IR 05000295/1988004

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Addendum to Insp Repts 50-295/88-04 & 50-304/88-05, Consisting of Comparisons of Results of Liquid Spike Sent to Plant & Criteria for Comparing Analytical Measurements
ML20195J513
Person / Time
Site: Zion  File:ZionSolutions icon.png
Issue date: 11/28/1988
From:
NRC OFFICE OF ENFORCEMENT (OE)
To:
Shared Package
ML20195J481 List:
References
50-295-88-04, 50-295-88-4, 50-304-88-05, 50-304-88-5, NUDOCS 8812020214
Download: ML20195J513 (2)


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o TABLE 2 U S NUCLEAR REGULATORY COMMISSION OFFICE OF INSPECTION AND ENFORCEMENT CONFIRMATORY MEASUREMENTS PROGRAM FACILITY: ZION FOR THE 1 QUARTER OF 1988


NRC-------


LICENSEE----

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SAMPLE ISOTOPE RESULT ERROR RESULT ERROR RA1IO REG T

L WASTE G BETA 1.NE-05 8.0E-07 1.4E-05 0.0E-01 8.4E-01 2.1E 01 A

H-3 6.6E-05 1.3E-06 1.!E-04 0.0E-01 1.6E 00 5.1E 01 D

SR-89 5.0E-04'

1.6E-05 4.6E-04 0.0E-01 9.1E-01 3.2E 01 A

SR-90 3.0E-05 1.2E-06 2.6E-05 0.0E-01 8.6E-01 2.5E 01 A

FE-55 6.5E-05 1.3E-06 6.1E-05 0.0E-01 9.4E-01 5.0E 01 A

T TEST RESULTSt AcAGREEMENT DsDISAGREEMENT onCRITERIA RELAXED NANO COMPARISON

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8G12O20214 881128 PDR ADOCK 05000295

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ATTACHMENT 1

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CRITERIA FOR COMPARING ANALYTICAL MEASUREMENTS

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This attachment provides criteria for comparing results of capability tests and verification measurements.

The criteria are based on an empirical relationship which combines prior experience and the accuracy needs of this program.

In these criteria, the judgment limits are variable in relation to the comparison of the NRC's value to its associated one sigma uncertainty.

As that ratio, referred to in this program as "Resolution", increases, the acceptability of a licensee's measurement should be more selective.

Conversely, poorer agreement should be considered acceptable as the resolution decreases.

The values in the ratio criteria may be rounded to fewer significant figures reported by the NRC Reference Laboratory, unless such rounding will result in a narrowed category of acceptance.

RESOLUTION RATIO = LICENSEE VALUE/NRC REFERENCE VALUE e1 Agreement

<4 0.4 - 2.5 4-

0.5 - 2.0 8-

0.6 - 1,66 16 - 50 0.75 - 1.33 51 - 200 0.80 - 1.25 200 -

0.85 - 1.18 l

l l

Some discrepancies may result from the use of different equipment, techniques, and for some specific nuclides.

These may be factored into the acceptance criteria and identified on the data sheet.

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