem/yr Total=17 mrem/yr Soil+2 mrem/yrExisting GW+0 mrem/yr Future GW The allowable dose for soil in this survey unit is 17 mrem/yr TEDE as shown by Equation 2 above. The concentration of residual radioac tivity resulting in 17 mrem/yr TEDE is designated as th e Operational DCGL, and has been established for the radionuclides of concern as provided in Table 2. Note, the EAST MOUNTAIN SIDE SURVEY UNIT 9527-0003 RELEASE RECORD Revision 1 7 survey design used a much smaller value for investigation than the Operational DCGL provided by Table 2 to conservatively account for the contribution to the total dose from existing and future groundwater which had not been established at the time of planning the FSS.

Table 2 - Radionuclide Specific Base Case Soil DCGL, Operational DCGLs and Required Minimum Detectable Concentrations Radionuclide (1) Base Case Soil DCGL (pCi/g) (2) Operational DCGL (pCi/g) (3) Required MDC (pCi/g) (4) H-3 4.12E+02 2.80E+02 1.65E+01 C-14 5.66E+00 3.85E+00 2.26E-01 Mn-54 1.74E+01 1.18E+01 6.96E-01 Fe-55 2.74E+04 1.86E+04 1.10E+03 Co-60 3.81E+00 2.59E+00 1.52E-01 Ag-108m 7.14E+00 4.86E+00 2.86E-01 Ni-63 7.23E+02 4.92E+02 2.89E+01 Sr-90 1.55E+00 1.05E+00 6.20E-02 Nb-94 7.12E+00 4.84E+00 2.85E-01 Tc-99 1.26E+01 8.57E+00 5.04E-01 Cs-134 4.67E+00 3.18E+00 1.87E-01 Cs-137 7.91E+00 5.38E+00 3.16E-01 Eu-152 1.01E+01 6.87E+00 4.04E-01 Eu-154 9.29E+00 6.32E+00 3.72E-01 Eu-155 3.92E+02 2.67E+02 1.57E+01 Pu-238 2.96E+01 2.01E+01 1.18E+00 Pu-239/240 2.67E+01 1.82E+01 1.07E+00 Pu-241 8.70E+02 5.92E+02 3.48E+01 Am-241 (5) 2.58E+01 1.75E+01 1.03E+00 Cm-243/244 2.90E+01 1.97E+01 1.16E+00 (1) Bold indicates those radionuclides considered to be Hard to Detect (HTD) (2) The Base Case Soil DCGLs for soil are specified by the LTP in Chapter 6 and are equivalent to 25 mrem/yr TEDE (3) The Operational DCGL is equivalent to 17 mrem/yr TEDE (4) The required MDC is equivalent to 1 mrem/yr TEDE (5) Americium-241 can be analyzed by gamma and alpha spectroscopy and is considered to be Easy to Detect (ETD). The preferred result is the alpha spectroscopy's when both analyses are performed. Another important facet of the DQO process is to identify the radionuclides of concern and determine the concentration variability. Characterization was performed in April 2005 as discussed in Section 2. Cesium-137 was found to be the predominate radionuclide of concern. Cobalt-60 was included in the EAST MOUNTAIN SIDE SURVEY UNIT 9527-0003 RELEASE RECORD Revision 1 8 survey design based on the 1997 scoping survey results. The basic statistical quantities (i.e., mean, standard deviation, median) for Cs-137 and Co-60 are provided in Table 1. Instrument DQOs included a verification of the ability of the survey instrument to detect the radiation(s) of interest relative to the DCGL. Survey instrument response checks were to be performed before issue and after the instrument had been used. Control and accountability of survey instruments was to be maintained to assure the quality and prevent the loss of data. Laboratory DQOs and analysis results were to be reported as actual calculated results. Results reported as less than Minimum Detectable Concentration (<MDC) would not be accepted for FSS. Sample report summaries were to include unique sample identification, analytical method, radionuclide, result, and uncertainty of two standard deviations, laboratory data qualifiers, units, and the required and observed MDC.

4. SURVEY DESIGN The level of effort associated with planning a survey is based on the complexity of the survey and nature of the hazards. To assist the FSS Engineers when preparing survey plans for FSS, guidance is provided in Procedure RPM 5.1-11, "Preparation of Final Status Survey Plans". By design, the FSSP meets the ALARA criteria for soils as specified in Chapter 4 of the LTP. The FSSP uses an integrated sample design that combines scanning surveys and sampling which can be either random or biased. Characterization was performed by Site Closure personnel in April 2005 to determine existing conditions and obtain radiological data for Final Status Survey (FSS). The DQO process determined that Cs-137 and Co-60 would be the radionuclides of concern (refer to Section 3). The sum of fractions or unity rule would be used with the individual Operational DCGLs because multiple radionuclides (Cs-137 and Co-60) were considered in the survey design. Other radionuclides identified during FSS would be evaluated to ensure adequate survey design and compliance with the unity rule. Surrogate DCGLs were not required for this survey unit based on process knowledge from FSS of nearby adjacent areas and via screening under LTP Section 5.4.7.2, "Gross Activity DCGLs". Radionuclide screening or de-selection is a process where an individual radionuclide or aggregate may be considered insignificant and eliminated from the FSS. The criteria for de-

selection are concentrations less than 5% for individual radionuclides and less than 10% for aggregates. The Elevated Measurement Comparison (EMC) did not apply to this survey unit since the survey unit is a Class 2 and discrete, elevated areas of contamination were not expected.

EAST MOUNTAIN SIDE SURVEY UNIT 9527-0003 RELEASE RECORD Revision 1 9 The Sign Test was selected as the non-parametric statistical test. The use of the Sign Test did not require the selection or use of a background reference area, which simplified survey design and implementation. This approach was

conservative since it included background Cs-137 as part of the sample set. The number of soil samples for FSS was determined in accordance with Procedure RPM 5.1-12, "Determination of the Number of Surface Samples for Final Status Survey." The Lower Bound of the Gray Region (LBGR) was set in accordance with Procedure RPM 5.1-11 to 0.79 to maintain the relative shift

(/) in the range of 1 and 3. A Prospective Power Curve was generated using COMPASS, a software package developed under the sponsorship of the United States Nuclear Regulatory Commission (USNRC) for implementation of the MARSSIM in support of the decommissioning license termination rule (10 CFR 20, Subpart E). The result of the COMPASS computer run showed adequate power for the survey design. Survey design specified fifteen (15) surface soil samples for non-parametric statistical testing. The grid pattern and locations of the soil samples were determined using Visual Sample Plan (VSP) in accordance with Procedure RPM 5.1-14 , "Identifying, and Marking Surface Sample Locations for Final Status Survey." Visual Sample Plan was created by Pacific Northwest National Laboratory (PNNL) for the United States Department of Energy. A systematic triangular grid pattern with a random starting point was selected for sample design, which is appropriate for a Class 2 area. Sample locations were identified using AutoCAD-Lt, a commercially available plotting software package with coordinates consistent with the Connecticut State Plane System. These coordinates were integrated with a GPS to locate sample locations in the field. Sample Measurement Locations for the design are listed with the GPS coordinates in Table 3. Table 3 -Sample Measurement Locations with Associated GPS Coordinates Designation Northing Easting 9527-0003-001F 237066.59 669086.55 9527-0003-002F 236929.20 669086.55 9527-0003-003F 236860.50 669046.89 9527-0003-004F 236860.50 669126.21 9527-0003-005F 236791.81 669007.23 9527-0003-006F 236791.81 669086.55 9527-0003-007F 236791.81 669165.88 9527-0003-008F 236723.11 669126.21 9527-0003-009F 236723.11 669205.54 9527-0003-010F 236723.11 669284.86 9527-0003-011F 236654.41 669165.88 9527-0003-012F 236654.41 669245.20 9527-0003-013F 236654.41 669324.52 9527-0003-014F 236585.72 669284.86 9527-0003-015F 236585.72 669364.19 EAST MOUNTAIN SIDE SURVEY UNIT 9527-0003 RELEASE RECORD Revision 1 10 A minimum of two (2) judgmental or biased samples were to be collected at locations selected by FSS Supervisi on based on professional judgment and observation during characterization and walkdowns to determine areas having the potential for residual radioactivity (e.g., runoff and collection, area disturbance). The number of judgmental samples represented 13% percent of the number of samples that would be used for non-parametric statistical testing.

Although Procedure RPM 5.1-11 only specified that 5% of the samples be selected for HTD analysis, three (3) soil samples or 20% of the number of samples that would be used for non-parametric statistical testing were randomly selected for HTD radionuclide analysis using the Microsoft Excel "RANDBETWEEN" function. Each sample would be sent off-site for a full suite analysis of the HTD radionuclides specified in the LTP, Table 2-12, "Radionuclides Potentially Present at Haddam Neck Plant." The implementation of survey specific quality control measures as referenced by Procedure RPM 5.1-24, "Split Sample Assessment for Final Status Survey," included the collection of two (2) soil samples for "split sample" analysis by the off-site laboratory. These locations were selected randomly using the Microsoft Excel "RANDBETWEEN" function. The number of quality control soil samples was determined to be 10% of fifteen (15) samples, rounded up to the next whole number. The LTP specifies that scanning will be performed in a combination of systematic and judgmental measurements for a Class 2 land area and cover 10% to 100% of the area. The fraction of scanning coverage was determined during the DQO process with the total amount and location(s) based on the likelihood of finding elevated activity during FSS. Approximately 25% of the survey unit was to be scanned based on the characterization survey and sampling results. For this Class 2 survey unit, the "Investigation Level" for area scanning and soil sample measurement results are those levels specified in LTP, Table 5-8, "Investigation Levels." Note, the survey design used a much smaller value for investigation than the Operational DCGL provided by Table 2 to conservatively account for the contribution to the total dose from existing and future groundwater which had not been established at the time of planning the FSS.

EAST MOUNTAIN SIDE SURVEY UNIT 9527-0003 RELEASE RECORD Revision 1 11 Table 4 - Synopsis of the Survey Design (1) Feature Design Criteria Basis Survey Unit Land Area 8,200 m 2 Based on AutoCAD-Lt and Visual Sample Plan calculationsNumber of Measurements 15 Type 1 and Type 2 errors were 0.05, sigma was 0.103 pCi/g, the LBGR was adjusted to 0.79 to maintain Relative Shift in the range of 1 and 3, Relative Shift was 2 Grid Spacing 25.1 Based on triangular grid Interval Spacing 21.7 Based on triangular grid Design DCGL 2.53 pCi/g Cs-137 1.52 pCi/g Co-60 To achieve 8 mrem/yr TEDE Operational DCGL 5.38 pCi/g Cs-137 2.59 pCi/g Co-60 To achieve 17 mrem/yr TEDE (2) to demonstrate compliance with Equation 2 of this Release Record Scan Survey unit Coverage Approximately 25%

of the area The LTP requires >10% area coverage for Class 2 Survey Units Soil Investigation Level 2.53 pCi/g Cs-137 1.52 pCi/g Co-60 The Operational DCGL meets the LTP criteria for a Class 2 survey unit Scan Investigation Level Detectable over background The LTP specifies investigation at the MDC SCAN for a Class 2 survey unit when the MDC SCAN is greater than the Operational DCGL (1) The survey design used a much smaller value for investigation than the Operational DCGL provided by Table 2 as the total dose from existing and future groundwater had not been established at the time of planning the FSS (2) The allowable dose for soil in this survey unit is 17 mrem/yr TEDE as the bounding dose from existing and future groundwater has been established based on field data (reference CY memo ISC 06-024 and the Final Status Survey Final Report Phase III)

5. SURVEY IMPLEMENTATION Final status survey field activities were conducted under Work Plan and Inspection Record (WP&IR) 2005-0054. The WP&IR package included a detailed FSSP, job safety analysis, job planning checklist and related procedures for reference. Daily briefings were conducted to discuss the expectations for job performance and the safety aspects of the survey. The "Daily Survey Journal" was used to document field activities and other information pertaining to the FSS.

Survey activities occurred September 1 through September 9, 2005. The scan areas were marked out and scanned for elevated readings (see Attachment 2 for Scan Area Results). Scanning was performed with an EAST MOUNTAIN SIDE SURVEY UNIT 9527-0003 RELEASE RECORD Revision 1 12 Eberline E-600 using a SPA-3 sodium iodide detector. The E-600 was operated in the rate-meter mode and used with audio response. The probe was positioned as close to the ground as possible and was moved at a scan speed of about 0.5 meters per second. Using GPS coordinates, sample measurement locations were identified and marked with a surveyor's flag for identification. At each sample measurement location, a one (1) meter radius around the sample flag was scanned for elevated

radiation levels. Fifteen (15) surface soil samples were collected and packaged in accordance with Haddam Neck Plant (HNP) Procedure RPM 5.1-3, "Collection of Sample Media for Final Status Survey" and FSS design. Samples were controlled, transported, stored, and transferred to the off-site laboratory using Chain-of-Custody (COC) protocol in accordance with Procedure RPM 5.1-5, "Chain of Custody for Final Status Survey Samples."

Three (3) samples (9527-0003-003F, 9527-0003-007F and 9527-0003-010F) were randomly selected for HTD radionuclide analysis by the off-site laboratory. Two (2) biased soil samples (9527-0003-016F and 9527-003-017F) were taken. These samples were analyzed using gamma spectroscopy by the off-site laboratory. The implementation of survey specific quality control measures included the collection of two (2) samples (9527-0003-008F and 9527-0000-011F) for "split sample" analysis by the off-site laboratory.

6. SURVEY RESULTS The seventeen (17) sample measurement locations identified in the FSS plan were scanned about a one (1) meter radius for elevated radiation levels. Table 5 provides an overview of the scan area survey. Scan area results are provided in Attachment 2.

Table 5- Scan Area Results for Sample Measurement Locations Sample Measurement Location Highest Logged Reading (kcpm) Action Level (1) (kcpm) > Action Level (2) 1 13.3 14.4 No 2 16.3 17.6 No 3 20.2 20.3 No 4 21.0 25.5 No 5 28.5 38.7 No 6 41.5 44.7 No 7 19.8 22.0 No 8 38.4 44.4 No

EAST MOUNTAIN SIDE SURVEY UNIT 9527-0003 RELEASE RECORD Revision 1 13 Table 5- Scan Area Results for Sample Measurement Locations Sample Measurement Location Highest Logged Reading (kcpm) Action Level (1) (kcpm) > Action Level (2) 9 18.7 20.4 No 10 19.1 22.4 No 11 36.0 40.8 No 12 18.6 22.3 No 13 18.2 21.7 No 14 17.6 21.1 No 15 16.7 18.8 No 16 33.3 42.1 No 17 27.5 30.1 No (1) The action level is based on a measurement above ambient background (2) Samples are collected from the location within the boundaries of the scan yielding a response above the action level Twenty-two (22) areas were scanned for elevated radiation levels. Several elevated areas were identified. Table 6 provides an overview of the scan area survey. Scan area results ar e provided in Attachment 2. Table 6- Scan Area Results Scan Area Highest Logged Reading (kcpm) Action Level (1) (kcpm) Elevated Reading Identification (2) Investigation Sample 1 16.2 18.0 None - no elevated areas identified None 2 17.3 18.0 None - no elevated areas identified None 3 19.0 20.0 None - no elevated areas identified None 4 20.5 23.0 None - no elevated areas identified None 5 20.5 23.7 None - no elevated areas identified None 6 19.8 29.5 None - no elevated areas identified None EAST MOUNTAIN SIDE SURVEY UNIT 9527-0003 RELEASE RECORD Revision 1 14 Table 6- Scan Area Results Scan Area Highest Logged Reading (kcpm) Action Level (1) (kcpm) Elevated Reading Identification (2) Investigation Sample 7 23.5 25.3 None - no elevated areas identified None 8 21.6 30.3 None - no elevated areas identified None 9 38.0 41.3 None - no elevated areas identified None 10 54.1 54.7 ER-02-15-1 9527-0003-018F 11 21.3 21.7 None - no elevated areas identified None 12 19.5 21.0 None - no elevated areas identified None 13 19.0 21.5 None - no elevated areas identified None 14 20.4 20.5 None - no elevated areas identified None 15 19.2 28.3 None - no elevated areas identified None 16 18.2 20.2 None - no elevated areas identified None 17 15.8 16.7 SC-03-10-0 None (3) 18 16.5 18.3 None - no elevated areas identified None 19 18.1 20.0 None - no elevated areas identified None 20 20.1 26.2 None - no elevated areas identified None EAST MOUNTAIN SIDE SURVEY UNIT 9527-0003 RELEASE RECORD Revision 1 15 Table 6- Scan Area Results Scan Area Highest Logged Reading (kcpm) Action Level (1) (kcpm) Elevated Reading Identification (2) Investigation Sample 21 21.1 31.6 None - no elevated areas identified None 22 35.5 42.5 None - no elevated areas identified None (1) The action level is based on a measurement above ambient background (2) ER and SC are abbreviations associated with the barcodes used in the field where ER stands for Elevated Reading and SC refers to Scan (3) Refer to Section 8 for additional detail The off-site laboratory employed for the radiological analyses of samples was General Engineering Laboratories, LLC, Charleston, South Carolina. The laboratory analyzed the fifteen (15) samples taken for non-parametric statistical testing, the associated duplicates, and the biased samples using gamma spectroscopy. Gamma spectroscopy analysis was performed to the required MDC. Gamma spectroscopy results identified radionuclides other than Cs-137 and Co-60 meeting the accepted criteria for detection (i.e., a result greater than two standard deviations uncertainty). All could be de-selected or excluded using the 5% and 10% rule described in Section 4. Cesium-137 was identified in all of the fifteen (15) samples. The average gamma spectroscopy results for Cs-137 were slightly higher than the concentrations of Cs-137 found in soil at off-site locations within the vicinity of the HNP as presented in the Health Physics TSD BCY-HP-0063.

None of the samples exceeded 37% of the Operational DCGL. Sample analysis did not require further investigation. A summary of the sample results is provided in Table 7.

Table 7- Summary of Soil Sample Results Sample Number Cs-137 pCi/g Co-60 pCi/g Fraction of the Operational DCGL (1) 9527-0003-001F 6.09E-01 1.55E-02 0.119 9527-0003-002F 5.75E-01 7.25E-03 0.110 9527-0003-003F 8.41E-01 3.86E-02 0.171 9527-0003-004F 1.83E+00 6.03E-02 0.363 9527-0003-005F 3.61E-01 2.23E-02 0.076 9527-0003-006F 5.09E-01 2.26E-03 0.095 9527-0003-007F 6.35E-01 1.53E-02 0.124 9527-0003-008F 1.62E+00 4.03E-02 0.317 9527-0003-009F 8.04E-01 0.00E+00 0.149 EAST MOUNTAIN SIDE SURVEY UNIT 9527-0003 RELEASE RECORD Revision 1 16 Table 7- Summary of Soil Sample Results Sample Number Cs-137 pCi/g Co-60 pCi/g Fraction of the Operational DCGL (1) 9527-0003-010F 1.28E+00 2.73E-02 0.248 9527-0003-011F 1.21E+00 4.53E-02 0.242 9527-0003-012F 9.49E-01 3.90E-02 0.191 9527-0003-013F 1.69E+00 5.26E-02 0.334 9527-0003-014F 9.92E-01 2.94E-02 0.196 9527-0003-015F 5.50E-01 3.11E-02 0.114 (1) The Operational DCGLs from Table 2 are 5.38 pCi/g for Cs-137 and 2.59 pCi/g for Co-60 and are used in conjunction with the unity rule to achieve 17 mrem/yr TEDE The off-site laboratory also processed three (3) samples for HTD analysis as required by the sample plan. The requested analyses included alpha spectroscopy, gas proportional counting, a nd liquid scintillation depending on the radionuclide and the measurement method. All analyses met the required MDC. Table 8 lists the results for those radionuclides meeting the accepted criteria for detection (i.e., a result greater than two standard deviations uncertainty) in more than one sample. Table 8 lists the results for the HTD radionuclides that could not be de-selected based on either the 5% and 10%

rules. Table 8-Hard-to-Detect Sample Results Sample Sr-90 (pCi/g) C-14 (pCi/g) Tc-99 (pCi/g) Fraction of the Operational DCGL (1) 9527-0003-003F 3.82E-03 1.25E-01 3.96E-01 8.23E-02 9527-0003-007F 1.60E-02 -4.21E-02 2.01E-01 2.78E-02 9527-0003-010F 2.42E-02 1.09E-01 6.04E-01 1.22E-01 (1) The Operational DCGLs are 1.05 pCi/g for Sr-90, 3.85 pCi/g for C-14 and 8.57 pCi/g for Tc-99 used in conjunction with the unity rule Two (2) biased samples were collected at locations selected by FSS Supervision based on professional judgment and observation. Gamma spectroscopy analysis was performed by the off-site laboratory to the required MDC. None of the samples exceeded 24% of the Operational DCGL. No further action or

investigations were re quired (see Table 9).

Table 9- Biased Sample Results Sample Number Cs-137 pCi/g Co-60 pCi/g Fraction of the Operational DCGL (1) 9527-0003-016F 1.12E+00 8.85E-02 0.242 9527-0003-017F 1.21E+00 2.31E-03 0.226 (1) The Operational DCGLs from Table 2 are 5.38 pCi/g for Cs-137 and 2.59 pCi/g for Co-60 and are used in conjunction with the unity rule to achieve 17 mrem/yr TEDE EAST MOUNTAIN SIDE SURVEY UNIT 9527-0003 RELEASE RECORD Revision 1 17 7. QUALITY CONTROL The off-site laboratory processed the split samples and performed gamma spectroscopy analysis. Thirteen percent (13%) of the samples were selected for analysis, which exceeds the 5% minimum required by the LTP. The data were evaluated using USNRC acceptance criteria specified in Inspection Procedure 84750 as detailed in HNP Procedure RPM 5.1-24, "Split Sample Assessment for Final Status Survey." There was acceptable agreement between field split results. The sample analysis vendor, General Engineering Laboratories, LLC, Charleston, South Carolina, maintains quality control and quality assurance plans as part of normal operation. Refer to Attachment 2 for data and data quality analysis results.

8. INVESTIGATIONS AND RESULTS One (1) localized area was found to verifiably exceed the investigation level during the scan area survey. A sample was collected from that location and was analyzed on-site using gamma spectroscopy. The analysis results for Cs-137

and C-60 are shown in Table 10. Table 10- Confirmatory Sample Results Sample Number Cs-137 pCi/g Co-60 pCi/g Fraction of the Operational DCGL (1) 9527-0003-18F 9.91E-01 7.84E-02 0.214 (1) The Operational DCGLs from Table 2 are 5.38 pCi/g for Cs-137 and 2.59 pCi/g for Co-60 and are used in conjunction with the unity rule to achieve 17 mrem/yr TEDE Additional scanning was performed in one (1) small location in February 2006 to obtain additional data relevant to the DQOs. The scanning was performed over an area of about six hundred square feet (600 ft 2). No elevated readings were identified.

9. REMEDIATION AND RESULTS Historically, no remedial action as described by MARSSIM Section 5.4 was performed in this survey unit prior to or as a result of the FSS. Health Physics TSD BCY-HP-0078, "ALARA Evaluation of Soil Remediation in Support of Final Status Survey," determined that remediation beyond that required to meet the release criteria to be unnecessary and that the remaining residual radioactivity in soil was ALARA.
10. CHANGES FROM THE FINAL STATUS SURVEY PLAN The survey was designed to 8 mrem/yr TEDE which was conservative and necessary at the time of FSS planning. It is no longer required as the total dose from existing and future groundwater has been established. The dose for soil used to demonstrate compliance with the LTP criteria is 17 mrem/yr TEDE as

discussed in Section 2 of this Release Record.

EAST MOUNTAIN SIDE SURVEY UNIT 9527-0003 RELEASE RECORD Revision 1 18 Three HTD radionuclides were reported in concentrations exceeding either the 5% and 10% rule for de-selection. Therefore, the individual Operational DCGLs for these radionuclides were included into sample design to demonstrate compliance with the unity rule and ensure adequate survey design in accordance with the DQOs. The result of the COMPASS computer run showed adequate power for the revised survey design. The revised survey design maintained the original fifteen (15) surface soil samples for non-parametric statistical testing.

11. DATA QUALITY ASSESSMENT (DQA) The DQO sample design and data were reviewed in accordance with Procedure RPM 5.1-23, "Data Quality Assessment," for completeness and consistency. The sampling design had adequate power as indicated by the Retrospective Power Curve. The Sign Test was performed on the data and compared to the original assumptions of the DQOs. The Sign Test shows that the survey unit passes FSS. Documentation was complete and legible. Surveys and sample collection were consistent with the DQOs and were sufficient to ensure that the survey unit was properly designated as Class 2. The preliminary data review consisted of calculating basic statistical quantities (e.g., mean, median, standard deviation). The range of the data, about 2.9 standard deviations, was not unusually large. The difference between the mean and median was 14% of the standard deviation. The difference is enough to indicate skewness in the data. The data was represented graphically through posting plots, a frequency plot, and a quantile plot. The frequency plot shows slight positive skewness as confirmed by the calculated skew of 0.5 and some bimodality probably due to the

differences in terrain and the collection of runoff. All data, assessments, and graphical representations are provided in Attachment

2. 12. ANOMALIES No anomalies were noted.
13. CONCLUSION Survey Unit 9527-0003 has met the final DQOs of the FSS. The ALARA criteria for soils as specified in Chapter 4 of the LTP were achieved. Elevated Measurement Comparison and reme diation was not required. The sample data passed the Sign Test. The null hypothesis was rejected. Graphical representation of data indicates significant positive skewness as that is probably due to the differences in terrain and the collection of runoff. The EAST MOUNTAIN SIDE SURVEY UNIT 9527-0003 RELEASE RECORD Revision 1 19 Retrospective Power Curve generated using COMPASS shows adequate power was achieved. The survey unit wa s properly designated as Class 2. The dose contribution from soil is less than 3 mrem/yr TEDE based on the average concentration of the samples used for non-parametric statistical sampling. This survey unit is affected by existing groundwater (reference CY memo ISC 06-024 and the Final Status Survey Final Report Phase III). The dose contribution from existing groundwater is bounded at 2 mrem/yr TEDE based on field data. This survey unit is not considered impacted by future groundwater radioactive contamination, as there are no concrete foundations or footings containing residual radioactive material within the groundwater saturated zone in the area (reference CY memo ISC 06-024). The dose contribution from future groundwater, the third dose component, is therefore 0 mrem/yr TEDE.
14. ATTACHMENTS 14.1 Attachment 1 - Figures 14.2 Attachment 2 - Sample and Statistical Data EAST MOUNTAIN SIDESURVEY UNIT 9527-0003RELEASE RECORDAttachment 1Figures(6 pages)

Feet02754 Feet02754 Feet02754 Feet02754 Feet02754 EAST MOUNTAIN SIDESURVEY UNIT 9527-0003RELEASE RECORDAttachment 2Sample and Statistical Data EAST MOUNTAIN SIDESURVEY UNIT 9527-0003RELEASE RECORDAttachment 2aSample Data(81 Pages)

TABLE OF CONTENTS General Narrative

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1 Chain of Custody

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4 Cooler Receipt Checklist

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8 Radiological Analysis

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11 Sample Data Summary

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25 Quality Control Data

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68 Page 1 of 77 Page 2 of 77 Page 3 of 77 Page 4 of 77 Page 5 of 77 Page 6 of 77 Page 7 of 77 Page 8 of 77 Page 9 of 77 Page 10 of 77 RADIOLOGICAL ANALYSIS Page 11 of 77 Radiochemistry Case NarrativeConnecticut Yankee Atomic Power Co. (YANK)SDG MSR#05-2244 Method/Analysis InformationProduct:Alphaspec Am241, Cm, Solid ALL FSSAnalytical Method:DOE EML HASL-300, Am-05-RC ModifiedPrep Method:Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method:Dry Soil PrepAnalytical Batch Number:467822Prep Batch Number:463017Dry Soil Prep GL-RAD-A-021 Batch Number:463013Sample IDClient ID145417017 9527-0003-003-F145417018 9527-0003-007-F 145417019 9527-0003-010-F1200948302 Method Blank (MB)1200948303 145417017(9527-0003-003-F) Sample Duplicate (DUP) 1200948304 145417017(9527-0003-003-F) Matrix Spike (MS)1200948305 Laboratory Control Sample (LCS)SOP ReferenceProcedure for preparation, analysis and reporting of analytical data are controlled by General EngineeringLaboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed inaccordance with GL-RAD-A-011 REV# 14.Calibration Information:Calibration Information All initial and continuing calibration requirements have been met.Standards InformationStandard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample GeometryAll counting sources were prepared in the same geometry as the calibration standards.Quality Control (QC) Information:Blank InformationThe blank volume is representative of the sample volume in this batch.Designated QCThe following sample was used for QC: 145417017 (9527-0003-003-F).QC InformationAll of the QC samples met the required acceptance limits.

Technical Information:

Holding TimeAll sample procedures for this sample set were performed within the required holding time.Preparation Information Page 12 of 77 All preparation criteria have been met for these analyses.Sample Re-prep/Re-analysisNone of the samples in this sample set required reprep or reanalysis.Miscellaneous Information:

NCR DocumentationNonconformance reports are generated to document any procedural anomalies that may deviate from referencedSOP or contractual documents. An NCR was not generated for this SDG.Manual IntegrationNo manual integrations were performed on data in this batch.

Qualifier informationManual qualifiers were not required.

Method/Analysis InformationProduct:Alphaspec Pu, Solid-ALL FSSAnalytical Method:DOE EML HASL-300, Pu-11-RC ModifiedPrep Method:Ash Soil PrepDry Soil Prep GL-RAD-A-021 Method:Dry Soil Prep Analytical Batch Number:467823Prep Batch Number:463017Dry Soil Prep GL-RAD-A-021 Batch Number:463013Sample IDClient ID145417017 9527-0003-003-F145417018 9527-0003-007-F145417019 9527-0003-010-F1200948313 Method Blank (MB)1200948314 145417017(9527-0003-003-F) Sample Duplicate (DUP)1200948315 145417017(9527-0003-003-F) Matrix Spike (MS) 1200948316 Laboratory Control Sample (LCS)SOP ReferenceProcedure for preparation, analysis and reporting of analytical data are controlled by General EngineeringLaboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed inaccordance with GL-RAD-A-011 REV# 14.Calibration Information:Calibration Information All initial and continuing calibration requirements have been met.Standards InformationStandard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample GeometryAll counting sources were prepared in the same geometry as the calibration standards.Quality Control (QC) Information:Blank InformationThe blank volume is representative of the sample volume in this batch.

Page 13 of 77 Designated QCThe following sample was used for QC: 145417017 (9527-0003-003-F).QC InformationAll of the QC samples met the required acceptance limits.

Technical Information:

Holding TimeAll sample procedures for this sample set were performed within the required holding time.Preparation InformationAll preparation criteria have been met for these analyses.Sample Re-prep/Re-analysisSample 1200948314 (9527-0003-003-F) was recounted due to high negative area.Miscellaneous Information:

NCR DocumentationNonconformance reports are generated to document any procedural anomalies that may deviate from referencedSOP or contractual documents. An NCR was not generated for this SDG.Manual IntegrationNo manual integrations were performed on data in this batch.

Qualifier informationManual qualifiers were not required.

Method/Analysis InformationProduct:Liquid Scint Pu241, Solid-ALL FSSAnalytical Method:DOE EML HASL-300, Pu-11-RC ModifiedPrep Method:Ash Soil PrepDry Soil Prep GL-RAD-A-021 Method:Dry Soil PrepAnalytical Batch Number:467827 Prep Batch Number:463017Dry Soil Prep GL-RAD-A-021 Batch Number:463013Sample IDClient ID145417017 9527-0003-003-F145417018 9527-0003-007-F 145417019 9527-0003-010-F1200948317 Method Blank (MB)1200948318 145417017(9527-0003-003-F) Sample Duplicate (DUP) 1200948319 145417017(9527-0003-003-F) Matrix Spike (MS)1200948320 Laboratory Control Sample (LCS)SOP ReferenceProcedure for preparation, analysis and reporting of analytical data are controlled by General EngineeringLaboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed inaccordance with GL-RAD-A-035 REV# 7.Calibration Information:

Page 14 of 77 Calibration Information All initial and continuing calibration requirements have been met.Standards InformationStandard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample GeometryAll counting sources were prepared in the same geometry as the calibration standards.Quality Control (QC) Information:Blank InformationThe blank volume is representative of the sample volume in this batch.Designated QCThe following sample was used for QC: 145417017 (9527-0003-003-F).QC InformationAll of the QC samples met the required acceptance limits.

Technical Information:

Holding TimeAll sample procedures for this sample set were performed within the required holding time.Preparation InformationAll preparation criteria have been met for these analyses.Sample Re-prep/Re-analysisNone of the samples in this sample set required reprep or reanalysis.Miscellaneous Information:

NCR DocumentationNonconformance reports are generated to document any procedural anomalies that may deviate from referencedSOP or contractual documents. An NCR was not generated for this SDG.Manual IntegrationNo manual integrations were performed on data in this batch.

Qualifier informationManual qualifiers were not required.

Method/Analysis InformationProduct:Gamma,Solid-FSS GAM & ALL FSSAnalytical Method:EML HASL 300, 4.5.2.3Prep Method:Dry Soil PrepAnalytical Batch Number:463112 Prep Batch Number:463010Sample IDClient ID145417001 9527-0003-008-F145417002 9527-0003-008-FS 145417003 9527-0003-011-F145417004 9527-0003-011-FS Page 15 of 77 145417005 9527-0003-012-F145417006 9527-0003-013-F145417007 9527-0003-014-F 145417008 9527-0003-015-F145417009 9527-0003-016-F145417010 9527-0003-017-F 145417011 9527-0003-001-F145417012 9527-0003-002-F145417013 9527-0003-004-F 145417014 9527-0003-005-F145417015 9527-0003-006-F145417016 9527-0003-009-F145417017 9527-0003-003-F145417018 9527-0003-007-F 145417019 9527-0003-010-F1200936934 Method Blank (MB)1200936935 145417001(9527-0003-008-F) Sample Duplicate (DUP) 1200936936 Laboratory Control Sample (LCS)SOP ReferenceProcedure for preparation, analysis and reporting of analytical data are controlled by General EngineeringLaboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed inaccordance with GL-RAD-A-013 REV# 10.Calibration Information:Calibration Information All initial and continuing calibration requirements have been met.Standards InformationStandard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample GeometryAll counting sources were prepared in the same geometry as the calibration standards.Quality Control (QC) Information:Blank InformationThe blank volume is representative of the sample volume in this batch.Designated QCThe following sample was used for QC: 145417001 (9527-0003-008-F).QC InformationAll of the QC samples met the required acceptance limits.

Technical Information:

Holding TimeAll sample procedures for this sample set were performed within the required holding time.Preparation InformationAll preparation criteria have been met for these analyses.Sample Re-prep/Re-analysisNone of the samples in this sample set required reprep or reanalysis.

Page 16 of 77 Miscellaneous Information:

NCR DocumentationNonconformance reports are generated to document any procedural anomalies that may deviate from referencedSOP or contractual documents. An NCR was not generated for this SDG.Additional CommentsThe relative percent difference for Bi-214 and Ra-226 failed precision requirements for duplicate 1200936935(9527-0003-008-F). However, when the relative error ratio is calculated for both isotopes (1.85444 for each)precision is demonstrated.

Qualifier informationQualifierReasonAnalyteSampleUIData rejected due to interference.Europium-155145417015Manganese-54145417005145417017UIData rejected due to low abundance.Cesium-134145417001145417007145417008145417009145417010145417014145417015145417016145417017Cobalt-601200936935145417016Europium-155145417008Niobium-94145417003Silver-108m145417014UIData rejected due to no valid peak.Americium-241145417002Cobalt-60145417002Potassium-401200936934 Method/Analysis InformationProduct:GFPC, Sr90, solid-ALL FSSAnalytical Method:EPA 905.0 ModifiedPrep Method:Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method:Dry Soil PrepAnalytical Batch Number:467346Prep Batch Number:463017 Dry Soil Prep GL-RAD-A-021 Batch Number:463013Sample IDClient ID145417017 9527-0003-003-F145417018 9527-0003-007-F145417019 9527-0003-010-F 1200947126 Method Blank (MB)1200947127 145495001(9802-0000-001RA-SBIV) Sample Duplicate (DUP)1200947128 145495001(9802-0000-001RA-SBIV) Matrix Spike (MS)1200947129 Laboratory Control Sample (LCS)

Page 17 of 77 SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General EngineeringLaboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed inaccordance with GL-RAD-A-004 REV# 9.Calibration Information:Calibration Information All initial and continuing calibration requirements have been met.Standards InformationStandard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample GeometryAll counting sources were prepared in the same geometry as the calibration standards.Quality Control (QC) Information:Blank InformationThe blank volume is representative of the sample volume in this batch.Designated QCThe following sample was used for QC: 145495001 (9802-0000-001RA-SBIV).QC InformationAll of the QC samples met the required acceptance limits.

Technical Information:

Holding TimeAll sample procedures for this sample set were performed within the required holding time.Preparation InformationAll preparation criteria have been met for these analyses.Sample Re-prep/Re-analysisSamples 1200947126 (MB) and 1200947127 (9802-0000-001RA-SBIV) were recounted due to a negative resultgreater than three times the error.Chemical RecoveriesAll chemical recoveries meet the required acceptance limits for this sample set.Miscellaneous Information:

NCR DocumentationNonconformance reports are generated to document any procedural anomalies that may deviate from referencedSOP or contractual documents. An NCR was not generated for this SDG.

Qualifier informationManual qualifiers were not required.

Method/Analysis InformationProduct:Liquid Scint Tc99, Solid-ALL FSSAnalytical Method:DOE EML HASL-300, Tc-02-RC Modified Page 18 of 77 Analytical Batch Number:464785Sample IDClient ID145417017 9527-0003-003-F145417018 9527-0003-007-F145417019 9527-0003-010-F 1200941136 Method Blank (MB)1200941137 145417018(9527-0003-007-F) Sample Duplicate (DUP)1200941138 145417018(9527-0003-007-F) Matrix Spike (MS) 1200941139 Laboratory Control Sample (LCS)SOP ReferenceProcedure for preparation, analysis and reporting of analytical data are controlled by General EngineeringLaboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed inaccordance with GL-RAD-A-005 REV# 12.Calibration Information:Calibration Information All initial and continuing calibration requirements have been met.Standards InformationStandard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample GeometryAll counting sources were prepared in the same geometry as the calibration standards.Quality Control (QC) Information:Blank InformationThe blank volume is representative of the sample volume in this batch.Designated QCThe following sample was used for QC: 145417018 (9527-0003-007-F).QC InformationAll of the QC samples met the required acceptance limits.

Technical Information:

Holding TimeAll sample procedures for this sample set were performed within the required holding time.Preparation InformationAll preparation criteria have been met for these analyses.Sample Re-prep/Re-analysisNone of the samples in this sample set required reprep or reanalysis.Miscellaneous Information:

NCR DocumentationNonconformance reports are generated to document any procedural anomalies that may deviate from referencedSOP or contractual documents. An NCR was not generated for this SDG.

Qualifier information Page 19 of 77 Manual qualifiers were not required.

Method/Analysis InformationProduct:Liquid Scint Fe55, Solid-ALL FSSAnalytical Method:DOE RESL Fe-1, ModifiedPrep Method:Ash Soil PrepDry Soil Prep GL-RAD-A-021 Method:Dry Soil PrepAnalytical Batch Number:464797 Prep Batch Number:463017Dry Soil Prep GL-RAD-A-021 Batch Number:463013Sample IDClient ID145417017 9527-0003-003-F145417018 9527-0003-007-F145417019 9527-0003-010-F1200941150 Method Blank (MB) 1200941151 145258021(9801-0000-Z2X 3-04) Sample Duplicate (DUP)1200941152 145258021(9801-0000-Z2X 3-04) Matrix Spike (MS)1200941153 Laboratory Control Sample (LCS)SOP ReferenceProcedure for preparation, analysis and reporting of analytical data are controlled by General EngineeringLaboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed inaccordance with GL-RAD-A-040 REV# 3.Calibration Information:Calibration Information All initial and continuing calibration requirements have been met.Standards InformationStandard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample GeometryAll counting sources were prepared in the same geometry as the calibration standards.Quality Control (QC) Information:Blank InformationThe blank volume is representative of the sample volume in this batch.Designated QCThe following sample was used for QC: 145258021 (9801-0000-Z2X 3-04).QC InformationAll of the QC samples met the required acceptance limits.

Technical Information:

Holding TimeAll sample procedures for this sample set were performed within the required holding time.Preparation InformationAll preparation criteria have been met for these analyses.

Page 20 of 77 Sample Re-prep/Re-analysisNone of the samples in this sample set required reprep or reanalysis.Miscellaneous Information:

NCR DocumentationNonconformance reports are generated to document any procedural anomalies that may deviate from referencedSOP or contractual documents. An NCR was not generated for this SDG.

Qualifier informationManual qualifiers were not required.

Method/Analysis InformationProduct:Liquid Scint Ni63, Solid-ALL FSSAnalytical Method:DOE RESL Ni-1, ModifiedPrep Method:Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method:Dry Soil PrepAnalytical Batch Number:464799Prep Batch Number:463017 Dry Soil Prep GL-RAD-A-021 Batch Number:463013Sample IDClient ID145417017 9527-0003-003-F145417018 9527-0003-007-F145417019 9527-0003-010-F 1200941154 Method Blank (MB)1200941155 145258021(9801-0000-Z2X 3-04) Sample Duplicate (DUP)1200941156 145258021(9801-0000-Z2X 3-04) Matrix Spike (MS) 1200941157 Laboratory Control Sample (LCS)SOP ReferenceProcedure for preparation, analysis and reporting of analytical data are controlled by General EngineeringLaboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed inaccordance with GL-RAD-A-022 REV# 7.Calibration Information:Calibration Information All initial and continuing calibration requirements have been met.Standards InformationStandard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample GeometryAll counting sources were prepared in the same geometry as the calibration standards.Quality Control (QC) Information:Blank InformationThe blank volume is representative of the sample volume in this batch.Designated QCThe following sample was used for QC: 145258021 (9801-0000-Z2X 3-04).QC Information Page 21 of 77 All of the QC samples met the required acceptance limits.

Technical Information:

Holding TimeAll sample procedures for this sample set were performed within the required holding time.Preparation InformationAll preparation criteria have been met for these analyses.Sample Re-prep/Re-analysisNone of the samples in this sample set required reprep or reanalysis.Miscellaneous Information:

NCR DocumentationNonconformance reports are generated to document any procedural anomalies that may deviate from referencedSOP or contractual documents. An NCR was not generated for this SDG.

Qualifier informationManual qualifiers were not required.

Method/Analysis InformationProduct:LSC, Tritium Dist, Solid-HTD2,ALL FSSAnalytical Method:EPA 906.0 ModifiedAnalytical Batch Number:467508Sample IDClient ID145417017 9527-0003-003-F145417018 9527-0003-007-F145417019 9527-0003-010-F1200947551 Method Blank (MB)1200947552 145495003(9802-0000-003RA-SBIV) Sample Duplicate (DUP)1200947553 145495003(9802-0000-003RA-SBIV) Matrix Spike (MS)1200947554 Laboratory Control Sample (LCS)SOP ReferenceProcedure for preparation, analysis and reporting of analytical data are controlled by General EngineeringLaboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed inaccordance with GL-RAD-A-002 REV# 10.Calibration Information:Calibration Information All initial and continuing calibration requirements have been met.Standards InformationStandard solution(s) for these analyses are NIST traceable and used before the expiration date(s).Sample GeometryAll counting sources were prepared in the same geometry as the calibration standards.Quality Control (QC) Information:Blank Information Page 22 of 77 The blank volume is representative of the sample volume in this batch.Designated QCThe following sample was used for QC: 145495003 (9802-0000-003RA-SBIV).QC InformationAll of the QC samples met the required acceptance limits.

Technical Information:

Holding TimeAll sample procedures for this sample set were performed within the required holding time.Preparation InformationAll preparation criteria have been met for these analyses.Sample Re-prep/Re-analysisSamples 1200947553 (9802-0000-003RA-SBIV) and 1200947554 (LCS) were recounted due to low/high recovery.Miscellaneous Information:

NCR DocumentationNonconformance reports are generated to document any procedural anomalies that may deviate from referencedSOP or contractual documents. An NCR was not generated for this SDG.

Qualifier informationManual qualifiers were not required.

Method/Analysis InformationProduct:Liquid Scint C14, Solid All,FSSAnalytical Method:EPA EERF C-01 ModifiedAnalytical Batch Number:464786Sample IDClient ID145417017 9527-0003-003-F145417018 9527-0003-007-F 145417019 9527-0003-010-F1200941140 Method Blank (MB)1200941141 145417017(9527-0003-003-F) Sample Duplicate (DUP) 1200941142 145417017(9527-0003-003-F) Matrix Spike (MS)1200941143 Laboratory Control Sample (LCS)SOP ReferenceProcedure for preparation, analysis and reporting of analytical data are controlled by General EngineeringLaboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed inaccordance with GL-RAD-A-003 REV# 8.Calibration Information:Calibration Information All initial and continuing calibration requirements have been met.Standards InformationStandard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Page 23 of 77 Sample GeometryAll counting sources were prepared in the same geometry as the calibration standards.Quality Control (QC) Information:Blank InformationThe blank volume is representative of the sample volume in this batch.Designated QCThe following sample was used for QC: 145417017 (9527-0003-003-F).QC InformationAll of the QC samples met the required acceptance limits.

Technical Information:

Holding TimeAll sample procedures for this sample set were performed within the required holding time.Preparation InformationAll preparation criteria have been met for these analyses.Sample Re-prep/Re-analysisNone of the samples in this sample set required reprep or reanalysis.Miscellaneous Information:

NCR DocumentationNonconformance reports are generated to document any procedural anomalies that may deviate from referencedSOP or contractual documents. An NCR was not generated for this SDG.

Qualifier informationManual qualifiers were not required.Certification StatementWhere the analytical method has been performed under NELAP certification, the analysis has met all of therequirements of the NELAC standard unless otherwise noted in the analytical case narrative.Review Validation:GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLPor CLP-like packaging will receive a third level validation upon completion of the data package.

The following data validator verified the information presented in this case narrative: Reviewer:______________________________________________________________________________

Page 24 of 77 SAMPLE DATA

SUMMARY

Page 25 of 77 GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report YANK001 Connecticut Yankee Atomic Power Co.

Client SDG: MSR#05-2244 GEL Work Order: 145417 Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.

    • Indicates the analyte is a surrogate compound.

This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC

standard operating procedures. Please direct any questions to your Project Manager, Cheryl Jones.

___________________________________________________________

Reviewed by T he Qualifiers in this report are defined as follows:

    • Indicates the analyte is a surrogate compound.

< Result is less than amount reported.

> Result is greater than amount reported.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

P The response between the confirmation and the primary columns is >40% Different.

R Sample results are rejected.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.

Y QC Samples were not spiked with this compound.

Z Paint Filter qualifier: Particulates passed through the filter. No free liquids were observed.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

for Page 26 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Gamma Spec Analysis Parameter Result Units QualifierAnalystDateTime 463112 2340 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

10/04/05 MJH1 U UUI U U U

U U U U 0.0951 0.0435 0.240 0.057 0.0369 0.032 0.0355 0.0778 0.0855 0.0706 0.0416 0.0528 0.0342 0.0293 0.233 0.057 0.030 0.031 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417001 TS YANK01204 Project: YANK001 Client ID:

Client 0.969 0.0305 0.605 1.13 0.00 1.62 0.0403 0.0816 0.894 1.11 0.018 0.00549 9.17 1.13 0.323

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

12.4%0.202 0.089 0.504 0.119 0.0773 0.067 0.0756 0.161 0.184 0.145 0.0857 0.110 0.0717 0.0613 0.511 0.119 0.0622 0.0648 The following Prep Methods were performed Dry Soil Prep09/15/05 463010 1501 TC1 Method Description Analyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description

TPU Uncertainty Vol. Recv.:

1 EML HASL 300, 4.5.2.3 1 LCMDA Page 27 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417001 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Sample ID:

Client Sample ID:

Batch E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 28 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Gamma Spec Analysis Parameter Result Units QualifierAnalystDateTime 463112 2341 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

10/04/05 MJH1 UUI U UUI U U

U U U U 0.0722 0.0317 0.165 0.0439 0.0285 0.0242 0.0227 0.064 0.0748 0.0567 0.0347 0.0471 0.0247 0.021 0.189 0.0439 0.0228 0.0226 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417002 TS YANK01204 Project: YANK001 Client ID:

Client 0.989 0.00 1.06 0.936 0.0318 1.37 0.00 0.0337 0.0449 0.959 1.05 0.00751 8.47 0.936 0.353

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

10.7%0.156 0.0651 0.353 0.0926 0.0604 0.0511 0.0498 0.133 0.162 0.116 0.0717 0.0979 0.0525 0.0445 0.423 0.0926 0.0475 0.0479 The following Prep Methods were performed Dry Soil Prep09/15/05 463010 1501 TC1 Method DescriptionAnalyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description

TPU Uncertainty Vol. Recv.:

1 EML HASL 300, 4.5.2.3 1 LC MDA Page 29 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417002 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Sample ID:

Client Sample ID:

Batch E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 30 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Gamma Spec Analysis Parameter Result Units QualifierAnalystDateTime 463112 2341 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

10/04/05 MJH1 U U U U U U UUI U 0.0506 0.0875 0.113 0.0271 0.0181 0.0167 0.015 0.0423 0.0446 0.0491 0.0275 0.0292 0.0135 0.0132 0.114 0.0271 0.0136 0.0142 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417003 TS YANK01204 Project: YANK001 Client ID:

Client 0.712 0.0335 0.553 0.961 0.0267 1.21 0.0453 0.0798 0.882 1.08 0.0148 0.00 14.9 0.96105 0.276

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

9.88%0.107 0.180 0.238 0.0569 0.0379 0.0348 0.0322 0.0877 0.0953 0.101 0.0566 0.0607 0.0285 0.0277 0.250 0.0569 0.0284 0.0299 The following Prep Methods were performed Dry Soil Prep09/15/05 463010 1501 TC1 Method DescriptionAnalyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description

TPU Uncertainty Vol. Recv.:

1 EML HASL 300, 4.5.2.3 1 LC MDA Page 31 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417003 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Sample ID:

Client Sample ID:

Batch BD Results below the MDC or low tracer recovery.

E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 32 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Gamma Spec Analysis Parameter Result Units QualifierAnalystDateTime 463112 1126 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

10/10/05 MJH1 U U U U U

U U U U 0.0568 0.0209 0.134 0.0308 0.0251 0.0175 0.0242 0.0441 0.0579 0.0339 0.0215 0.032 0.0176 0.0168 0.139 0.0308 0.0166 0.0165 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417004 TS YANK01204 Project: YANK001 Client ID:

Client 0.658 0.00577 0.408 0.833 0.0478 1.05 0.0425 0.0679 0.782 0.949 0.032 0.0126 11.6 0.833 0.000114 0.259

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

10.9%0.122 0.043 0.285 0.0653 0.0528 0.0371 0.0518 0.092 0.125 0.0701 0.0448 0.0668 0.0376 0.0356 0.313 0.0653 0.0347 0.0351 The following Prep Methods were performed Dry Soil Prep09/15/05 463010 1501 TC1 Method DescriptionAnalyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description

TPU Uncertainty Vol. Recv.:

1 EML HASL 300, 4.5.2.3 1 LC MDA Page 33 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417004 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Sample ID:

Client Sample ID:

Batch E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 34 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Gamma Spec Analysis Parameter Result Units QualifierAnalystDateTime 463112 1127 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

10/10/05 MJH1 U U U U U

U UUI U U 0.0806 0.0308 0.160 0.0403 0.0277 0.025 0.0317 0.054 0.0775 0.049 0.0302 0.0385 0.0211 0.021 0.193 0.0403 0.0195 0.0243 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417005 TS YANK01204 Project: YANK001 Client ID:

Client 0.726 0.0206 0.634 0.838 0.0404 0.949 0.039 0.0194 0.0401 0.0508 0.703 0.854 0.00 8.19 0.838 0.0211 0.274

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

9.95%0.175 0.0635 0.346 0.0861 0.0594 0.0531 0.0685 0.114 0.169 0.102 0.0629 0.0811 0.0458 0.0449 0.438 0.0861 0.0411 0.0516 The following Prep Methods were performed Dry Soil Prep09/15/05 463010 1501 TC1 Method DescriptionAnalyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description

TPU Uncertainty Vol. Recv.:

1 EML HASL 300, 4.5.2.3 1 LC MDA Page 35 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417005 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Sample ID:

Client Sample ID:

Batch E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 36 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Gamma Spec Analysis Parameter Result Units QualifierAnalystDateTime 463112 1159 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

10/10/05 MJH1 U U U U U U U U 0.0709 0.0322 0.149 0.0365 0.0244 0.0208 0.0207 0.0579 0.0647 0.0516 0.034 0.0424 0.0206 0.0184 0.188 0.0365 0.0206 0.0208 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417006 TS YANK01204 Project: YANK001 Client ID:

Client 0.750 0.0235 0.740 0.748 0.0254 1.69 0.0526 0.0256 0.783 0.919 10.8 0.748 0.00858 0.282

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

10.3%0.152 0.0658 0.318 0.0772 0.0518 0.0441 0.0451 0.120 0.140 0.106 0.0701 0.0881 0.0439 0.039 0.415 0.0772 0.0429 0.0438 The following Prep Methods were performed Dry Soil Prep09/15/05 463010 1501 TC1 Method DescriptionAnalyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description

TPU Uncertainty Vol. Recv.:

1 EML HASL 300, 4.5.2.3 1 LC MDA Page 37 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417006 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Sample ID:

Client Sample ID:

Batch E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 38 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Gamma Spec Analysis Parameter Result Units QualifierAnalystDateTime 463112 1201 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

10/10/05 MJH1 U UUI U U U

U U U U 0.055 0.0961 0.111 0.0287 0.0208 0.0158 0.0206 0.0419 0.0441 0.0541 0.0274 0.0316 0.0172 0.0144 0.153 0.0287 0.0152 0.016 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417007 TS YANK01204 Project: YANK001 Client ID:

Client 0.990 0.0764 0.654 1.05 0.00 0.992 0.0294 0.0463 0.986 1.22 0.0133 11.8 1.05 0.00581 0.294

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

12%0.116 0.198 0.234 0.060 0.0435 0.0331 0.0435 0.0871 0.0945 0.111 0.0564 0.0655 0.0362 0.0303 0.330 0.060 0.0316 0.0334 The following Prep Methods were performed Dry Soil Prep09/15/05 463010 1501 TC1 Method DescriptionAnalyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description

TPU Uncertainty Vol. Recv.:

1 EML HASL 300, 4.5.2.3 1 LC MDA Page 39 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417007 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Sample ID:

Client Sample ID:

Batch E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 40 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Gamma Spec Analysis Parameter Result Units QualifierAnalystDateTime 463112 1202 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

10/10/05 MJH1 U UUI U U U UUI U U U 0.0444 0.0518 0.109 0.0279 0.0192 0.0131 0.0155 0.0381 0.0433 0.048 0.0229 0.0265 0.0157 0.0129 0.124 0.0279 0.013 0.0146 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417008 TS YANK01204 Project: YANK001 Client ID:

Client 0.959 0.583 1.04 0.00 0.550 0.0311 0.0316 0.00 1.02 1.07 11.7 1.04 0.000447 0.286

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

11.4%0.0939 0.106 0.228 0.0581 0.0399 0.0274 0.0328 0.0788 0.0918 0.0981 0.047 0.0549 0.0328 0.0269 0.268 0.0581 0.027 0.0305 The following Prep Methods were performed Dry Soil Prep09/15/05 463010 1501 TC1 Method DescriptionAnalyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description

TPU Uncertainty Vol. Recv.:

1 EML HASL 300, 4.5.2.3 1 LC MDA Page 41 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417008 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Sample ID:

Client Sample ID:

Batch E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 42 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Gamma Spec Analysis Parameter Result Units QualifierAnalystDateTime 463112 1713 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

10/10/05 MJH1 U UUI U U U U U U 0.071 0.0882 0.157 0.0395 0.0276 0.0208 0.0203 0.0553 0.0636 0.0621 0.0311 0.0418 0.0199 0.0192 0.153 0.0395 0.0209 0.0206 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417009 TS YANK01204 Project: YANK001 Client ID:

Client 0.833 0.0183 0.479 0.752 0.00 1.12 0.0885 0.00156 0.0179 0.0755 0.922 0.816 10.6 0.752 0.0187 0.257

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

6.49%0.155 0.182 0.338 0.084 0.0587 0.0445 0.0456 0.116 0.141 0.128 0.0648 0.0876 0.0432 0.041 0.356 0.084 0.0439 0.0441 The following Prep Methods were performed Dry Soil Prep09/15/05 463010 1501 TC1 Method DescriptionAnalyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description

TPU Uncertainty Vol. Recv.:

1 EML HASL 300, 4.5.2.3 1 LC MDA Page 43 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417009 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Sample ID:

Client Sample ID:

Batch E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 44 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Gamma Spec Analysis Parameter Result Units QualifierAnalystDateTime 463112 1714 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

10/10/05 MJH1 U UUI U U U

U U U U 0.0711 0.0906 0.160 0.0398 0.0285 0.0221 0.0248 0.0587 0.0716 0.0646 0.0323 0.0383 0.0228 0.0221 0.201 0.0398 0.020 0.0196 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417010 TS YANK01204 Project: YANK001 Client ID:

Client 0.991 0.0558 0.741 0.948 0.00 1.21 0.00231 0.0249 0.0408 0.0411 1.01 1.10 0.0154 0.0397 12.0 0.948 0.308

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

7.26%0.153 0.187 0.340 0.0842 0.0602 0.0469 0.0539 0.123 0.155 0.133 0.0669 0.0802 0.0485 0.0465 0.444 0.0842 0.0419 0.0417 The following Prep Methods were performed Dry Soil Prep09/15/05 463010 1501 TC1 Method DescriptionAnalyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description

TPU Uncertainty Vol. Recv.:

1 EML HASL 300, 4.5.2.3 1 LC MDA Page 45 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417010 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Sample ID:

Client Sample ID:

Batch E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 46 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Gamma Spec Analysis Parameter Result Units QualifierAnalystDateTime 463112 1715 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

10/10/05 MJH1 U U U U U

U U U U 0.0658 0.113 0.137 0.0318 0.0231 0.0187 0.0195 0.0482 0.0548 0.0572 0.0278 0.0363 0.0203 0.0167 0.176 0.0318 0.0158 0.0169 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417011 TS YANK01204 Project: YANK001 Client ID:

Client 1.05 0.0926 0.904 1.13 0.0397 0.609 0.0155 0.025 0.0512 1.21 1.25 0.00598 0.0014 12.6 1.13 0.352

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

13.6%0.140 0.233 0.291 0.0672 0.0488 0.0394 0.0424 0.100 0.119 0.118 0.0574 0.0754 0.043 0.0353 0.385 0.0672 0.0331 0.0358 The following Prep Methods were performed Dry Soil Prep09/15/05 463010 1501 TC1 Method Description Analyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description

TPU Uncertainty Vol. Recv.:

1 EML HASL 300, 4.5.2.3 1 LCMDA Page 47 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417011 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Sample ID:

Client Sample ID:

Batch E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 48 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Gamma Spec Analysis Parameter Result Units QualifierAnalystDateTime 463112 1715 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

10/10/05 MJH1 U U U U U

U U U U 0.0871 0.0429 0.210 0.0495 0.0397 0.0274 0.0286 0.0722 0.0794 0.0687 0.0389 0.0548 0.0274 0.0276 0.244 0.0495 0.0262 0.0275 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417012 TS YANK01204 Project: YANK001 Client ID:

Client 1.33 1.42 1.18 0.0815 0.575 0.00725 0.067 0.0639 1.19 1.20 0.000401 0.025 10.7 1.18 0.00536 0.398

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

8.13%0.189 0.088 0.448 0.105 0.0837 0.0584 0.0628 0.151 0.174 0.141 0.0808 0.114 0.0588 0.0585 0.544 0.105 0.055 0.0584 The following Prep Methods were performed Dry Soil Prep09/15/05 463010 1501 TC1 Method DescriptionAnalyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description

TPU Uncertainty Vol. Recv.:

1 EML HASL 300, 4.5.2.3 1 LC MDA Page 49 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417012 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Sample ID:

Client Sample ID:

Batch E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 50 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Gamma Spec Analysis Parameter Result Units QualifierAnalystDateTime 463112 1716 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

10/10/05 MJH1 U U U U U

U U U U 0.0944 0.114 0.201 0.0544 0.0335 0.0308 0.029 0.0764 0.0716 0.076 0.0468 0.051 0.0283 0.0259 0.217 0.0544 0.0288 0.0305 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417013 TS YANK01204 Project: YANK001 Client ID:

Client 1.12 1.03 0.980 0.0174 1.83 0.0603 0.0359 1.13 1.17 0.0159 0.0141 9.76 0.980 0.017 0.327

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

19.1%0.205 0.236 0.433 0.115 0.0715 0.0653 0.0642 0.160 0.160 0.157 0.0967 0.107 0.061 0.0553 0.496 0.115 0.0603 0.0645 The following Prep Methods were performed Dry Soil Prep09/15/05 463010 1501 TC1 Method DescriptionAnalyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description

TPU Uncertainty Vol. Recv.:

1 EML HASL 300, 4.5.2.3 1 LC MDA Page 51 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417013 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Sample ID:

Client Sample ID:

Batch E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 52 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Gamma Spec Analysis Parameter Result Units QualifierAnalystDateTime 463112 1716 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

10/10/05 MJH1 U UUI U U U

U U U UUI 0.0599 0.0753 0.134 0.0335 0.0219 0.0174 0.0201 0.0481 0.0551 0.0525 0.0267 0.0336 0.0167 0.0165 0.195 0.0335 0.0173 0.0198 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417014 TS YANK01204 Project: YANK001 Client ID:

Client 0.812 0.571 0.597 0.00 0.361 0.0223 0.0671 0.0657 0.852 0.847 0.0216 0.00176 9.82 0.597 0.00 0.271

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

5.26%0.130 0.156 0.289 0.0713 0.0469 0.0373 0.0442 0.101 0.121 0.109 0.0556 0.0707 0.0363 0.0353 0.429 0.0713 0.0365 0.042 The following Prep Methods were performed Dry Soil Prep09/15/05 463010 1501 TC1 Method DescriptionAnalyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description

TPU Uncertainty Vol. Recv.:

1 EML HASL 300, 4.5.2.3 1 LC MDA Page 53 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417014 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Sample ID:

Client Sample ID:

Batch E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 54 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Gamma Spec Analysis Parameter Result Units QualifierAnalystDateTime 463112 1717 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

10/10/05 MJH1 U UUI U U U UUI U U U 0.0797 0.026 0.162 0.0391 0.028 0.0228 0.0232 0.0497 0.0709 0.0414 0.0294 0.0405 0.0252 0.019 0.192 0.0391 0.0191 0.0219 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417015 TS YANK01204 Project: YANK001 Client ID:

Client 0.965 0.00226 0.812 0.945 0.00 0.509 0.00226 0.00 1.11 1.00 0.020 0.00397 10.5 0.945 0.0101 0.331

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

8.68%0.172 0.0536 0.347 0.0832 0.0596 0.0485 0.0512 0.105 0.155 0.086 0.0612 0.0848 0.0538 0.0406 0.432 0.0832 0.0402 0.0464 The following Prep Methods were performed Dry Soil Prep09/15/05 463010 1501 TC1 Method DescriptionAnalyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description

TPU Uncertainty Vol. Recv.:

1 EML HASL 300, 4.5.2.3 1 LC MDA Page 55 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417015 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Sample ID:

Client Sample ID:

Batch E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 56 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Gamma Spec Analysis Parameter Result Units QualifierAnalystDateTime 463112 1717 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

10/10/05 MJH1 U UUI UUI U U

U U U U 0.0562 0.0989 0.127 0.0326 0.0222 0.0199 0.0212 0.0464 0.0472 0.0628 0.0294 0.0333 0.0187 0.0159 0.153 0.0326 0.0155 0.0181 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417016 TS YANK01204 Project: YANK001 Client ID:

Client 1.05 0.0271 0.876 0.947 0.00 0.804 0.00 0.0822 0.998 1.19 0.0029 11.4 0.947 0.0235 0.263

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

7.74%0.120 0.205 0.269 0.0687 0.0467 0.0417 0.0453 0.0969 0.102 0.130 0.0608 0.0697 0.0396 0.0334 0.335 0.0687 0.0325 0.0381 The following Prep Methods were performed Dry Soil Prep09/15/05 463010 1501 TC1 Method DescriptionAnalyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description

TPU Uncertainty Vol. Recv.:

1 EML HASL 300, 4.5.2.3 1 LC MDA Page 57 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417016 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Sample ID:

Client Sample ID:

Batch E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 58 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Alpha Spec Analysis R ad Gamma Spec Analysis R ad Gas Flow Proportional Counting R ad Liquid Scintillation Analysis Parameter Result Units QualifierAnalystDateTime Alphaspec Am241, Cm, Solid ALL FSS Liquid Scint C14, Solid All,FSS 467822 467823 467827 463112 467346 467508 1538 1538 1047 1718 2222 1352 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

Tritium 10/08/05 10/08/05 10/11/05 10/10/05 10/06/05 10/11/05 BJB1 BJB1 BJB1 MJH1 EXW1 BXF1 U U U U U U U UUI U U U U UUI U U U U 0.0912 0.0524 0.0792 0.0563 0.184 7.45 0.0671 0.0717 0.155 0.0394 0.0269 0.0195 0.0243 0.0527 0.0636 0.0585 0.0302 0.0392 0.0195 0.0196 0.190 0.0394 0.019 0.0187 0.0102 5.14 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417017 TS YANK01204 Project: YANK001 Client ID:

Client 0.0905 0.0169 0.101 0.0365 1.15 0.0385 0.645 0.969 0.00 0.841 0.0386 0.0658 0.00216 0.0131 1.01 1.09 0.00 0.0047 11.0 0.969 0.00166 0.281 0.00382

362 Injun Hollow Road Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch 12.7%0.259 0.193 0.235 0.190 0.444 15.5 0.143 0.148 0.328 0.0827 0.0566 0.0412 0.0521 0.110 0.137 0.121 0.0627 0.0818 0.0416 0.0412 0.414 0.0827 0.0397 0.0396 0.0212 10.7 Mt

TPU Uncertainty Vol. Recv.:

1 2 3 4 5 6 LC MDA Page 59 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Liquid Scintillation Analysis Parameter Result Units QualifierAnalystDateTime Liquid Scint C14, Solid All,FSS

464786 464797 464799 464785 0752 0410 1931 0500 pCi/g pCi/g pCi/g pCi/g

09/22/05 09/24/05 09/24/05 09/27/05 SLN1 BXF1 BXF1 BXF1 U U U 0.0873 34.4 7.12 0.168 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417017 YANK01204 Project: YANK001 Client ID:

0.125 0.396 362 Injun Hollow Road Surrogate/Tracer recovery Recovery%Test Acceptable Limits Sample ID:

Client Sample ID:

Batch A P

C arrier/Tracer Recovery C arrier/Tracer Recovery C arrier/Tracer Recovery C arrier/Tracer Recovery Alphaspec Am241, Cm, Solid ALL 94 100 89 65 79 94 0.177 71.0 14.9 0.348 The following Prep Methods were performed A sh Soil Prep D ry Soil Prep 09/16/05 09/15/05 463017 463013 1531 1456 TC1 TC1 Method Description Analyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description TPU Uncertainty Vol. Recv.:

1 2 3

4 5

6 7

8 9

1 0

EML HASL 300, 4.5.2.3

EPA 905.0 Modified

EPA 906.0 Modified

7 8 9

10 LCMDA Page 60 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417017 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Client Sample ID:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

C arrier/Tracer Recovery 88 Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 61 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Alpha Spec Analysis R ad Gamma Spec Analysis R ad Gas Flow Proportional Counting R ad Liquid Scintillation Analysis Parameter Result Units QualifierAnalystDateTime Alphaspec Am241, Cm, Solid ALL FSS Liquid Scint C14, Solid All,FSS 467822 467823 467827 463112 467346 467508 1121 1538 1103 1718 2222 1424 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

Tritium 10/08/05 10/08/05 10/11/05 10/10/05 10/06/05 10/11/05 BJB1 BJB1 BJB1 MJH1 EXW1 BXF1 U U U U U U U U U U U U U U U U U 0.0792 0.0407 0.071 0.0358 0.143 7.51 0.0828 0.117 0.159 0.0464 0.0291 0.0239 0.0262 0.0659 0.0652 0.0725 0.042 0.0499 0.0266 0.0225 0.231 0.0464 0.0239 0.0254 0.0112 4.77 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417018 TS YANK01204 Project: YANK001 Client ID:

Client 0.0636 0.0239 0.694 0.774 0.756 0.0392 0.635 0.0153 0.0997 0.0424 0.929 0.959 0.0157 0.0086 7.72 0.756 0.0113 0.268 0.016 2.79

362 Injun Hollow Road Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch 10.3%0.243 0.178 0.226 0.157 0.371 15.6 0.179 0.242 0.347 0.0988 0.0624 0.0514 0.0577 0.139 0.145 0.150 0.0874 0.105 0.0571 0.0481 0.513 0.0988 0.0506 0.0541 0.0234 9.93 Mt

TPU Uncertainty Vol. Recv.:

1 2 3 4 5 6 LC MDA Page 62 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Liquid Scintillation Analysis Parameter Result Units QualifierAnalystDateTime Liquid Scint C14, Solid All,FSS

464786 464797 464799 464785 0926 0427 1948 0517 pCi/g pCi/g pCi/g pCi/g

09/22/05 09/24/05 09/24/05 09/27/05 SLN1 BXF1 BXF1 BXF1 U U U

U 0.0826 39.7 6.98 0.178 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417018 YANK01204 Project: YANK001 Client ID: 8.63 0.201 362 Injun Hollow Road Surrogate/Tracer recovery Recovery%Test Acceptable Limits Sample ID:

Client Sample ID:

Batch A P

C arrier/Tracer Recovery C arrier/Tracer Recovery C arrier/Tracer Recovery C arrier/Tracer Recovery Alphaspec Am241, Cm, Solid ALL 87 85 88 49 75 95 0.167 81.9 14.6 0.369 The following Prep Methods were performed A sh Soil Prep D ry Soil Prep 09/16/05 09/15/05 463017 463013 1531 1456 TC1 TC1 Method Description Analyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description TPU Uncertainty Vol. Recv.:

1 2 3

4 5

6 7

8 9

1 0

EML HASL 300, 4.5.2.3

EPA 905.0 Modified

EPA 906.0 Modified

7 8 9

10 LCMDA Page 63 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417018 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Client Sample ID:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

C arrier/Tracer Recovery 83 Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 64 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Alpha Spec Analysis R ad Gamma Spec Analysis R ad Gas Flow Proportional Counting R ad Liquid Scintillation Analysis Parameter Result Units QualifierAnalystDateTime Alphaspec Am241, Cm, Solid ALL FSS Liquid Scint C14, Solid All,FSS 467822 467823 467827 463112 467346 467508 1121 1537 1120 1719 2222 2119 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g

Tritium 10/08/05 10/08/05 10/11/05 10/10/05 10/06/05 10/09/05 BJB1 BJB1 BJB1 MJH1 EXW1 BXF1 U U U U U U U U U U U U U U U U 0.0356 0.00 0.0505 0.190 0.157 7.38 0.140 0.0527 0.339 0.0697 0.0482 0.0399 0.0422 0.0979 0.113 0.0872 0.0509 0.067 0.0352 0.031 0.367 0.0697 0.0334 0.0371 0.00775 4.63 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417019 TS YANK01204 Project: YANK001 Client ID:

Client 0.0932 0.0359 0.0163 1.25 0.0126 1.28 0.990 0.0502 1.28 0.0273 0.0819 0.0823 1.40 1.32 12.6 0.990 0.455 0.0242 5.11

362 Injun Hollow Road Sample ID:

Receive Date:

Client Sample ID:

Matrix:

Collect Date:

Collector:

Moisture:

Batch 14.6%0.156 0.0973 0.186 0.471 0.404 15.4 0.298 0.108 0.712 0.147 0.102 0.084 0.0909 0.204 0.243 0.180 0.106 0.140 0.0751 0.0658 0.800 0.147 0.070 0.0782 0.0163 9.67 Mt

TPU Uncertainty Vol. Recv.:

1 2 3 4 5 6 LC MDA Page 65 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC R ad Liquid Scintillation Analysis Parameter Result Units QualifierAnalystDateTime Liquid Scint C14, Solid All,FSS

464786 464797 464799 464785 1100 0444 2005 0534 pCi/g pCi/g pCi/g pCi/g

09/22/05 09/24/05 09/24/05 09/27/05 SLN1 BXF1 BXF1 BXF1 U U U 0.0808 36.7 7.22 0.177 DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417019 YANK01204 Project: YANK001 Client ID:

0.109 0.604 362 Injun Hollow Road Surrogate/Tracer recovery Recovery%Test Acceptable Limits Sample ID:

Client Sample ID:

Batch A P

C arrier/Tracer Recovery C arrier/Tracer Recovery C arrier/Tracer Recovery C arrier/Tracer Recovery Alphaspec Am241, Cm, Solid ALL 81 89 91 67 75 92 0.164 75.7 15.1 0.366 The following Prep Methods were performed A sh Soil Prep D ry Soil Prep 09/16/05 09/15/05 463017 463013 1531 1456 TC1 TC1 Method Description Analyst Date Time Prep Batch Mt The following Analytical Methods were performed Method Description TPU Uncertainty Vol. Recv.:

1 2 3

4 5

6 7

8 9

1 0

EML HASL 300, 4.5.2.3

EPA 905.0 Modified

EPA 906.0 Modified

7 8 9

10 LCMDA Page 66 of 77 Certificate of Analysis GENERAL ENGINEERING LABORATORIES, LLC Parameter Result Units QualifierAnalystDateTime DF Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Company : Haddam Neck Plant East Hampton, Connecticut 06424 October 13, 2005 Report Date:

Address : Soils PO# 002332 Project: 145417019 YANK01204 Project: YANK001 Client ID:

362 Injun Hollow Road Notes: The Qualifiers in this report are defined as follows :

Sample ID:

Client Sample ID:

Batch** Indicates the analyte is a surrogate compound.

B Target analyte was detected in the sample as well as the associated blank.

BD Results below the MDC or low tracer recovery.

E Concentration of the target analyte exceeds the instrument calibration range.

H Analytical holding time exceeded.

J Indicates an estimated value.

U Target analyte was analyzed for but not detected above the MDL or LOD.

UI Uncertain identification for gamma spectroscopy.

d The 2:1 depletion requirement was not met for this sample h Sample preparation or preservation holding time exceeded.

C arrier/Tracer Recovery 83 Mt TPU Uncertainty Vol. Recv.: LCMDA The above sample is reported on a dry weight basis.

Page 67 of 77 QUALITY CONTROL DATA Page 68 of 77 QC Summary GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Rad Alpha Spec 467822 467823 Batch Batch Americium-241 Curium-242

Curium-243/244 Americium-241 Curium-242 Curium-243/244 Americium-241 Curium-242 Curium-243/244 Americium-241 Curium-242 Curium-243/244 Plutonium-238 Parmname Mr. Pete Hollenbeck Contact: Connecticut Yankee Atomic Power Client : Haddam Neck Plant East Hampton, Connecticut October 13, 2005 Report Date:

Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time BJB1 BJB1 10/08/05 10/11/05 15:38 14:16 QC-0.0395-0.00877-0.0306 13.1-0.00664 15.2-0.0244-0.0136 0.00 11.8 0.00 15.0-0.0225 NOM Sample 0.0905 0.0169 0.101 0.0905 0.0169 0.101 0.0365 Range (0% - 100%)

(0% - 100%)

(0% - 100%)

(75%-125%)

(75%-125%)

(75%-125%)

(75%-125%)

(0% - 100%)

Qual U U U U U U U U U QC1200948303 145417017 QC1200948305 QC1200948302 QC1200948304 145417017 QC1200948314 145417017 RPD%REC%104 99 92 96 12.6 15.3 12.8 15.7 DUP LCS MB MS DUP 145417 Workorder:

362 Injun Hollow Road U U U U U U U+/-0.131+/-0.0673+/-0.129+/-0.131+/-0.0673+/-0.129+/-0.046+/-0.0172+/-0.030+/-1.17+/-0.013+/-1.26+/-0.0544+/-0.0189+/-0.0544+/-1.13+/-0.0631+/-1.27 Uncert: Uncert: Uncert: Uncert: Uncert: Uncert: Uncert: Uncert: Uncert: Uncert: Uncert: Uncert: TPU: TPU:

TPU: TPU: TPU: TPU: TPU: TPU: TPU: TPU: TPU: TPU:+/-0.131+/-0.0673+/-0.129+/-0.131+/-0.0673+/-0.129+/-0.0463+/-0.0172+/-0.0303+/-1.97+/-0.013+/-2.22+/-0.0545+/-0.019+/-0.0544+/-1.82+/-0.0631+/-2.23 N/A N/A N/A N/APage1 of9 Page 69 of 77 QC Summary GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Rad Alpha Spec Rad Gamma Spec 467823 467827 463112 Batch Batch Batch Plutonium-239/240 Plutonium-238 Plutonium-239/240 Plutonium-238 Plutonium-239/240 Plutonium-238 Plutonium-239/240 Plutonium-241 Plutonium-241 Plutonium-241

Plutonium-241 Actinium-228 Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time BJB1 M JH 1 10/08/05 10/08/05 10/08/05 10/11/05 10/11/05 10/11/05 10/11/05 10/10/05 15:37 15:38 15:37 11:54 12:28 11:37 12:11 17:25 QC 0.0673 0.0182 10.3 0.0229-0.113 0.0564 12.0-1.87 101-8.5 99.9 0.812 NOM Sample-0.133 0.0365-0.133-5.83-5.83 0.969 Range (0% - 100%)

(75%-125%)

(75%-125%)

(75%-125%)

(75%-125%)

(0% - 100%)

(75%-125%)

(75%-125%)

(0% - 100%)

Qual U U U U U U U QC1200948316 QC1200948313 QC1200948315 145417017 QC1200948318 145417017 QC1200948320

QC1200948317 QC1200948319 145417017 QC1200936935 145417001 RPD%REC%89 102 78 75 11.6 11.8 131 133 LCS MB MS DUP LCS MB MS DUP 145417 Workorder:

U U U U U+/-0.0824+/-0.123+/-0.0824+/-0.123+/-8.59+/-8.59+/-0.286+/-0.104+/-0.0924+/-0.122+/-1.07+/-0.0607+/-0.108+/-0.162+/-1.26+/-9.21+/-12.1

+/-7.78

+/-12.0+/-0.215 Uncert: Uncert: Uncert: Uncert: Uncert: Uncert: Uncert: Uncert: Uncert: Uncert:

Uncert: Uncert: Uncert: TPU: TPU: TPU: TPU: TPU: TPU: TPU: TPU: TPU: TPU: TPU:

TPU:+/-0.0825+/-0.124+/-0.0825+/-0.124+/-8.62+/-8.62+/-0.104+/-0.0926+/-0.122+/-1.62+/-0.0607+/-0.109+/-0.163+/-1.94+/-9.21+/-17.7

+/-7.86+/-17.4+/-0.211 N/A N/A 18Page2 of9 Page 70 of 77 QC Summary GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 463112 Batch Americium-241 Bismuth-212

Bismuth-214 Cesium-134 Cesium-137 Cobalt-60 Europium-152

Europium-154 Europium-155 Lead-212 Lead-214 Manganese-54 Niobium-94

Potassium-40 Radium-226 Silver-108m Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time QC-0.0231 0.468 0.919 0.0135 1.55 0.00-0.00881-0.0262 0.0249 0.927 1.02 0.00343 0.0198 8.54 0.919-0.00309 NOM Sample 0.0305 0.605 1.13 0.00 1.62 0.0403-0.0406

-0.0161 0.0816 0.894 1.11 0.018 0.00549 9.17 1.13-0.00168 Range (0% - 100%)

(0% - 100%)

(0% - 100%)

(0% - 20%)

(0% - 100%)

(0% - 100%)

(0% - 100%)

(0% - 100%)

(0% - 20%)

(0% - 20%)

(0% - 100%)

(0% - 100%)

(0% - 20%)

(0% - 100%)

(0% - 100%)

Qual U U UUI U U U U U U RPD%REC%145417 Workorder:

  • U UUI U U U U U U U+/-0.051+/-0.546+/-0.178+/-0.064+/-0.180+/-0.040+/-0.0963+/-0.122+/-0.0838+/-0.119+/-0.192+/-0.0408

+/-0.0351+/-1.13+/-0.178+/-0.0371+/-0.146+/-0.340

+/-0.139+/-0.0296+/-0.138+/-0.0495+/-0.0632+/-0.0624+/-0.065+/-0.119+/-0.156+/-0.0229+/-0.0181+/-0.994+/-0.139+/-0.0213 Uncert: Uncert: Uncert:

Uncert: Uncert: Uncert:

Uncert: Uncert: Uncert: Uncert: Uncert:

Uncert: Uncert: Uncert:

Uncert: Uncert: TPU: TPU: TPU: TPU: TPU:

TPU: TPU: TPU:

TPU: TPU: TPU:

TPU: TPU: TPU: TPU: TPU:+/-0.280+/-0.050+/-0.535+/-0.174+/-0.0627+/-0.176+/-0.0392+/-0.0944+/-0.120+/-0.0821+/-0.117

+/-0.188+/-0.040+/-0.0344+/-1.11+/-0.174+/-0.143+/-0.333+/-0.137+/-0.0291+/-0.135+/-0.0485+/-0.0619+/-0.0611

+/-0.0637+/-0.116+/-0.153+/-0.0225+/-0.0178+/-0.974

+/-0.137 N/A 26 21 148 4 42 N/A N/A 106 4 8 136 113 7 21 N/APage3 of9 Page 71 of 77 QC Summary GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 463112 Batch Thallium-208 Actinium-228 Americium-241 Bismuth-212 Bismuth-214 Cesium-134

Cesium-137 Cobalt-60 Europium-152

Europium-154 Europium-155 Lead-212 Lead-214 Manganese-54

Niobium-94 Potassium-40 Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time10/10/0511:27 QC 0.319 0.998 24.3 1.18 0.00375 0.194 10.1 15.2-0.197 0.337-0.148 0.295 0.014 0.182-0.0783 0.0345 NOM Sample 0.323 Range (0% - 100%)

(75%-125%)

(75%-125%)

(75%-125%)

Qual U U U U U U U U U U U U QC1200936936 RPD%REC%100 107 107 24.4 9.39 14.3 LCS 145417 Workorder:

+/-0.083+/-0.0622+/-1.01+/-0.972+/-1.61+/-0.370+/-0.243+/-0.628

+/-0.866+/-0.426+/-0.462+/-0.465+/-0.228

+/-0.305+/-0.215+/-0.179 Uncert: Uncert: Uncert: Uncert: Uncert:

Uncert: Uncert: Uncert: Uncert: Uncert:

Uncert: Uncert: Uncert:

Uncert: Uncert: TPU: TPU: TPU: TPU:

TPU: TPU: TPU:

TPU: TPU: TPU:

TPU: TPU: TPU: TPU: TPU:

TPU:+/-0.0364+/-0.0813+/-0.0209+/-0.061+/-0.993+/-0.952+/-1.58+/-0.363+/-0.238+/-0.616

+/-0.848+/-0.418+/-0.452

+/-0.456+/-0.223+/-0.299

+/-0.211+/-0.176 1Page4 of9 Page 72 of 77 QC Summary GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 463112 Batch Radium-226 Silver-108m Thallium-208 Actinium-228 Americium-241

Bismuth-212 Bismuth-214 Cesium-134

Cesium-137 Cobalt-60 Europium-152

Europium-154 Europium-155 Lead-212 Lead-214 Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time10/10/0517:19 QC 0.00375-0.0313 0.0438 0.0454-0.0224 0.0816 0.0459-0.000772 0.00609 0.0144 0.000976 0.002-0.0285 0.0217 0.022 NOM Sample Range (75%-125%)

Qual U U U U U U U U U U U U U U U QC1200936934 RPD%REC%MB 145417 Workorder:

+/-1.66+/-0.370+/-0.167+/-0.205+/-0.053+/-0.075+/-0.141+/-0.0533+/-0.0159+/-0.0171+/-0.00964

+/-0.0443+/-0.0455+/-0.037+/-0.0413

+/-0.0318 Uncert: Uncert: Uncert:

Uncert: Uncert: Uncert: Uncert: Uncert:

Uncert: Uncert: Uncert: Uncert: Uncert:

Uncert: Uncert: Uncert: TPU: TPU:

TPU: TPU: TPU: TPU:

TPU: TPU: TPU:

TPU: TPU: TPU: TPU: TPU:

TPU: TPU:+/-1.63+/-0.363+/-0.164

+/-0.201+/-0.0519+/-0.0735+/-0.138+/-0.0523+/-0.0156+/-0.0167+/-0.00945

+/-0.0434+/-0.0446

+/-0.0362+/-0.0405+/-0.0312Page5 of9 Page 73 of 77 QC Summary GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec Rad Gas Flow Rad Liquid Scintillation 463112 467346 464785 Batch Batch Batch Manganese-54 Niobium-94 Potassium-40 Radium-226 Silver-108m

Thallium-208 Strontium-90 Strontium-90 Strontium-90

Strontium-90 Technetium-99 Technetium-99

Technetium-99 Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time E XW 1 BXF1 10/12/05 10/07/05 10/12/05 10/07/05 09/27/05 09/27/05 09/27/05 19:34 19:14 19:34 19:13 06:25 07:00 06:08 QC-3.220E-05 0.00618 0.00 0.0459 0.00302 0.0256-0.00366 1.21 0.00261 1.25 0.0721 11.3 0.194 NOM Sample-0.00109-0.00109 0.201 Range (0% - 100%)

(75%-125%)

(75%-125%)

(0% - 100%)

(75%-125%)

Qual U U UUI U U U U U U U QC1200947127 145495001 QC1200947129

QC1200947126

QC1200947128 145495001 QC1200941137 145417018 QC1200941139 QC1200941136 RPD%REC%102 105 89 1.18 1.18 12.7 DUP LCS MB MS DUP LCS MB 145417 Workorder:

U U U+/-0.0095+/-0.0095+/-0.170+/-0.0187+/-0.015+/-0.237+/-0.0533+/-0.0167+/-0.0179+/-0.0076+/-0.0755+/-0.00407

+/-0.117+/-0.163+/-0.432 Uncert: Uncert: Uncert: Uncert:

Uncert: Uncert: Uncert: Uncert:

Uncert: Uncert: Uncert: Uncert: TPU: TPU:

TPU: TPU: TPU:

TPU: TPU: TPU: TPU:

TPU: TPU: TPU:+/-0.0095+/-0.0095+/-0.170+/-0.0183+/-0.0147+/-0.232+/-0.0523

+/-0.0164+/-0.0175+/-0.0076+/-0.0836+/-0.00407

+/-0.123+/-0.163+/-0.513 N/A 0Page6 of9 Page 74 of 77 QC Summary GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Rad Liquid Scintillation 464785 464786 464797 464799 Batch Batch Batch Batch Technetium-99 Carbon-14 Carbon-14 Carbon-14 Carbon-14 Iron-55 Iron-55 Iron-55 Iron-55 Nickel-63 Nickel-63 Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time SLN1 BXF1 BXF1 09/27/05 09/22/05 09/22/05 09/22/05 09/22/05 09/24/05 09/24/05 09/24/05 09/24/05 09/24/05 09/24/05 06:43 15:41 18:49 14:07 17:15 05:36 06:10 05:18 05:53 20:55 21:28 QC 11.5 0.0911 6.48-0.0611 6.07-7.41 698 20.3 737-2.29 532 NOM Sample 0.201 0.125 0.125-24.8-24.8-4.8 Range (75%-125%)

(0% - 100%)

(75%-125%)

(75%-125%)

(0% - 100%)

(75%-125%)

(75%-125%)

(0% - 100%)

(75%-125%)

Qual U U U U U QC1200941138 145417018 QC1200941141 145417017 QC1200941143

QC1200941140

QC1200941142 145417017 QC1200941151 145258021 QC1200941153 QC1200941150 QC1200941152 145258021 QC1200941155 145258021 QC1200941157 RPD%REC%90 95 86 90 94 92 12.7 6.80 7.05 777 788 577 MS DUP LCS MB MS DUP LCS MB MS DUP LCS 145417 Workorder:

U U U U U U+/-0.170+/-0.106+/-0.106+/-49.7+/-49.7+/-7.84+/-0.146+/-0.466+/-0.0952+/-0.162+/-0.0937+/-0.171+/-57.3+/-74.7+/-53.6+/-75.1+/-8.07+/-23.8 Uncert: Uncert: Uncert: Uncert:

Uncert: Uncert: Uncert: Uncert: Uncert:

Uncert: Uncert: Uncert: TPU: TPU: TPU: TPU: TPU: TPU: TPU: TPU:

TPU: TPU: TPU: TPU:+/-0.170+/-0.106+/-0.106+/-49.8+/-49.8+/-7.85+/-0.146+/-0.546+/-0.0952+/-0.191+/-0.0937+/-0.196+/-57.3+/-86.0+/-53.6+/-87.7+/-8.07+/-30.0 0 N/A N/APage7 of9 Page 75 of 77 QC Summary GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Rad Liquid Scintillation 464799 467508 Batch Batch Nickel-63 Nickel-63 Tritium Tritium Tritium Tritium Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time BXF1 09/24/05 09/24/05 10/10/05 10/13/05 10/10/05 10/13/05 20:38 21:11 04:53 02:10 04:21 01:38 QC 0.688 502 5.48 2.43 0.341 50.9 NOM Sample-4.8 3.73 3.73 Range (75%-125%)

(0% - 100%)

(75%-125%)

(75%-125%)

Qual U U U QC1200941154 QC1200941156 145258021 QC1200947552 145495003 QC1200947554

QC1200947551 QC1200947553 145495003 Notes: The Qualifiers in this report are defined as follows:

RPD%REC%86 80 76 582 3.03 67.2 MB MS DUP LCS MB MS 145417 Workorder:

    • B BD E H J U UI X d h Indicates the analyte is a surrogate compound.

Target analyte was detected in the sample as well as the associated blank.

Results below the MDC or low tracer recovery.

Concentration of the target analyte exceeds the instrument calibration range.

Analytical holding time exceeded.

Indicates an estimated value.

Target analyte was analyzed for but not detected above the MDL or LOD.

Uncertain identification for gamma spectroscopy.

Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.

The 2:1 depletion requirement was not met for this sample Sample preparation or preservation holding time exceeded.

U U U+/-7.84+/-6.27+/-6.27+/-8.18+/-22.6+/-5.58+/-0.368

+/-0.435+/-9.06 Uncert: Uncert: Uncert: Uncert: Uncert: Uncert: TPU: TPU: TPU: TPU:

TPU:

TPU:+/-7.85+/-6.27+/-6.27+/-8.18+/-28.4+/-5.58+/-0.370+/-0.435+/-9.10 0Page8 of9 Page 76 of 77 QC Summary GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com ParmnamePage9 of9 Units Anlst Date Time QC NOM Sample Range Qual RPD%REC%145417 Workorder:

N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more.

    • Indicates analyte is a surrogate compound.

^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

Page 77 of 77

EAST MOUNTAIN SIDESURVEY UNIT 9527-0003RELEASE RECORDAttachment 2bSample and Scan Area Data(9 Pages)

SAMPLE LOCATION SCANS 9527-0003Log DateLog TimeE600 S/NProbe S/N12800144151330009/06/20052:19 PM1109100515800175941630009/06/20052:24 PM1109100518400203362020009/06/20052:27 PM1109100523300254782100009/06/20052:29 PM1109100536000387082850009/06/20052:32 PM1109100541800447184150009/06/20052:36 PM1109100520000220181980009/06/20052:46 PM1109100541500444073840009/07/20051:33 PM1109100518500204411870009/06/20052:49 PM1109100520400224381910009/06/20052:53 PM1109100538000407823600009/07/20051:30 PM1109100520200222281860009/07/200511:22 AM1109100519700217031820009/07/200511:16 AM1109100519100210721760009/07/200511:20 AM1109100516900187551670009/07/200511:18 AM1109100539300421293330009/07/20051:39 PM1109100527700300752750009/07/20051:42 PM11091005Survey Unit 9527-0003Backgound(cpm)Action Level(cpm)Results(cpm)Sample Name9527-03-SL-00-01-09527-03-SL-00-02-09527-03-SL-00-03-09527-03-SL-00-04-09527-03-SL-00-10-09527-03-SL-00-11-09527-03-SL-00-12-09527-03-SL-00-05-09527-03-SL-00-06-09527-03-SL-00-07-09527-03-SL-00-08-0Survey Release Record Scan Area Results9527-03-SL-00-17-0AboveAL9527-03-SL-00-13-09527-03-SL-00-14-09527-03-SL-00-15-09527-03-SL-00-16-09527-03-SL-00-09-0AL - Action Level 9527-0003 SCAN AREAS 1 THROUGH 8Log DateLog TimeE600 S/NProbe S/N14700164301470009/07/20058:25 AM1105100614600163241510009/07/20058:27 AM1105100614200159011470009/07/20058:29 AM1105100614600163241480009/07/20058:31 AM1105100614200159011540009/07/20058:36 AM1105100615200169601580009/07/20058:38 AM1105100615600173831590009/07/20058:39 AM1105100616200180161620009/07/20058:41 AM1105100616200180161580009/07/20058:42 AM1105100615200169601440009/07/20058:44 AM1105100615100168541560009/07/20058:46 AM1105100615000167481610009/07/20058:48 AM1105100615500172771520009/07/20058:51 AM1105100615200169601640009/07/20058:53 AM1105100614700164301580009/07/20058:55 AM1105100617200190721550009/07/20058:57 AM1105100618100200201510009/07/20058:58 AM1105100616200180161730009/07/20059:01 AM1105100619900219131620009/07/20059:02 AM1105100616400182281700009/07/20059:04 AM1105100619000209671560009/07/200510:35 AM1105100616800186501720009/07/200510:38 AM1105100619300212831660009/07/200510:40 AM1105100615300170651660009/07/200510:42 AM1105100618900208621440009/07/200510:47 AM1105100617500193881640009/07/200510:48 AM1105100616500183331590009/07/200510:50 AM1105100617100189661850009/07/200510:51 AM1105100618100200201590009/07/200510:53 AM1105100618100200201900009/07/200510:54 AM1105100617900198091670009/07/200511:05 AM1105100618900208621740009/07/200511:06 AM1105100619600215981730009/07/200511:08 AM11051006Survey Unit 9527-0003Backgound(cpm)Action Level(cpm)Results(cpm)Sample Name9527-03-SC-01-01-09527-03-SC-01-02-09527-03-SC-01-03-09527-03-SC-01-04-09527-03-SC-01-05-09527-03-SC-01-06-09527-03-SC-01-07-09527-03-SC-01-08-09527-03-SC-01-09-09527-03-SC-01-10-09527-03-SC-01-11-09527-03-SC-01-12-09527-03-SC-01-13-09527-03-SC-01-14-09527-03-SC-01-15-09527-03-SC-01-16-09527-03-SC-01-17-09527-03-SC-01-18-09527-03-SC-01-19-09527-03-SC-01-20-09527-03-SC-01-21-09527-03-SC-01-22-09527-03-SC-01-23-09527-03-SC-01-24-09527-03-SC-01-25-09527-03-SC-01-26-09527-03-SC-01-27-09527-03-SC-01-28-09527-03-SC-01-29-09527-03-SC-01-30-09527-03-SC-01-31-09527-03-SC-01-32-09527-03-SC-01-33-0Survey Release Record Scan Area ResultsAboveALAL - Action Level 9527-0003 SCAN AREAS 1 THROUGH 8Log DateLog TimeE600 S/NProbe S/NSurvey Unit 9527-0003Backgound(cpm)Action Level(cpm)Results(cpm)Sample NameSurvey Release Record Scan Area ResultsAboveAL17500193881880009/07/200511:10 AM1105100620500225431840009/07/200511:11 AM1105100618900208621920009/07/200511:13 AM1105100621100231731850009/07/200511:15 AM1105100619800218081960009/07/200511:16 AM1105100620900229632050009/07/200511:19 AM1105100620700227532000009/07/200511:21 AM1105100616600184391640009/07/20051:28 PM1105100618800207571810009/07/20051:30 PM1105100618300202311720009/07/20051:32 PM1105100616900187551720009/07/20051:38 PM1105100620100221231620009/07/20051:39 PM1105100618600205461730009/07/20051:41 PM1105100621600236971780009/07/20051:43 PM1105100617300191771890009/07/20051:45 PM1105100620900229631820009/07/20051:46 PM1105100621600236972050009/07/20051:48 PM1105100623600257921780009/07/20051:55 PM1105100625100273611800009/07/20051:57 PM1105100627200295541750009/07/20051:59 PM1105100624700269431750009/07/20052:00 PM1105100626900292411840009/07/20052:03 PM1105100628100304921930009/07/20052:04 PM1105100627900302841950009/07/20052:07 PM1105100625600278831940009/07/20052:10 PM1105100626700290321720009/07/20052:12 PM1105100627100294491980009/07/20052:14 PM1105100623200253742350009/07/20052:37 PM1105100625200274662000009/07/20052:39 PM1105100622700248502210009/07/20052:41 PM1105100625200274662230009/07/20052:42 PM1105100624100263162170009/07/20052:44 PM1105100625600278832000009/07/20052:45 PM110510069527-03-SC-01-34-09527-03-SC-01-35-09527-03-SC-01-36-09527-03-SC-01-37-09527-03-SC-01-38-09527-03-SC-01-39-09527-03-SC-01-40-09527-03-SC-01-41-09527-03-SC-01-42-09527-03-SC-01-43-09527-03-SC-01-44-09527-03-SC-01-45-09527-03-SC-01-46-09527-03-SC-01-47-09527-03-SC-01-48-09527-03-SC-01-49-09527-03-SC-01-50-09527-03-SC-01-51-09527-03-SC-01-52-09527-03-SC-01-53-09527-03-SC-01-54-09527-03-SC-01-55-09527-03-SC-01-56-09527-03-SC-01-57-09527-03-SC-01-58-09527-03-SC-01-59-09527-03-SC-01-60-09527-03-SC-01-61-09527-03-SC-01-62-09527-03-SC-01-63-09527-03-SC-01-64-09527-03-SC-01-65-09527-03-SC-01-66-0AL - Action Level 9527-0003 SCAN AREAS 1 THROUGH 8Log DateLog TimeE600 S/NProbe S/NSurvey Unit 9527-0003Backgound(cpm)Action Level(cpm)Results(cpm)Sample NameSurvey Release Record Scan Area ResultsAboveAL22400245362140009/07/20052:47 PM1105100626400287192110009/07/20052:47 PM1105100622400245362250009/07/20052:49 PM1105100629400318471910009/07/20052:50 PM1105100631100336172150009/07/20052:52 PM1105100630500329922120009/07/20052:53 PM1105100629100315352130009/07/20052:55 PM1105100623600257922010009/07/20052:57 PM1105100632200347612070009/07/20052:58 PM1105100627900302842160009/07/20052:59 PM1105100628900313262040009/07/20053:01 PM1105100629800322641900009/07/20053:02 PM1105100626600289281880009/07/20053:03 PM1105100635000376701980009/07/20053:05 PM110510069527-03-SC-01-67-09527-03-SC-01-68-09527-03-SC-01-69-09527-03-SC-01-70-09527-03-SC-01-71-09527-03-SC-01-72-09527-03-SC-01-73-09527-03-SC-01-74-09527-03-SC-01-75-09527-03-SC-01-76-09527-03-SC-01-77-09527-03-SC-01-78-09527-03-SC-01-79-09527-03-SC-01-80-0AL - Action Level 9527-0003 SCAN AREA 9 THROUGH 16Log DateLog TimeE600 S/NProbe S/N41800447182670009/08/20058:48 AM1105100634700373582790009/08/20058:50 AM1105100633800364242780009/08/20058:53 AM1105100637800405752920009/08/20058:55 AM1105100637300400563330009/08/20058:57 AM1105100638500413002960009/08/20059:00 AM1105100638300410933080009/08/20059:02 AM1105100638500413003800009/08/20059:05 AM1105100639500423363260009/08/20059:09 AM1105100645400484413720009/08/20059:13 AM1105100650500537073650009/08/20059:17 AM1105100648400515403290009/08/20059:21 AM1105100652800560793420009/08/20059:24 AM1105100649500526754230009/08/20059:29 AM1105100651500547394310009/08/20059:32 AM1105100609/09/200510:32 AM110510069527-03-ER-02-15-151500547395410009/08/20051:26 PM1105100652700559763310009/08/20059:36 AM1105100651700549453780009/08/20059:38 AM1105100653900572134090009/08/20059:42 AM1105100652900561824100009/08/20059:47 AM1105100652500557704230009/08/20059:50 AM1105100619000209671820009/08/200510:06 AM1105100617700195991870009/08/200510:09 AM1105100618500204411810009/08/200510:11 AM1105100618900208621950009/08/200510:13 AM1105100619800218081740009/08/200510:15 AM1105100619400213882030009/08/200510:17 AM1105100620000220181950009/08/200510:19 AM1105100619700217032130009/08/200510:21 AM1105100619500214931820009/08/200510:25 AM1105100620100221232030009/08/200510:28 AM1105100619900219131830009/08/200510:44 AM1105100618800207571840009/08/200510:46 AM11051006Survey Unit 9527-0003Backgound(cpm)Action Level(cpm)Results(cpm)Sample Name9527-03-SC-02-01-09527-03-SC-02-02-09527-03-SC-02-03-09527-03-SC-02-04-09527-03-SC-02-05-09527-03-SC-02-06-09527-03-SC-02-07-09527-03-SC-02-08-09527-03-SC-02-09-09527-03-SC-02-10-09527-03-SC-02-11-09527-03-SC-02-12-09527-03-SC-02-13-09527-03-SC-02-14-09527-03-SC-02-15-09527-03-SC-02-16-09527-03-SC-02-17-09527-03-SC-02-18-09527-03-SC-02-19-09527-03-SC-02-20-09527-03-SC-02-21-09527-03-SC-02-22-09527-03-SC-02-23-09527-03-SC-02-24-09527-03-SC-02-25-09527-03-SC-02-26-09527-03-SC-02-27-09527-03-SC-02-28-09527-03-SC-02-29-09527-03-SC-02-30-09527-03-SC-02-31-09527-03-SC-02-32-0Survey Release Record Scan Area ResultsAboveALAL - Action Level 9527-0003 SCAN AREA 9 THROUGH 16Log DateLog TimeE600 S/NProbe S/NSurvey Unit 9527-0003Backgound(cpm)Action Level(cpm)Results(cpm)Sample NameSurvey Release Record Scan Area ResultsAboveAL19100210721760009/08/200510:48 AM1105100619000209671950009/08/200510:50 AM1105100619500214931890009/08/200510:52 AM1105100618400203361920009/08/200510:53 AM1105100619000209671830009/08/200510:58 AM1105100618400203361850009/08/200510:59 AM1105100618100200201730009/08/200511:01 AM1105100617100189661810009/08/200511:03 AM1105100619600215981700009/08/200511:05 AM1105100618200201251830009/08/200511:06 AM1105100619000209671750009/08/200511:07 AM1105100619600215981740009/08/200511:08 AM1105100618600205461830009/08/200511:10 AM1105100618300202311880009/08/200511:12 AM1105100617900198091870009/08/200511:13 AM1105100619500214931900009/08/200511:14 AM1105100617000188611800009/08/200511:15 AM1105100618100200201880009/08/200511:17 AM1105100619000209671890009/08/20051:56 PM1105100618500204412040009/08/20051:57 PM1105100618600205461840009/08/20051:59 PM1105100618500204411730009/08/20052:00 PM1105100617700195991760009/08/20052:02 PM1105100618200201251790009/08/20052:03 PM1105100617900198091710009/08/20052:05 PM1105100618200201251890009/08/20052:06 PM1105100618400203361770009/08/20052:07 PM1105100618200201251880009/08/20052:10 PM1105100626600289281900009/08/20052:13 PM1105100624800270471800009/08/20052:14 PM1105100626000283011740009/08/20052:16 PM1105100626600289281780009/08/20052:18 PM1105100627000293451840009/08/20052:19 PM110510069527-03-SC-02-33-09527-03-SC-02-34-09527-03-SC-02-35-09527-03-SC-02-36-09527-03-SC-02-37-09527-03-SC-02-38-09527-03-SC-02-39-09527-03-SC-02-40-09527-03-SC-02-41-09527-03-SC-02-42-09527-03-SC-02-43-09527-03-SC-02-44-09527-03-SC-02-45-09527-03-SC-02-46-09527-03-SC-02-47-09527-03-SC-02-48-09527-03-SC-02-49-09527-03-SC-02-50-09527-03-SC-02-51-09527-03-SC-02-52-09527-03-SC-02-53-09527-03-SC-02-54-09527-03-SC-02-55-09527-03-SC-02-56-09527-03-SC-02-57-09527-03-SC-02-58-09527-03-SC-02-59-09527-03-SC-02-60-09527-03-SC-02-61-09527-03-SC-02-62-09527-03-SC-02-63-09527-03-SC-02-64-09527-03-SC-02-65-0AL - Action Level 9527-0003 SCAN AREA 9 THROUGH 16Log DateLog TimeE600 S/NProbe S/NSurvey Unit 9527-0003Backgound(cpm)Action Level(cpm)Results(cpm)Sample NameSurvey Release Record Scan Area ResultsAboveAL29100315351730009/08/20052:21 PM1105100626000283011920009/08/20052:23 PM1105100627700300751770009/08/20052:25 PM1105100625900281971580009/08/20052:26 PM1105100627400297621880009/08/20052:28 PM1105100618300202311820009/08/20052:41 PM1105100617700195991700009/08/20052:43 PM1105100619500214931630009/08/20052:45 PM1105100617800197041750009/08/20052:46 PM1105100618400203361590009/08/20052:47 PM1105100617900198091740009/08/20052:50 PM1105100618900208621560009/08/20052:52 PM1105100615000167481510009/08/20052:54 PM1105100616400182281490009/08/20052:56 PM1105100615400171711660009/08/20052:59 PM110510069527-03-SC-02-66-09527-03-SC-02-67-09527-03-SC-02-68-09527-03-SC-02-69-09527-03-SC-02-70-09527-03-SC-02-71-09527-03-SC-02-72-09527-03-SC-02-73-09527-03-SC-02-74-09527-03-SC-02-75-09527-03-SC-02-76-09527-03-SC-02-77-09527-03-SC-02-78-09527-03-SC-02-79-09527-03-SC-02-80-0AL - Action Level 9527-0003 SCAN AREAS 17 THROUGH 22Log DateLog TimeE600 S/NProbe S/N16000178051520009/08/20053:01 PM1105100616500183331300009/08/20053:03 PM1105100616600184391490009/08/20053:04 PM1105100615600173831680009/08/20053:05 PM1105100614600163241480009/08/20053:08 PM1105100615900177001430009/08/20053:09 PM1105100615000167481580009/08/20053:10 PM1105100614000156891530009/08/20053:12 PM1105100617800197041560009/08/20053:14 PM11051006132001484014900+09/08/20053:16 PM1105100615500172771630009/09/20058:13 AM1105100615800175941520009/09/20058:15 AM1105100616500183331560009/09/20058:18 AM1105100616500183331650009/09/20058:20 AM1105100614700164301550009/09/20058:22 AM1105100616000178051520009/09/20058:24 AM1105100616300181221650009/09/20058:26 AM1105100616300181221410009/09/20058:28 AM1105100615000167481600009/09/20058:31 AM1105100617000188611490009/09/20058:32 AM1105100618800207571800009/09/20058:37 AM1105100618000199151640009/09/20058:38 AM1105100617500193881580009/09/20058:40 AM1105100618600205461620009/09/20058:42 AM1105100618400203361690009/09/20058:44 AM1105100618900208621610009/09/20058:46 AM1105100617800197041620009/09/20058:48 AM1105100617400192831520009/09/20058:50 AM1105100617800197041590009/09/20058:53 AM1105100618100200201810009/09/20058:54 AM1105100625100273611880009/09/20059:39 AM1105100624400266291760009/09/20059:40 AM1105100621600236971810009/09/20059:42 AM11051006Survey Release Record Scan Area ResultsAboveAL9527-03-SC-03-32-09527-03-SC-03-33-09527-03-SC-03-28-09527-03-SC-03-29-09527-03-SC-03-30-09527-03-SC-03-31-09527-03-SC-03-24-09527-03-SC-03-25-09527-03-SC-03-26-09527-03-SC-03-27-09527-03-SC-03-20-09527-03-SC-03-21-09527-03-SC-03-22-09527-03-SC-03-23-09527-03-SC-03-16-09527-03-SC-03-17-09527-03-SC-03-18-09527-03-SC-03-19-09527-03-SC-03-14-09527-03-SC-03-15-09527-03-SC-03-10-09527-03-SC-03-11-09527-03-SC-03-12-09527-03-SC-03-13-09527-03-SC-03-06-09527-03-SC-03-07-09527-03-SC-03-08-09527-03-SC-03-09-09527-03-SC-03-02-09527-03-SC-03-03-09527-03-SC-03-04-09527-03-SC-03-05-09527-03-SC-03-01-0Survey Unit 9527-0003Backgound(cpm)Action Level(cpm)Results(cpm)Sample NameAL - Action Level 9527-0003 SCAN AREAS 17 THROUGH 22Log DateLog TimeE600 S/NProbe S/NSurvey Release Record Scan Area ResultsAboveALSurvey Unit 9527-0003Backgound(cpm)Action Level(cpm)Results(cpm)Sample Name22600247451890009/09/20059:43 AM1105100625100273611690009/09/20059:45 AM1105100624300265251800009/09/20059:47 AM1105100624000262112010009/09/20059:48 AM1105100620000220181740009/09/20059:50 AM1105100624900271521720009/09/20059:52 AM1105100623300254781570009/09/20059:54 AM1105100626300286141960009/09/20059:56 AM1105100626600289282000009/09/20059:58 AM1105100629400318471940009/09/200510:00 AM1105100631300338251920009/09/200510:02 AM1105100631500340331920009/09/200510:04 AM1105100629200316392110009/09/200510:07 AM1105100630500329921840009/09/200510:08 AM1105100632200347611850009/09/200510:10 AM1105100630700332012000009/09/200510:11 AM1105100631800343452020009/09/200510:13 AM1105100639700425443550009/09/200510:53 AM1105100635100377743440009/09/200510:55 AM1105100639500423362860009/09/200510:57 AM1105100637300400562940009/09/200511:00 AM1105100636400391233540009/09/200511:02 AM1105100634900375662680009/09/200511:04 AM1105100633800364243200009/09/200511:07 AM1105100631200337212850009/09/200511:09 AM1105100632600351772580009/09/200511:11 AM1105100632800353852470009/09/200511:13 AM110510069527-03-SC-03-58-09527-03-SC-03-59-09527-03-SC-03-60-09527-03-SC-03-54-09527-03-SC-03-55-09527-03-SC-03-56-09527-03-SC-03-57-09527-03-SC-03-50-09527-03-SC-03-51-09527-03-SC-03-52-09527-03-SC-03-53-09527-03-SC-03-46-09527-03-SC-03-47-09527-03-SC-03-48-09527-03-SC-03-49-09527-03-SC-03-44-09527-03-SC-03-45-09527-03-SC-03-40-09527-03-SC-03-41-09527-03-SC-03-42-09527-03-SC-03-43-09527-03-SC-03-36-09527-03-SC-03-37-09527-03-SC-03-38-09527-03-SC-03-39-09527-03-SC-03-34-09527-03-SC-03-35-0AL - Action Level EAST MOUNTAIN SIDESURVEY UNIT 9527-0003RELEASE RECORDAttachment 2cSplit Sample Assessment Forms(2 Pages)

EAST MOUNTAIN SIDESURVEY UNIT 9527-0003RELEASE RECORDAttachment 2dPreliminary Data Forms(2 Pages)

EAST MOUNTAIN SIDESURVEY UNIT 9527-0003RELEASE RECORDAttachment 2eGraphical Representation of Data(4 Pages)

EAST MOUNTAIN SIDESURVEY UNIT 9527-0003RELEASE RECORDAttachment 2fSign Test Calculation(1 Page)

EAST MOUNTAIN SIDESURVEY UNIT 9527-0003RELEASE RECORDAttachment 2gCOMPASS DQA Surface Soil Report withRetrospective Power Curve(4 Pages)