Text

Discharge Monitoring Report for Fourth Quarter 2016
	ML17054C886
Person / Time
Site:	Diablo Canyon
Issue date:	01/20/2017
From:	Cortina D; Pacific Gas & Electric Co
To:	; Document Control Desk, Office of Nuclear Reactor Regulation, State of CA, Regional Water Quality Control Bd
References
	DCL-2017-500
	Download: ML17054C886 (149)
	v • d • e

m Pacific Gas and Electric Company*

Diablo Canyon Power Plant P. 0. Box 56 Avila Beach, CA 93424 PG&E Letter DCL-2017-500 Electronic Submission CIWQS Web Application January 20, 2017 California Regional Water Quality Control Board Central Coast Region Attn: Monitoring and Reporting Review Section 895 Aerovista, Suite #101 San Luis Obispo, CA 93401-7906 In accordance with Order 90-09, NPDES No: CA0003751, the 4th Quarter 2016 repor.t on Discharge Self-Monitoring at Diablo Canyon Power Plant (DCPP) is provided. This letter and accompanying report summary has been attached to the State CIWQS application data submittal (eSMR). State DMR Forms are additionally incorporated in the CIWQS electronic data submittal (eDMR).

Facility Name: Pacific Gas & Electric Company Diablo Canyon Power Plant Address: P.O. Box 56 Avila Beach, CA 93424 Contact Person: Bryan Cunningham Job

Title:

Supervisor, ~nvironmental Operations Phone Number: (805) 545-4439 .

WDR/NPDES Order Number: . Order No. 90-09, NPDES No. CA000~751 Type of Report: (check one) QUARTERLY ANNUAL

~ D Quarter: (check one):

Year: 2016 . (Annual Reports for DCPP are Jan~Dec)

Violation(s) (Place an X by the ~ No (there are no violations to report) D Yes Note: Reference Item 5 of Overview appropriate choice): Section regarding an exceedence of the calculated California Ocean Plan limit for Total Residual Chlorine (TRC) at Discharge Outfall 001 during Unit-1 conduit treatment.

PG&E Letter DCL-2017-500 CRWQCB Central Coast Region January 20, 2017 Page 2 If Yes is marked (complete a-g):

a) Parameter(s) in Violation:

b) Section(s) of WDR/NPDES Violated:

"c) Reported Value(s):

d) WDR/NPDES Limit/Condition:

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e) Dates of Violation(s): , (If "YES", see overview section of attached report)

(reference page of report/data sheet) f) Explanation of Cause(s): (If "YES", see overview section of attached report)

(attach adqitional information as needed) g) Corrective Action(s): (If "YES", see overview section of attached report)

(attach additional information as needed)

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PG&E Letter DCL-2017-500 .

CRWQCB Central. Coast Region January 20, 2017 Page 3 I certify under penalty of law that this document, the CIWQS data submittal, and all associated attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. The results of the influent and effluent monitoring presented are the observed results of the measurements and analyses required by the monitoring program, and is neither an assertion of the adequacy of any** \

I instrument reading or analytical result, nor an endorsement of the appropriateness of any analytical or measurement procedure. I am aware that there are significant penalties for submitting false information, iricluding th~ possibility of fine and imprisonment for knowing violations.

If you have any questions or concerns regarding the report provided, or require additional information, please ~ontact Bryan Cunningham at (805) 545-4439.

Sincerely,

'Name: David Cortina

Title:

Manager, Chemistry and Environmental Operations - Diab/a Canyon Power Plant 2017500/cdg/bkc

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PG&E Letter DCL-2017-500 CRWQCB Central Coast Region January 20, 2017 Page4 cc: PDF Formatted Copy of CIWQS Application Submittal:

Regional Administrator Licensing Assistant, Operations Branch U.S. Nuclear Regulatory Commission Region IV 1600 East Lamar Boulevard Arlington, TX 76011-4511 Hardcopy Print-Out of CIWQS Application Submittal:

u.s.* N1,Jclear"ReguLatory Cpmmission D.ocument Control Desk Washington, D.C. 20555-0001 Chris Newport NRC Senior Resident Inspector U.S. Nuclear Regulatory Commission Diablo Canyon Power Plant 104/5

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PACIFIC GAS AND ELECTRIC COMPANY Fourth Quarter 2016 REPORT ON DISCHARGE MONITORING AT DIABLO CANYON POWER PLANT

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TABLE OF CONTENTS OVERVIEW ................................................................................ 1

SUMMARY

OF MONITORING PROGRAM A. Monitoring of Plant Influent and Effluent.......................... 2 B. Monitoring of Receiving Waters ...................... ~ ................ 3 C. Sodium Bromide Treatment Program.............................. 3 APPENDIX 1: NPDES Discharge Points r

OVERVIEW

1. During the fourth quarter of 2016, discharges occurred from Discharge Paths 001 (once through cooling water}, 001 B, 001 D, 001 E, 001 F, 001p, 001 H, 001 L, 001 N, 001 P, 002, 003, 004, and 005 through 015. No discharges occurred from Discharge Paths 0011, 001 J, 001 K, 001 M, 016 and 017. A list of all of the permit discharge pathways, including name and number, is provided in Appendix 1. (

2. The substances listed in Table B of the California Ocean Plan were each analyzed for and reported in the permit renewal application and application updates for Diablo Canyon Power Plant (DCPP) submitted in 1994, 2001, and 2011. There have been no changes in activities conducted at the plant that would have significantly affected the results previously reported in the above referenced documents.* Ocean Plan Table B substances not analyzed for this quarter were not added to any plant discharge streams.

3. Required annual reporting parameter for pathway 001 N Sludge Monitoring - quantity (during removal). Approximately 48-tons of water-saturated sludge was removed from the Diablo Canyon Waste Water Treatment Unit in October 2016. The solid fraction of this material was measured at 0.9%, making the solid fraction 0.4-tons.

4. During the fourth quarter of 2016, mainte~ance activities that required draining of closed cooling water systems were performed, and are summarized below. PG&E received concurrence from the CCRWQCB in response to letters dated July 19, 1995 (PG&E Letter DCL-95-156), May 23, 1996 (PG&E Letter DCL-96-522), and May 19, 1997 (PG&E Letter DCL-97-533) regarding the use of glutaraldehyde and isothiazolin to control microbiological growth and*corrosion in DCPP's closed cooling water systems.

Discharges are drained at a flow rate such that the chronic toxicity level remains below the "No Observable Effect Concentration" (NOEC) at NPDES Discharge 001.

- Total Volume Glutaraldehyde lsothiazolin Oil & Grease Date System Suspended (gallons) (mg/I) (mg/I as Cl") (mg/I)

Solids (mg/I) 11 /15/1 B Unit-2 CCW 2,700 99 0 < 2.0 < 1.4

5. On December 02, 2016, a brief Total Residual Chlorine (TRC) spike occurred on the Unit-1 outfall monitor at the start of the routine 04:00 chemical treatment cycle. The resultant monitored peak value was 142-ppb TRC for Discharge 001, an exceedance of the 89~ppb calculated Ocean Plan limit for TRC discharge during a 20-minute cooling water conduit chlorination treatment. The event was not- an exceedence of the 200-ppb NPDES permit limit for TRC.

Regional Water Quality Control Board staff (von Langen) was notified of the event via voice-mail message on Monday December 05, 2016 following evaluation of chlorine injection system monitoring data and confirmation that an exceedance had occurred.

Review of injection system operations, including associated condenser waterbox and discharge outfall chlorine: monitor data, determined that an excessive concentration of chemical had been injected into seawater Conduit 1-1 during the scheduled treatment cycle. Chemical treatment to Conduit 1-1 was subsequently suspended pending determination of the cause.

An investigation of chemical skid equipment conditions in conjunction with system testing determined cause of the excessive injection was failure of a sodium hypochlorite supply isolation valve to fully-close during system flushing. Failure of the isolation valve

resulted in concentrated sodium hypochlorite instead of deionized water being pumped into the chemical line leading to the 1-1 Conduit during the water flushing phase of pump skid operations at the enq of the prior injection cycle. The 1-1 Conduit chemical

line had therefore effectively been flushed-out and laid-up with concentrated sodium hypochlorite instead of water. At the. start of the subsequent treatment cycle at 04:00 on December 02, the sodium hypochlorite in the line was injected into the 1-1 Conduit resulting in a brief excessive concentration of chemical in the seawater flow. This in turn resulted in an excessive residual chlorine concentration at the Unit-1 outfall during the treatment cycle. ,

Corrective action involved replacement of the identified faulty sodium hypochlorite supply line isolation valve. Subsequent system testing and operation determined the valve replacementadequately resolved this equipment-related issue.

6. Two events affected the results of continuous chlorine monitoring at Discharge 001 during the fourth quarter 2016. For these events, engineering evaluations were subsequently completed as authorized by the Regional Board in accordance with PG&E's January 5, 1994 letter. The engineering evaluations were based on condenser water box chlorine measurements, recorded chemical injection rates, circulating water pump status, and discharge chlorine readings before and after the period in question.

Based on these factors, estimates for results during the affected periods were generated. The event intervals, affected monitor, .number of affected results, the cause(s), and corrective action(s) have been tabulated below. Results from the engineering evaluations were a_ll below the applicable 89-µg/L discharge limit.

Affected Affected Interval Cause Corrective Actions Monitor Readings 10/26/16 to Low monitor response Unit-2 16 Monitor recalibrated.

11/02/16 during QC-check.

11/16/16 to High monitor response Unit-1 39 Monitor recalibrated.

11/23/16 during QC-check.

SUMMARY

. OF MONITORING PROGRAM A. Monitoring of Plant Influent and Effluent

1. The results of the October, November, and December 2016 plant influent and effluent monitoring have been reported via the CIWQS web application to which this letter is attached.

2. The laboratory report for one acute bioassay on water sampled from Discharge 001, performed December 21st through December 25th, 2016, is attached to the CIWQS application submittal'. The acute bioassay results show that toxicity was 0.0 TUa (no acute toxicity).

Note: The 0.0 TUa value is not included in the CIWQS application spreadsheet as the formatting of the data spreadsheet does not accommodate zero value entries.

3. The laboratory report for one chronic bioassay on water sampled from Discharge

_ 001, performed December 20th through December 22"d, 2016. The chronic bioassay results show that toxicity was 1.00 TUc (no chronic toxicity).

B. Monitoring of Receiving Waters

1. Ecological Studies at Diablo Canyon

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.Ecological studies in the vicinity of Diablo Cove conducted during the fourth quarter continued under the Diablo Canyon Receiving Water Monitoring Program (RWMP) as requested in a letter from the Central Coast Regional Water Quality Control Board (CCRWQCB) dated December 9, 1998, and as detailed in a letter (PG&E Letter DCL-99-503) dated January 8, 1999. This program includes tasks from the Ecological Monitoring Program (EMP) with additional stations and increased sampling frequencies. The RWMP replaces the !=MP and the Thermal Effects Monitoring Program (TEMP). *

2. In Situ Bioassay Results ofthe Mussel Watch Program will be reported to the CCRWQCB directly

) from the California Department of Fish and Wildlife (CDF&W) in the Department's periodic report for this program.

C. Sodium Bromide Treatment Program

Diablo Canyon Power Plant is continuing the use of sodium bromide and sodium hypochlorite to control macrofouling growth for both Units. Both circulating water conduits of each Unit can be chemically treated simultaneously. Each treated conduit typically receives a twenty-minute injection every four hours (six injections a day) of sodium bromide in combination with sodium hypochlorite.

Each chemical injection treatment attempts to achieve a target concentration in the range of 250-300 parts per billion (ppb) Total Residual Oxidant (TRO) when measured at the inlet waterbox of the condenser. Discharge TRO concentrations measured at the plant outfall remained below NPDES permit limitations and the calculated Ocean Plan limit throughout the quarter, with exception of an equipment-related event in December that resulted in one calculated Ocean Plan limit exceedance for Unit-1 during treatment

. (Reference Item 5 ofOverview Section).

Both conduits of Unit 1 were treated with simultaneous injections of sodium bromide and sodium hypochlorite six times a day throughput the majority of the fourth quarter.

However, several extended interruptions in conduit treatment occurred due to planned or emergent system maintenance activities and equipment upgrades. In October, Unit-1 1 conduit treatment was suspended for approximately one-week leading rnto and during a scheduled seawater conduit cleaning curtailment. Conduit treatment to both units was also suspended for several days during November due to an equipment maintenance

clearance.

Conduit 1-1 treatment was suspended for approximately one week in December to evaluate the cause and implement corrective actions following an excessive chemical injection event (Reference Item 5 of Overview Section). Treatment of both unit main seawater conduits was additionally suspended twice for several days during December to facilitate scheduled equipment upgrade and replacement activities at the intake chemical injection skid.

Both conduits of Unit-2 were treated with simultaneous injections of sodium bromide and sodium hypochlorite six times a day throughput the majority of the fourth quarter.

Conduit treatment to both units was suspended for several days during November due to an equipment maintenance clearance. Treatment of both unit main seawater conduits was additionally suspended twice for several days during December to facilitate scheduled equipment upgrade and replacement activities at the intake chemical injection skid.

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APPENDIX 1

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DIABLO CANYON POWER PLANT NPDES DISCHARGE POINTS DISCHARGE NUMBER DESCRIPTION 001 Once-Though Cooling Water .

001 A Firewater Systems 001 B Auxiliary Salt Water Cooling System 001 c Discharge Deleted 001 D ' Liquid Radioactive Waste Treatment System 001 E Service Cooling Water System

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001 F Turbine Building Sump 001 G Make-Up Water System Waste Effluent 001 H Condensate Demineralizer Regenerant 0011 Seawater Evaporator Slowdown 001 J Condensate Pumps Discharge Header Overboard 001 K Condenser Tube Sheet Lea'k Detection Dump Tank Overboard 001 L Steam Generator Slowdown 001 M Wastewater Holding and Treatment System 001 N Sanitary Wastewater Treatment System 001 p Seawater Reverse Osmosis System Slowdown 002 Intake Structure Building Floor Drains 003 Intake Screen Wash 004 Bio Lab and Storm Water Runoff 005,008,009,013,014,015 Yard Storm Drains 006,007, 010,011,012 Storm Water Runoff 016 Bio Lab Seawater Supply Pump

- Valve Drain 017 Seawater Reverse Osmosis System Slowdown Drain

CIWQS Web Application Submittal Print Out and Attached Supporting Documents I

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eSMR PDF Report Summary: Quarterly SMR ( MONNPDES ) report for Q4 2016 Summary : Quarterly SMR ( MONNPDES) report for Q4 2016 su bmitted by david cortina (Che m istry and Environmenta l Services Manager) on Facility Name: PG&E Diablo Ca nyon Power Plant Order Number: R3-1990-0009 Waterboard Office : Regi on 3 - Centra l Coast Case Worker: Peter Von Langen Report Effective Dates : 10/01/2016 - 12/31/2016 No Discharge Periods Name Description Dates Comments Diablo M-001 Diablo M-OOlD Diablo M-OOlF Dia blo M-OOlG Diablo M-OOlH Dia blo M-001 1 10/01/2016 - 12/31/2016 Plant Seawater Evaporators no longer in service.

Diablo M-OOlj 10/01/2016 - 12/31/2016 Conde nsate Pump Discharge Header not drained during 4016 . No effluent discharaed.

Diablo M-OOlK 10/01/2016 - 12/31/2016 Plant Conde nser Tube Sheet Leak Detection Dump Tank no longer in service .

Diablo M-OOlL Diablo M-OOlM 10/01/2016 - 12/31/2016 Waste Ho lding and Treatment System (WHAT) not discharged during 4016.

Di sc harge is intermittent, used as reauired .

Diablo M-OOlN Diablo M-OOlP Diablo M-002 Diablo M-00 3 Diablo M-004 Diablo M-005 Diablo M-008 Diablo M-009 Diablo M-013 Diablo M-015 Diablo M-0 16 10/01/2016 - 12/31/2016 Bio Lab Seawater Supply Line Valve Box not drained during 4016 . No effluent discharaed.

Diablo M-017 10/01/2016 - 12/31/2016 Seawater RO System Slowdown Line not dra ined du ring 4016. Discharge rare Iv used.

Diablo M-INF Self-Determined Violations No Violations Entered Page 1 of 32

Attachments File Name File Description Date Uploaded File Size Excel workbook sh o wing calculations of all averaged resu lts Attachme nt 1

2016 4th Qtr DCPP NPDES Worksheets.pdf 01/19/201 7 258950 bytes be ina re oorted for oeriod.

Attachm ent 2

2016 4th Qtr DCPP NPD ES Contract Lab Results .

Co ntract lab res ults for period. 01/19/2017 4960291 bytes od f Cover Letter (Uploaded File)

Title Date Uploaded File Size PGE DCL2017 50 0 4th-Q 2016 DSMR Su mma . df 01/20/20 17 2169879 b tes Data Summary Analytical Results Collection Sample Sample Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time, Lab Rep, Result, ML, Priority, Location Depth !ml Matrix Analvtical Method Analvsis Date Lab Batch Units RL OA Codes Comments Data Source 10/04/2016 " " CD F_Ana lytica l_Ca l

" " Ammonia, Tot al (as N) = 0.15 No See Attac hm ent 2, M-001 10:07:00 1 " cu lated_Ol2020 17.

" water A4500 NH mg/L " Contract Lab Report 10114/2016 " " zio 10/19/2016 " " Annua l. See CDF _Ana lytical_Ca l

" " Arsen ic, Tota l = 1.28 No M-001 08 :25:0 0 1 " Attac hm ent 2, cu lated_Ol202017.

" water E200.8 ug/L "

11/14/2016 " " Co ntract Lab Reoo rt. zio 10/19/2016 " " Annu al. See CD F_Analytica l_Ca l

" " Cadm ium, Tota l = 0.044 No M-001 08:25:00 1 " Attac hm ent 2, cul at ed_Ol202017 .

" water E200 .8 ug/L "

11/14/2016 " " Contract Lab Report. zip 10/04/2016 " 5 CDF_Ana lytica l_Ca l

" " Chromi um (Tota l) ND No M-001 10:07:00 1 " cu lat ed_Ol202017 .

" water DU ug/L "

10/26/2016 " " zip 11/03/2016 " 5 CDF_Ana lytical_Ca l

" " Chromium (Tota l) ND No M-001 09:45 :00 1 " cu lated_Ol202017 .

" wat er DU ug/L "

11117/2016 " " zio 12/08/2016 " 5 CDF_Ana lytica l_Ca l

" Chro mium (Total) ND No M-001 10:15:00 1 " cu lated_Ol202017 .

" water DU ug/L "

12/12/2016 " " zip 12/20/2016 " " CDF _Ana lyti cal_Ca l

" Chronic Toxicity =l No See Attachment 2, M-001 10:45:00 1 " cu lated_Ol2020 17.

" water DU TUc " Contract Lab Report 12/21/2016 " " zip 11/03/2016 " " CDF _Analytica l_Ca l

" Cop pe r, Total = 9.9 No M-001 09:45:00 1 " culated_Ol2020 17.

" water DU ug/L "

11117/2016 " " zio 10/04/2016 " 5 CDF _Analytical_Ca l

" " Coppe r, Tota l

DNQ 9 No M-001 10:07:00 1 " culated_Ol202017.

" water DU ug/L "

10/27/2016 " 10 zip 12/08/2016 " 5 CD F_Analytical_Ca l

" " Cop per, Tota l DNQ 9.3 No M-001 10:15 :00 1 " culat ed_Ol202017.

" water DU ug/L "

12/12/2016 " 10 zip 10/19/2016 " .0009 Annua l. See CDF_Ana lytica l_Ca l

" " Cyan id e, Tot al (a s CN) ND No M-001 08:25:00 1 " Attachm ent 2, cu lat ed_Ol202017.

" water E335.4 mg/L "

10/24/2016 " " Contract Lab Report. zip 10/19/2016 " " Ann ual. See CDF _Ana lytica l_Ca l

" " Lead, Tota l = 0.056 No M-001 08:25:00 1 " Attachment 2, culated_Ol202017.

" water E200.8 ug/L "

11/14/2016 " " Contract Lab Report. zip 10/19/2016 " .06 Ann ual. See CDF _Analytica l_Ca l

" " Mercury, Total DNQ 0.47 No M-001 08:25 :00 1 " Attac hm ent 2, cul ated_Ol2020 17 .

" water El 631 ng/L "

10/25 /2016 " .5 Contract Lab Reoort. zio 10/04/2016 " 5 CD F_Analytical_Ca l

" " Nickel, Tota l ND No M-001 10:07:00 1 " culated_01202017.

water DU ug/L "

10/26/2016 " " zip Page 2 of 32

Collection Sample Sample Date, Field Re p, MDL, Review Method, Type, Paramete r, Sample Time, Lab Rep, Result, ML, Priority, Location Deoth !ml Matrix Analvtlcal Method Analvsls Date Lab Batch Unit s RL OA Codes Comments Data Source

- - Nickel, Tota l 11/03/2016 - ND 5

No CDF_Ana lytica l_Ca l M-001

- water DU 09:45:00 1 ug/L

- - cu lated_01202017.

1111712016 - - zio

- - Nickel. Total 12/08/2016 - ND 5

No CDF_Ana lytical_Ca l M-001

- water DU 10:15:00 1 ug/L - -

cu lated_01202017 .

12112120 16 - - zio

- - PCB-1016 10/19/2016 - ND

.0094 No Annual. See CDF_Ana lyti ca l_Ca l M-001

- wa ter SW8082 08:25:00 1 ug/L - - Attachment 2, culated_01202017.

1012912016 - - Contra ct Lab Reoort. zio

- - PCB-1221 10/1 9/2016 - ND

.0094 No Annual. See CDF _Ana lytical_Cal M-001

- water SW8082 08:25:00 1 ug/L - -

Attachment 2, cu lated_01202017 .

10/29/2016 - - Contract Lab Report. zip

- - PCB-1232 10/19/2016 - ND

.0094 No Annual. See CDF_Ana lytical_Cal M-001

- water SW8082 08:25 :00 1 ug/L - - Attachment 2, culated_01202017 .

10/29/2016 - - Co nt ract Lab Report. zip 10/19/2016 - .0094 Annua l. See CDF_Analytical_Ca l M-001 - - PCB-1242 08:25 :00 1 ND No Attachment 2, cu lated_01202017 .

- water SW8082 10/29/2016 - ug/L

- - Contract Lab Reoort. zio

- - PCB-1248 10/19/2016 - ND

.0094 No Annua l. See CDF_Ana lytica l_Cal M-001

- water SWB082 08:25:00 1 ug/L - - Attachment 2, culated_Ol202017.

1012912016 - - Contra ct Lab Reoort. zio

- - PCB-1254 10/19/2016 - ND

.0094 No Annua l. See CDF_A nal ytica l_Ca l M-001

- water SWBO B2 08:25:00 1 ug/L - - Attachment 2, culated_01202017.

10/29/2016 - - Co ntract Lab Reoort. zio

- - PCB-1260 10/19/2016 - ND

.0094 No Ann ual. See CDF_Ana lytica l_Ca l M-001

- wate r SW8082 08:25:00 1 ug/L Attachment 2, cu lated_01202017.

1012912016 - - Contract Lab Reoort . zio

- - pH 10/04/2016 - = 7.9 - No CDF_Ana lytical_Ca l M-001 10:07 :00 1 - culated_01202017 .

- water A4500HB 1010412016 - SU

- - zio 11/03/2016 - - CDF _Ana lytica l_Ca l M-001 - - pH 09:45:00 1

= 8.08 - No cu lated_01202017.

- water A4500HB 11/03/2016 - SU

- - zip

- - pH 12/08/2016 - = B.02 - No CDF_Ana lytica l_Ca l M-001

- water A4500HB 10:15:00 1 SU culated_Ol202017 .

12/08/2016 - - zip

- - Phenols, Ch lori nated 10/19/2016 - ND

.57 No Annua l. See CDF_Ana lytical_Ca l M-001

- water DU 08:25:00 1 ug/L

- - Attachment 2, culated_01202017.

1110112016 - - Contract Lab Reoort . zi p

- - Pheno ls, Non-c hlorinated 10/19/2016 - ND 3.03 No Annua l. See CDF_A na lytica l_Ca l M-001

- water DU 08:25:00 1 ug/L

- - Atta chment 2, culated_01202017 .

11/01/2016 - - Contract Lab Report. zi p 10/19/2016 - .004 Annual. See CDF_Ana lytica l_Ca l M-001

- - Silver, Total 08:25 :00 1 ND No Attachment 2, cu lated_Ol202017 .

- water E200 .8 11/14/2016 - ug/L

- - Contract Lab Reoort. zip

- - Titanium , Tota l 10/19/2016 - ND

.4 No Annual. See CDF_Analytical_Ca l M-001

- water DU 08:25:00 1 ug/L - - Attachment 2, cu lated_01202017 .

11/18/2016 - - Contract Lab Report. zip

- - Zinc, Total 10/04/2016 - ND 5

No CDF_Ana lytical_Ca l M-001

- water DU 10:07 :00 1 ug/L - -

cu lated_01202017.

10/27 /2016 - - zip

- - Zinc, Tota l 11/03/2016 - ND 5

No CDF_Ana lytica l_Ca l M-001

- water DU 09:45:00 1 ug/L

- - cu lated_Ol202017.

ll/17/2016 - - zip 12/08/2016 - 5 CDF_Anal ytica l_Ca l M-001 - - Zin c, Tota l 10:15:00 1 ND

- No cu lated_01202017.

- water DU 12112/2016 - ug/L

- - zip Page 3 of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time, La b Rep, Result, ML, Priority, Location Deoth !ml Matri x Ana lvtlcal Method Analvsls Date La b Batch Units RL IOA Codes Comme nts Data Source

- - Boron, Total 10/04/2016 - = 1580 - No CDF_Analytical_Cal M-OOlD

- water DU 15 :10:00 1 mg/L Annua l ana lysis. cu lated_01202017.

10/26/2016 - - zip

- - Hydrazine 10/04/2016 - ND 3

No CDF_Analytical_Cal M-0010

- water DU 15:10:00 1 ug/L - - Annua l ana lysis. culated_01202017.

10/12/2016 - - zip

- - Lithium, Total 10/04/2016 - = 826 - No CDF_Analytical_Ca l M-OOlD

- water DU 15:10:00 1 ug/L - -

Annua l ana lys is. culated_01202017.

10/27/2016 - zip

- Oil and Grease 12/01/2016 -

= 5.3 - No CDF _Analytical_Ca l M-OOlF

- water E1664A 07:37:00 1 mg/L

- - cu lated_01202017.

12/01/2016 - - zip

- - Oi l and Grease 10/03/2016 - DNQ 3 1.4 No CDF_A nalytical_Ca l M-OOlF

- water El664A 16:00:00 1 mg/L

- - culated_01202017.

10/18/2016 - 5 zip 11/03/2016 - 1.4 CDF_Ana lytica l_Ca l M-OOlF - - Oi l and Grease 07:20:00 1 DNQ 2.4

- No cu lated_01202017.

- water E1664A ll/17 /2016 - mg/L 5 - zip

- - Oi l and Grease 10/06/2016 - ND 1.4 No CDF_Ana lytica l_Ca l M-OOlG

- water El664A 10:55 :00 1 mg/L

- - culated_01202017.

10/2712016 - - zip

- - Total Suspen ded So lids (TSS) 10/06/2016 - ND 2

No CDF_Ana lytical_Ca l M-OOlG

- water A2540D 10:55:00 1 mg/L

- - cu lated_01202017.

10/06/2016 - - zip

- - Tota l Suspended So lids (TSS) 11/09/20 16 - ND 2

No CDF_Ana lytica l_Ca l M-OOlG

- water A2540D 12 :00:00 1 - -

cu lated_01202017.

mg/L 11/09/2016 - - zio

- - Total Suspended So li ds (TSS) 12/07 /2016 - ND 2

No CDF_Ana lytical_Ca l M-OOlG 09:20:00 1 - culated_01202017.

- water A2540D 12/07/2016 - mg/L

- - zip

- - Ammonia, Total (as N) 10/17 /2016 - = 7300 - No Ann'I sludg e-See CDF_Analytical_Cal M-OOlN

- water A4500NH 10:30:00 1 mg/Kg

- - Attachment 2 cu lated_01202017.

10/19/2016 - - Contract Lab Report zio

- - Boron, Tota l 10/17 /2016 - = 180 - No Ann'I slud ge-See CDF _Ana lytical_Ca l M-OOlN

- water SW6010B 10:30:00 1 mg/Kg Attachment 2 cu lated_01202017.

10/25/2016 - - Co ntra ct Lab Report zip

- - Cadm ium, Tota l 10/17 /2016 - = 1.6 - No Ann' I sludg e-See CDF_Analytica l_Cal M-OOlN

- water SW6020 10:30:00 1 mg/Kg

- - Attachment 2 cu lated_01202017.

10/25/201 6 - - Co ntract Lab Report zip

- - Chrom ium (Tota l) 10/17 /2016 - = 9.4 - No Ann' I sludge-See CDF_Analytica l_Ca l M-OOlN

- water SW6020 10: 30 :00 1 mg/Kg

- - Attachment 2 culated_01202017.

10125/2016 - - Contra ct Lab Report zip

- - Copper, Total 10/17 /2016 - = 430 - No Ann' I sludge-See CDF_Analytica l_Cal M-OOlN

- water SW6020 10:30:00 1 mg/Kg - - Attachment 2 cu lated_01202017.

10/25/2016 - - Contract Lab Report zip

- - Lead, Total 10/17 /2016 -

= 7.1 - No Ann'I sludge-See CDF_Analytical_Cal M-OOlN

- water SW6020 10:30:00 1 mg/Kg

- - Attachment 2 cu lated_Ol202017.

10/25/2016 - - Contract Lab Report zip

- - Mercury, Tota l 10/17 /2016 - = 0.23 - No Ann'I sludg e-See CDF_Analytical_Ca l M-OOlN

- water SW7471A 10:30 :00 1 mg/Kg - - Atta chment 2 cu lated_01202017 .

10/25/2016 - - Contract Lab Report zip

- - Nickel, Total 10/17/2016 - = 11 - No Ann' I sludge-See CDF_Analytical_Ca l M-OOlN 10:30:00 1 - Attachment 2 cu lated_01 202017.

- water SW6020 10/25/2016 - mg/Kg

- - Contract Lab Report zip 10/ l 7/2016 - 110 Ann' I slud ge-See CDF_Ana lytica l_Ca l M-OOlN - - Nitrate, Tota l (as N) 10:30:00 1 ND

- No Attachment 2 cu lated_01202017.

- water E300.0 10/26/2016 - mg/Kg

- - Contract Lab Report zip Page 4 of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time, Lab Rep, Result, ML, Priority, Location Deoth fml Matrix Analvtical Method Analvsls Date Lab Batch Units RL loA Codes Comments Data Source

- - Oil and Grease 11/01/2016 - ND 97000 No Ann 'I slud ge-See CDF _Ana lytica l_Ca l M-OOlN 09:25:00 1 - Attachment 2 cu lated_Ol202017.

- water DU 11/1 0/2016 - mg/Kg

- - Contract Lab Repo rt zip

- - pH 10/17/2016 - =7

- No Ann'I sludg e-See CDF_Ana lytica l_Ca l M-OOlN

- water A4500HB 10:30:00 1 SU

- - Attachment 2 culated_Ol202017.

10/20/2016 - - Contract Lab Report zip

- - Phosp horus. Total (as P) 10/17 /2016 - = 26000

- No Ann' I sludg e-See CDF _Analytica l_Ca l M-OOlN

- wat er E200 .8 10:30:00 1 mg/Kg

- - Attachment 2 cu lated_Ol202017.

10/25/2016 - - Contract Lab Report zip

- - Tota l Kj eldah l Nitrog en (TKN) (as N) 10/17/2016 - = 76000

- No Ann 'I sludge-See CDF_Ana lytica l_Ca l M-OOlN

- water E351.2 10:30:00 1 mg/Kg

- - Attachme nt 2 cu lated_Ol202017.

10125/201 6 - - Co ntra ct Lab Report zip

- - Tota l Solids (TS) 11/01/2016 - = 9.6 - No Ann' I sludg e-See CDF_Analytica l_Ca l M-OOlN

- wate r DU 09 :2S :OO 1 ppth

- - Attachment 2 cu lated_Ol202017.

11/04/2016 - - Contract Lab Report zip 10/17 /201 6 - - Ann' I sludg e-See CD F_Anal ytica l_Ca l M-OOlN - - Tota l So lid s (TS) 10:30 :00 1

= 9600 No Attachment 2 cu lated_Ol202017 .

- water A2540B 10/25/2016 - mg/L

- - Contract Lab Report zip

- - Zinc, Total 10/17/2016 - = 740

- No Ann' I sludg e-See CDF_Ana lytical_Ca l M-OOlN

- water SW6020 10:30:00 1 mg/Kg

- - Attachment 2 cu lated_Ol202017 .

10/25/2016 - - Contract Lab Report zip

- - Oi l and Grease 10/10/2016 - ND 1.4 No CDF_Ana lytica l_Ca l M-OOlP

- water El664A 10:20:00 1 mg/L

- - culated_Ol202017.

10/27 /2016 - - zip

- - Oi l and Grease 10/06/2016 - ND 1.4 No CDF_Ana lytica l_Ca l M-002

- water El664A 09:30:00 1 mg/ L - - cu lated_Ol202017.

10/27/2016 - - zip

- - pH 10/06/2016 - = 7.97

- No CDF _Analytical_Ca l M-002

- water A4500HB 09 :30 :00 1 SU

- - culated_Ol2020 17 .

10/06/2016 - - zip

- - pH 11/10/2016 - = 8 .003

- No CDF _Analytica l_Ca l M-002

- water A4500 HB 12:20:00 1 SU cul ated_Ol202017.

11/ 10/2016 - - zip

- - pH 12/05/2016 - = 8.02

- No CDF_Analytica l_Ca l M-002

- wa ter A4500 HB 13:15:00 1 SU

- - cu lated_Ol2020 17.

12/05/2016 - - zip

- - Tota l Suspe nded So lids (TSS) 11/10/2016 - = 6. 1

- No CDF_A nal ytica l_Ca l M-002 12 :20 :00 1 - culated_Ol202017.

- water A2540D mg/L -

11110/2016 - - zip

- - Tota l Suspended So lid s (TSS) 10/06/2016 - DNQ 3 2

No CDF_Ana lytica l_Cal M-002 09:30 :00 1 - cul ated_Ol202017.

- water A2540 D mg/L s - zip 10/06/2016

- - Tota l Suspended So lid s (TSS) 12/05/2016 - DNQ 3.3 2

No CDF_Ana lytica l_Cal M-002

- water A2540D 13 :15 :00 1 mg/L

- - cu lated_Ol202017.

12/0512016 - 5 zip

- Oi l and Grease 10/06/2016 - ND 1.4 No CDF_A nalytica l_Ca l M-003

- water El664A 09: 10:00 1 mg/L

- - cu lated_Ol2020 17.

10127/2016 - - zip

- pH 10/06/2016 - = 7.92 - No CDF_Ana lytica l_Ca l M-003

- water A4500 HB 09: 10:00 1 SU culated_Ol2020 17.

10/06/2016 - - zip

- pH 11/07/2016 - = 8.07

- No CDF_Ana lytica l_Ca l M-003

- wate r A4500 HB 12:47:00 1 SU

- - cu lated_Ol202017.

11/07/2016 - - zip

- - pH 12/05/2016 - = 8.04

- No CDF_Ana lytica l_Ca l M-003

- water A4500 HB 13:00:00 1 SU

- - cu lated_Ol202017 .

12/05/2016 - - zip Pag e 5 of 32

Collection Sa mple Sample Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time, Lab Rep, Result, ML, Priority, Location Depth !ml Matri x Ana lvtical Method Analvsis Date La b Batch Units RL IOA Codes Comments Data Source

- - Oil and Grease 10/ 06/2016 - ND 1.4 No CDF_Analytical_Ca l M-004

- water El664A 09:45:00 1 mg/ L cu lated_Ol202017.

10/2712016 - - zip

- - pH 10/06/2016 - = 7.94 -

No CDF_Ana lytical_Ca l M-004

- water A4500 HB 09:45:00 1 SU

- - cu lated_Ol202017.

10/06/2016 - - zio

- - pH ll/07 /2016 - = 8.04 - No CDF_Analytical_Ca l M-004

- water A4500 HB 13:00:00 1 SU culated_Ol202017.

11/07 /2016 - - zip

- - pH 12/07 /2016 - = 7.92 - No CDF _Analytical_Cal M-004

- water A4500HB 08:45:00 1 SU - - culated_Ol202017.

12/0712016 - - zio

- - Oil and Grease 10/28/2016 - ND 1.4 No CDF _Ana lytical_Ca l M-005 11:50:00 1 - Annual ana lysis. cu lated_Ol202017.

- water El664A 11/09/2016 - mg/L

- - zip

- - Oi l and Grease 10/28/2016 - DNQ 2.1 1.4 No CDF_Analytical_Cal M-008

- water El664A 10:40:00 1 mg/L

- - Annua l ana lysis . culated_Ol202017 .

11/09/2016 - 5 zip

- - Oi l and Grease 10/28/2016 - DNQ 1.6 1.4 No CDF_Analytical_Cal M-009

- wa ter El664A 09:15:00 1 mg/ L Annua l ana lysis. cu lated_Ol202017.

11/.09/2016 - 5 zio

- - Oi l and Grease 10/28/2016 - ND 1.4 No CDF_Analytica l_Ca l M-013

- water El664A 11:30:00 1 mg/L

- - An nu al analys is. cu lated_Ol202017.

11/09/2016 - - zio

- - Oi l and Grease 10/28/2016 - DNQ 2.3 1.4 No CDF_A nalytica l_Ca l M-015

- wat er El664A 11:15:00 1 mg/L An nual ana lys is. cu lated_Ol202017.

11/09/2016 - 5 zip

- - Ammonia, Tota l (as N) 10/04/2016 - = 0.19 - No See Attachment 2, CDF_Analytical_Ca l M-INF 09:55:00 1 - culated_Ol202017.

- water A4500NH 10/14/2016 -

mg/L

- - Contract Lab Report zio

- - Arsenic, Total 10/19/2016 -

= 1.31 - No Annua l. See CDF_Analytical_Cal M-INF

- water E200.8 08:15 :00 1 ug/L - - Attachment 2, culated_Ol202017.

11/14/2016 - - Contract Lab Report. zip

- - Cadmium, Tota l 10/19/2016 - = 0.052 - No Annual. See CDF_Analytical_Ca l M-INF

- water E200.8 08:15:00 1 ug/L

- - Attachment 2, cu lated_Ol202017.

11/14/2016 - - Contract Lab Report. zip

- - Cyanide, Tota l (as CN) 10/19/2016 - ND

.0009 No Annual. See CDF_Analytica l_Cal M-I NF

- water E335.4 08:15:00 1 mg/L

- - Attachment 2, cu lated_Ol202017.

10/24/2016 - - Contract Lab Report. zip

- - Lead, Tota l 10/ 19/2016 - = 0.077 - No Annua l. See CDF_Analytica l_Ca l M-INF

- wa ter E200.8 08:15 :00 1 ug/L - - Attachment 2, cu lated_Ol202017.

11/14/2016 - - Contract Lab Report. zip

- - Mercury, Tota l 10/19/2016 - DNQ 0.34

.06 No Ann ual. See CDF_Ana lytica l_Ca l M-INF 08:15:00 1 - - Attachment 2, cu lated_Ol202017.

- water El631 10/25/2016 - ng/L

.5 Contract Lab Report. zio

- - PCB-1016 10/19/2016 - ND

.0094 No Annual. See CDF_Ana lytical_Ca l M-INF

- water SW8082 08:15:00 1 ug/L - - Attac hment 2, cu lated_Ol202017.

10/29/2016 - - Contract Lab Report. zip

- - PCB-1221 10/19/2016 - ND

.0094 No Annual. See CDF_Analytica l_Ca l M-INF 08:15:00 1 - Attachme nt 2, culated_Ol202017 .

- water SW8082 10/29/2016 - ug/L

- - Contract La b Reoort. zip

- - PCB-1232 10/19/2016 - ND

.0094 No Annua l. See CDF_Ana lytica l_Ca I M-INF

- wa ter SW8082 08 :1 5:00 1 ug/L - - Attac hment 2, cu lated_Ol202017.

10/29/2016 - - Contract Lab Report. zip

- - PCB-1242 10/ 19/2016 - ND

.0094 No Ann ual. See CDF _Ana lytica l_Ca l M-INF

- water SW8082 08: 15 :00 1 ug/L

- - Attachment 2, cu lated_Ol202017.

10/2912016 - - Contract Lab Report. zip Pa ge 6 of 32

Collection Sa mple Sample Date , Field Re p, MDL, Review Method, Type , Parameter, Sample Time, Lab Re p, Result, ML, Priority, Location Deoth (m) Matrix Analytical Method Analvsls Date Lab Batc h Units RL OA Codes Comments Dat a Source

- - PCB-1248 10/19/2016 - ND

.0094 No Annua l. See CDF_Analytica l_Cal M-INF

- water SW8082 08:15:00 1 ug/L

- - Attachment 2, cu lated_Ol202017 .

10/29/2016 - - Contract Lab Report. zip

- - PCB-1254 10/19/2016 - ND

.0094 No Annua l. See CDF_Analytica l_Ca l M-INF

- water SW8082 08 :15 :00 1 ug/L

- - Attachment 2, cu lated_Ol202017.

10/29/2016 - - Co ntract Lab Report. zip

- - PCB-1 260 10/19/2016 - ND

.0094 No Annua l. See CDF_Analytica l_Ca l M-INF water SW8082 08: 15:00 1 ug/L

- - Attac hm ent 2, culated_Ol202017.

10/29/2016 - - Co ntract Lab Repo rt . zip

- - pH 10/04/2016 - = 7.87

- No CDF_Analytica l_Ca l M-INF

- water A4500H 09:55:00 1 SU - - cu lated_Ol202017.

10/04/2016 - - zip

- - pH 11/03/2016 - = 8.07

- No CDF_Analytica l_Ca l M-INF 09:33:00 1 - cu lated_Ol202017.

- water A4500H 11/03/2016 - SU

- - zip

- - pH 12/08/2016 - =8

- No CDF_Analytical_Cal M-INF

- water A4500H 10:05:00 1 SU

- - cu lated_Ol2020 17.

12/08/2016 - - zip

- - Phenols, Ch lorinated 10/19/2016 - ND

.57 No Annua l. See CDF_Analytica l_Ca l M-INF

- water DU 08:15:00 1 ug/L - - Attachment 2, cu lated_Ol202017.

11/0112016 - - Contract Lab Report. zip

- - Pheno ls, Non-ch lorinated 10/ 19/2016 - ND 3.03 No Annua l. See CDF_Ana lytical_Cal M-INF

- water DU 08: 15:00 1 ug/L - - Attachme nt 2, cu lated_Ol202017.

11/0 112016 - - Contract Lab Report. zip

- - Si lver, Tota l 10/19/2016 - DNQ 0.018

.004 No Annua l. See CDF _Ana lytica l_Ca l M-INF

- water E200 .8 08: 15:00 1 ug/L

- - Attachment 2, cu lated_Ol202017.

11/14/2016 - .02 Contract Lab Report . zip

- - Titanium, Tota l 10/19/2016 - ND

.4 No Annual. See CDF_Analytica l_Ca l M-INF

- wate r DU 08:15:00 1 ug/ L - -

Attachment 2, cu lated_Ol202017.

11/18/2016 - - Contract Lab Report. zip Calc ulated Valu es Collection Sample Sample Date , Field Rep, MDL, Review Method, Type, Parameter, Sample Time, Lab Rep, Result , ML, Priority, Location Deoth !ml Matrix Ca lculation Tvoe Analvsis Date Lab Bat ch Units RL iOA Codes Comments Dat a Source

- - Ch lorine Usage 10/01/2016 - = 690

- No Monthly avg result. CDF_Analytica l_Ca l M-001

- water 30-Day Avg of Daily Avgs 00: 00 :00 1 lb/day

- - See Attac hment 1, cu lated_Ol202017 .

10/3 1/2016 - - Tab 2 zip

- - Ch lorine Usage 11/01/2016 - = 668 - No Monthly avg resu lt. CDF_A na lytica l_Ca l M-001

- water 30-Day Avg of Daily Avgs 00:00:00 1 lb/day

- - See Attachm en t 1. cu lated_Ol202017.

11/30/2016 - - Tab 3 zip

- - Chlorine Usage 12/01/2016 - = 372

- No Monthly avg resu lt. CDF_Ana lytical_Ca l M-001

- water 30-Day Avg of Da il y Avgs 00:00:00 1 lb/day - - See Attachment 1, cul ated_Ol202017 .

12/31/2016 - - Tab 4 zip

- - Chlorine, Tota l Residua l 10/01/2016 - = 13 - No Monthly avg resu lt. CDF_Ana lytical_Ca l M-001 00:00:00 1 - See Attachment 1, cu lated_Ol202017 .

- water 30-Day Avg of Dai ly Maxs ug/L -

10/31/2016 - - Tab 2 zip 11/01/2016 - - Monthly avg res ult. CDF_Analytica l_Ca l M-001

- - Ch lorine, Tota l Res idual 00 :00 :00 1

= 15

- No See Attachment 1, cu lated_Ol202017 .

- water 30-Da y Avg of Dai ly Maxs 11/30/2016 - ug/L

- - Tab 3 zip

- - Ch lorine, Tota l Residua l 12/01/2016 - = 23

- No Month ly avg result. CDF_Analytica l_Ca l M-001

- water 30-Day Avg of Da ily Maxs 00 :00 :00 1 ug/L See Attachment 1, cu lated_Ol202017.

12/03/2016 - - Tab 4 zip

- - Flow 10/01/2016 - = 2486

- No CDF_Analytical_Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD - -

cu lated_Ol202017 .

10/01/2016 - - zip

- - Flow 10/02/2016 - = 2486

- No CDF_Analytical_Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD

- - cu lated_Ol202017.

10/02/2016 - - zip Page 7 of 32

Collection Sa mpl e Sam ple Date, Field Re p, MDL, Review Met hod, T ype, Paramete r, Sample Time, Lab Rep, Result, ML, Priority, Locat ion Denth !ml Matri x Calculation Tvne Ana lvsls Date Lab Batch Units RL OA Codes Comments Dat a Source

- - Flow 10/03/2016 - - 2486 - No CDF Analytical Cal M-001

- water Dai ly Discharge 00 :00:00 1 MGD

- - culated 01202017.

10/03/2016 - - zip

- - Flow 10/04/2016 - - 2486

- No CDF Analytical Cal M-001 00:00:00 1 - cu lated 01202017.

- water Daily Discharge 10/04/2016 - MGD

- zip

- - Flow 10/05/2016 - - 2486

- No CDF Ana lytica l Ca l M-001

- water Daily Discha rge 00:00:00 1 MGD - - cu lated 01202017.

10/0512016 - - zip

- - Flow 10/06/2016 -

- 2486

- No CDF Ana lytica l Ca l M-001

- water Daily Discharge 00 :00 :00 1 MGD - - cu lated 01202017.

10/06/2016 - - zip

- - Flow 10/07 /2016 - - 2486

- No CDF Analytical Cal M-001

- water Dai ly Discharge 00:00 :00 1 MGD - - cu lated 01202017 .

10/07/2016 - - zip

- - Flow 10/08/2016 - - 2486

- No CDF Analytica l Cal M-001 00:00:00 1 - culated 01202017.

- water Daily Discharge 10/08/2016 -

MGD

- - zip

- - Flow 10/09/2016 - - 2486

- No CDF Analytical Cal M-001

- water Daily Discharge 00:00:00 1 MGD

- - culated 01202017.

10/09/2016 - - zip

- - Flow 10/10/2016 - - 2486

- No CDF Ana lytical Ca l M-001

- water Da il y Discha rge 00:00:00 1 MGD - - cu lated 01202017.

10110/2016 - - zip

- - Flow 10/11/2016 - - 2486

- No CDF Analytical Ca l M-001

- water Daily Discharge 00:00:00 1 MGD

- - cu lated 01202017.

10111/2016 - - zip

- - Flow 10/12/2016 -

- 2486

- No CDF Analytical Ca l M-001

- water Daily Discharge 00 :00:00 1 MGD - -

cu lated 01202017.

10/12/2016 - - zip

- - Flow 10/13/2016 - - 2486

- No CDF Ana lytical Ca l M-001

- wate r Daily Discharge 00:00:00 1 MGD cu lated 01202017.

10/13/2016 - - zip

- - Flow 10/14/2016 - - 2486 - No CDF Analytica l Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD cu lated 01202017.

10/14/2016 - - zip

- - Flow 10/15/2016 - - 2486

- No CDF Analytical Ca l M-001

- wate r Daily Discha rge 00:00:00 1 MGD cu lated 01202017 .

10115/2016 - - zip

- - Flow 10/16/2016 - - 2486

- No CDF Analytical Ca l M-001

- water Daily Discharge 00:00:00 1 MGD

- - culat ed 01202017 .

1011612016 - - zin

- - Flow 10/17 /2016 - - 2000 - No CDF Analytical Ca l M-001

- water Daily Discharge 00:00:00 1 MGD

- - cu lated 01202017.

10117/2016 - - zip

- - Flow 10/18/2016 - - 1891

- No CDF Analytical Ca l M-001

- water Daily Discharge 00:00 :00 1 MGD - - culated 01202017 .

10/1812016 - - zin

- - Flow 10/19/2016 - - 1933

- No CDF Ana lytica l Ca l M-001 00:00:00 1 - cu lated 01202017.

- water Daily Discha rge MGD

- zio 10/ 19/2016

- - Flow 10/20/2016 -

- 1874

- No CDF_Analytica l Ca l M-001

- water Dai ly Discharge 00:00 :00 1 MGD

- - cu lated_Ol202017 .

10/20/2016 - - zip

- - Flow 10/21/2016 - - 1874 - No CDF Analytical Ca l M-001 00:00:00 1 - cu lated 01202017.

- water Dai ly Discharge 1012112016 - MGD

- zio Page B of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time, Lab Rep, Result, ML, Priority, Location Deoth Im) Matrix Calculation Type Analysis Date Lab Batch Units RL IQA Codes Comments Data Source

- - Flow 10/22/2016 - 2450 No CDF Ana lytical Ca l M-001

- water Da il y Discharge 00 :00 :00 1 MGD

- - cu lated 01202017 .

10/22/2016 - - zip

- - Flow 10/23/2016 - 2486 - No CDF Ana lytica l Ca l M-001

- water Dai ly Discharge 00 :00 :00 1 MGD - - cu lated 01202017.

10/23/2016 - - zip

- - Flow 10/24/2016 - 2486

- No CDF Ana lytical Ca l M-001

- water Da il y Discharge 00:00:00 1 MGD cul ated 01202017.

10/24/2016 - - zip

- - Flow 10/25 /2016 - 2486

- No CDF Ana lytical Ca l M-001

- water Dai ly Discha rge 00:00 :00 1 MGD

- - cu lated 01202017 .

10/25/2016 - - zip

- - Flow 10/26/2016 - 2486

- No CDF Ana lytica l Ca l M-001

- water Daily Discharge 00:00:00 1 MGD

- - cu lated 01202017.

10/26/2016 - - zip

- - Flow 10/27 /2016 - 2486

- No CDF Analytical Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD

- - cul ated 01202017 .

10/27/2016 - - zip

- - Flow 10/28/2016 - 2486

- No CDF Analytical Ca l M-001 00 :00:00 1 - cu lated 01202017 .

- water Dai ly Discharge 10/28/2016 - MGD

- - zip

- - Flow 10/29/2016 - 2486

- No CD F Analytical Ca l M-001

- water Daily Discha rge 00:00:00 1 MGD - -

cu lated 01202017.

10/29/2016 - - zip

- - Flow 10/30/2016 - 2486

- No CDF Ana lytical Ca l M-001

- water Da il y Discharg e 00 :00:00 1 MGD

- - cu lat ed 012020 17.

10/30/2016 - - zip

- - Flow 10/3 1/20 16 - 2486

- No CDF Analytical Ca l M-00 1

- water Dai ly Discharge 00 :00:00 1 MGD - - cu lated 01202017 .

10/3112016 - - zip

- - Flow 11/01/2016 - 2486

- No CDF Analytical Ca l M-001

- water Dai ly Discha rge 00 :00:00 1 MGD

- - cul ated 012020 17 .

11/01/2016 - - zip

- - Flow 11/02/2016 - 2486

- No CDF Ana lytica l Ca l M-001

- water Daily Disc harge 00:00 :00 1 MGD - -

cu lat ed 01202017 .

11/02/20 16 - - zip

- - Flow 11/03/2016 - 2486 - No CDF Analytica l Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD

- - cu lated 01202017 .

11/03/2016 - - zip

- - Flow 11/04/20 16 - 2486 - No CDF Ana lytica l Ca l M-001

- water Da il y Disc harge 00:00:00 1 MGD

- - cu lated 01202017.

11104/2016 - - zip

- - Flow 11/05/2016 - 2486

- No CDF Ana lytica l Ca l M-001

- water Dai ly Discharg e 00:00:00 1 MGD

- - culated 012020 17.

11/05/2016 - - zip

- - Flow 11/06/2016 - 2486 - No CDF Ana lytical Ca l M-001 00 :00 :00 1 - culated 01202017.

- water Daily Discharge 11/06/2016 - MGD

- - zip

- - Flow 11/07/2016 - 2486

- No CDF Analytica l Ca l M-001

- water Da il y Disc harge 00:00:00 1 MGD

- - culated 01202017 .

11/07/2016 - - zip

- - Flow 11/08/2016 - 2486

- No CDF Ana lytica l Ca l M-001 water Dai ly Discharge 00:00 :00 1 MGD - - cul ated 01202017.

11/08/2016 - - zip

- - Flow 11/09/2016 - 2486

- No CDF Ana lytica l Ca l M-001

- water Dai ly Di scharg e 00:00 :00 1 MGD - - cul ated 01202017.

11/09/2016 - - zip Pa ge 9 of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time, Lab Rep, Result, ML, Priority, Location Denth Im) Matrix Calculation Tvoe Analvsis Date Lab Batch Units RL IOA Codes Comments Data Source

- - Flow 11/10/2016 - - 2192 - No CDF Ana lytica l Ca l M-001

- water Dai ly Discharge 00:00 :00 1 MGD - - cul at ed 01202017.

11/1012016 - - zip

- - Flow 11/11/2016 - - 2479

- No CDF Analytical Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD

- - cu lated 01202017.

11111/2016 - - zip

- - Flow 11/12/2016 - - 2486

- No CDF Ana lytica l Ca l M-001

- water Dai ly Discharge 00 :00:00 1 MGD

- - cu lated 01202017.

11/12/2016 - - zip

- - Flow 11/13/2016 - - 2486

- No CDF Analytica l Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD

- - cu lated 01202017 .

11/13/2016 - - zip

- - Flow 11/14/2016 - - 248 6

- No CDF Ana lytica l Ca l M-001

- water Daily Discharge 00:00:00 1 MGD

- cu lated 01202017.

11/14/2016 - - zip

- - Flow 11/15/2016 - - 2486

- No CDF Analytical Ca l M-001

- water Dai ly Discharge 00:00 :00 1 MGD

- - cu lated 01202017.

11/1 5/2016 - - zip

- - Flow 11/16/2016 - - 2486 No CDF Ana lytical Ca l M-001 00 :00 :00 1 - cu lated 01202017.

- water Da il y Discharge MGD -

1111612016 - - zip

- - Flow l l/l 7/2016 -

- 2486

- No CDF Ana lytica l Ca l M-001

- water Da ily Disc harge 00 :00:00 1 MGD

- - cu lated 01202017.

11/17/2016 - - zip

- - Flow 11/18/2016 -

- 2486

- No CDF Ana lytica l Ca l M-001

- water Dai ly Disc harge 00 :00:00 1 MGD

- - cu lated 01202017.

11/18 /2016 - - zin

- - Flow 11/19/2016 - - 2486

- No CDF Ana lytica l Ca l M-001

- water Dai ly Discharge 00 :00:00 1 MGD

- - cu lated_Ol202017.

11/19/2016 - - zio

- - Flow 11/20/2016 - - 2486

- No CDF Ana lytica l Ca l M-001

- water Daily Discharg e 00:00:00 1 MGD

- - cu lated 012020 17.

11/20/2016 - - zip

- - Flow 11/21/2016 - - 2486

- No CDF Analytica l Ca l M-001

- water Daily Discharge 00:00:00 1 MGD cu lated 01202017 .

11/21/2016 - - zip

- - Flow 11/22/2016 - - 2486

- No CDF Analytical Cal M-001

- water Daily Discharg e 00:00:00 1 MGD - -

culated 01202017.

11/2212016 - - zin

- - Flow 11/23/2016 - - 2486 No CDF Analytical Ca l M-001

- water Da ily Discharge 00:00:00 1 MGD

- - cu lated 01202017.

11123/20 16 - - zio

- - Flow 11/24/2016 - - 2486 - No CDF Analytica l Cal M-001

- water Daily Discharge 00 :00 :00 1 MGD

- - culat ed 01202017.

11124/2016 - - zio

- - Flow 11/25 /2016 - - 2486

- No CDF Ana lytica l Ca l M-001

- water Dai ly Discharge 00 :00:00 1 MGD

- - cu lated 01202017 .

11/25/2016 - - zin

- - Flow 11/26/2016 - - 2486

- No CDF Ana lytica l Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD

- - cu lated 01202017.

11/26/2016 - - zip

- - Flow 11/27 /2016 - - 2486 - No CDF Analytica l Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD

- - cu lated 01202017.

11/27/2016 - - zip

- - Flow 11/28/2016 - 2486

- No CDF Analytica l Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD

- - cu lated 01202017.

1112812016 - - zio Page 10 of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method , Type, Pa rameter, Sample Time, Lab Rep, Result, ML, Priority, Location Depth !ml Matri x Calculation T vpe Ana lvsls Date Lab Batch Units RL OA Codes Comments Data Source

- - Flow 11/29/2016 - 2486

- No CDF Analytica l Ca l M-001

- wa t er Dai ly Discharge 00:00:00 1 MGD

- - cu lated 01202017.

11/29L2016 - - zip

- - Flow 11/30/2016 - 2486

- No CDF Ana lytica l Ca l M-001

- wat er Dai ly Discha rge 00:00 :00 1 MGD

- - cu lated 01202017 .

11/30/2016 - - zip

- - Flow 12/ 01/20 16 - 2486

- No CDF Analytica l Ca l M-001

- water Da ily Disc harge 00:00:00 1 MGD culated 01202017.

12/01/2016 - - zip

- - Flow 12/02/2016 - 2486

- No CDF Analytica l Ca l M-001

- water Daily Discharge 00 :00 :00 1 MGD

- - cu lated 01202017 .

12/02/2016 - - zip

- - Flow 12/03/2016 - 2486

- No CDF Ana lytica l Ca l M-001

- wat er Dai ly Discharge 00 :00:00 1 MGD

- - cu lated 01202017.

12/ 03/2016 - - zip

- - Flow 12/04/20 16 - 2486

- No CDF Ana lytica l Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD cu lated 01202017.

12/04/2016 - - zip

- - Flow 12/05/2016 - 2486

- No CDF Analytica l Ca l M-001

- water Dai ly Discha rge 00:00 :00 1 MGD

- - cu lated 01202017.

12/0512016 - - zip

- - Flow 12/06/2016 - 2486

- No CDF Ana lytica l Ca l M-001

- wat er Dai ly Discharge 00 :00 :00 1 MGD culated 01202017.

12/06/2016 - - zip

- - Flow 12/07 /2016 - 2486

- No CDF Ana lyt ica l Ca l M-001

- water Dai ly Discha rge 00:00:00 1 MGD

- - cu lated 01202017.

12/07/2016 - - zip

- - Flow 12/08/2016 - 2486

- No CDF Ana lytica l Ca l M-001

- water Dai ly Discharge 00 :00:00 1 MGD

- - cu lated 01202017.

12/08/2016 - - zip

- - Flow 12/09/2016 - 2486

- No CDF Ana lytica l Ca l M-001

- wate r Dai ly Discharge 00:00:0 0 1 MGD

- - cu lated 01202017 .

12/09/2016 - - zip

- - Flow 12/10/2016 - 2486

- No CD F Ana lytica l Ca l M-001

- water Dai ly Discha rge 00:00:00 1 MGD

- - cu lated 01202017.

12/10/2016 - - zip

- - Flow 12/11/2016 - 2486

- No CDF Analytica l Cal M-001 00:00:00 1 - cu lated 01202017.

- wa ter Da ily Discharge 12/11/2016 -

MGD

- - zip

- - Flow 12/12/20 16 - 2486

- No CDF Analytica l Ca l M-001

- water Da ily Disc harg e 00:00:00 1 MGD

- - cu lated 01202017.

12/12 /2016 - - zip

- - Flow 12/ 13/2016 - 2486

- No CDF Ana lytica l Ca l M-001

- water Daily Discha rge 00:00:00 1 MGD cu lated 01202017.

12/13/2016 - - zip

- - Flow 12/14/2016 - 2486 - No CDF Analytical Cal M-001

- wat er Daily Discha rge 00:00:00 1 MGD cu lat ed 01202017.

12/14/2016 - - zip

- - Flow 12/1 5/2016 - 2486 - No CDF Analytica l Ca l M-001

- water Da il y Disc harge 00 :00:00 1 MGD

- - culated 01202017.

12/15/2016 - - zip

- - Flow 12/16/2016 - 2486

- No CDF Analytica l Cal M-001 water Dai ly Disc harge 00:00:00 1 MGD

- - cu lated 01202017 .

12/16/2016 - - zip

- - Flow 12/l 7 /2016 - 2486

- No CDF Ana lytica l Ca l M-001

- water Dai ly Disc harge 00:00:00 1 MGD cu lated 01202017.

12/17/2016 - - zip Page 11of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time, Lab Rep, Result, ML, Priority, Location Denth !ml Matrix Calculation Tvne Analvsis Date Lab Batch Units RL IOA Codes Comments Data Source

- - Flow 12/18/2016 - - 2486

- No CDF_Ana lytica l_Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD cu lated 01202017.

12/18/2016 - - zio

- - Flow 12/19/2016 - - 2486

- No CDF Analytica l Ca l M-001 00 :00 :00 1 - cu lated 01202017.

- water Dai ly Discharge 1211912016 - MGD

- - zio

- - Flow 12/20/2016 - - 2486

- No CDF Ana lytica l Ca l M-001 water Da il y Disc harge 00:00:00 1 MGD

- - cu lated 01202017.

12/20/201 6 - - zip

- - Flow 12/21/2016 - - 2486

- No CDF Ana lytica l Ca l M-001

- wat er Dai ly Discharge 00:00:00 1 MGD cu lated 01202017 .

12/2112016 - - zip

- - Flow 12/22/2016 - - 2486

- No CDF_Analytica l Ca l M-001

- water Daily Discha rge 00:00:00 1 MGD cu lated 01202017.

12/22/2016 - - zip

- - Flow 12/23/2016 - - 2486

- No CDF Analytical Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD - - cu lated 01202017 .

12/23/2016 - - zip

- - Flow 12/24/2016 - - 2486 - No CDF Ana lytica l Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD - - cu lated 01202017.

12/2412016 - - zip

- - Flow 12/25 /2016 - - 248 6

- No CDF Analytica l Ca l M-001

- water Dai ly Disc harge 00:00:00 1 MGD

- - cu lated 012020 17.

1212512016 - - zio

- - Flow 12/26/2016 - - 2486

- No CDF_Ana lytica l Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD

- - cu lated 01202017.

12 ' 2612016 - - zip

- - Flow 12/27 /2016 - - 2486 - No CDF Analytical Ca l M-001

- water Daily Discharge 00:00:00 1 MGD - -

culated 01202017.

12'27/2016 - - zio

- - Flow 12/28/2016 - - 2486

- No CDF Analytical Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD - - cu lated 01202017.

12/28/2016 - - zip

- - Flow 12/29/2016 - 2486

- No CDF Analytical Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD

- - cu lated 01202017.

12/29/2016 - - zip

- - Flow 12/ 30/2016 - - 2486

- No CDF Analytical Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD

- - cu lated 012020 17.

12'3 012016 - - zip

- - Flow 12/31/2016 - - 2486

- No CDF Ana lytica l Ca l M-001

- water Dai ly Discharge 00:00:00 1 MGD cu lated 01202017.

12/31/2016 - - zio

- - Tempe rature 10/01/2016 - - 74.2

- No CDF Ana lytical Ca l M-001 00:00:00 1 - culated 01202017.

- water 24-hour Average 10'0112016 - Degrees F

- - zin

- - Temperature 10/02/2016 - - 73.3 - No CDF Analytical Ca l M-001

- water 24-hour Average 00 :00:00 1 Degrees F

- - cu lated 01202017.

10102 /2016 - - zio

- - Temperature 10/03/2016 - - 72 .7

- No CDF_Ana lytica l Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F - - cu lated 012020 17 .

10/03/2016 - - zin

- - Temperature 10/04/2016 - - 73 .2

- No CDF Ana lyti ca l Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017 .

10/04/2016 - - zio

- - Temperature 10/05/2016 - - 72 .8

- No CDF Ana lytical Ca l M-001

- water 24-ho ur Average 00:00:00 1 Degrees F - - cul ated 01202017 .

10105/2016 - - zin Page 12 of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time, Lab Rep, Result, ML, Priority, Location Denth !ml Matrix Calculation Tvne Analvsis Date Lab Batch Units RL IOA Codes Comments Data Source

- - Temperature 10/06/2016 - - 72.5

- No CDF Analytica l Ca l M-001

- water 24-hour Average 00 :00 :00 1 Degrees F

- - cu lated 01202017.

10/06/2016 - - zip

- - Temperature 10/07/2016 - - 73 .3 - No CDF Analytica l Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F - - cu lated 01202017.

10/0712016 - - zip

- - Tempe rature 10/08/2016 - - 74.1

- No CDF Analytica l Ca l M-001

- water 24-hou r Average 00:00:00 1 Degrees F

- - cu lated 01202017.

10/0812016 - - zio

- - Temperature 10/09/2016 - - 75.7

- No CDF Analytica l Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017.

10/09/2016 - - zip

- - Temperature 10/10/2016 -

- 74.7

- No CDF Ana lytical Cal M-001

- water 24-hour Average 00 :00:00 1 Degrees F

- - cu lated 01202017.

10/10/2016 - - zip

- - Temperature 10/11/2016 - - 74.6

- No CDF Analytical Cal M-001

- water 24-hour Average 00:00:00 1 Degrees F cu lated 01202017 .

10/11/2016 - - zip

- - Temperature 10/12/2016 - - 75 .l No CDF Analytica l Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F - - cu lated 01202017.

10/12/2016 - - zip

- 10/13/2016 - - CDF Analytica l Ca l M-001 - Temperature 00 :00 :00 1

- 75.l No cu lated 01202017.

- water 24-hour Average 10/13/20 16 -

Degrees F

- - zip

- - Temperature 10/14/2016 -

- 75.8

- No CDF Ana lytica l Ca l M-001

- water 24-hour Average 00:00 :00 1 Degrees F

- - cu lated 01202017.

10114/2016 - - zip

- - Temperature 10/15/2016 - - 76.9

- No CDF Analytica l Cal M-001

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017 .

10/15/2016 - - zip

- - Temperature 10/16/2016 -

- 77.6

- No CDF Analytical Cal M-001

- water 24-hour Average 00 :00:00 1 Degrees F

- - cu lated 01202017.

10/16/2016 - - zip

- - Temperature 10/17 /2016 - - 78 .5

- No CDF Ana lytical Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F culated 01202017.

10/17/2016 - - zip

- - Temperature 10/18/2016 - - 76 .3

- No CDF Analytica l Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F - - cu lated 01202017.

1011 8/2016 - - zin

- - Temperature 10/19/20 16 - - 75.7 - No CDF Analytical Ca l M-001

- water 24-hour Average 00 :00:00 1 Degrees F

- - cu lated 01202017.

10119/2016 - - zio

- - Temperature 10/20/2016 - - 75.7

- No CDF Analytica l Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017 .

10/20/2016 - - zin

- - Temperature 10/21/2016 - - 76.2

- No CDF Ana lytica l Ca l M-001

- water 24-hour Average 00 :00:00 1 Degrees F

- - cu lated 01202017 .

10121/2016 - - zio

- - Temperature 10/22/2016 - - 74.6 No CDF Ana lytica l Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017.

10/22/2016 - - zip

- - Temperature 10/23/2016 -

- 75.3

- No CDF Analytica l Ca l M-001

- water 24-hou r Average 00:00 :00 1 Degrees F - - cu lated 01202017.

10/23/2016 - - zio

- - Tempe rature 10/24/2016 - - 76 .1

- No CDF Analytical Cal M-001

- water 24-hour Average 00:00:00 1 Degrees F - - cul ated 01202017 .

10/24/2016 - - zip Page 13 of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method, Type, Paramet er, Sample Time, Lab Rep, Result, ML, Priority, Location Denth !ml Matrix Calculation Tvne Analvsl!; Date Lab Batch Units RL nA Codes Comments Data Source

- - Temperature 10/25/2016 -

- 77.3

- No CDF Analytical Ca l M-001

- water 24-hour Average 00:00 :00 1 Degrees F - - cu lated 01202017.

10/25/2016 - - zip

- - Temperature 10/26/2016 - - 77.3

- No CDF_Analytica l Ca l M-001

- water 24-hour Average 00:00 :00 1 Degrees F

- - cu lated 01202017 .

10/26/2016 - - zio

- - Temperat ure 10/27/2016 - - 76 .7 - No CDF Analytica l Cal M-001

- water 24-hour Average 00:00:00 1 Degrees F - - cu lated 01202017.

10/27/2016 - - zip

- - Temperature 10/28/20 16 - - 77.4

- No CDF _Analytica l Ca l M-001 00:00:00 1 - cu lated 01202017.

- water 24-hour Ave rage 10/28/2016 - Deg rees F

- - zip

- - Temperatu re 10/29/2016 - - 78 .2

- No CDF Analytical Cal M-001

- water 24-hour Average 00 :00 :00 1 Degrees F

- - cu lated 01202017.

10/29/2016 - - zip

- - Temperature 10/30/2016 - - 78.6

- No CDF Ana lytica l Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F - - cu lated 01202017.

10/30/2016 - - zio

- - Temperatu re 10/ 31/2016 - - 78 .6 - No CDF Ana lytica l Ca l M-001

- water 24-ho ur Average 00:00:00 1 Degrees F

- - cu lated 01202017 .

10/3112016 - - zip

- - Tem perature 11/01/2016 - - 78

- No CDF Ana lytica l Ca l M-001

- water 24-hour Average 00:00 :00 1 Degrees F

- - cul ated 012020 17.

11101/2016 - - zip

- - Tempe rature 11/02/2016 - - 77.2

- No CDF Ana lytica l Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017.

11102/2016 - - zio

- - Temperature 11/03 /2016 - - 76.9

- No CDF Analytica l Ca l M-001 00:00 :00 1 - cu lated 01202017.

- water 24-hour Average 11103/2016 - Degrees F

- - zip

- - Temperat ure 11/04/2016 - - 77.4 - No CDF Analytica l Ca l M-001

- water 24-hour Ave rage 00 :00:00 1 Deg rees F

- - cu lated 01202017.

11/04/2016 - - zio

- - Temperature 11/05/2016 - 77.3

- No CDF Analytical Ca l M-001

- water 24-hour Ave rage 00:00:00 1 Degrees F

- - cu lated 01202017.

11/05/2016 - - zip

- - Temperature 11/ 06/2016 - - 76 .2

- No CDF Ana lytica l Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017.

11/0612016 - - zio

- - Temperatu re 11/07/2016 - - 76 .6

- No CDF Analytica l Ca l M-001

- water 24-ho ur Average 00:00:00 1 Degrees F - -

cu lated 01202017.

11/07/2016 - - zio

- - Tempe rature 11/08/2016 - - 77 .1

- No CDF Analytical Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F - -

cu lated 01202017 .

11/08/2016 - - zin

- - Temperat ure 11/09/2016 - - 76.8

- No CDF Analytical Ca l M-001

- water 24-hour Average 00:00 :00 1 Degrees F

- - cu lated 01202017 .

11109/2016 - - zio

- - Temperature 11/10/2016 - - 77.4 - No CDF Analytica l Cal M-001

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017 .

11/10/2016 - - zio

- - Tempe rature 11/11/2016 - - 77.3

- No CDF Ana lytica l Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017.

11/11/2016 - - zio

- - Tempe rature 11/12/2016 - - 77.1

- No CDF_Ana lytica l Ca l M-001

- wate r 24-hou r Average 00 :00 :00 1 Deg rees F - -

culated 01202017 .

11/12/2016 - - zin Page 14 of 32

Collect ion Sample Sample Date, Field Re p, MDL, Re view Method, Type, Parameter, Sample Time, Lab Rep, Result, ML, Priority, Location Deoth (ml Matrix Calculation Tvoe Analvs ls Date Lab Batch Units RL OA Codes Comments Data Source

- - Temperature 11/13/2016 - - 77.3

- No CDF Anal ytica l Ca l M-001

- water 24-hour Average 00 :00:00 1 Deg rees F

- - cu lated 01202017.

11113/2016 - - zip

- - Tempe rature 11/14/2016 - - 77 .3 - No CDF Analytical Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F

- - culated 01202017.

11/14/2016 - - zip

- - Temperature 11/15/2016 - - 77 .2

- No CDF Analyti ca l Ca l M-001

- water 24-hour Average 00 :00 :00 1 Degrees F

- - cu lated 01202017.

11/15/2016 - - zio

- - Tempe rature 11/16/2016 - - 75.9 - No CDF Ana lytica l Ca l M-001 00 :00:00 1 - cu lated 01202017.

- water 24-hour Average 11/16/2016 - Deg rees F

- - zip

- - Temperature 11/17/2016 - - 73.9 - No CDF Analytica l Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F - - cu lated 01202017.

11/17/2016 - - zip

- - Temperature 11/18/2016 - - 75

- No CDF Analytica l Ca l M-001

- water 24-hour Average 00:00 :00 1 Degrees F

- - cu lated 01202017 .

11/18/2016 - - zip

- - Temperature 11/19/2016 - - 75 .3 - No CDF Analytical Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017.

11/19/2016 - - zip

- - Tem perature 11/20/2016 - - 75.8 - No CDF Ana lytical Cal M-001

- water 24-hour Averag e 00 :00:00 1 Degrees F - - cu lated 01202017.

11/2012016 - - zip

- - Temperature 11/21/2016 - - 76.1 - No CDF Ana lytica l Ca l M-001

- water 24-ho ur Averag e 00:00:00 1 Degrees F - - cu lated 01202017.

11/2112016 - - zip

- - Temperature 11/22/2016 - - 76. 1

- No CDF Ana lytical Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F - -

cu lated 01202017.

11122/2016 - - zip

- - Temperature 11/23/2016 - - 75.7

- No CDF Analytical Ca l M-001

- water 24-h our Average 00:00:00 1 Degrees F cu lated 0120201 7.

11/23/2016 - - zip

- - Temperature 11/24/2016 - 75.7 - No CDF Analytical Ca l M-001 00:00 :00 1 - cu lated 01202017 .

- water 24-hour Average 11/24/2016 - Degrees F

- - zip

- - Tem perature 11/25/2016 - - 76.5

- No CD F Analytical Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F - - c u~ted 01202017.

11125 /2016 - - zip

- - Temperature 11/26/2016 - - 76.3

- No CDF Analytica l Ca l M-001 water 24-hour Average 00 :00 :00 1 Degrees F - - cul ated 012020 17.

11/26/2016 - - zip

- - Temperature 11/27 /2016 - - 75.7

- No CDF Ana lytica l Ca l M-001 00:00:00 1 - cu lated 01202017.

- water 24-hour Average 11/27/2016 - Degrees F

- - zio

- - Temperature 11/28/2016 - - 74.3

- No CDF Analytical Ca l M-001 00:00:00 1 - cu lated_Ol202017 .

- water 24-hour Average 11/28/2016 - Degrees F

- - zin

- - Temperature 11/29/2016 - - 73.4 - No CDF Analytica l Ca l M-001

- wate r 24-hour Average 00:00:00 1 Degrees F

- - culated 012020 17.

11/29/20 16 - - zio

- - Temperature 11/30/2016 - - 73 .6

- No CDF Analytica l Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017.

11/30/2016 - - zip

- - Temperature 12/01 /2016 - - 73.4

- No CDF Ana lytica l Ca l M-001

- water 24-hour Average 00 :00:00 1 Degrees F cu lated 01202017.

12101/2016 - - zin Page 15 of 32

Collection Sa mple Sample Date, Field Re p, MDL, Re view Method, Type, Parameter, Sample Time, Lab Rep, Result, ML, Priority, Locat ion De pth (m) Matrix Ca lculation Type Analysis Date Lab Batch Un it s RL !QA Codes Comments Dat a Source

- - Temperature 12/02/2016 - 73.4 - No CDF Analytical Ca l M-001 00:00:00 1 - cu lated 01202017.

- water 24-hour Average 12/02/2016 - Degrees F

- - zip

- - Temperature 12/03/2016 - 73.4

- No CDF Analytical_Cal M-001

- water 24-hour Average 00:00:00 1 Degrees F - - culated 01202017.

12/03/2016 - - zip

- - Temperature 12/04/2016 - 73.9

- No CDF Ana lytica l Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017.

12/04[2016 - - zip

- - Temperature 12/05/2016 - 73.3

- No CDF Analytica l Ca l M-001

- water 24-hour Average 00:00 :00 1 Degrees F - - cu lated 01202017 .

12/0512016 - - zip

- - Temperature 12/06/2016 - 72.9

- No CDF Analytical Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F - - cu lated 01202017.

12/06/2016 - - zip

- - Temperature 12/07 /2016 - 72.7

- No CDF Ana lytical Cal M-001 00:00:00 1 - cu lated 01202017.

- water 24-hour Average 12/07 /2016 -

Degrees F

- - zip

- - Temperature 12/08/2016 - 73.4 - No CDF Analytical Cal M-001

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017.

12/08/2016 - - zip

- - Temperature 12/09/2016 - 74.1

- No CDF Analytica l Ca l M-001

- water 24-ho ur Ave rage 00:00:00 1 Deg rees F

- - cu lated 01202017.

12/09/2016 - - zip

- - Temperature 12/10/2016 - 74.l

- No CDF Analytica l Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F cu lated 01202017 .

12/10/2016 - - zip

- - Temperature 12/11/2016 - 74.2

- No CDF Analytical Cal M-001

- water 24-hour Average 00:00:00 1 Degrees F - - cu lated 01202017 .

12/11/2016 - - zip

- - Temperature 12/12/2016 - 73 .8 No CDF Analytical Ca l M-001 00 :00 :00 1 - culated 01202017.

- water 24-hour Average 12/12/2016 - Deg rees F

- - zip

- - Temperature 12/13/2016 - 74.3 - No CDF Ana lytical Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017.

12/13/2016 - - zip

- - Temperature 12/14/2016 - 74.3

- No CDF Ana lytical Ca l M-001

- wate r 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017.

12/14/2016 - - zip

- - Tempe rat ure 12/ 15/2016 - 74.1

- No CDF Analytica l Ca l M-001 00 :00 :00 1 - cul ated 01202017.

- water 24-hour Average 12/15/2016 -

Deg rees F

- - zip

- - Temperature 12/16/2016 - 74

- No CDF Analytica l Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F

- - culated 01202017 .

lZ,116/2016 - - zip

- - Temperature 12/17/2016 - 72.6

- No CDF Ana lytical Ca l M-001

- water 24-hour Average 00:00:00 1 Degrees F culated 01202017.

12/17/2016 - - zip

- - Tempe rature 12/18/2016 - 72.9 - No CDF Analytical Ca l M-001 00 :00 :00 1 - - cu lated 01202017 .

- water 24-hour Average 12/18/2016 - Deg rees F

- zip

- Temperature 12/19/2016 - 73

- No CDF Analytica l Ca l M-001

- water 24-hour Ave rage 00:00:00 1 Degrees F - - cu lated 01202017.

12/19/2016 - - zip

- - Temperature 12/20/2016 - 73.4

- No CDF Ana lytica l Ca l M-001

- water 24-hour Ave rage 00:00:00 1 Degrees F - -

cu lated 01202017.

12/20/2016 - - zip Page 1 6 of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time, Lab Rep, Result, ML, Priority, Location Denth !ml Matrix Calculation Tvne Analvsis Date Lab Batch Units RL iOA Codes Comments Data Source

- Temperature 12/21/2016 - - 73

- No CD F Ana lytica l Ca l M-001

- water 24-hour Ave rage 00:00:00 1 Deg rees F

- - cu lated 01202017.

12/2112016 - - zip

- - Tempera ture 12/22/2016 - - 73. 1

- No CD F Analytical Ca l M-001

- water 24-hour Average 00 :00:00 1 Degrees F - - cu lated 01202017.

12122/2016 - - zip

- - Temperature 12/23/2016 - - 73 - No CDF Ana lytical Ca l M-001

- water 24~hour Average 00:00:00 1 Degrees F

- - culated 01202017.

12/23/2016 - - zip

- - Temperature 12/24/2016 - - 73.4

- No CDF Ana lytical Cal M-001

- water 24-hour Ave rage 00:00:00 1 Degrees F cu lated 01202017 .

1212412016 - - zio

- - Temperature 12/25/2016 - - 72 .7 - No CDF Ana lytica l Ca l M-001 water 24-h our Average 00:00.:00 1 Degrees F cu/ ated 01202017.

12/25/2016 - - zip

- - Tempe rature 12/26/2016 -

- 72 .6

- No CDF Analytica l Ca l M-001

- water 24-hou r Average 00:00:00 1 Deg rees F

- - cu lated 01202017.

12/26/2016 - - zip

- - Tempe rature 12/27/2016 -

- 72.4

- No CDF Analytical Ca l M-001 00 :00:00 1 - cu lated 01202017 .

- water 24-hou r Average 12/27 /2016 -

Degrees F - zip

- - Tempe rature 12/28/2016 - 72.7 No CDF Ana lytica l Ca l M-001 00:00:00 1 - culated 01202017.

- water 24-hour Average 12128/2016 - Degrees F

- - zip

- - Temperatu re 12/29/2016 - - 73 .3

- No CDF Ana lytica l Ca l M-001

- water 24-hour Ave rage 00:00:00 1 Deg rees F

- - cu lated 01202017 .

12129/2016 - - zip

- - Temperatu re 12/30/2016 - - 73.4

- No CD F Analytica l Ca l M-001

- water 24-ho ur Ave rage 00:00:00 1 Degrees F

- - cu lated 01202017.

12/3012016 - - zip

- - Temperature 12/31/2016 - - 73. 1

- No CDF Ana lytica l Ca l M-001

- water 24-hou r Average 00:00:00 1 Degrees F cu /ated 01202017.

12/31/2016 - - zip

- - Tempe rature 10/01/2016 - 78.6 - No CDF Analytical Ca l M-001

- water Daily Maximum 00 :00 :00 1 Degrees F

- - cul ated 01202017.

10/31/2016 - - zio

- - Tempe rature 11/01/2016 - - 78

- No CDF Analytica l Ca l M-001

- water Da il y Maximum 00:00 :00 1 Degrees F

- - cu lated 01202017.

11130/2016 - - zip

- - Temperatu re 12/01/2016 -

- 74.3

- No CDF Ana lytica l Ca l M-001

- water Dai ly Max imum 00:00:00 1 Deg rees F

- - cu lated 01202017.

12/31/2016 - - zio

- - Temperature 10/01/2016 - - 19 - No CDF Ana lytica l Ca l M-001

- water De lta f rom Background 00:00:00 1 Degrees F

- - cu lated 01202017.

1010112016 - - zin

- - Temperature 10/02/2016 - - 19.1

- No CDF Ana lytical Ca l M-001

- water De lta from Background 00:00:00 1 Degrees F - - culated 01202017.

10102/2016 - - zio

- - Tempe rature 10/03/2016 - - 19 No CDF Analytical Ca l M-001

- water De lta from Backgro und 00:00:00 1 Degrees F - - cul ated 01202017.

10/03/2016 - - zip

- - Tempe rature 10/04/2016 - - No CD F Ana lytica l Ca l

- 19 M-001

- water De lta from Background 00:00:00 1 Deg rees F

- - cul ated 01202017.

10/04/2016 - - zip

- - Tempe rature 10/05/20 16 -

- 19

- No CDF Analytica l Cal M-001

- water De lta from Background 00 :00 :00 1 Degrees F

- - cu lated 01202017 .

10/05/2016 - - zip Page 17 of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time, Lab Rep, Result, ML, Priority, Locat ion Denth !ml Matrix Ca lculation Tvne Analvsis Dat e La b Batch Units RL QA Code s Comments Dat a Source

- - Temperature 10/06/2016 - - 18.9

- No CDF Ana lytical Ca l M-001

- water De lta from Background 00:00:00 1 Degrees F

- - cu lated 01202017 .

10/06/2016 - - zip

- - Temperature 10/07 /2016 - - 19

- No CDF Ana lytica l Ca l M-001 00 :00 :00 1 - cu lated 01202017.

- water De lta from Background 10/07 /2016 - Degrees F

- - zip

- - Tempe rature 10/08/2016 - - 18.9

- No CDF Ana lytical Cal M-0 01

- water De lta from Background 00 :00 :00 1 Degrees F - - culated 01202017.

10/08/2016 - - zip

- - Tempera ture 10/09/2016 - - 19.4 - No CDF Ana lytical Ca l M-001

- water De lta f rom Bac kground 00 :00:00 1 Deg rees F

- - cu lated 01202017.

10/ 09/2016 - - zip

- - Temperature 10/10/2016 - - 18.8

- No CDF Analytical Cal M-001

- water Delta from Background 00:00:00 1 Degrees F - - cu lated 01202017 .

10/10/2016 - - zip

- - Temperature 10/11/2016 - - 19.l

- No CDF_Ana lytica l Ca l M-001

- water De lta from Background 00:00:00 1 Degrees F cu lated 01202017.

10/11/2016 - - zip

- - Tem perature 10/12/2016 - - 19.1

- No CDF Analytica l Ca l M-001

- 00: 00 :00 1 - cu lated 01202017.

water De lta from Background 10/12/2016 - Degrees F

- - zip

- - Tempe rature 10/13/2016 - - 18.9

- No CDF Ana lytica l Ca l M-001

- water De lta fro m Backgro und 00:00:00 1 Deg rees F

- - cu lated 01202017.

10/13 /2016 - - zip 10/14/2016 - - CDF Ana lytica l Ca l M-001

- - Tempe ratu re 00:00:00 1

- 19

- No cu lated 01202017 .

- water De lta from Background Degrees F -

10114/2016 - - zip

- - Temperature 10/15/2016 - - 19.2

- No CDF Ana lytical Ca l M-001

- water Delta from Background 00:00 :00 1 Deg rees F

- - culated 0120201 7.

10/15/2016 - - zip

- - Temperature 10/16/2016 - - 19.4 - No CDF Analytical Ca l M-001

- wate r De lta f rom Bac kground 00:00:00 1 Deg rees F

- - cu lated 01202017.

10/ 16/2016 - - zip

- - Temperature 10/l 7 /2016 - - 19.7 - No CDF Analytical Ca l M-001

- water De lta from Background 00:00:00 1 Degrees F - - cu lated 012020 17 .

10/l 7 /2016 - - zip

- - Tempe rature 10/1 8/2016 - - 19.8

- No CDF Ana lytica l Ca l M-001

- wate r De lt a f rom Background 00:00:00 1 Deg rees F - -

culated 01202017.

10/18/2016 - - zip

- - Tempe rature 10/19/2016 - - 19.4

- No CDF Analytical Ca l M-001 00 :00 :00 1 - culated 01202017.

- wa ter De lta from Backgrou nd 10119/2016 -

Deg rees F

- - zio

- - Temperature 10/20/2016 -

- 19.6

- No CDF Analytical Ca l M-001

- 00:00:00 1 - cu lated 01202017.

water De lta from Background 10120/2016 - Degrees F

- - zin

- - Tempera ture 10/21/2016 - - 19.7

- No CDF Analytica l Ca l M-001

- water Delta from Background 00:00:00 1 Degrees F - - cu lated 01202017 .

10/21/2016 - - zio

- - Temperature 10/22/2016 - - 18.6

- No CDF Analytica l Ca l M-001

- water Delta from Background 00:00:00 1 Degrees F

- - cu lated 012020 17.

10/22/2016 - - zin

- - Temperature 10/23/2016 - - 18.9

- No CDF Ana lytica l Ca l M-001 00:00:00 1 - cu lated 012020 17.

- water De lta from Bac kgroun d Degrees F -

10/23 /201 6 - - zio

- - Temperature 10/24/2016 - - 19

- No CDF Ana lytical Ca l M-001

- 00:00:00 1 - cu lated_Ol202017.

water De lta from Background

- Degrees F 10124/2016 ZIP Page 18 of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method, Ty pe, Parameter, Sample Time , Lab Rep, Resu lt, ML, Priority, Location Denth Im\ Matrix Ca lcu lation Tvoe Analvsis Date Lab Batch Units RL IQA Codes Comments Data Source

- - Temperature 10/25/2016 - - 19 - No CDF Analytical Ca l M-001

- water Delta from Background 00:00:00 1 Degrees F

- - cu lated 012020 17 .

10/25/2016 - - zip

- - Temperature 10/26/2016 - - 18.9

- No CDF Analytical Cal M-001

- water De lta from Background 00:00:00 1 Degrees F cu lated 01202017.

10/26/2016 - - zip

- - Te mperature 10/27/2016 - - 18.5

- No CDF Analytical Ca l M-001

- water De lta from Backgro und 00:00:00 1 Degrees F

- - culated 012020 17.

10/2712016 - - zip

- - Temperatu re 10/28/2016 - - 19.1 - No CDF_Analytica l Cal M-001

- water Delta from Background 00:00:00 1 Deg rees F

- - cu lated 01202017.

1012812016 - - zio

- - Temperature 10/29/2016 - - 19

- No CDF Analytical Cal M-001

- water Delta from Background 00:00:00 1 Degrees F

- - cu lated 01202017.

10/29/2016 - - zip

- - Temperature 10/30/2016 - = 19

- No CDF Analytica l Ca l M-001

- water De lta from Background 00:00:00 1 Degrees F

- - cu lated 01202017.

10/30/2016 - - zip

- - Tempe rature 10/31/2016 - - 19 - No CDF Analytical Ca l M-001 00:00:00 1 - culated 01202017.

- water De lta from Background 10/3112016 - Degrees F

- - zip

- - Temperature 11/01/2016 - - 18.9 - No CDF Analytica l Ca l M-001

- water De lta from Background 00 :00 :00 1 Deg rees F

- - cu lated 01202017 .

11/0112016 - - zio

- Temperature 11/02/2016 - - 19

- No CDF Analytical Ca l M-001

- water Delta from Background 00 :00:00 1 Degrees F

- - cu lated 01202017 .

11102/2016 - - zip

- - Temperature 11/03/2016 - - 18.9

- No CDF Analytical Cal M-001

- water Delta from Background 00:00:00 1 Degrees F cu lated 01202017 .

11103/2016 - - zip

- - Temperature 11/04/2016 - - 19.1

- No CDF Analytical Ca l M-001

- water De lta from Backgro und 00:00:00 1 Degrees F

- - cu lated 01202017 .

11/04/2016 - - zip

- - Temperature 11/05/2016 - - 19.1 - No CDF Analytica l Ca l M-001 00:00 :00 1 - culated 01202017 .

- water De lta from Background 11/05/2016 - Degrees F

- - zip

- - Tempe rature 11/06/2016 - - 18.9 No CDF Analytical Ca l M-001

- water De lta from Background 00 :00 :00 1 Deg rees F

- - cu lated 01202017 .

11/06/2016 - - zip

- - Tempe rature 11/07/2016 - - 19.1 - No CDF Analytical Ca l M-001

- water Delta from Backgro und 00:00:00 1 Degrees F

- - cu lated 01202017.

11/0712016 - - zio

- - Temperature 11/08/2016 - - 19.4

- No CDF Analytical Ca l M-001

- water De lta from Background 00:00:00 1 Degrees F

- - cu lated 01202017.

11108/2016 - - zio

- - Temperature 11/09/2016 - - 19.6 - No CDF Analytical Ca l M-001 00:00:00 1 - cu lated 01202017.

- water De lta from Background 11/09/2016 - Degrees F

- zio

- - Tempe rature 11/10/2016 - - 19.7

- No CDF Analytical Ca l M-001

- water De lta from Background 00 :00:00 1 Degrees F - - cu lated 01202617.

11/10/2016 - - zio

- - Temperature 11/11/2016 - - 19

- No CDF Analytica l Ca l M-001 water De lta from Background 00 :00:00 1 Degrees F

- - cu lated 01202017.

11/11/2016 - - zip

- - Temperatu re 11/12/2016 - - 19.1

- No CDF_Ana lytica l Ca l M-001

- water Delta from Background 00:00:00 1 Degrees F

- - cu lated 01202017 .

11/12/2016 - - zip Page 19 of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time, Lab Rep, Result, ML, Priority, Location Denth fml Matrix Calculation Tvoe Analvsis Date Lab Batch Units RL OA Codes Comments Data Source

- - Temperature 11/13/2016 - - 19.2 - No CDF Ana lytical Cal M-001

- water Delta from Background 00 :00:00 1 Degrees F - - cu lated 01202017 .

11/13/2016 - - zip

- - Temperature 11/14/2016 - - 19.1 - No CD F Ana lytica l Ca l M-001

- water Delta from Background 00:00:00 1 Degrees F - - culated 01202017 .

11/14/2016 - - zio

- - Temperature 11/15 /2016 - - 19.2

- No CDF Analytical Ca l M-001

- water Delta from Background 00:00:00 1 Deg rees F

- - cu lated 01202017 .

11/15/2016 - - zip

- - Temperature 11/16/2016 - - 19.2

- No CDF Ana lytica l Ca l M-001

- water Delta from Background 00:00:00 1 Degrees F

- - cu lated 012020 17.

11/16/2016 - - zip

- - Temperature 11/17 /2016 - - 18.8

- No CDF Ana lytica l Ca l M-001 water De lta from Background 00:00:00 1 Degrees F

- - cu lat ed 01202017.

11/17/2016 - - zip

- - Temperature 11/18/2016 - - 18.8

- No CDF Ana lytical Cal M-001

- water De lta from Background 00:00:00 1 Degrees F

- - cu lated 012020 17.

11/18/2016 - - zip

- - Tempe rature 11/19/2016 - - 18.9

- No CDF Ana lytica l Ca l M-001

- water De lta from Background 00:00:00 1 Degrees F culated 01202017.

11/19/2016 - - zip

- - Tempe rature 11/20/2016 - - 19

- No CDF Analytical Ca l M-001 00:00:00 1 - cu lated 01202017.

- water De lta from Background

- Degrees F

- - zip 11120/2016

- - Temperature 11/21/2016 - - 19.1 - No CD F Analytical Ca l M-001 00:00:00 1 - culated 01202017.

- water Delta from Background 11121/2016 - Degrees F

- - zio

- - Temperature 11/22/2016 - - 19

- No CDF Analytica l Ca l M-001

- water Delta from Background 00:00:00 1 Deg rees F

- - cu lated 012020 17 .

11122/2016 - - zip

- - Temperature 11/23/2016 - - 19 - No CDF Analytica l Ca l M-001

- water Delta from Background 00:00:00 1 Degrees F

- - cu lated 01202017 .

11/23/2016 - - zip

- - Temperature 11/24/2016 - 18.8

- No CDF Ana lytica l Ca l M-001

- water Delta from Background 00:00:00 1 Degrees F

- - cu lated 01202017.

11/24/2016 - - zio

- - Tempe rature 11/25/2016 - - 18.9

- No CDF Analytica l Ca l M-001

- water Delta from Background 00:00 :00 1 Degrees F

- - culated 01202017.

11/25/2016 - - zip

- - Temperature 11/26/2016 - - 18.9 - No CDF Analytical Ca l M-001

- water De lta from Background 00:00:00 1 Degrees F

- - cu lated 01202017.

11/26/2016 - - zin

- - Tempe rature 11/27/2016 - - 18.9

- No CDF Analytical Ca l M-001

- water De lta from Background 00:00:00 1 Degrees F

- - cu lated 012020 17 .

11/27 /2016 - - zio 11/28/2016 - - CDF Analytica l Ca l M-001 - - Temperature 00:00:00 1

- 19

- No cu lated 01202017.

- water De lta from Background 11128/2016 -

Deg rees F

- - zio

- - Temperature 11/29/2016 - - 18.8

- No CDF Analytica l Ca l M-001

- water Delta from Background 00:00 :00 1 Degrees F

- - cu lated 01202017.

11/29/2016 - - zip

- - Temperature 11/30/2016 - - 18.9

- No CDF Analytica l Ca l M-001

- water Delta from Background 00:00:00 1 Degrees F

- - cu lated 01202017.

11/30/2016 - - zip

- - Temperature 12/01/2016 - - 18.8 - No CDF Analytical Ca l M-001

- water Delta from Background 00:00:00 1 Degrees F

- - cu lated 01202017.

12/01/2016 - - zip Page 20 of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time, Lab Rep, Result, ML, Priority, Location Depth !ml Matrix Calculation Type Analysis Date Lab Bat ch Units RL QA Codes Comments Dat a Source 12/02/2016 - - CDF Analytical Ca l M-001 - - Temperature 00:00:00 1 18.7

- No cu lated 01202017.

- wate r De lta fro m Backgro und 12/0212016 - Degrees F

- - zip 12/03/2016 - - CDF Ana lytical_Ca l M-001 - - Tem perature 00:00 :00 1 18.7 No cu lated 01202017 .

- water De lta from Backgro und 12/03/2016 - Degrees F

- - zip

- - Tempe rature 12/04/201 6 - 18.B

- No CDF Ana lytica l Ca l M-001 00 :00 :00 1 - cul at ed 01202017.

- water Delta from Backgrou nd 12/04/2016 - Degrees F

- - zip

- - Temperature 12/05/2016 - 18.8 - No CDF Ana lytica l Ca l M-001

- wate r De lta from Background 00:00:00 1 Degrees F

- - cu lated 01202017 .

12/05/2016 - - zip

- Tem perature 12/06/2016 - 18.9 - No CDF Ana lytica l Ca l M-001

- wate r De lta f ro m Bac kgroun d 00:00:00 1 Degrees F

- - cu lated 012020 17.

12/06/2016 - - zip

- - Tempera ture 12/07 /2016 - 18.8

- No CDF Ana lytica l Ca l M-001

- water Delta from Backgrou nd 00 :00 :00 1 Deg rees F

- - culat ed 01202017.

12/07/2016 - - zip

- - Temperature 12/08/2016 - 18.9 - No CD F Ana lytical Ca l M-001 00:00:00 1 - cu lated 01202017.

- wate r De lta from Bac kground 12/08/2016 - Degrees F

- - zip

- - Tem peratu re 12/09/2016 - 19.l

- No CDF Analytica l Ca l M-001

- wat er De lta fro m Bac kgroun d 00:00 :00 1 Degrees F

- - cul ated 012020 17.

12/09/2016 - - zip

- - Tempera ture 12/10/2016 - 19.1 - No CDF Analytical Ca l M-001

- water De lta from Backgrou nd 00:00:00 1 Deg rees F

- - culated 01202017.

12/10/2016 - - zip

- - Temperature 12/11/2016 - 19.l

- No CDF Ana lytical Ca l M-001

- water Delta f rom Bac kground 00 :00 :00 1 Degrees F

- - cu lated 01202017.

12/11/2016 - - zip

- - Tem perat ure 12/12/2016 - 19. 1

- No CDF Ana lytica l Ca l M-001

- wat er De lta f ro m Bac kground 00:00:0 0 1 Degrees F

- - culated 012020 17.

12/12/2016 - - zip

- - Tempe rature 12/ 13/2016 - 19

- No CDF Analytical Ca l M-001

- water De lta fro m Background 00:00:00 1 Degrees F

- - culated 01202017.

12/13/2016 - - zip

- - Tempera ture 12/14/2016 - 19

- No CDF Analytica l Cal M-001

- water De lta from Background 00:00 :00 1 Degrees F

- - cu lated 01202017.

12/14/2016 - - zip 12/ 15/2016 - - CDF Ana lyt ical Ca l M-001 - - Temperature 00:00:0 0 1 18.9

- No cu lated 012020 17.

- water De lta fro m Backgro und 12/15/2016 - Degrees F

- - zip

- - Tempera t ure 12/16/2016 - 18.9 - No CDF Analytical Ca l M-001 00:00 :00 1 - cu lated 01202017.

- wate r De lta from Background 12/16/2016 -

Deg rees F

- - zip 12/17/2016 - - CDF Analytica l Ca l M-001

- - Tempera ture 00 :00:00 1 18.7

- No culated 01202017.

- water De lta fro m Bac kground 12/1712016 - Deg rees F

- - zip

- - Temperat ure 12/ 18/2016 - 18.6

- No CDF Analytica l Ca l M-001

- water Delta from Bac kground 00:00:00 1 Degrees F

- - cu lated 01202017.

12/18/2016 - - zip 12/19/2016 - - CDF Analytical Ca l M-001 - - Temperature 00 :00 :00 1 18.6 No culated 01202017.

- water De lta from Background 12/19/2016 - Degrees F

- - zip

- - Tem perature 12/20/2016 - 18.7

- No CDF Analytica l Ca l M-001

- water De lt a fro m Bac kground 00:00:00 1 Deg rees F - - cu lated 01202017 .

12/20/2016 - - zip Page 2 1of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time, Lab Rep, Result, ML, Priority, Location Denth lml Matrix Calculation Tvne Analvsls Date Lab Batch Units RL IOA Codes Comments Data Source

- - Temperature 12/21/2016 - - 18.6

- No CDF_Analytica l Ca l M-001

- water Delta from Background 00:00:00 1 Degrees F

- - culated 01202017.

12/2112016 - - zip

- - Temperature 12/22/2016 - - 18.7

- No CDF Analytical Cal M-001

- water Delta from Background 00:00:00 1 Degrees F

- - cu lated 01202017 .

12/22/2016 - - zio

- - Tempe rature 12/23/2016 - - lB.B

- No CDF Ana lytica l Ca l M-001

- water De lta from Background 00:00:00 1 Degrees F

- - cu lated 01202017 .

12/23/2016 - - zip

- - Temperature 12/24/2016 - - lB.6

- No CDF Ana lytica l Ca l M-001

- water De lta from Background 00:00:00 1 Degrees F - -

cu lated 01202017 .

12/2412016 - - zip

- - Temperatu re 12/25/2016 - - lB .7

- No CDF Ana lytical Ca l M-001

- water De lta from Background 00:00:00 1 Degrees F

- - cu lated 01202017 .

12/25/2016 - - zip

- - Temperature 12/26/2016 - - 18.7

- No CDF _Ana lytica l Ca l M-001

- water De lta from Background 00:00:00 1 Degrees F

- - cu lated 01202017.

12/26/2016 - - zip

- - Temperature 12/27 /2016 - - 18.6

- No CDF Analytical Cal M-001 00:00:00 1 - cu lated 01202017 .

- water De lta from Background 12/2712016 - Degrees F

- - zip 12/28/2016 - - CDF Analytica l Cal M-001 - - Temperature 00:00:00 1

- 18.6

- No cu lated 01202017.

- water De lta from Background 12/2B/2016 - Degrees F

- - zip

- - Temperatu re 12/ 29/2016 - - lB.7

- No CDF Ana lytica l Ca l M-001

- water Delta from Background 00:00:00 1 Degrees F - - cu lated 01202017 .

1212912016 - - zip

- - Temperature 12/30/2016 - - 18.7 - No CDF Ana lytical Ca l M-001

- water Delta from Background 00:00:00 1 Degrees F cu lated 01202017.

12130/2016 - - zip

- - Temperature 12/31/2016 - - lB .7 - No CDF Analytical Cal M-001

- water De lta from Background 00:00:00 1 Degrees F

- - cu lated 01202017.

12/31/2016 - - zio

- - Temperature 10/01/2016 - - 75.6

- No CDF Analytica l Ca l M-001

- water Mthly Avg of Daily Avgs 00:00:00 1 Degrees F

- - culated 01202017.

10/31/2016 - - zip

- Temperature 11/01/2016 - - 76.2 - No CDF Analytica l Ca l M-001

- water Mthly Avg of Dai ly Avgs 00:00:00 1 Degrees F

- - cu lated 01202017 .

11130/2016 - - ziD

- - Temperature 12/01/2016 - - 73.4

- No CDF Analytica l Ca l M-001

- water Mthly Avg of Dai ly Avgs 00:00:00 1 Degrees F

- - cul ated 01202017 .

1213112016 - - zio

- - Cadmium, Tota l 10/04/2016 - DNQ 0.22

.043 No See Attachment 2, CDF Analytical Ca l M-0010

- water 90-Day Mean 00 :00 :00 1 ug/L - - Contract Lab Report cu lated 01202017 .

11128/2016 - .5 zip

- - Chromium (Total) 10/04/2016 - -3 - No See Attachment 2, CDF Analytical Cal M-0010 water 90-Day Mean 00:00:00 1 ug/L

- - Contract Lab Report cu lated 01202017.

11/2812016 - - zio

- - Copper, Tota l 10/04/2016 - DNQ 2.9

.5 No See Attachment 2, CDF_Ana lytica l Ca l M-0010

- water 90-Day Mean 00:00:00 1 ug/L - - Contract Lab Report cu lated 01202017.

11/28/2016 - 5 zip

- - Lead , Total 10/04/2016 - - O.Bl - No See Attachment 2, CDF Ana lytica l Ca l M-0010 00:00:00 1 - cu lated 01202017.

- water 90-Day Mean ug/L

- Contract Lab Report zio 11/28/2016

- - Mercury, Tota l 10/04/2016 - ND

.08 No See Attachment 2, CDF _Analytical Ca l M-0010

- water 90-Day Mean 00:00 :00 1 ug/L

- - Contract Lab Report cul ated 01202017 .

11128/2016 - - zio Page 22 of 32

Collect ion Sam ple Sample Date, Field Rep, MDL, Review Method, Type, Pa rameter, Sample Time, Lab Rep, Result, ML, Priority, Location Deoth !ml Matrix Calculation Tvoe Analvsls Date Lab Batch Units RL OA Codes Comments Data Source 10/04/2016 - .4 CDF _Ana lytica l_Ca l M-OOlD

- - Ni cke l. Tota l 00:00:00 1 DNQ 1.8

- No See Attachment 2, cu lated_Ol202017.

- water 90-Day Mean 11/2812016 - ug/L 5

- Contract Lab Report zip

- - Oi l and Grease 10/11/2016 - DNQ 1.4 1.4 No Quarte rly avg res ult. CDF_Analytica l_Cal M-OOlD 00 :00:00 1 - See Att . 1, Tabs 1, cu lated_Ol202017 .

- water 90-Day Mean 1212112016 - mg/L 5

- 5, 6, 7 zio

- - Si lver, Total 10/04/2016 - DNQ 0.12

.1 No See Attachment 2, CDF_Analytica l_Ca l M-OOlD

- water 90-Day Mea n 00:00:00 1 ug/L

- - Contract Lab Report cu lated_Ol202017.

11/2812016 - 1 zio

- - Total Suspended So lids (TSS) 10/11/2016 - <5 - No Monthly avg resu lt. CDF_Ana lytica l_Ca l M-OOlD 00:00 :00 1 - - See Attachment 1, cu lated_Ol202017 .

- water 30-Day Avg of Dai ly Avgs 10/2712016 - mg/L

- Tab 5 ziD

- - Tota l Suspended So li ds (TSS) 11/03/2016 - <5

- No Monthly avg resu lt. CDF_Analytica l_Ca l M-OOlD

- water 30-Day Avg of Daily Avgs 00 :00:00 1 mg/L

- - See Attachment 1, cu lated_Ol202017.

11/23/2016 - - Tab 6 zip

- - Tota l Suspended So lids (TSS) 12/13/2016 - <5

- No Monthly avg result. CDF_Ana lytica l_Ca l M-OOlD 00:00 :00 1 - See Attachment 1. cu lated_Ol202017.

- water 30-Day Avg of Dai ly Avgs 12/21/2016 - mg/L

- - Tab 7 zip

- - Zinc, Tota l 10/04/2016 - = 59

- No See Attachment 2, CDF_Ana lytica l_Ca l M-OOlD 00:00:00 1 - - cu lated_Ol202017 .

- water 90-Day Mean 11/2812016 - ug/L Contract Lab Report zio 10/02/2016 - 5 CDF_Analytica l_Ca l M-OOlF

- - Cadmi um , Tota l 00 :00:00 1 ND

- No culated_Ol2020 17.

- water 7-Day Average (Mean) 10109/2016 - ug/L

- - zi n

- - Chromium (Tota l) 10/02/2016 - = 38.6

- No CDF_Ana lytical_Ca l M-OOlF

- water 7-Day Average (Mean) 00 :00:00 1 ug/L

- - culated_Ol202017.

10109/2016 - - ziD

- - Coppe r, Tota l 10/02/2016 - = 13 .9

- No CDF_Ana lytical_Ca l M-OOlF

- water 7-Day Average (Mean) 00:00:00 1 ug/L

- - cu lated_Ol202017.

10/09/2016 - - zio

- - Lead, Tota l 10/02/2016 - = 19.9 - No CDF _Ana lytica l_Ca l M-OOlF 00:00:00 1 - - cu lated_Ol202017.

- water 7-Day Average (M ea n) 10/09/2016 -

ug/L

- zio 10/02/2016 - .08 CDF_Analytica l_Ca l M-OOlF - - Merc ury, Tota l 00:00 :00 1 ND

- No See Attachment 2, cu lated_Ol202017.

- water 7-Day Average (Mean) 10/09/2016 - ug/L

- - Contract Lab Report zio

- - Nickel, Tota l 10/02/2016 - = 45 .9

- No CDF_Analytica l_Ca l M-OOlF 00:00 :00 1 - cu lated_Ol202017.

- water 7-Day Average (M ean) 1010912016 - ug/L

- - zip 10/02/2016 - 5 CDF_Ana lytica l_Ca l M-OOlF - - Silver, Total 00:00:00 1 ND

- No cu lated_Ol202017 .

- water 7-Day Average (Mean) 10/09/2016 - ug/L

- - zio

- - Tota l Sus pended So lids (TSS) 12/01/2016 - =6

- No Monthly avg resu lt. CDF _Analytica l_Ca l M-OOlF

- water 30-Day Avg of Dai ly Avgs 07 :37 :00 1 mg/L - - See Atta chment 1, cu lated_Ol202017.

12/0112016 - - Tab 13 zio

- - Tota l Suspend ed So lids (TSS) 10/03/2016 - DNQ 3 2

No Monthly avg resu lt. CDF_Analytica l_Ca l M-OOlF

- water 30-Day Avg of Da ily Avgs 16:00:00 1 mg/L

- - See Attachment l, cu lated_Ol202017.

10/0412016 - 5 Tab 11 zio

- - Total Suspended So lids (TSS) 11/03/2016 - DNQ 2 2

No Monthly avg result. CDF_Ana lytica l_Ca l M-OOlF 07:20:00 1 - See Attachment 1, cu lated_Ol202017.

- water 30-Day Avg of Dai ly Avgs 11/03/2016 - mg/L 5

- Tab 12 zio

- - Zinc, Tota l 10/02/2016 - = 16.8

- No CDF_Analytical_Cal M-OOlF water 7-Day Average (Mean) 00:00:00 1 ug/L

- - culated_Ol202017.

10/09/2016 - - zip

- Cadmium, Tota l 10/03/2016 - ND 5

No Avg of qtrly CDF_Analytical_Ca l M-OOlH

- water 90-Day Mean 00:00 :00 1 ug/L

- - composites. See Att cu lated_Ol202017.

12/06/2016 - - 1, Tab 1 zip Page 23 of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time , Lab Re p, Result, ML, Priority, Locat ion Deoth Im\ Matrix Calculation T voe Analvsls Date Lab Batch Units RL OA Codes Comments Data Source

- - Chromium (Total) 10/03/2016 - = 24 - No Avg of qt rly CDF_Ana lytica l_Ca l M-OOlH

- water 90-Day Mean 00:00:00 1 ug/L

- - composites . See Att cu lated_Ol202017 .

12/06/2016 - - 1, Tab 1 zip

- - Copper, Tota l 10/03/2016 - = 29 - No Avg of qtrly CDF_Ana lytical_Ca l M-OOlH

- water 90-Day Mea n 00:00:00 1 ug/L - - composites . See Att cu lated_Ol202017.

12106/2016 - - 1, Tab 1 zio

- - Lead, Total 10/03/2016 - = 24 - No Avg of qtrly CDF_Analytica l_Ca l M-OOlH

- water 90-Day Mea n 00:00:00 1 ug/L - - composit es . See Att cul ated_Ol2020 17.

1210612016 - - 1, Tab 1 zip

- - Mercury, Tot al 10/03/2016 - ND

.08 No Qtrly avg - Att 1 Tab CDF_Ana lytica l_Ca l M-OOlH

- water 90-Day Mean 00:00:00 1 ug/L

- - 1 & Att 2 Contract cu lated_Ol202017.

12/06/2016 - - Lab Report zip

- - Nickel, Tota l 10/03/2016 - = 16 - No Avg of qtrl y CDF_Analytical_Cal M-OOlH

- water 90-Day Mean 00 :00:00 1 ug/L

- - compos ites. See Att cu lated_Ol202017 .

12/06/2016 - - 1, Tab 1 zip

- - Oi l and Grease 10/02/2016 - ND 1.4 No Avg res ult for qtrl y CDF_Ana lytica l_Ca l M-OOlH 00:00:00 1 - samp les. See Att 1, cu lated_Ol202017.

- water 90-Day Mean 10/02/2016 - mg/L

- - Tab 1 zio

- - Silver, Tota l 10/03/2016 - ND 5

No Avg of qtrly CDF_Ana lytica l_Ca l M-OOlH

- water 90-Day Mean 00:00:00 1 ug/L

- - composites. See Att culated_Ol202017 .

1210612016 - - 1. Tab 1 zip 10/02/2016 - 2 Mont hly avg res ult. CDF_Analytical_Ca I M-OOlH - - Tota l Suspended So lids (TSS) 00 :00:00 1 ND

- No See Attac hment 1, culated_Ol202017.

- wa ter 30-Day Ave rage 10102 12016 - mg/L

- - Tab 11 zip

- - Tota l Suspended So lids (TSS) 11/01/2016 - DNQ 2 2

No Monthly avg res ul t. CDF _Analytica l_Ca l M-OOlH

- water 30-Day Avg of Da il y Avg s 00:00:00 1 mg/L

- - See Atta chment 1, culated_Ol202017.

1110212016 - 5 Tab 12 zio

- - Tota l Suspended So lids (TSS) 12/01/2016 - ND 2

No Mont hly avg result. CDF_Ana lytical_Ca l M-OOlH

- water 30-Day Avg of Dai ly Avgs 00:00:00 1 mg/L See Attachment 1, cu lated_Ol202017 .

12101/2016 - - Tab 13 zip

- - Zinc. Tota l 10/03/2016 - < 10

- No Avg of qtrly CDF_Ana lytica l_Ca l M-OOlH

- wat er 90-Day Mean 00:00:00 1 - - composites. See Att cu lated_Ol20201 7.

ug/L 12/06/2016 - - 1, Tab 1 zip

- - Cadmi um . Tota l 10/05/2016 - ND 5

No Avg of qtrly CDF_Analytical_Ca I M-OOlL

- water 90-Day Mean 00 :00 :00 1 ug/L

- - composit es . See Att culated_Ol 202017.

12/0712016 - - 1, Tab 1 zio 10/05/2016 - 5 Avg of qtrly CDF_Analytica l_Ca l M-OOlL - - Chrom ium (Tota l) 00 :00:00 1 ND

- No com posit es. See Att cu lated_Ol202017.

- water 90-Day Mea n 12107/2016 - ug/L

- - 1, Ta b 1 zip

- - Cop per. Tot al 10/05 /2016 - = 11 - No Avg of qtrly CDF_Ana lytica l_Ca l M-OOlL

- water 90-Day Mea n 00:00:00 1 ug/L - - com pos ites. See Att culated_Ol202017.

12107 12016 - - 1, Tab 1 zio

- - Lead, Tota l 10/05/2016 - ND 5

No Avg of qtrly CDF_Ana lytical_Ca l M-OOlL

- water 90-Day Mean 00:00 :00 1 ug/L composites . See Att cu lated_Ol202017 .

12/07 /2016 - - 1, Tab 1 zip

- - Mercury, Tota l 10/05/2016 - ND

.08 No Qtrly avg - Att 1 Tab CDF _Analytical_Ca l M-OOlL

- water 90-Day Mean 00:00:00 1 ug/L

- - 1 & Att 2 Contract cu lated_Ol202017.

1210712016 - - Lab Reoort zio

- - Ni cke l. Total 10/05/2016 - ND 5

No Avg of qtrly CDF_Ana lytica l_Ca l M-OOlL

- water 90-Day Mean 00 :00 :00 1 ug/L

- - com pos ites. See Att cul ated_Ol20201 7.

12/0712016 - - 1, Tab 1 zip

- - Oi l and Grease 10/03/2016 - ND 1.4 No Avg resu lt for qtrly CDF_Ana lytical_Ca l M-OOlL water 90-Day Mea n 00:00:00 1 mg/L

- - samp les. See Att 1, cu lated_Ol202017.

10/03/2016 - - Tab 1 zip

- - Si lver. Tota l 10/05/2016 - ND 5

No Avg of qtrly CDF_Ana lytica l_Ca l M-OOlL

- water 90-Day Mea n 00:00:00 1 ug/L - -

com pos ites. See Att cu lated_Ol202017.

12/07 /2016 - - 1, Tab 1 zip Page 24 of 32

Collection Sa mple Sample Date, Field Re p, MDL, Review Method, Type, Paramet e r, Sample Time, Lab Rep, Result, ML, Priority, Locat ion Deoth fml Matrix Calculation Tvoe Analvsls Date La b Batch Un its RL OA Codes Comments Dat a Source

- - Total Suspended Solids (TSS) 10/03/2016 - 2 Monthly avg resu lt. CDF_Ana lyti cal_Ca l M-OOlL ND No 00:00:00 1 - See Attachment 1, culated_Ol202017.

- water 30-Day Avg of Dai ly Avgs 1010312016 - mg/L

- - Tab 11 zip

- - Tota l Suspen ded Solids (TSS) 11/02/2016 - ND 2

No Monthly avg resu lt. CDF_Analytica l_Ca l M-OOlL

- water 30-D ay Avg of Dai ly Avgs 00 :00 :00 1 mg/L

- - See Attachment 1, cu lated 01202017 .

11/02/2016 - - Tab 12 zio

- - Total Suspen ded Solids (TSS) 12/05/2016 - 2 Monthly avg resu lt. CDF_Analytica l_Ca l ND No M-OOlL

- water 30-Day Avg of Dai ly Avgs 00:00:00 1 mg/L

- - See Attachment 1, cu lated_Ol2020 17.

12/0512016 - - Tab 13 zio

- - Zinc, Total 10/05/2016 - ND 5

No Avg of qtrly CDF_Analytica l_Ca l M-OOlL

- water 90-Day Mea n 00:00:00 1 ug/L

- - com posites . See Att cul ated_01202017 .

12/07/2016 - - 1, Tab 1 zio

- - Oi l and Grease 10/04/2016 - ONO 0.24

.24 No Monthly avg - Att 1 CDF_Ana lytica l_Ca l M-OOlN

- water 30-Day Avg of Dai ly Avgs 00:00:00 1 mg /L - - Tab 8 & Att 2 Contr. culated_Ol202017.

10/25/2016 - 5 Lab Rpt. zip

- - Oi l and Grease 11/02/2016 - ONO 0 .24

.24 No Monthly avg - Att 1 CDF _Ana lytical_Ca l M-OOlN 00:00:00 1 - Tab 9 & Att 2 Contr. cu lated 01202017.

- water 30-Day Avg of Daily Avgs 11/21/2016 - mg/L 5

- Lab Rot. zip

- - Oi l and Grease 12/01/2016 - ONO 1.1 1.1 No Monthly avg - Att 1 CDF_Analytica l_Ca l M-OOlN

- water 30-Day Avg of Daily Avgs 00:00 :00 1 mg/L

- - Tab 10 & Att 2 cu lated 01202017.

12127 /2016 - 5 Co ntr. Lab Rot. zio

- - Settlea ble So lids 10/04/2016 -

< 0.1

- No Monthly avg - Att 1 CDF_Analytica l_Ca l M-OOlN

- water 30-Day Avera ge 00 :00 :00 1 ml/L

- - Tab 8 & Att 2 Co nt r. cu lated 01202017.

1012712016 - - Lab Rot. zio

- - Settleab le So lid s 11/02/2016 - ONO 0. 1

.1 No Monthly avg - Att 1 CDF_Analytica l_Ca l M-OOlN

- water 30-Day Average 00:00 :00 1 ml/L

- - Tab 9 & Att 2 Co ntr. culated_Ol 202017.

11/21/2016 - .1 Lab Rot . zio

- - Settleab le So li ds 12/01/2016 - ONO 0.1

.1 No Monthly avg - Att 1 CDF_Analytica l_Ca l M-OOlN

- water 30-Day Average 00:00:00 1 ml/L

- - Tab 10 & Att 2 culated_Ol202017.

12/2712016 - .1 Contr. Lab Rot . zio

- - Total Suspen ded Solids (TSS) 10/04/2016 - =9

- No Month ly avg - Att 1 CDF_Analytical_Ca l M-OOlN

- wate r 30-Day Avg of Daily Avgs 00:00:00 1 mg/L

- - Tab 8 & Att 2 Contr. cu lated 01202017.

10/27 /2016 - - Lab Rpt. zio

- - Total Suspen ded So lids (TSS) 11/02/2016 - =7

- No Monthl y avg - Att 1 CDF_Ana lytica l_Ca l M-OOlN

- water 30-Day Avg of Dai ly Avg s 00:00:00 1 mg/L

- - Tab 9 & Att 2 Contr. cu lated 01202017 .

11/21/2016 - - Lab Rpt. zip

- - Total Suspend ed So lids (TSS) 12/01/2016 - = 12 - No Monthly avg - Att 1 CDF_Ana lytica l_Ca l M-OO lN

- water 30-Day Avg of Dai ly Avgs 00:00:00 1 mg/L

- - Tab 10 & At t 2 culated_Ol202017 .

12/2712016 - - Co ntr. Lab Rot. zio

- - pH 10/10/2016 -

= 7 .7

- No See Attachment #1, CDF_Ana lytica l_Ca l M-OOlP 10:20:00 1 - cu lated_Ol202017.

- water Daily Average (Mean)

- SU

- - Tab 11 zio 10/10/2016

- - pH 11/10/2016 - = 7.9

- No See Attachment #1, CDF_Analytica l_Ca l M-OOlP

- water Dai ly Average (Mean) 08 :40 :00 1 SU

- - Tab 12 cu lated 01202017.

11110/2016 - - zio

- - pH 12/07 /2016 - = 7.6 - No See Attachment #1, CDF_Ana lytica l_Ca l M-OOlP

- water Dai ly Average (Mean) 09 :00: 00 1 SU

- - Tab 13 culated_Ol202017.

12107/2016 - - zio

- - Total Suspended So lids (TSS) 10/10/2016 - = 9.8

- No Monthly avg resu lt . CDF_Ana lytica l_Ca l M-OOlP 00:00:00 1 - See Attachment 1, cu lated_Ol202017 .

- water 30-Day Avg of Dai ly Avg s 10/10/2016 - mg/L

- - Tab 11 zip

- - Total Suspen ded Solids (TSS) 11/10/2016 - = 15

- No Month ly avg result . CDF _Ana lytica l_Ca l M-OOlP

- water 30-Day Avg of Da ily Avgs 00:00 :00 1 mg/L See Attachment 1, cu lated_Ol202017 .

11/1012016 - - Tab 12 zio

- - Total Suspend ed So lids (TSS) 12/07/2016 - = 16

- No Monthly avg res ult . CDF _Ana lytica l_Ca l M-OOlP 00 :00 :00 1 - See Attachment l, cul ated_Ol202017 .

- water 30-Day Avg of Da ily Avgs 12107120 16 -

mg/L

- - Tab 13 ZiD Page 25 of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time, Lab Rep, Result, ML, Priority, Location De pth !ml Matrix Calculation Tvoe Analvsis Date Lab Batch Units RL IOA Code s Comments Data Source

- - Total Suspen ded So lids (TSS) 11/07/2016 - =6

- No Monthly avg resu lt. CDF _Analytica l_Ca l M-003

- water 30-Day Avg of Daily Avgs 12 :47:00 1 mg/L - - See Attachment 1, cul ated_Ol2020 17.

11/09/2016 - - Tab 12 zip

- - Tota l Suspended So lid s (TSS) 10/06/20 16 - DNQ 2 2

No Monthly avg result. CDF_Ana lytica l_Ca l M-003

- water 30-Day Avg of Da ily Avgs 09: 10:00 1 mg/ L

- - See Attach ment 1, cu lated_Ol202017.

10/06/2016 - 5 Tab 11 zip

- - Total Suspended So lids (TSS) 12/05/2016 - DNQ 3 2

No Monthly avg res ult . CDF _Analytical_Ca I M-003

- water 30-Da y Avg of Dai ly Avgs 13:00:00 1 mg/L

- - See Attac hment 1, cu lated_Ol202017.

12/05/2016 - 5 Tab 13 zio

- - Chro mium (Tota l) 10/04/2016 - ND 5

No Quarterly avg result. CDF_Analytical_Ca l M-INF

- water 90-Day Mean 00:00:00 1 ug/L

- - See Attachment 1, culated_Ol202017.

12/08/2016 - - Tab 1. zip

- - Copper, Total 10/04/2016 - DNQ 8 5

No Quarterly avg result. CDF_Ana lytica l_Ca l M-INF

- water 90-Day Mean 00:00:00 1 ug/L See Attachment 1, cu lated_Ol2020 17.

12/08/2016 - 10 Ta b 1. zip 10/04/2016 - 5 Quarte rly avg resu lt. CDF _Ana lytical_Ca l M-INF - - Nickel, Tota l 00:00:00 1 ND

- No See Attachment 1, culated_Ol202017.

- water 90-Day Mea n ug/L

- - Tab 1. zip 12/08/2016

- - Tempera tu re 10/01/2016 - = 55.2

- No CDF _Anal ytica l_Ca l M-INF

- water 24-hour Average 00:00:00 1 Deg rees F

- - culated_Ol202017.

10/01/2016 - - zip

- - Tempera ture 10/02/2016 - = 54.2

- No CDF_Analytical_Ca l M-INF

- water 24-hour Ave rage 00 :00:00 1 Degrees F

- - culated_Ol202017.

10/02/2016 - - zip

- - Temperature 10/03/201 6 - = 53.7

- No CDF_Analytica l_Ca l M-INF

- water 24-hour Average 00 :00 :00 1 Degrees F

- - culated_Ol202017.

10/03/2016 - - zip

- - Temperature 10/04/2016 - = 54 .2

- No CDF_Ana lytica l_Cal M-INF

- water 24-ho ur Ave rage 00:00:00 1 Deg rees F

- - culated_Ol202017.

10/04/2016 - - zip

- - Temperature 10/05/2016 - = 53.8 - No CDF_Analytical_Ca l M-INF

- wate r 24-hour Average 00 :00 :00 1 Degrees F - - cu lated_Ol202017.

10/05/2016 - - zip

- - Temperature 10/06/2016 - = 53.6

- No CDF_Analytical_Ca l M-INF

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated_Ol202017.

10/06/2016 - - zip

- - Temperature J 10/07/2016 - = 54.3

- No CDF_Ana lytica l_Ca l M-INF

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated_Ol2020 17 .

10/07/2016 - - zip

- - Tem perature 10/08/2016 - = 55 .2

- No CDF_Ana lytica l_Ca l M-INF

- water 24-hour Average 00:00:00 1 Degrees F - - cu lated_Ol202017 .

10/08/2016 - - zip

- - Tem perature 10/09/2016 - = 56.3 - No CDF _Ana lytical_Ca l M-INF

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated_Ol202017.

10/09/2016 - - zip

- - Tempe rature 10/10/2016 - = 55.9

- No CDF_Analytica l_Ca l M-INF

- water 24-hour Average 00 :00 :00 1 Degrees F

- - culated_Ol202017.

10/10/2016 - - zio

- - Temperatu re 10/11/2016 - = 55.5

- No CDF_Analytica l_Ca l M-INF

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated_Ol202017.

10/11/2016 - - zi p

- - Temperature 10/12/2016 - = 56

- No CDF_Analytica l_Ca l M-INF

- water 24-ho ur Average 00:00:00 1 Degrees F - - cu lated_Ol202017.

10/12/2016 - - zio

- - Temperat ure 10/13/2016 - = 56 .2 - No CDF_A nalytica l_Ca l M-INF

- water 24-hour Ave rag e 00:00:00 1 Degrees F

- - cu lated_Ol202017.

10/13/2016 - - zip Page 26 of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time , Lab Rep, Result, ML, Priority, Locati on Denth fml Matrix Calculation Tvne Analvsls Date Lab Batch Units RL OA Codes Comments Data Source

- - Te m perature 10/ 14/2016 - - 56 .8

- No CDF Analytica l Ca l M-INF

- water 24-hou r Average 00:00: 00 1 Degrees F

- - cu lated 01202017 .

10/1412016 - - zip

- - Temperature 10/15/2016 -

- 57.7

- No CDF Analytical Ca l M-INF

- water 24-ho ur Ave rage 00:00:00 1 Deg rees F

- - cu lated 01202017.

10/15 /2016 - - zip

- - Tempe rat ure 10/16/2016 - - 58 .2

- No CDF Ana lytica l Ca l M-INF

- water 24-hour Ave rage 00:00:00 1 Deg rees F

- - cu lated 01202017.

1011612016 - - zip

- - Te m pe rature 10/l 7 /2016 - - 58.8

- No CDF Analytica l Ca l M-INF

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017.

10117/2016 - - zip

- - Te m pe rature 10/18/2016 - - 56 .5

- No CDF Ana lytica l Ca l M-INF

- water 24-hou r Ave rage 00:00:00 1 Degrees F - - cu lated 01202017.

10/ 18/2016 - - zip

- - Temperature 10/19/2016 - - 56.3

- No CDF Analytica l Ca l M-INF

- water 24-ho ur Ave rage 00 :00 :00 1 Degrees F

- - cu lated 01202017.

10/19/2016 - - zip

- - Temperature 10/20/2016 - - 56.l

- No CDF Ana lytica l Ca l M-INF

- wate r 24-h our Ave rage 00:00:00 1 Degrees F

- - culat ed 012020 17.

10/20/2016 - - zip

- - Temperature 10/21/2016 - - 56 .5

- No CDF Ana lytica l Ca l M-INF

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017 .

1012112016 - - zip

- - Tem perat ure 10/22/2016 - - 56

- No CDF Ana lytical Ca l M-INF

- water 24-hour Average 00:00:00 1 Degrees F cu lated 01202017.

10/22/2016 - - zip

- - Temperature 10/23/2016 - - 56.4

- No CDF Ana lytical Cal M-INF

- water 24-hour Average 00:00:00 1 Degrees F - - cu lated 01202017.

1012312016 - - zip

- - Tem peratu re 10/24/2016 - - 57. 1

- No CDF Ana lytica l Ca l M-INF

- water 24-hour Average 00:00 :00 1 Degrees F - - cu lated 01202017.

10/24/201 6 - - zip

- - Tempe rature 10/25/2016 - - 58.3

- No CDF Ana lytica l Ca l M-INF 00:00:00 1 - cu lated 01202017.

- water 24-hour Average 10/25/2016 - Deg rees F

- - zip

- - Tempe rature 10/26/2016 - - 58.4 - No CDF Analytica l Ca l M-INF

- water 24-hou r Average 00:00:00 1 Deg rees F

- - culated 01202017.

10/26/2016 - - zip

- - Tempera ture 10/27 /2016 -

- 58.2

- No CDF Analytica l Ca l M-INF

- water 24-hour Average 00:00:00 1 Deg rees F

- - cu lated 01202017.

10/27 /2016 - - zip

- - Temperature 10/28/2016 - - 58.3

- No CDF Ana lytica l Ca l M-INF

- water 24-hour Ave rage 00:00:00 1 Deg rees F

- - cu lated 01202017.

10/28/2016 - - zio

- - Temperature 10/29/20 16 - - 59.2

- No CDF Ana lytica l Ca l M-INF

- water 24-hour Ave rage 00:00:00 1 Degrees F

- - cu lated 01202017.

10/29/2016 - - zip

- - Temperature 10/30/2016 - - 59 .6

- No CDF Ana lytica l Ca l M-INF

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017.

10/30/2016 - - zio

- - Temperature 10/31/2016 - - 59.6

- No CDF Ana lytica l Ca l M-INF

- water 24-hour Average 00:00:00 1 Degrees F cu lated 01202017 .

10/31/2016 - - zio

- - Temperature 11/01/2016 - - 59.l

- No CDF Ana lytica l Ca l M-INF

- water 24-hour Ave rage 00:00:00 1 Deg rees F

- - cu lated 01202017.

11/01/20 16 - - zip Page 2 7 of 32

Collection Sample Sa mple Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time, Lab Rep, Result, ML, Priority, Location Depth (m) Matrix Calculation Type Analysis Date La b Batch Un it s RL iOA Codes Comments Data Source

- - Temperature 11/02/2016 - 58.2

- No CDF Analytica l Ca l M-INF

- water 24-ho ur Average 00 :00:00 1 Degrees F

- - cu lated 01202017.

ll/02_L2016 - - zip

- - Temperatu re 11/03/2016 - 58

- No CDF Ana lytica l Cal M-INF

- water 24-hour Average 00 :00 :00 1 Degrees F

- - cu lated 01202017.

11/03/2016 - - zip

- - Temperatu re 11/04/2016 - 58.3

- No CDF Ana lytica l Ca l M-INF

- water 24-hour Average 00 :00 :00 1 Degrees F

- - cu lated 01202017.

11/04/2016 - - zip

- - Te m pe rature 11/05/2016 - 58.2

- No CDF Ana lytica l Ca l M-I NF

- water 24-hou r Average 00:00:00 1 Deg rees F

- - culated 01202017.

11/05 /2016 - - zip

- - Temperature 11/06/2016 - 57.3

- No CDF Ana lytica l Ca l M-I NF

- water 24-hour Ave rage 00:00:00 1 Deg rees F

- - cu lated 01202017.

11/06/2016 - - zip

- - Tempe ratu re 11/07 /201 6 - 57.5

- No CDF Ana lytica l Ca l M-INF

- water 24-hou r Average 00:00:00 1 Degrees F

- - culated 01202017.

11/07/2016 - - zip

- - Temperatu re 11/08/2016 - 57.7

- No CDF Analytica l Ca l M-INF 00:00:00 1 - culated 01202017.

- wat er 24-h ou r Ave rage 11/08/2016 - Deg rees F

- - zip

- - Temperatu re 11/09/2016 - 57.2

- No CDF Analytica l Ca l M-INF

- water 24-hour Average 00 :00 :00 1 Deg rees F

- - culated 012020 17.

11/09/2016 - - zip

- - Tempera t ure 11/10/2016 - 57 .7

- No CDF Analytica l Ca l M-INF

- water 24-ho ur Ave rage 00:00:00 1 Degrees F

- - culated 012020 17.

11/10/2016 - - zip

- - Temperature 11/11/2016 - 58.3

- No CDF Ana lytical Ca l M-INF 00 :00:00 1 - cu lated 01202017 .

- water 24-hour Ave rage 11/11/2016 - Degrees F

- - zip

- - Tem perature 11/12/2016 - 58 - No CDF Analytical Ca l M-INF

- wat er 24-hour Average 00:00 :00 1 Degrees F cu lated 01202017.

11/12/2016 - - zip 11/13/2016 - - CDF Ana lytical Ca l M-INF - - Tem perature 00:00:00 1 58 .1

- No cu lated 01202017 .

- water 24-hour Average 11/13 /20 16 - Degrees F

- - zip 11/14/2016 - - CDF Ana lytica l Ca l M-INF - - Temperature 00 :00 :00 1 58.2

- No cu lated 01202017.

- water 24-hour Average

- Deg rees F

- - zip 11/14/20 16

- - Temperature 11/ 15/2016 - 58

- No CDF Ana lytica l Ca l M-INF

- water 24-hou r Average 00 :00:00 1 Degrees F

- - cu lated 01202017.

11/15/2016 - - zip

- - Tem perature 11/16/2016 - 56.7

- No CDF Ana lytical Ca l M-INF

- water 24-ho ur Average 00:00 :00 1 Degrees F

- - cu lated 01202017.

11/16/2016 - - zip

- - Tempera ture ll/l 7/201 6 - 55.l

- No CDF Analytical Ca l M-INF

- water 24-ho ur Ave rage 00:00:00 1 Degrees F

- - cul ated 01202017.

11/17/2016 - - zip

- - Tempe rature 11/18 /2016 - 56.2 - No CDF Analytica l Ca l M-INF 00:0 0:00 1 - cu lated 01202017.

- water 24-hour Ave rage 11/18/2016 - Degrees F

- - zip

- - Temperature 11/19/2016 - 56.4

- No CDF Ana lytica l Ca l M-INF

- water 24-hour Average 00:00:00 1 Degrees F culated 01202017.

11/19/2016 - - zip 11/20/2016 - - CDF Ana lytica l Ca l M-INF - - Temperature 00 :00 :00 1 56 .8

- No culated 01202017.

- water 24-hour Average Deg rees F

- - zip 1]120/2016 Pag e 2 8 of 32

Collection Sample Sample Date, Field Re p, MDL, Review Method, Type, Paramet e r, Sample Time, Lab Re p, Result, ML, Priority, Location Denth !ml Matrix Calculation Tvne Analvsis Date La b Batch Units RL OA Codes Comments Dat a Source

- - Temperature 11/21/2016 - - 57

- No CDF Ana lytica l Ca l M-INF

- water 24-hour Average 00:00 :00 1 Degrees F

- - culated 01202017.

11/21/2016 - - zio

- - Temperatu re 11/22/2016 - - 57.1

- No CDF_Analytica l Ca l M-INF

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017.

11/22/2016 - - zip

- - Tempe rature 11/23/2016 - - 56 .7

- No CDF Analytica l Ca l M-INF

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017.

11/23/2016 - - zio

- - Tempera t ure 11/24/2016 - - 56.9

- No CDF Analytica l Ca l M-INF 00:00 :00 1 - cu lated 01202017 .

- water 24-hour Average 11/2412016 - Degrees F

- - zip

- - Temperature 11/25/2016 - - 57.6 - No CDF_Ana lytical Ca l M-INF

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017.

11/25/2016 - - zip

- - Temperature 11/26/2016 - - 57.4 - No CDF Analytica l Ca l M-INF

- water 24-hour Average 00 :00:00 1 Degrees F

- - culated 01202017.

11/26/2016 - - zip

- - Temperature

ll/27 /2016 - - 56.8 - No CDF Analytical Cal M-INF 00:00:00 1 - culated 01202017.

- water 24-hour Average 11/27 /2016 - Degrees F

- - zip

- - Temperature 11/28/2016 - - 55.3

- No CDF Ana lytical Ca l M-INF

- water 24-hour Average 00:00 :00 1 Deg rees F

- - cu lated 01202017.

11/28/2016 - - zip

- - Temperature 11/29/2016 - - 54.6

- No CDF Ana lytica l Ca l M-INF

- water 24-hour Ave rage 00 :00 :00 1 Deg rees F

- - cu lated_Ol202017, 11/29/2016 - - zip

- - Temperature 11/30/2016 - - 54.7 - No CDF Analytica l Ca l M-INF

- water 24-hour Ave rage 00:00:00 1 Degrees F - - cu lated 01202017.

11/30/2016 - - zip

- - Temperature 12/01/2016 - - 54 .6

- No CDF__Analytical Ca l M-INF

- water 24-hour Average 00:00 :00 1 Degrees F

- - cu lated 01202017.

12/01/2016 - - zip

- - Temperature 12/02/2016 - - 54.7

- No CDF Analytica l Ca l M-INF

- water 24-hour Average 00:00 :00 1 Degrees F

- - cu lated 01202017.

12/02/2016 - - zin

- - Tempe rature 12/03/2016 - - 54.7 - No CDF Ana lytica l Ca l M-INF

- wate r 24-hou r Average 00:00:00 1 Degrees F

- - culated 01202017.

12103/2016 - - zio

- - Tem peratu re 12/04/2016 - - 55 .l

- No CDF Ana lytical Ca l M-INF

- water 24-hour Average 00:00:00 1 Degrees F - -

cu lated 01202017, 12/04/2016 - - zio

- - Temperature 12/05/2016 - - No CDF Analytical Ca l

- 54.5 M-INF

- water 24-hour Ave rage 00:00:00 1 Degrees F

- - culated 01202017.

12/05/2016 - - zio

- - Temperature 12/06/2016 - - 54

- No CDF Analytical Cal M-INF

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017.

12/06/2016 - - zio

- - Temperature 12/07 /2016 - - 53.9 - No CDF Ana lytica l Ca l M-INF

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017, 12/07/2016 - - zio

- - Tempe rature 12/08/2016 - - 54.5 - No CDF Ana lytica l Ca l M-INF 00:00:00 1 - cu lated 01202017.

- water 24-hou r Average 12/08/2016 - Deg rees F

- - zio

- - Temperature 12/09/2016 - - 55

- No CDF Analytical Ca l M-INF 00:00:00 1 - - cu lated 01202017.

- water 24-hour Average 12109/2016 -

Deg rees F

- zio Pa ge 29 of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time, Lab Rep, Result, ML, Priority, Location Denth (ml Matrix Calculation Tvoe Analvsis Dat e Lab Batch Units RL OA Codes Comments Data Source

- - Temperat ure 12/10/2016 - - 55

- No CDF Ana lytica l Ca l M-INF 00:00 :00 1 - cu lated 012020 17.

- water 24-hour Average 12/10/2016 -

Deg rees F

- - zip

- - Tem perature 12/11/2016 - - 55.1

- No CDF Ana lytica l Ca l M-INF

- water 24-hour Average 00 :00 :00 1 Degrees F - - cu lated 012020 17.

12/11/2016 - - zip

- - Tem perature 12/ 12/2016 - - 54.7

- No CDF Ana lytica l Ca l M-INF

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 01202017 .

12/12/2016 - - zip

- - Te mperature 12/13/2016 - - 55.3

- No CDF Analytica l Ca l M-INF

- water 24-hour Average 00:00:00 1 Degrees F

- - cu lated 012020 17.

12/13/2016 - - zip

- - Tempe rature 12/14/2016 - - 55 .3

- No CDF Ana lytica l Ca l M-INF

- water 24-hour Average 00:00 :00 1 Degrees F

- - cul ated 01202017 .

12/ 14/2016 - - zip

- - Tem perature 12/15/2016 - - 55.2 No CDF Ana lytica l Ca l M-INF 00:00:00 1 - cu lated 012020 17.

- water 24-hour Ave rage

- Deg rees F

- zip 12/15/2016

- - Temperature 12/16/2016 - - 55. l

- No CDF Ana lytica l Cal M-INF

- water 24-ho ur Ave rage 00 :00 :00 1 Deg rees F

- - cu lated 01202017.

12/16/2016 - - zip

- - Temperature 12/17/2016 - - 53.9

- No CDF Ana lytica l Ca l M-INF

- water 24-hour Average 00 :00 :00 1 Deg rees F

- - cu lated 01202017.

12117/2016 - - zip

- - Te m perature 12/ 18/2016 - - 54 .3

- No CDF Analytica l Ca l M-INF

- water 24-hour Ave rage 00:00:00 1 Deg rees F

- - cu lated 01202017.

12118/2016 - - zip

- - Te m perature 12119/2016 - - 54.4

- No CDF Analytica l Ca l M-INF

- water 24-hour Ave rage 00:00:00 1 Degrees F

- - cu lated 01202017.

12119/2016 - - zip

- - Tempe rature 12/20/2016 - - 54.7

- No CDF Analytica l Ca l M-INF

- wate r 24-hou r Average 00 :00: 00 1 Degrees F

- - culated 01202017 .

12120/2016 - - zip

- - Tempe rature 12/21/2016 - - 54.4

- No CDF Ana lytica l Ca l M-INF

- wate r 24-hour Average 00 :00:00 1 Degrees F cu lated 01202017.

12/21/2016 - - zip

- - Tempera ture 12/22/2016 - - 54.4

- No CDF Ana lytica l Ca l M-INF 00:00 :00 1 - cu lated 012020 17.

- water 24-hour Average 12122/2016 - Deg rees F

- - zio

- - Temperature 12/23/2016 - - 54.2

- No CDF Ana lytica l Ca l M-INF

- wa ter 24-ho ur Average 00:00:00 1 Deg rees F - - cul ated 012020 17.

12/23/2016 - - zip

- - Temperatu re 12/24/2016 - - 54.8

- No CDF Analytica l Ca l M-INF

- wa ter 24-hour Ave rage 00 :00 :00 1 Deg rees F

- - culated 01202017.

12/24/2016 - - zio

- - Temperat ure 12/25/2016 - - 54

- No CDF Ana lytica l Ca l M-I NF

- water 24-hour Ave rage 00:00:00 1 Degrees F

- - cu lated 01202017 .

12/25/2016 - - zin

- - Te m perature 12/26/2016 - - 53.9 - No CDF Ana lytica l Ca l M-INF

- water 24-ho ur Average 00:00 :00 1 Degrees F

- - culated 012020 17.

12/26/2016 - - zip

- - Tempe ratu re 12/27/2016 - - 53.8

- No CDF Ana lytical Ca l M-INF 00:00:00 1 cul ated 01202017.

- wate r 24-hou r Average 12/27 /2016 -

Degrees F

- zip

- - Temperatu re 12/28/2016 - - 54.1 - No CDF Ana lytical Ca l M-I NF

- water 24-ho ur Average 00:00 :00 1 Degrees F

- - culated 01202017 .

12128/2016 - - zip Pag e 3 0 of 32

Collection Sample Sample Date, Field Rep, MDL, Review Method, Type, Parameter, Sample Time, Lab Rep, Result, ML, Priority, Location Deoth lml Matrix Calculation Tvoe Analvsls Date Lab Batch Units RL OA Codes Comments Data Source

- - Tempe rature 12/29/2016 - = 54.6 - No CDF _Ana lytica l_Ca l M-INF

- water 24-h ou r Average 00:00:00 1 Degrees F - - cu lated_Ol202017 .

12/29/2016 - - zio 12/30/2016 - - CDF_Analytical_Cal M-INF - - Temperature 00:00:00 1

= 54.7 - No cu lated_Ol202017 .

- water 24-hour Average 12130/2016 - Degrees F

- - zio 12/31/2016 - - CDF_Ana lytica l_Cal M-INF - - Temperature 00:00:00 1

= 54.4 -

No culated_Ol202017.

- water 24-hou r Average 1213112016 - Degrees F

- - zio

- - Temperature 10/01/2016 -

= 59 .6 - No CDF_Ana lytica l_Cal M-INF

- water Dai ly Maximum 00 :00:00 1 Degrees F - - cu lated_Ol202017 .

10/3112016 - - zip

- - Temperature 11/01/2016 - = 59.1 - No CDF_Analytical_Ca l M-INF

- water Dai ly Maximum 00:00 :00 1 Degrees F

- - culated_Ol202017.

11/30/2016 - - zip

- - Temperature 12/01/2016 - = 55 .3 - No CDF_Ana lytical_Ca l M-INF

- water Da il y Maxim um 00:00 :00 1 Degrees F - -

cu lated_Ol202017.

12/31/2016 - - zip 10/01/2016 - - CDF _Analytical_Ca l M-INF - - Temperature 00 :00 :00 1

= 56.5 - No cu lated_Ol202017.

- water Mthly Avg of Daily Avgs 1013112016 -

Degrees F

- - zio

- - Temperature 11/01/2016 - = 57. 2 - No CDF_Analytical_Ca I M-INF

- water Mt hly Avg of Da il y Avgs 00 :00:00 1 Degrees F

- - culated_Ol202017 .

1113012016 - - zio

- - Temperature 12/01/2016 - = 54.6 - No CDF_Ana lytica l_Ca l M-INF 00:00:00 1 - cu lated_Ol202017.

- water Mthly Avg of Dai ly Avgs 1213112016 - Degrees F

- - zio 10/04/2016 - 5 Quarterly avg resu lt . CDF_Analytical_Ca l M-INF

- - Zinc , Tota l 00:00:00 1 ND

- No See Attachment 1, cu lated_Ol202017.

- water 90-Day Mean 1210812016 - ug/L

- - Tab 1. zip Lab Batches No La b Batc h Data Ava il a bl e I Re porte d Certificate I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.

I certify that I am david cortina and am authorized to submit this report on behalf of PG&E Diablo Canyon Power Plant. I understand that I am submitting the following report(s):

- Quarterly SMR ( MONNPDES) report for Q4 2016 (due 01/20/2017)

I understand that data submitted in this report(s) can be used by authorized agencies for water quality management related analyses and enforcement actions, if required.

I am also aware that my user ID, password, and answer to a challenge question constitute my electronic signature and any information I indicate I am electronically certifying contains my signature. I understand that my electronic signature is the legal equivalent of my handwritten signature. I certify that I have not violated any term in my Electronic Signature Agreement and that I am otherwise without any reason to believe that the confidentiality of my password and challenge question answers have been compromised now or at any time prior to this submission. I understand that this attestation of fact pertains to the implementation, oversight, and enforcement of a federal Page 3 1 of 32

environmental program and must be true to the best of my knowledge.

Name: david cortina

Title:

Chemistry and Environmental Services Manager Page 32 of 32

Attachment 1 - 2016 4th Qtr DCPP NPDES Worksheets.xlsm Diablo Canyon Power Plant - NPDES Data Worksheets 4th Quarter 2016 Tab Information Go To Tab 1 1 Miscellaneous Quarterly Averages Go To Tab 2 2 Circulating Water Chlorine Residual - October Go To Tab 3 3 Circulating Water Chlorine Residual - November Go To Tab4 4 Circulating Water Chlorine Residual - December Go To Tab 5 5 001 D Flow Weiahted Averaaes For TSS and O&G - October I

GoToTab6 6 001 D Flow Weiahted Averaaes For TSS and O&G - November GoToTab7 7 001 D Flow Weighted Averages For TSS and O&G - December GoToTab8 8 001 N TSS, SS and O&G - October Go To Tab 9 9 001 N TSS, SS and O&G - November Go To Tab 10 10 001 N TSS, SS and O&G - December Go To Tab 11 11 Miscellaneous Duolicates - October Go To Tab 12 12 Miscellaneous Duplicates - November Go To Tab 13 13 Miscellaneous Duplicates - December Navigation

Attachment 1

2016 4th Qtr DCPP NPDES Worl<sheets.xlsm A B I c I D E I F I G I H I I J K 1 Miscellaneous Quarterly Average Calculations fo r Quarterlv eSMR I 2 I I I 3 - For Influent Ouarte rfv Metals, fill in hiahli ahte d cells onlv. Subseauent cells will be filled in a utomatica llv.

4 10 ua/ L is DCPP lab Reoortina Limit. 5 ua/L is DCPP Jab MDL 5

Analysi s Result for Daily Nume rical Reporting Average Sample Date Lab Parameter Results 6 D te Avera ae Avera ae Ouarterlv Averaae for Q uarter 7

8 10141201-s-1 1012612016 DCPP Influent Cr NDl 5\ 0 0 0 NDl5\

9 111312016 11 11712016 DCPP Influent Cr ND(5) 0 10 121812016 12/ 12/2016 I DCPP Influent Cr ND(5) 0 11 12 10/4/2016 10127/2016 DCPP Influent Cu DNQ l6.6\ 7 8 8 DNQ18\

13 I 11 1312016 11 11712016 DCPP Influent Cu DNQl 8.1\ 8 14 12181~ 1212016 DCPP Influent Cu DNQ(7.8) 8 15 16 101412016 1012612016 I DCP P Influ ent Ni ND15\ 0 0 0 ND15\

17 11 13/2016 11 11712016 DCP P Influent Ni NDl 5\ 0 18 121812016 1211212016 DCPP Influent Ni NDC5) 0 19 20 101412o h o12112016 I DCPP Influent Zn ND(5) 0 0 0 NDC5l 21 I 111312016 11 11712016 I DCPP Influent Zn ND(5) 0 22 12/8/~ 12 1 12/ 2016 ~ DCPP Influent Zn NDC5\ 0 23 24 Quarterfv Oil and Grease Averaaes 25 5.0 mq/L is DCP P lab Reportin q Li mit. 1.4 mQ/L is DC PP lab MDL 26 Analys is Resu lt fo r Numerical Reporti ng Average Sample Date Locatio n Unit Parameter Results Daily Average 27 Date Avera ge Quarterly Average for Quarter 28 10/212016 1011812016 001 H 1 O&G ND11 .4\ 0.0 0.0 0.0 NDl1.4\

29 1012/2016 1011812016 001 H 2 O&G ND11 .4\ 0.0 30 31 1013/2016 10118/2016 001 L 1 O&G NDC1 .4 \ 0.0 0 .0 0 .0 NDl1.4 \

32 101312016 1011812016 001 L 2 O&G NDC1.4\ 0.0 33 34 Quarterly 001 0 LRW O il and Grease - Refer to Worksheet 5 6 and 7 for Monthly Ave raae Calculations.

Result Average Numerica l Quarterly Reporting Average for Month for O&G Average Quarter 35 Averane 36 October ND11 .4\ 0 .0 0.8 DNQ 1.4\

37 November DNQ l2.5\ 2.5 38 December NDC1 .4\ 0 .0 39 40 Quarte rly Metals Composite Ave ra Qes 41 10 "q/L is DCP P la b Re portino Li mit. 5 " Q/L is DCP P lab MDL.

42 First Aliq: tst Ali quot Loc ation Result for Numerical Reporting Average Unit Parameter Results 43 Date Date Avera ge Quarterly Average for Quarte r 44 101312016 1216/2016 001H 1 Aq NDC5) 0 0 ND/5\

45 101312016 121512016 I 001H 2 Ao ND(5) 0 1013120~21612016 46 47 I 1001 H 1 Cd ND15\ 0 0 ND(5) 48 10/312016 121512016 001 H 2 Cd ND15\ 0 49 I 50 I 10/312016 121612016 001H 1 Cr 20 20 24 24 51 10/312016 121512016 001H 2 Cr 27 27 52 53 I 101312016 121612016 001H 1 Cu 23 23 29 29 54 I 1013/2016 121512016 001H 2 Cu 34 34 1 013120~21612016 55 56 001H 1 Ni 15 15 16 16 57 101312016 12/5/2016 001H 2 Ni 17 17 1013120~/6/2016 58 59 001H 1 Pb 27 27 24 24 60 1013/2016 12/5/2016 001H 2 Pb 20 20 1013120~/612016 61 62 001 H 1 Zn NDC5) 0 7 < 10 63 1013120 16 12/512016 001 H 2 Zn 13 13 1013120~216/2016 64 65 001 H 1 Hg ND(0.080) 0.00 0.00 ND{Q.080) 66 10 131~ 121512016 001H 2 Hg ND(0.080) 0.00 67 68 69 101512016 I 121712016 001L 1 Ao ND(5) 0 0 ND(5) 70 101512016 121712016 001L 2 Ao NDC5\ 0 1015120~1712016 71 I 72 00 1L 1 Cd NDC5\ 0 0 ND15\

73 101512016 121712016 001L 2 Cd NDC5\ 0 74 I 75 101512016 L,z1712016 001L 1 Cr ND(5) 0 0 NDl 5\

76 1015/20 16 121712016 001 L 2 Cr ND(5) 0 77 I 78 1015120 M 21712016 001L 1 Cu ND/5\ 0 11 11 79 101512016 121712016 001 L 2 Cu 22 22 1015120~1712016 80 I 81 001L 1 Ni NDC5) 0 0 NDC5\

82 -1 01512016 1217/2016 001L 2 Ni ND(5) 0 1015120~2n12015 83 84 001 L 1 Pb NDC5\ 0 0 ND15\

85 101512016 121712016 001L 2 Pb NDl 5\ 0

~1712016 86 87 101512016 001L 1 Zn ND(5) 0 0 ND(5) 88 1015120 16 121712016 001L 2 Zn NDl5\ 0

~21712016 89 90 101512016 001L 1 Ho NDC0.080\ 0 .00 0.00 ND!0.080\

91 101512016 121712016 001L 2 Ho NDI0.0801 0.00

Attachment 1 - 201 6 4th Qtr DCPP NPDES Worksheets.xlsm I A B c D E F G H I J K L M N 0 p 1

2 Chlorine for eSMR 3

4 FILL IN ONLY SHADED/COLORED CELLS 5

6 Date 7 10/1/2016 10/212016 10/3/2016 10/41201 6 10/5/2016 10/6/2016 1017/2016 10/8/2016 10/9/2016 10/10/2016 10/11/2016 10/12/2016 10/13/201 6 10/14/2016 10/15/2016 8 Unit 1 TRC loob <10 < 10 <10 < 10 no iniection 18 32 24 14 15 18 15 18 no iniection no injection 9 <10 < 10 <10 <10 no iniection 20 35 22 <10 15 22 12 20 no iniection no iniection 10 <10 < 10 <10 <10 no iniection 22 24 14 < 10 13 20 <10 13 no iniection no iniection 11 < 10 < 10 <10 no iniection 17 35 22 11 12 no iniection no iniection 22 74 no iniection no iniection 12 <1 0 < 10 <10 no iniection 17 29 18 <10 <10 no iniection no injection <10 <10 no iniection no injection 13 <10 <10 <10 no iniection 14 32 24 11 <10 24 14 17 no injection no iniection no injection 14 Unit 1 Cl2 Use (lbs 417 .6 417.6 417.6 208.8 208.8 417 .6 41 7.6 417 .6 417.6 278 .4 266.4 345.6 288.0 0.0 0.0 15 Unit 2 TRC !eeb) <10 < 10 <10 < 10 no inj ection 18 31 23 14 15 16 23 18 <10 <10 16 <10 < 10 <10 < 10 no iniection 18 31 25 10 15 18 23 19 12 <10 17 <10 < 10 <10 < 10 <10 18 25 15 10 13 13 21 16 <10 <10 18 <10 < 10 <10 no iniection 16 31 21 13 12 no iniection no iniection 15 10 <10 <10 19 < 10 < 10 <10 no injection 16 31 21 11 <10 18 15 15 <10 <10 <10 20 <10 <10 <10 no ini ecti on 16 31 21 13 12 15 18 16 <10 <10 < 10 21 Unit 2 Cl2 Use llbsl 432.0 432.0 432.0 216 288 432 432 432 432 360 360 432 432 432 432 22 23 0 0 0 0 17 35 35 24 14 24 22 22 74 0 0 24 0 0 0 0 16 31 31 25 14 18 18 23 19 12 0 25 Dally Maxi mum TRC (ppb) 0 0 0 0 17 35 35 25 14 24 22 23 74 12 0 26 Da ily Cl2 Use (lbs) 850 850 850 425 497 850 850 850 850 638 626 778 720 432 432 27 28 29 30 31 32 33 34 35 2

Attachment 1 - 2016 4th Qtr DCPP NPDES Worksheets.xlsm I Q R s T u v w x y z AA AB AC AD AE AF AG 1

2 3

4 5

6 7 *10/16/2016 10/17/2016 10/18/2016 10/19/2016 10/20/2016 10/21/2016 10/22/2016 10/23/2016 10/24/2016 10/25/2016 10/26/2016 10/27/2016 1012812016 10/291201 6 1013012016 10131 /2016 8 no iniection no injection no iniection no iniection <7 <7 <7 < 10 <10 <10 <10 <10 <10 <10 <10 <10 9 no injection no injection no injection no injection <7 <7 <10 < 10 < 10 <10 < 10 <10 <10 < 10 <10 <10 10 no iniection no injection no injection no injection <7 <7 <10 <10 <10 <10 < 10 <10 <10 < 10 <10 < 10 11 no iniection no iniection no iniection no ini ection <7 <7 <10 <10 <10 no injection < 10 <10 < 10 <10 <10 <10 12 no injection no iniection no iniection <10 <7 <7 <10 <10 <10 12 <10 <10 < 10 <10 <10 <10 13 no injection no injection no injection <7 <7 <7 <10 <10 <10 <10 < 10 <10 < 10 <10 <10 < 10 14 0.0 0.0 0.0 43.2 172.8 172.8 268.8 345.6 345. 6 252.0 345.6 345 .6 345.6 345.6 345.6 345.6 15 <10 <10 < 13 13 < 13 < 13 13 <10 <10 <10 < 10 10 < 10 <10 10 10 16 <10 <13 < 13 17 17 < 13 <10 <10 <10 <10 < 10 11 10 10 11 11 17 <1 0 < 13 < 13 15 < 13 < 13 <10 <10 <10 <10 < 10 <10 <10 <10 11 10 18 <10 < 13 <13 <13 < 13 < 13 <10 <10 <10 no injection < 10 < 10 <10 < 10 <10 <10 19 < 10 <13 <13 <10 <13 <13 <10 <10 <10 <10 < 10 < 10 <10 < 10 11 <10 20 < 10 < 13 < 13 <13 <13 <13 < 10 <10 <10 <10 < 10 < 10 <10 < 10 <10 <10 21 432 436.8 446.4 451 .2 460.8 460.8 460.8 460.8 460.8 384 460.8 460.8 460.8 460.8 460.8 460.8 22 23 0 0 0 0 0 0 0 0 0 12 0 0 0 0 0 0 24 0 0 0 17 17 0 13 0 0 0 0 11 10 10 11 11 25 0 0 0 17 17 0 13 0 0 12 0 11 10 10 11 11 26 432 437 446 494 634 634 730 806 806 636 806 806 806 806 806 806 27 Chlo rine loob) (lbs/day)

Monthly 28 Averaa e 13 690 29 MONTHLY CHLORINE USE: 21 ,389 lbs. Maximum 74 850 30 Minimum 0 425 31 Ver ifv that valu es have correct references.

32 Verified that the ca lcs all end at AF for a 31 dav month. M68X 11-07-2016 33 34 35 I

Attachment 1 - 20 16 4th Qtr DCPP NPDES Worksheets.xtsm A 8 c D E F G H I J K L M N 0 p 1

2 Chlorine for eSMR 3

4 FILL IN ONLY SHADED/COLORED CELLS 5

6 Date 7 11/1/2016 11 /2/2016 11/3/2016 11 /4/2016 11 /5/2016 11/6/2016 1117/2016 11 /8/2016 11 /9/2016 11 /10/2016 11 /11/2016 11/12/2016 11 /13/2016 11 /14/2016 11/15/2016 8 Un it 1 TRC 1oob} <10 <10 <10 <10 <10 12 14 13 13 20 <13 <10 <10 <10 <10 9 <10 <10 <10 <10 <10 <10 14 <10 13 20 14 <10 <10 <10 <10 10 <10 <10 <10 <10 <10 <10 12 <10 12 13 <10 <10 <10 <10 <10 11 <10 <10 <10 <10 <10 <10 12 <10 20 17 <10 <10 <10 no injection <10 12 <10 <10 <10 <10 <10 <10 <10 <10 17 17 <10 <10 <10 <10 no injection 13 <10 <10 <10 <10 <10 13 11 11 17 14 <10 <10 <10 <10 no iniection 14 Unit 1 Cl2 Use (lbs} 345.6 345.6 345.6 345.6 345.6 350.4 360.0 360.0 360.0 360.0 360.0 360.0 360.0 300.0 240.0 15 Unit 2 TRC loob} 10 10 <10 <10 <10 <10 <10 <10 <10 10 <7 <10 <10 <10 <10 16 10 10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 17 10 10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 18 <10 <10 <10 <10 <10 <10 <10 <10 <10 <7 <10 <10 <10 no injection <10 19 <10 <10 <10 <10 <10 <10 <10 <10 <10 <7 <10 <10 <10 <10 no injection 20 <10 <10 <10 <10 <10 <10 <10 <10 <10 <7 <10 <10 <10 <10 no iniection 21 Unit 2 Cl2 Use (lbsl 460.B 460.B 460.B 460.B 460.B 460.B 460.8 460.B 460.8 316.B 309.6 345.6 345.6 235.2 124.B 22 23 0 0 0 0 0 13 14 13 20 20 14 0 0 0 0 24 10 10 0 0 0 0 0 0 0 10 0 0 0 0 0 25 Dally Maximum TRC (ppb) 10 10 0 0 0 13 14 13 20 20 14 0 0 0 0 26 Da ily Cl 2 Use (lbs) 806 806 806 806 806 811 821 821 821 677 670 706 706 535 365 27 28 29 30 31 32 33 34 35 3

Attachment 1 - 20 16 4th Qtr DCPP NPDES Worksheets.xlsm Q R s T u v w x y z AA AB AC AD AE AF AG 1

2 3

4 5

6 7 11/16/2016 11/17/201 6 11 /18/201 6 11 /1912016 11 /20/201 6 11121/2016 11/22/2016 1112312016 1112412016 1112512016 1112612016 11/2712016 11 /2812016 11 /29/2016 11130/2016 8 no injection 10 <10 < 10 < 10 < 10 <10 <1 0 68 15 12 <10 13 18 15 9 no injection 10 < 10 <10 < 10 < 10 <10 <10 74 14 12 <10 15 18 14 10 no iniection 11 <10 <10 <10 < 10 < 10 <10 12 62 < 10 11 15 18 13 11 no iniection <10 <10 <10 <10 <10 <10 11 15 <10 < 10 <10 15 17 no injection 12 10 10 <10 <10 <10 < 10 < 10 11 15 14 < 10 24 22 15 17 13 10 <10 <10 <10 < 10 <10 <10 11 15 12 <10 11 18 15 32 14 120.0 352.8 316.8 316.8 316.8 316.8 316.8 316.8 316.8 302 .4 288.0 288.0 288.0 283.2 196.3 15 no injection 18 15 11 < 10 <10 11 10 <10 10 <10 < 10 11 16 18 16 no iniection 19 15 12 < 10 < 10 10 < 10 11 <10 <10 < 10 13 16 16 17 no injection 18 12 12 10 <10 < 10 < 10 11 <10 <10 <10 12 16 13 18 10 13 11 11 < 10 11 < 10 < 10 11 <10 < 10 <10 13 16 no iniection 19 13 18 12 11 < 10 10 <10 < 10 11 10 < 10 <10 13 16 13 20 16 16 12 11 < 10 < 10 < 10 < 10 10 <10 < 10 <10 16 16 15 21 156 367.2 331.2 331.2 331.2 33 1.2 331.2 33 1.2 33 1.2 331.2 331.2 33 1.2 331.2 326.4 252 22 23 10 11 0 0 0 0 0 11 74 62 12 24 22 18 32 0 24 16 19 15 12 10 11 11 10 11 10 0 0 16 16 18 0 25 16 19 15 12 10 11 11 11 74 62 12 24 22 18 32 0 26 276 720 648 648 648 648 648 648 648 634 619 619 619 610 448 0 27 Chlorine 1nnb) ll bs/davl Monthly 28 Average 15 668 29 MONTHLY CHLORI NE USE : 20,044 lbs. Maximu m 74 821 30 Minimum 0 276 31 Ver ifv that va lues have correct referen ces.

32 33 34 35 3

Attachment 1 - 20 16 4th Qtr DCPP NPDES Worksheets.xlsm A B c D E F G H I J K L M N 0 p 1

2 Chlorine for eSMR 3

4 FILL IN ONLY SHADED/COLORED CELLS 5

6 Date 7 12/1/2016 12/2/2016 12/3/2016 12/412016 12/5/2016 1216/2016 12/7/2016 1218/2016 1219/2016 12110/2016 12111 /2016 12112/2016 12/13/2016 12114/2016 12115/2016 8 Unit 1 TRC loob) 12 14 14 < 10 12 no iniection <10 <10 <10 <10 < 10 <10 <10 no iniection no iniection 9 <10 142 14 <10 no iniection no iniection <10 <10 <10 <10 < 10 < 10 no injection no injection no injection 10 <10 15 14 <10 no iniection no iniection <10 <10 < 10 <10 < 10 <10 no injection no injection no iniection 11 <10 12 12 <10 no iniection no iniection 12 <10 <10 < 10 <10 <10 no iniection no iniection no iniection 12 13 18 <10 12 no iniection <10 < 10 <10 < 10 < 10 <10 <10 no iniection <10 < 10 13 12 14 <10 <10 no injection <10 < 10 <10 <10 < 10 <10 <10 no iniection no iniection <10 14 Unit 1 Cl2 Use libs) 273.6 273.6 273.6 273.6 45 .6 27.6 11 5.2 11 5.2 11 5.2 115.2 115.2 115.2 19.2 33.6 36.0 15 Unit 2 TRC loobl 13 15 13 11 13 no iniection <10 21 19 18 18 19 19 no injection no injection 16 16 15 15 11 no iniection no iniection <10 21 18 18 18 21 no injection no injection no iniection 17 13 12 13 11 no iniection no iniection <10 21 18 18 18 19 no iniection no iniection no iniection 18 13 11 12 11 no iniection no iniection 21 19 18 18 16 21 no iniection no iniection no iniection 19 13 15 12 12 no iniection < 10 21 19 19 18 <10 < 10 no injection no injection 10 20 15 16 11 12 no iniection < 10 23 19 18 16 19 19 no injection no iniectlon 11 21 Unit 2 Cl2 Use (lbs l 302 .4 302.4 302 .4 302.4 50.4 55.2 230.4 230.4 230.4 230 .4 192 192.0 38.4 0.0 36.0 22 23 13 142 14 12 12 0 12 0 0 0 0 0 0 0 0 24 16 16 15 12 13 0 23 21 19 18 19 21 19 0 11 25 Daily Maximum TRC {ppb) 16 142 15 12 13 0 23 21 19 18 19 21 19 0 11 26 Da ily Cl2 Use (lbs ) 576 576 576 576 96 83 346 346 346 346 307 307 58 34 72 27 28 29 30 31 32 33 34 35 4

Attachment 1 - 2016 4th Qtr DCPP NPDES Worksheets.xlsm Q R s T u v w x y z AA AB AC AD AE AF AG 1

2 3

4 5

6 7 12116/2016 12117/2016 12/18/2016 12/1912016 1212012016 12121/2016 1212212016 1212312016 12/2412016 1212512016 1212612016 1212712016 1212812016 12/2912016 1213012016 12131/2016 8 <10 17 14 11 12 12 18 22 18 20 20 18 20 17 18 20 9 <10 18 15 11 12 11 18 20 18 24 18 18 17 17 22 20 10 < 10 20 12 <10 12 < 10 18 20 18 24 18 18 17 15 17 17 11 < 10 17 <1 0 <10 11 17 20 20 18 22 18 19 17 18 18 17 12 13 15 < 10 <10 13 18 20 20 20 22 18 19 18 18 20 17 13 17 15 11 <10 11 18 20 18 20 24 17 20 17 18 20 17 14 134.4 216.0 201.6 20 1.6 201.6 20 1.6 201.6 20 1.6 201 .6 201.6 201.6 20 1.6 20 1.6 201.6 20 1.6 20 1.6 15 11 18 18 11 16 13 21 25 23 25 23 21 21 21 23 25 16 11 19 16 13 15 12 21 23 23 28 23 21 21 21 25 25 17 10 19 15 12 15 11 23 25 23 31 23 21 21 21 23 23 18 11 19 12 13 13 19 25 25 23 28 21 21 21 25 23 21 19 12 18 11 13 13 21 25 25 25 25 21 21 21 25 25 21 20 16 19 12 15 13 23 25 23 25 25 21 21 21 25 25 21 21 134.4 230.4 230.4 230.4 230.4 230 .4 230 .4 232.6 244.8 244.8 244.8 244. 8 244.8 244.8 244 .8 244 .8 22 23 17 20 15 11 13 18 20 22 20 24 20 20 20 18 22 20 24 16 19 18 15 16 23 25 25 25 31 23 21 21 25 25 25 25 17 20 18 15 16 23 25 25 25 31 23 21 21 25 25 25 26 269 446 432 432 432 432 432 434 446 446 446 446 446 446 446 446 27 Chl o rine (ppb) (lbs/day)

Mo nthly 28 Averan e 23 372 29 MONTHLY CHLORINE USE: 11 ,523 lbs. Maximum 142 576 30 Minimum 0 34 31 Verify that values have correct references.

32 33 34 35 4

Attachment 1 - 2016 4th Qtr DCPP NPDES Worl<sheets.xlsm A B I c I D I E F G H I J K L M N 0 2 I I 3 LRW TSS Data I 5 2.0 mg/Lis MDL. 5.0 mg/L Is Reporting Limit.

6 Results are reported to the Water Board to whole numbers onlv !no tenths I.

8 System Batch Tank Volume Discharge Date Status Fiiter 1 Filter 2 Net TSS TSS for avg. Unused Volumes Weight Weighted TSS 9 LRW 89 ORR 0-1 9,618 10/11/201610:10 0 0.7 #N/A ND(21 0.0 0.49 0.00 10 LRW 90 LDT C>-1 9,659 10/11/201614:40 0 0.4 #N/A ND(2) 0.0 0.49 0.00

'11 LRW LDT 0-1 dup 0.3 #N/A NDl2l 12 LRW 91 ORR C>-2 10/13/2016 9:15 0 7,840 13 LRW 92 ORR 0-1 10/14/2016 9:40 0 10,071 14 LRW 93 CDT (}.2 529 10/271201611 :50 0 22.0 0.0 22.0 24.3 0.03 0.65 15 LRW CDT 0-2 dup 27.4 0.9 26.5 16 LRW 94 ORR C>-2 10128/2016 6:40 0 10,077 17 LRW 18 LRW 19 LRW 20 LRW 21 LRW 22 LRW 23 LRW 24 LRW 25 LRW 26 LRW 27 LRW 28 LRW 29 LRW 30 LR W 31 LRW 32 LRW 33 LRW 34 LRW 35 LRW 36 LRW 37 LRW 38 LRW 39 40 total volume of samoled tanks : 19,806 total sum of volume welahts: 1.00 Monthly LRW TSS Average 41 42 Reoort <5 because CDT 0-2 >5 43 44 45 001D O&G Data 47 1.4 mg /Li s MDL. 5.0 mg/L Is Reporting Limit.

48 Results are reoorted to the Water Board to the nearest tenth ma/L.

50 System Batch Tank Volume Di scharge Date Status Result O&G for avg. Weight Weighted O&G 51 LRW 89 ORR (}.1 9,618 10/11/2016 10:10 0 NDl1.4) 0.0 0.49 0.00 52 LRW 90 LDT C>-1 9,659 10/11 /2016 14:40 0 ND(1.4) 0.0 0.49 0.00 53 LRW 93 CDT 0-2 529 10/2712016 11 :50 0 NDl1.4l 0.0 0.03 0.00 54 LRW 55 LRW 56 LRW 57 LRW

~ LRW 59 LRW 60 61 total volume of sampled tanks: 19,806 total sum of volume weights: 1. 00 Monthly O&G Average 62 I 63 I I Report ND (1 .4) 64 I I

Attachment 1 - 2016 4th Qtr DCPP NPDES Worl<sheets.xlsm A B I c I D I E F G H I J K L M N 0 2 I 3 LRW TSS Data I 5 2.0 mg/L is MDL. 5.0 mg/L Is Reporting Limit.

6 Results are reported to the Water Board to whole numbers only (no tenths}.

....!. System Batch Tank Volume Discharge Date Status Filter 1 Fiiter 2 Net TSS TSS for avg. Unused Volumes Weight Weighted TSS 9 LRW 95 ORR 0-1 5,075 11/3/20168:15 0 0.0 #N/A ND(2) 0.0 0. 17 0.00 10 LRW 96 LDT 0-1 14,989 11/4/2016 9:25 0 0.2 #N/A ND(2) 0.0 0.49 0.00 11 LRW LDT 0-1 dup 0.4 #N/A ND(2) 12 LRW 97 ORR 0-2 11/9/20161 2:00 0 8,633 13 LRW 99 LDT 0-2 11 /10/2016 9:30 0 14,989 14 LRW 98 CDT 0-1 533 11/1012016 15:45 0 31.5 0.0 31.5 30.0 0.02 0.52 15 LRW CDT 0-1 dup 29.0 0.5 28.5 16 LRW 100 ORR 0-1 11/16/2016 9:10 0 8,667 17 LRW 101 ORR 0-2 11/211201613:50 0 7,975 18 LRW 102 PWR 0-2 9,924 11123/2016 8:40 0 0.0 #N/A ND(2) 0 0.33 0.00 19 LRW 103 LDT 0-1 11/3012016 8:15 0 14,989 20 LRW 21 LRW 22 LRW 23 LRW 24 LRW 25 LRW 26 LRW 27 LRW 28 LRW 29 LRW 30 LRW 31 LRW 32 LRW 33 LRW 34 LRW 35 LRW 36 LRW 37 LRW 38 LRW 39 40 total volume of samoled tanks: 30,521 total sum of volume weiahts: 1.00 Monthly LRW TSS Ave rage 41 ~

42 Reoort ~~RL 43 44 45 001D O&G Data 47 1.4 mg/L Is MDL. 5.0 mg/L Is Reoortlng Limit.~~

~~48 Results are reoorted to the Water Board to th e nearest tenth ma/L.~~

50 System Batch Tank Volume Discharge Date Status Result O&G for avg. Weight Weighted O&G 51 LRW 98 CDT 0-1 533 11/101201615:45 0 2.5 2.5 1.00 2.50 52 LRW 53 LRW 54 LRW 55 LRW 56 LRW 57 LRW SB LRW 59 LRW 60 61 total volume of samoled tanks: 533 total sum of volume weiahts: 1.00 Monthly O&G Average 62 63 Reoort DNQ r2. Sl I 64 I 6

Attachment 1 - 2016 4th Qtr DCPP NPDES Worl<sheets.xlsm I A B c D E F G H I J K L M N 0 2 I I 3 LRW TSS Data I 5 2.0 mg/L is MDL. 5.0 mg/L Is Reoortlna Limit.

~~6 Results are reoorted to the Water Board to whole numbers onlv (no tenths).~~

B Svstem Batch Tank Volume Discharae Date Status Filter 1 Fiiter 2 NetTSS TSS forava. Unused Volumes Welaht Welahted TSS 7 LRW 104 PWR 0-1 12/112016 10:20 0 9,205 10 LRW 105 CDT 0-2 460 12113/2016 8:53 0 41 .1 0.4 40.7 39.7 0.02 0.63

'11 LRW CDT 0-2 dup 38.7 0.0 38.7 12 LRW 106 PWR 0-2 7,335 12/13/201611:42 0 0.2 #N/A ND(2) 0.0 0.25 0.00 13 LRW 107 LDT 0-2 14,989 12/20/2016 9:20 0 0.2 #N/A ND(2) 0.0 0.52 0.00 14 LRW LDT 0-2 dup 0.3 #N/A NDl2l 15 LRW 108 FDR 0-2 6,185 12/21/2016 7:05 0 4.2 #N/A DNQ(4.2) 0.0 0.21 0.00 16 LRW 109 PWR 0-1 1212212016 7:53 0 9,061 17 LRW 110 FDR 0-1 12/28/2016 7:00 0 10,499 18 LRW 111 PWR 0-2 12/29/2016 8:00 0 719 19 LRW 20 LRW 21 LRW 22 LRW 23 LRW 24 LRW 25 LRW 26 LRW 27 LRW 28 LRW

29 LRW 30 LRW 31 LRW 32 LRW 33 LRW 34 LRW 35 LRW 36 LRW 37 LRW 38 LRW 39 40 tota l volume of samoled tanks: 28,969 tota l sum of volume weia hts : 1.00 Monthly LRW TSS Average 41 .
42 Report <5 Because CDT 0-2 >RL 43 44 45 001D O&G Data 47 1.4 mg/L Is MDL. 5.0 mg/L Is Reporting Limit.
48 Results are reoorted to the Water Board to the neareot tenth mall.
50 Syotem Batch Ta nk Volume Discharge Date Status Resu lt O&G for avg. Weight Weighted O&G 51 LRW 105 CDT 0-2 460 12113/2016 8:53 0 ND(1.4) 0.0 0.03 0.00 52 LRW 106 PWR 0-2 7,335 12113/201611 :42 0 ND(1.4) 0.0 0.52 0.00 53 LRW 108 FDR 0-2 6,185 12121/2016 7:05 0 NDl1.4) 0.0 0.44 0.00 54 LRW 55 LRW 56 LRW 57 LRW 58 LRW 59 LRW 60 61 tota l volume of sampled tanks: 13,980 total sum of volume weiahts: 1.00 Monthly O&G Average 62 63 Report ND! 1.4) I 64 I
Attachment 1 - 2016 4th Qtr DCPP NPDES Worksheets.xlsm A B c D E F G H 2
3 001N Monthly AYeraQe Calculations 4 NOTE: Values <ReoortinQ Limit are treated as 0 when aYeraQed with values ?: RL.
5 All Results on t his sheet are included in Vendor Laboratorv Data 6
7 0.24 mg/L is O&G method 1664 MDL for BSK Lab.
8 5.0 mg/Lis O&G Method 1664 Reporting Limit.
9 Results are reported to the Water Board to the nearest tenth mg/L.
10 11 Oil and Grease (mQ/Ll 12
- Numerical Daily Results for Monthly Report Monthly Date Result Average Qualifier 14 AveraQe AveraQe AYeraQe 15 10/4/2016 DNQ (O 30) 0.23 DNQ 0.23 0.16 16 10/4/2016 ND(0.24) Report DNQ(0.24) 17 10/4/2016 DNQ(0.39) 18 10/11/2016 ND(0.24) 0.20 DNQ 0.20 Daily Maximum 19 10/11/2016 ND(0.24) 0.2 20 10/11/2016 DNQ(059) 21 10/17/2016 ND(0.24) 0.10 DNQ 0.10 22 10/17/2016 ND(0.24) 23 10/17/2016 DNQ (0.30) 24 10/25/2016 ND(0.24) 0.10 DNQ 0.10 25 10/25/2016 ND(0.24) 26 10/25/2016 DNQ(O 30) 27 28 29 30 31 32 Total Suspended Solids (mg/L)
Date Result Numerical Resu lt Monthly Average 34 35 10/4/2016 9 9 9 36 10/11/2016 16 16 37 10/17/2016 4 4 Daily Maximum 38 10/25/2016 7 7 16 39 40 41 42 Settleable Solids (mill)
Date Result Numerical Result Monthly Average 44 45 10/4/2016 0.1 0.1 0.0 46 10/11/2016 DN Q(0.1) 0.0 <0.1 because 10/1 result ;;,RL 47 10/17/2016 DNQ(0.1) 0.0 Daily Maximum 48 10/25/2016 DNQ(O 1) 00 0.1 49 50 51 52 8
Attachment 1 - 2016 4th Qtr DC PP NPDES Worksheets.xlsm A B c D E F G H 2
3 001N Monthly Average Calculations 4 NOTE: Values <Reporting Limit are treated as 0 when averaged with values ~ RL.
5 All Results on this sheet are included in Vendor Laboratory Data 6
7 0.24 mq/L is O&G method 1664 MDL for BSK Lab.
8 5.0 mq/L is O&G Method 1664 Reoortinq Limit.
9 Results are reported to the Water Board to the nearest tenth mq/L.
10 11 Oil and Grease (mg/L) 12 Numerical Daily Results for Monthly Report Monthly Date Result Average Qua lifier 14 Averacie Avera(le Avera(le 15 11/2/2016 DNQ(0.29) 0.43 DNQ 0.43 0.23 16 11/212016 DNQ(0.30) Report DNQ(O 24) 17 11/2/2016 DN Q(0.69) 18 11/8/2016 ND(0.24) 000 ND 0.00 Daily Maximum 19 11/8/2016 ND(0.24) 0.4 20 11/8/2016 NDI024) 21 11/16/2016 DNQ (0.40) 0.36 DNQ 0.36 22 11/16/2016 DNQ(0.39) 23 11/16/2016 DNQ (0.30) 24 11/21/2016 ND(0.24) 0.13 DNQ 0.13 25 11/21/2016 DNQ(0.40) 26 11/21/2016 ND(024) 27 28 29 30 31 32 Total Suspended Solids (mQ/L)
Date Result Numerical Result Monthly Average 34 35 11/2/2016 9 9 7 36 11/8/2016 10 10 37 11/16/2016 4 4 Daily Maximum 38 11/21/2016 4 4 10 39 40 41 42 Settleable Solids (ml/L)
Date Result Numerical Result Monthly Average 44 45 11/2/2016 11/ 0.0 DNQ(0.1) 46 11/8/2016 DN QI0.1l 00 Report DNQ(0.1l 47 11/16/2016 DN Q(01) 0.0 Da ily Maximum 48 11/21/2016 DN Q(0.1) 0.0 0.0 49 50 51 52 9
Attachment 1 - 2016 4th Qtr DCPP NPDES Worksheets.xlsm A B c D E F G H 2
3 001N Monthly Average Calculations 4 NOTE: Values <Reporting Limit are treated as 0 when averaged with values 2 RL.
5 All Results on this sheet are included in Vendor Laboratory Data 6 -
7 0.24 mq/L is O&G method 1664 MDL for BSK Lab. (ONE-TIME EXCEPTION 12119/2016 sample MDL=1 .1 mg/L) 8 5.0 mq/L is O&G Method 1664 ReportinQ Limit.
9 Results are reported to the Water Board to the nearest tenth mq/L.
10 11 Oil and Grease (mg/L) 12 Numerical Daily Results for Monthly Report Monthly Date Result Average Qualifier 14 Averaqe Average Averaae 15 12/1/2016 DNQ(1 .0) 0.90 DNQ 0.90 0.88 16 12/1/2016 DNQ (0.79) Report DNQ(1.1) 17 12/1/2016 DNQ (0.90) 18 12/6/2016 DNQ(0.59) 0.20 DNQ 0.20 Daily Maximum 19 12/6/2016 ND(0.24) 1.67 20 12/6/2016 ND(0.24) 21 12/13/2016 DNQ (16) 1.63 DNQ 1.63 22 12/13/2016 DNQ(1.4) 23 12/13/2016 DNQ (1 .9) 24 I 12/19/2016 ND(1 .1) 0.00 ND 000 25 12/19/2016 ND(1.1) 26 12/19/2016 ND(1 .1) 27 12/27/2016 DNQ (1.8) 1.67 DNQ 1.67 28 12/27/2016 DNQ (1 .6) 29 12/27/2016 DNQ (1.6l 30 31 32 Total Suspended Solids (mq/L)
Date Result Numerical Result Monthly Average 34 35 12/1/2016 23 23 12 36 12/6/2016 5 5 37 12/13/2016 20 20 Daily Maximum 38 12/19/2016 5 5 23 39 12/27/2016 6 6 40 41 42 Settleable Solids (mill)
Date Result Numerical Result Monthly Average 44 45 12/1/2016 DNQ (0.1) 0.0 DNQ(01) 46 12/6/2016 DNQ(0.1) 00 Reoort DNQ (0.11 47 12/13/2016 DNQ (01 ) 0.0 Daily Maximum 48 12/19/2016 DNQ(0.1) 0.0 0.0 49 12/27/2016 DNQ (01) 00 50 51 52 10
Attachment 1 - 2016 4th Qtr DCPP NPDES Worksheets.x1sm A B c D E F G H I J K L M N 2
3 Miscellaneous Da ily Duplicate/Averacie and Monthh Averacie Calculations for eSMR 4
5 Duplicate pH Averacies 6
7 Date Time Analvsis Date Location Unit Parameter Result Averaqe 8
9 10/10/2016 10:20 10/10/2016 001P N/A pH 7.70 7.7 10 10/10/2016 10:20 10/10/2016 001P N/A pH 7.71 11 12 13 Monthly TSS Averaqes 14 15 2 mg/Lis MDL. 5 mg/Lis Reporting Limit.
16 Results are reported to the Water Board to whole numbers only (no tenths). Numerical Reported 17 TSS for Daily Monthly Monthly 18 Date Time Analysis Date Location Unit Sample TSS Filtrate TSS Net TSS Averacie Averacie Averacie Averacie 19 I 20 10/3/2016 16:00 10/4/2016 001F NIA 2.7 0.0 DNQ(3) 2.7 3.0 3.0 DNQ(3) 21 10/3/2016 16:00 10/4/2016 001F N/A 3.3 0.1 DNQ(3) 3.2 22 23 10/2/2016 21 :10 10/2/2016 001H 1 1.0 0.0 ND(2) 0.0 0.0 0.0 ND(2) 24 10/2/2016 2:30 10/2/2016 I 001H 2 0.3 0.0 ND(2) 0.0 25 26 10/3/2016 13:40 10/3/2016 001L 1 0.0 #N/A ND(2) 0.0 0.0 0.0 ND(2) 27 10/3/201 6 13:50 10/3/2016 001L 2 0.0 #N/A ND(2) 0.0 28 I 29 10/10/2016 8:20 10/10/2016 001P N/A 4.2 0.6 DNQ(3.6) 0.0 9.8 9.8 10 30 10/10/2016 10:20 10/10/2016 001P N/A 10.7 0.9 9.8 9.8 31 10/10/2016 13:30 10/10/2016 001P N/A 20.8 1.3 19.5 19.5 32 33 10/6/20 16 9:10 10/6/2016 003 N/A 3.4 1.0 DN Q(2.4) 2.4 2.4 2.4 DNQ(2) 34 10/6/2016 9:10 10/6/2016 003 N/A 2.9 0.5 DNQ(2.4) 2.4 35 36 37 38 39 40 41 42 43 44 45 11
Attachment 1 - 2016 4th Qtr DCPP NPDES Worksheets.xlsm A B c D E F G H I J K L M N 2
3 Miscellaneous Daily Duplicate/Averac:ie and Month I\ Averac:ie Calculations for eSMR 4
5 Duplicate pH Averages 6
7 Date Time Analysis Date Location Unit Parameter Result Averac:ie 8
N/A -
9 11/10/2016 8:40 11/10/2016 001 P pH 7.85 7.9 10 11 /10/20 16 8:40 11/10/201 6 001P ,lll.8.. pH 7.85 11 12 13 Monthly TSS Averac:ies 14 15 2 mg/Lis MDL. 5 mc:i/L is Reportinc:i Limit.
16 Results are reported to the Water Board to whole numbers only (no tenths) . Numerical Reported 17 TSS for Daily Monthly Monthly 18 Date Time Analysis Date Location Unit Sample TSS Filtrate TSS Net TSS Averac:ie Average Averac:ie Averac:ie
~IA 19 20 11 /3/2016 7:20 111312016 001 F 2.1 0.0 DN Q(2. 1) 2.1 2.0 2.0 DNQ(2) 21 11/3/2016 7: 20 11 /3/2016 001 F NIA 2.3 0.4 DN Q(1 .9) 1.9 22 23 11/1/20 16 16:40 11/1/2016 00 1H 1 6.7 1.9 DN Q(4.8) 4.8 4.8 2.4 DN Q(2) 24 11/2/20 16 9:30 11 /2/2016 001 H 2 0.2 0.2 ND(2) 0.0 0.0 25 26 11 /2/201 6 7:15 11 13/2016 00 1L 1 0.0 #N/A ND(2) 0.0 0.0 0.0 ND(2) 27 11 /2/2016 7:20 11 /3/2016 00 1L 2 0.0 #NIA ND(2) 0.0 28 29 11/1012016 8:40 1111012016 001P NIA 37. 6 0.7 36.9 36 .9 15.4 15.4 15 30 11/1012016 12: 00 11 /10/2016 001 P N/A 9.9 0.7 9.2 9.2 31 11/10/2016 14:35 11 /10/2016 001P N/A 1.2 1.1 ND(2) 0.0 32 33 11 /7/2016 12:47 11 /9/20 16 003 N/A 6.3 0.2 6.1 6.1 6.2 6.2 6 34 1117/2016 12:47 11 /9/2016 003 N/A 6.7 0.4 6. 3 6.3 35 36 37 38 39 40 41 42 43 44 45 12
Attachment 1 - 20 16 4th Qtr DCPP NPDES Worksheets.xlsm A B c D E F G H I J K L M N 2
3 Miscellaneous Daily Duplicate/Average and Month!\ Average Calculations for eSMR 4
5 Duplicate pH Avera<1es 6
7 Date Time Analysis Date Location Unit Parameter Result Avera<1e 8
9 1217/2016 9:00 1217/2016 00 1P N tA pH 7.60 7.6 10 1217/2016 9:00 1217/2016 00 1P /A pH 7. 65 11 12 13 Monthly TSS Averages 14 15 2 m<1/L is MDL. 5 m<1/L is Reportinq Limit.
16 Results are reported to the Water Board to whole numbers only (no tenths). Numerical Reported 17 TSS for Daily Monthly Monthly 18 Date Time Analysis Date Location Unit Sample TSS Fi ltrate TSS Net TSS Average Average Average Average
~/A 19 20 12/1/2016 7:37 12/1/2016 00 1F 6.0 0.0 6.0 6.0 5.5 5.5 6 21 12/1/2016 7:37 12/1/2016 00 1F N/A 5.3 0.3 5.0 5.0 22 23 12/1 /2016 15:15 12/1/2016 001 H 1 4.9 4.2 ND(2) 0.0 0.0 0.0 ND(2) 24 12/1 /2016 14:55 12/1/2016 001 H 2 0.4 0.2 ND(2) 0.0 25 26 12/5/201 6 8:30 12/5/2016 001L 1 0.0 #N/A ND(2) 0.0 0.0 0.0 ND(2) 27 12/5/2016 8:40 12/5/201 6 001 L 2 0.0 #N/A ND (2) 0.0 28 29 12/7/2016 9:00 12/7/2016 00 1P N/A 3.9 0.8 DN Q(3.1) 0.0 16.3 16.3 16 30 12/7/2016 12:05 1217/2016 00 1P N/A 1.8 0.6 ND(2) 0.0 31 1217/2016 15:00 1217/2016 00 1P NIA 49.1 0.3 48 .8 48.8 32 33 12/5/2016 13:00 12/5/2016 003 N/A 3.6 0.1 DNQ(3.5) 3.5 3.4 3.4 DNQ(3) 34 12/5/20 16 13:00 12/5/2016 003~ N/A 3.3 0.1 DNQ(3 .2) 3.2 35 36 37 38 39 40 41 42 43 44 45 13
Diablo Canyon Power Plant 2016 Fourth Quarter Contract Lab Results PDF Page Description 2-4 001 N Oil & Grease - 10/04/2016 5-7 001N Oil & Grease-10/11/2016 8-10 001 N Oil & Grease -10/17/2016 11 - 13 001 N Oil & Grease -10/25/2016 14-16 001 N Oil & Grease -11/02/2016 17 -19 001 N Oil & Grease -11/08/2016 20-22 001N Oil & Grease-11/16/2016 23-25 001N Oil & Grease-11/21/2016 26-28 001 N Oil & Grease - 12/01/2016 29-31 001N Oil & Grease-12/06/2016 32-34 001N Oil & Grease-12/13/2016 35-37 001N Oil & Grease-12/19/2016 38-40 001 N Oil & Grease -12/27/2016 41 001 N Suspended Solids, Settleable Solids - 10/04/2016 42 001N Suspended Solids, Settleable Solids-10/11/2016 43 001 N Suspended Solids, Settleable Solids - 10/17/2016 44 001 N Suspended Solids, Settleable Solids - 10/25/2016 45 001 N Suspended Solids, Settleable Solids - 11/02/2016 46 001 N Suspended Solids, Settleable Solids - 11/08/2016 47 001 N Suspended Solids, Settleable Solids -11/16/2016 48
001 N Suspended Solids, Settleable Solids -11/21/2016 49 001N Suspended Solids, Settleable Solids-12/01/2016 50 001 N Suspended Solids, Settleable Solids - 12/06/2016 51 001 N Suspended Solids, Settleable Solids - 12/13/2016 52 001 N Suspended Solids, Settleable Solids - 12/19/2016 53 001 N Suspended Solids, Settleable Solids - 12/27/2016 001 D Mercury - 10/04/2016 to 11/28/2016 Composite 001 F Mercury - 10/02/2016 to 10/09/2016 Composite 001 H, Unit 1 Mercury-10/03/2016 to 12/06/2016 Composite 54 001 H, Unit 2 Mercury- 10/03/2016 to 12/05/2015 Composite 091 L, Unit 1 Mercury-10/05/2016 to 12/07/2016 Composite 001 L, Unit 2 Mercury- 10/05/2016 to 12/07/2016 Composite 55 001 D Metals - 10/04/2016 to 11/28/2016 Composite 56-57 . Intake, Discharae 001 Ammonia as Nitrogen - 10/04/2016 58-62 Discharge 001 Acute Toxicity Test-12/20/2016 63-79 Dischan::ie 001 Chronic Toxicity Test-12/20/2016 Intake, Discharge 001 Annual Cyanide, Mercury, Metals, 80-87 PCB's, Chlorinated and Non-Chlorinated Phenolics -
10/19/2016 001 N Annual Sludge pH, Nitrate as Nitrogen, Total Kjeldahl 88-89 Nitrogen, Ammonia as Nitrogen, Phosphorus, Oil and Grease, Mercury, Metals, Moisture - 10/17/2016 and 11/01/2016 I
A6J0428r Main Project - e COC Trace (MDLs) 16-5718 DCWWTP Certificate of Analysis Sample ID: A6J0428-01 Sample Date -Time: 10/04/16 - 08:13 Sampled By: Jim Wysong Matrix: Water Sample
~~Description:~~
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A6J0428 FINAL 10182016 1327 Printed: 10/18/2016 Page 3of11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
A6J0428 Main Proje.ct - e COC Trace (MDLs) 16-5718 DCWWTP Certificate of Analysis Sample ID: A6J0428-02 Sample Date -Time: 10/04/16 - 08:24 Sampled By: Jim Wysong Matrix: Water Sample
~~Description:~~
Decant Arm. Sample Type: Grab BSK Associates Fresno Organics Oil and Grease 11664)
Total Oil & Grease EPA1664A ND 0.24 5.0 mg/L A613833 10/07/16 10/09/16
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A6J0428 Main Project - e COC Trace (MDLs) 16-5718 DCWWTP Certificate of Analysis Sample ID: A6J0428-03 Sample Date -Time: 10/04/16 - 08:37 Sampled By: Jim Wysong Me1trix:- Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease (1664)
Total Oil & Grease EPA 1664A 0.39 0.24 . 5.0 mg/L A613833 10/07/16 10/09/16
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A6J1335 Main Project - e COC Trace (MDLs) 16-5895 DCVV\/VTP Certificate of Analysis Sample ID: A6J1335-01 Sample Date - Time: 10/11/16 - 08:30 Sampled By: Jim Wysong Matrix: *Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease 11664)
Total Oil & Grease EPA 1664A ND 0.24 5.0 mg/L A614354 10/18/16 10/19/16
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A6J1335 Main Project - e COC Trace (MDLs) 16-5895 DC\1\1\NTP Certificate of Analysis Sample ID: A6J1335-02 Sample Date -Time: 10/11/16- 08:44 Sampled By: Jim \Nysong Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease (1664)
Total Oil & Grease EPA 1664A ND 0.24 5.0 mg/l A614354 10/18/16 10/19/16 A6J1335 FINAL 10252016 0904 Printed: 10/25/2016 Page 4of11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
A6J1335 Main Project"'. e COC Trace (MDLs) 16-5895 DC\l\/Wf P Certificate of Analysis Sample ID: A6J1335-03 Sample Date -Time: 10/11/16 - 08:55 Sampled By: Jim Wysong Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease 11664)
Total Oil & Grease EPA 1664A 0.59 0.24 5.0 mg/L A614354 10/18/16 10/19/16 A6J1335 FINAL 10252016 0904 Printed: 10/25/2016 Page 5of11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
A6J1979 Main Project - e COC Trace (MDLs) 16-6018 DC\1\1\NTP Certifi~ate of Analysis Sample ID: A6Ji979-01 Sample Date -Time: 10/17/16 - 09:12 Sampled By: Client Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics
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A6J1979 Main Project - e COC Trace (MDLs) 16-6018 DCWNTP Certificate of Analysis Sample ID: A6J 1979-02 Sample Date - Time: 10/17/16 - 09:21 Sampled By: Client \ . Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease (1664)
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A6J1979 Main Project - e COC Trace (MDLs) 16-6018 DCVVWTP Certificate of Analysis Sample ID: A6J1979-03 Sample Date -Time: 10/17/16 - 09:31 Sampled By: Client Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease 116641
- Total Oil & Grease EPA 1664A 0.30 0.24 5.0 mg/L A614516 10/20/16 10/22116 A6J1979 FINAL 10252016 0916 Printed: 10/25/2016 Page 5of11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com -
A6J3024 Main Project - e COC Trace (MDLs) 16-6218 DC\1\1\NTP Certificate of Analysis Sample ID: A6J3024-01 Sample Date -Time: 10/25/16 - 09:20 Sampled By: Jim Wysong Matrix: Water Sample
~~Description:~~
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A6J3024 Main Project - e COC Trace (MDLs) 16-6218 DC\MNf P Certificate of Analysis Sample ID: A6J3024-02 Sample Date -Time: 10/25/16- 09:30 Sampled By: Jim Wysong Matrix: Water Sample
~~Description:~~
Decant Arm .sample Type: Grab BSKAssociates Fresno Organics Oil and Grease (1664)
Total Oil & Grease EPA 1664A ND 0.24 5.0 mg/L A614943 10/28/16 10/30/16 A6J3024 FINAL 11032016 1449 Printed: 11/03/2016 Page 4of11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
A6J3024 Main Project - e COC Trace (MDLs) 16-6218 DC\A/INTP Certificate of Analysis Sample ID: A6J3024-03 Sample Date -Time: 10/25/16 - 09:41 Sampled By: Jim Wysong Matrix: Water Sample
~~Description:~~
Decant Ami Sample Type: Grab BSK Associates Fresno Organics Oil and Grease 11664!
Total Oil & Grease EPA 1664A 0.30 0.24 5.0 mg/l A614943 10/28/16. 10/30/16 J A6J3024 FINAL 11032016 1449 Printed: 11 /03/2016 Page 5 of 11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
A6K0461 Main Project - e COC Trace (MDLsJ 16-6405 DC\M'\/TP Certificate of Analysis Sample ID: A6K0461-01 Sample Date -Time: 11/02/16 - 07:33 Sampled By: Jim Wysong Matrix: Water Sample
~~Description:~~
Decant Ann Sample Type: Grab BSK Associates Fresno Org*anics Oil and Grease (16641 Total Oil & Grease EPA 1664A 0.29 0.24 5.0 mg/l A615608 11/11/16 11/13/16 I
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ASSOCIATES A6K0461 Main Project - e COC Trace (MDLs) 16-6405 DCVVWTP
<::ertificate of Analysis Sample ID: A6K0461-02 Sample Date -Time: 11/02/16 - 07:44 Sampled By: Jim \Nysong
~~Matrix: Water Sample~~
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease 11664!
Total Oil & Grease EPA 1664A 0.30 0.24 5.0 mg/L A615608 11/11/16 11/13/16 A6K0461FINAL11162016 1701 Printed: 11/16/2016 QA-RP-0001-10 Final.rpt www.BSKAssociates.com Page 4 of 11 I.
A6K0461 Main Project - e COC Trace (MDLs) 16-6405 DC\1\1\/VTP Certificate of Analysis Sample ID: A6K0461-03 Sample Date -Time: 11/02/16- 07:54 Sampled By: J.im Wysong Matrix: Water Sample
~~Description:~~
~~Decant Arm Sample Type: Grab BSK Associates Fresno Organics~~
~~Oil and Grease (1664!~~
Total Oil & Grease EPA 1664A 0.69 0.24 5.0 mg/L A615608 11/11/16 11/13/16
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A6K1949 Main Project - e COC Trace (MDLs) 16-6760 DCWWTP Certificate of Analysis Sample ID: A6K1949-01 Sample Date - Time: 11 /16/16 - 11 :13 Sampled By: Jim Wysong Matrix: Water Sample
~~Description:~~
Decant Arm Sar:nple Type: Grab BSK Associates Fresno Organics Oil and Grease (16641 Total Oil & Grease EPA 1664A 0.40 0.24 5.0 mg/L A616123 11/23/16 11/30/16 J
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A6K1949 Main Project - e COC Trace (MDLs) 16-6760 DCWWTP Certificate of Analysis Sample ID: A6K1949-02 Sample Date -Time: 11/16/16- 11:30
~~Sampled By: *Jim Wysong Matrix: Water Sample~~
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease (16641 Total Oil &.Grease EPA 1664A 0.39 0.24 5.0 mg/L A616123 11123/16 11/30/16 J A6K1949 FINAL 12052016 1250 Printed: 1215/2016 QA-RP-0001-10 Final.rpt Page 4of11 www.BSKAssociates.com
A6K1949 Main Project - e COC T~ace (MDLs) 16-6760 DCWWTP Certificate of Analysis Sample ID: A6K1949-03 Sample Date - Time: 11 /16/16 - 11 :48 Sampled By: Jim Wysong Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease 11664)
Total Oil & Grease EPA 1664A 0.30 0.24 5.0 mg/L A616123 11/23/16 11/30/16 J A6K1949 FINAL 12052016 1250 Printed: 12/5/2016 Page 5 of 11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
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ASSOCIATES A6K1069 Main Project - e COC Trace (MDLs) 16-6570 Severn Trent Services (DCVIM/TP)
Certificate of Analysis Sample ID: A6K1069-01 Sample Date -Time: 11/08/16- 10:45 Sampled By: Jim M. Wysong Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease 116641 Total Oil & Grease EPA 1664A ND 0.24 5.0 mg/L A615661 11/14/16 11/15/16 A6K1069 FINAL 11172016 1709 Printed: 11/17/2016 Page 3of10 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
A6K1069 Main Project - e COC trace (MDLs) 16-6570 Severn Trent Services (DC\/VV\/TP)
Certificate of Analysis Sample ID: A6K1069-02 Sample Date -Time: 11/08/16 - 10:55 Sampled By: Jim M. Wysong Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease 11664)
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A6K1069 Main Project - e COC Trace (MDLs) 16-6570 Severn Trent Services (DCVVVVTP)
Certificate of Analysis Sample ID: A6K106.9-03 Sample Date - Time: 11 /08/16 - 11 :04 Sampled By: Jim M. Wysong. Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease 11664)
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A6K2290 Main Project - e COC Trace (MDLs) 16-6851 DCWWTP ASSOCIATES Certificate of Analysis Sample ID: A6K2290-01 Sample Date -Time: 11/21/16 - 08:09 Sampled By: Jim Wysong
~~Matrix: Water Sample~~
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics t
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A6K2290 Main Project - e COC Trace (MDLs) 16-6851 DCWWTP _
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~~Description:~~
~~Decant Arm~~
~~Sample Type: Grab BSK Associates Fresno Organics Oil and Grease (1664)~~
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A6K2290 Main Project - e COC Trace (MDLs) 16-6851 DCWWTP Certificate of Analysis Sample ID: A6K2290-03 Sample Date -Time: 11/21/16 - 08:32 Sampled By: Jim Wysong Matrix: Water Sample
~~Description:~~
.Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease (1664)
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~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease 11664)
Total Oil & Grease EPA 1664A 1.0 0.24 . 5.0 mg/L A616707 12/10/16 12/.11/16 A6L0182 FINAL 12162016 1135 Printed: 12/16/2016 Page 3of11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
A6L0182
. Main Project - e COC Trace (MDLs) 16-7041 DCCWTP Certificate of Analysis Sample ID: A6L0182-02 Sample Date -Time: 12/01/16 - 08:57 Sampled By: Client Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease (1664)
Total Oil & Grease EPA 1664A 0.79 0.24 5.0 mg/L A616707 )2/10/16 12/11/16.
A6L0182 FINAL 12162016 1135 Printed: 12/16/2016 Page 4 of 11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
A6L0182 Main Project - e COC Trace (MDLs) 16-7041 DCCWTP Certificate of Analysis Sample ID: A6L0182-03 Sample Date -Time: 12/01/16 - 09:08 Sampled By: Client Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics
- --- -~~---------------- - - - - - - - - - - - - - - -
Oil and Grease (1664)
Total Oil & Grease EPA 1664A 0.90 . 0.24 5.0 mg/L . 1 A616707 12/10/16 12/11/16 J A6L0182 FINAL 12162016 1135 Printed: 12/16/2016 Page 5of11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
A6L0616 JVJain Project - e COC Trace (MDLs) 16-7133 DCVWJTP Certificate of Analysis Sample ID: A6L0616-01 Sample Da_te -Time: 12/06/16 - 08:31 Sampled By: . J. \/Vysong Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease 116641 Total Oil & Grease .EPA 1664A 0.59 0.24 5.0 mg/L A616893 12/14/16 12/15/16 J A6L0616 FINAL 12212016 1608 Printed: 1?/21/2016 Page 3 of 11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
A6L0616 Main Project - e COC Trace (MDLs) 16-7133 DC\/V\Nf P Certificate of Analysis Sample ID: A6L0616-02 Sample Date - Time: 12/06/1'6 - 08:43 Sampled By: J. Wysong Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease 116641 Total Oil & Grease EPA 1664A ND 0.24 5.0 mg/L A616893 12/14/16 12/15/16 A6L0616 FINAL 12212016 1608 Printed: 12/21/2016 Page 4of11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
A6L0616 Main Project- e COC Trace (MDLs) 16-7133 DCVVVVTP Certificate of Analysis Sample ID: A6L0616-03 Sample Date -Time: 12/06/16 - 08:58 Sampled By: J. \/\/ysong Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease 11664)
Total Oil & Grease EPA 1664A ND 0.24 5.0 mg/l A616893 _12/14/16 12/15/16 A6L0616 FINAL 12212016 1608 Printed: 12121/2016 Page 5of11 QA-RP-0001-10 Final.rpt
~~www.BSKAssociates.com~~
B=
ASSOCIATES Certificate of Analysis A6L1419 Main Project - e COC Trace (MDLs) 16-7309 DCVWJTP Sample ID: A6L 1419-01 Sample Date -Time: 12/13/16 - 09:16 Sampled By: Client Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Laboratory Fresno Organics Oil and Grease 1166481 Total Oil & Grease EPA 16648 1.6 1.1 5.0 mg/L A617363 12/26/16 12/26/16 I
ASL 1419 FINAL 12282016 1124 Printed: 12/28/2016
~~Page 3 of 11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com~~
A6L 1419 Main Project - e COC Trace (MDLs) 16-7309 DCWNTP Certificate of Analysis Sample ID: A6L 1419-02 Sample Date - Time: 12/13/16 - 09:27 Sampled By: Client Matrix: Water Sample
~~Description:~~
~~Decant Arm Sample Type: Grab BSK Associates Laboratory Fresno Organics Oil and Grease 1166481~~

~~---- --- - - - - -- ------- - ____ d Total Oil & Grease EPA 16648 1.4 1.1 5.0 mg/l A617363 12/26/16 12/26/16~~

/
A6L1419 FINAL 12282016 1124 Printed: 12/28/2016 Page 4 of 11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
B=
ASSOCIATES Certificate of Analysis A6L1419 Main Project - e COC Trace (MDLs) 16-7309 DC\MNTP Sample ID: A6L 1419-03 Sample Date - Time: 12/13/16 - 09:38 Sampled By: Client Matrix: Water Sample
~~Description:~~
Decant Arm *Sample Type: Grab BSK Associates Laboratory Fresno Organics Oil and Grease 1166481 Total Oil & Grease EPA 16648 1.9 1.1 5.0 mg/l A617363 12126/16 12126/16 ASL 1419 FINAL 12282016 1124 Printed: 12/28/2016 Page 5of11 QA-RP-0001-10 Final.rpt . www.BSKAssociates.com
B=
ASSOCIATES A6L2125 Main Project - e COC Trace (MDLs) 16-7429 DCWWTP Certificate of Analysis Sample ID: A6L2125-01 Sample Date - Time: 12/19/16 - 11 :41 Sampled By: Jim Wysong Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Laboratory Fresno Organics nalyte M
~----
1
~~Oil and Grease (16648)~~
Total Oil & Grease EPA 16648 ND 1.1 5.0 mg/l A700199 01/05/17 01/06/17 A6L2125 FINAL 01062017 1520 Printed: 1/6/2017 Page 3of11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
B=
ASSOCIATES Certificate of Analysis A6L2125 Main Project - e COC Trace (MDLs) 16-7429 DCWWTP Sample ID: A6L2125-02 Sample Date - Time: 12/19/16 - 11 :53.
Sampled By: Jim Wysong Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab
\
BSK Associates Laboratory Fresno Organics Oil and Grease 116648)
Total Oil & Grease EPA 16648 ND 1.1 5.0 mg/L A700199 01/05/17 01/06/17 A6L2125 FINAL01062017 1520 Printed: 1/6/2017 Page 4of11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
A6L2125 Main Project - e COC Trace (MDLs) 16-7429 DCWWTP Certificate of Analysis Sample ID: A6L2125-03 Sample Date - Time: 12/19/16 - 12:08 Sampled By: Jim Wysong Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Laboratory Fresno Organics Oil and Grease 116648)
Total Oil & Grease " EPA 16648 ' ND 1.1 5.0 mg/L A700199 01/05/17 01/06/17
/
/
A6L2125 FINAL 01062017 1520 Printed: 1/6/2017 I
Page 5 of 11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
A6L2735 Main Project - .e COC Trace (MDLs) 16-7557 DCWWTP Certificate of Analysis Sample ID: A6L2735-01 Sample Date -Time: 12/27/16 - 08:40 Sampled By: Jim Wysong Matrix: Water Sample
~~Description:~~
~~Decant Arm Sample Type: Grab BSK Associates Laboratory Fresno Organics Oil and Grease (16648)~~
Total Oil & Grease EPA 16648 1.8 1.1 5.0 mg/L A700001 01/02/17 01 /04/17 82.2, J A6L2735 FINAL 01042017 1107 Printed: 1/4/2017 Page 3 of 11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
A6L2735 Main Project - e COC Trace (MDLs) 16-7557 DCWWTP Certificate of Analysis Sample ID: A6L2735-02 Sample Date -Time: 12/27/16 - 08:51 Sampled By: Jim Wysong Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Laboratory Fresno Organics RL Units Mull Batch Prepared
-~---------------
Analyzed Qual I
Oil and Grease (16648)
Total Oil & Grease EPA 16648 1.6 1.1 5.0 mg/L A700001 01/02/17 01 /04/17 B2.2, J A6L2735 FINAL 01042017 1107 Printed: 1/4/2017 Page 4of11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
A6L2735 Main Project - e COC Trace (MDLs) 16-7557 DCWWTP Certificate of Analysis
/
Sample ID: A6L2735-03 Sample Date -Time: 12/27116 - 09:03 Sampled By: Jim Wysong Matrix: Water Sample
~~Description:~~
Decant Arm Sample Type: Grab BSK Associates Laboratory Fresno Organics Oil and Grease (16648)
Total Oil & Grease EPA 16649 .1.6 1.1 5.0 mg/L A700001 01/.02117 01/04/17 82.2, J
\.
. A6L2735 FINAL01042017 1107 Printed: 1/4/2017 Page 5of11 QA-RP-0001-10 Final.rpt www.BSKAssociates.com
Abalone Coast Analytical, Inc. Order #: 16-5718 141 Suburban Rd, Ste C-1 San Luis Obispo CA, 93401 Date/Time Rec'd: 10/4/16 1512 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWTP
~~Contact:~~
Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP Sample# Sample Description Date I Time Analysis Method Result MDL RL Oil Factor Units Completed
-1 Decant Arm 10/4/16 0813 Suspended Solids SM*2540 D. 9. 2.57 3. 1 mg/L 10/06/16
-2 Decant Arm 10/4/16 0830 Settleable Solids SM 2540 F. 0.1 0.1 1 mUL 10/04/16
-6 Influent PRT 10/4/16 0810 Suspended Solids SM 2540 D. 567. 2.57 3. 1 mg/L 10/06/16 SUB Oil & Grease Report Completion date: 10/7/16 Reviewed:
~~~~~~~~~~~~~~~~
Amanda Smith, Lab Director Definitions:
mUL =milliliters per liter (ppm) mg/L = milligrams per liter (ppm)
MDL= Method Detection Limit RL = Reporting Limit ND = Analyte NOT DETECTED at or above MDL QA/QC Results Description Run Date Test Method Result Units Difference %
16-5740-2 10/6/2016 Suspended Solids SM 25400 10. mg/L Acceptable
_Duplicate 16-5740-2 10/6/2016 Suspended Solids Dup. SM 25400 , 11. mg/L 104% Rec 10/6/2016 Suspended Solids SM 25400 <3. mg/L < 5% of Average
Abalone Coast Analytical? Inc. Order #: 16-5895
/
141 Suburban Rd, Ste C-1 San Luis Obispo CA, 93401 OatefTime Rec'd: 10/11/16 1325 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWTP
~~Contact:~~
Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP Sample# Sample Description Date I Time Analysis Method Result MDL - RL Oil Factor Units Completed
-1 Decant Arm 10/11/16 0830 Suspended Solids SM 2540 D. 16. 2.57 3. 1 mg/L 10/13/16
-2 Decant Arm 10/11/16 0845 Settleable Solids SM 2540 F. <0.1 0.1 1 mUL 10/11/16
-2 Influent PRT 10/11/16 0815 Suspended Solids SM 2540 D. 468. 2.57 3. 1 mg/L 10/13/16 SUB 011 & Grease Report Completion date: 10/14/16 Reviewed:
~~~~~~~~~~~~~~~~~
Amanda Smith, Lab Director Definitions:
mUL =milliliters per liter (ppm)
, mg/L = milligrams per liter (ppm)
MDL = Method Detection Limit RL = Reporting Limit ND = Analyte NOT DETECTED at or abov~ MDL QA/QC Results Description Run Date Test Method Result Units Difference %
16-5838-3 10/13/2016 Suspended Solids SM 25400 315. mg/L Acceptable Duplicate 16-5838-3 10/13/2016 Suspended Solids Oup. SM 25400 283. mg/L 90% Rec 10/13/2016 Suspen_ded Solids SM 25400 <3. mg/L < 5% of Average
Abalone CoastAnalytical, Inc. Order#: 16-6018 141 Suburban Rd, Ste C-1 San Luis Obispo CA, 93401 Date/Time Rec'd: 10/17/16 1502 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWTP ,
~~Contact:~~
Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP Sample# Sample Description Date I Time Analysis Method Result MDL RL Oil Factor Units Completed
-1 Decant Arm 10/17/16 0912 Suspended Solids SM 2540 D. 4. 2.57 3. 1 mg/L 10/18/16
-2 Decant Arm 10/17/16 0930 Settleable Solids SM 2540 F. <0.1 0.1 1 mUL 10/18/16
-3 Influent PRT 10/17/16 0920 Suspended Solids SM 2540 D. 204. 2.57 3. 1 mg/L 10/18/16 SUB Oil & Grease Report Completion date: 10/21/16 Reviewed:
~~~~~~~~~~~~~~~~~
~~Amanda Smith, Lab Director Definitions:~~
mUL = milliliters per liter (ppm) mg/L = milligrams per liter (ppm)
MDL= Method Detection Limit RL = Reporting Limit ND = Analyte NOT DETECTED at or above MDL QA/QC Results Description Run Date Test Method . Result Units Difference %
16-6002-1 10/18/~016 Suspended Solids SM 25400 I 18. mg/L Acceptable Duplicate 16-6002-1 10/18/2016 Suspended Solids Dup. SM 25400 19. mg/L 93% Rec 10/18/201 S Suspended Solids SM 25400 <3. mg/L < 5% of Average
Abalone Coast Analytical, Inc. Order #: 16-6218 141 Suburban Rd, Ste C-1 San Luis Obispo CA, 93401 Date/Time Rec'd: 10/25/16 1331 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWTP
~~Contact:~~
Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP Sample# Sample Description Date I Time Analysis . Metl)od Result MDL RL Oil Factor Units Completed
-1 Decant Arm 10/25/16 0920 Suspended Solids SM 2540 D. 7. 2.5.7 3. 1 mg/L 10/27/16
-2 Decant Arm 10/25/16 0935 Settleable Solids SM 2540 F. <0.1 0.1 1 mUL 10/25/16
-~
-6 Influent PRT 10/25/16 0945 Suspended Solids SM 2540 D. 856. 2.57 3. 1 mg/L 10/27/16 SUB 011 & Grease Report Completion date: 10/31/16 Reviewed:
Amanda Smith, Lab Director Definitions:
mUL = milliliters per liter (ppm) mg/L =milligrams per liter (ppm)
MDL = Method Detection Limit
~~RL = Reporting Limit ND = Analyte NOT DETECTED at or above MDL QA/QC Results Description Run Date Test Method Result Units Difference %~~
16-6218-1 10/27/2016 Suspended Solids SM 25400 7. mg/L 100% , Acceptable Duplicate 16-6218-1 10/27/2016 Suspended Solids Dup. SM 25400 7. mg/L 100%
100% Rec 16-6218-1 10/27/2016 Suspended Solids SM 25400 <3. mg/L < 5% of Average
Abalone Coast Analytical, Inc. Order#: 16-6570 141 Suburban Rd, Ste C-1 San Luis Obispo CA, 93401 OatefTime Rec'd: 11 /8/16 1340 Phone: 595-1080 Fax: 595-1080 Diablo* Canyon WWTP
~~Contact:~~
Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP Sample# Sample Description Date I Time Analysis Method
~~Result MDL RL Oil Factor Units Completed~~
-1 Decant Arm 11/8/16 1045 Suspended Solids SM 2540 D. ...- 10. 2.57 3. 1 mg/L 11/10/16
-2 Decant Arm 11 /8/16 1100 Settleable Solids SM 2540 F. <0.1 0.1 1 mUL 11/08/16 SUB Oil & Grease Report Completion date: 11/15/16 Reviewed: ~~~~~~~~~~~~~~~~
Amanda Smith, Lab Director Definitions:
mUL = milliliters per liter (ppm) mg/L = milligrams per liter (ppm)
MDL= Method Detection Limit RL = Reporting Limit ND = Analyte NOT DETECTED at or above MDL QA/QC Results Description Run Date Test Method Result Units Difference%
6576-1 11/10/2016 Suspended Solids SM 25400 84. mg/L Acceptable
~:-'. '
Duplicate 6576-1 11/10/2016 Suspended Solids Oup. SM 25400 82. mg/L 2%
Blank 11/10/2016 Suspended Solids SM 25400 <3. mg/L < 5% of Average
Abalone Coast Analytical, Inc. Order #: 16-6405 141 Suburban Rd, Ste C-1 San Luis Obispo CA, 93401 OatefTime Rec'd: 11/2/16 1342
-Phone: 595-1080 Fax: 595-1080
)
Diablo Canyon WWTP
~~Contact:~~
Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCVV.WTP Sample# Sample Description Date I Time Analysis Method Result MDL RL Oil Factor Units Completed
-1 Decant Arm 11/2/16 0733 Suspended Solids SM 2540 D. 9. 2.57 3. 1 mg/L 11/03/16
-2 Decant Arm 11/2116 0745 Settleable Solids SM 2540 F. <0.1 0.1 1 mUL 11/02/16 SUB Oil & Grease Report Completion date: 1117/16 Reviewed:
~~~~~~~~~~~~~~~~~
Amanda Smith, Lab Director Definitions:
mUL = milliliters per liter (ppm) mg/L = milligrams per liter (ppm)
MDL= Method Detection Limit RL =Reporting Limit ND = Analyte NOT DETECTED at or above MDL QA/QC Results Description Run Date Test Method Result Units Difference %
16-6358-1 11 /3/2016 Suspended Solids SM 25400
82. mg/L Acceptable Duplicate 16-6358-1 11 /3/2016 Suspended Solids Oup. SM 25400 82. mg/L 100% Rec 11 /3/2016 Suspended Solids SM 25400 <3. mg/L < 5% of Average
Abalone Coast Analytical, Inc. Order#: 16-6760 141 Suburban Rd, ~te C-1 San Luis Obispo CA, 93401 ~ OatefTime Rec'd: 11 /16/16 1256 Phone: 595-1080Fax: 595-1080 Diablo Canyon WWTP
~~Contact:~~
Jim Wysong 320 Beta Court '
Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP /
Sample# Sample Description Date I Time Analysis Method Result MDL RL Oil Factor Units Completed
-1 Decant Arm 11 /16/16 1113 Suspended Solids SM 2540 D. 4. 2.57 3. 1 mg/L 11/17/16
.-2 Decant Arm 11/16/16 0745 Settleable Solids SM 2540 F. <0.1 0.1 1 mUL 11/16/16 SUB 011 & Grease Report Completion date: 11/21/16 Reviewed:
~~~~~~~~~~~~~~~~~
Amanda Smith, Lab Director Definitions:
mUL = milliliters per liter (ppm) mg/L = milligrams per liter (ppm)
MDL=* Method Detection Limit RL '= Reporting Limit ND = Analyte NOT DETECTED at or above MDL QA/QC Results Description Run Date Test Method Result Units Difference %
16-6760-1 11/17/2016 Suspended Solids SM 25400 5. mg/L 100% Acceptable Duplicate 16-6760-1 11 /17 /2016 Suspended Solids Oup. SM 25400 5. mg/L 100%
100% Rec Blank 11/17/2016 Suspended Solids SM 25400 <3. mg/L < 5% of Average
Abalone Coast Analytical, Inc. Order#: 16-6851 141 Suburban Rd, Ste C-1 San Luis Obispo CA, 93401 Date/Time Rec'd: 11/21/161339 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWTP
~~Contact:~~
Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP Sample# Sample Description Date I Time Analysis Method Result MDL RL Oil Factor Units Completed
-1 Decant Arm 11/21/16 0809 Suspended Solids SM 2540 D. 4. 2.57 3. 1 mg/L 11/22/16
-2 Decant Arm 11/21/16 0825 Settleable Solids SM 2540 F. <0.1 0.1 1 mUL 11/22/16 SUB 011 & Grease Report Completion date: 11/23/16 Reviewed:
~~~~~~~~~~~~~~~~
Amanda Smith, Lab Director Definitions:
mUL = milliliters per liter (ppm}
mg/L = milligrams per liter (ppm)
MDL = Method Detection Limit RL =Reporting Limit ND = Analyte NOT DETECTED at or above MDL QA/QC Results Description Run Date Test Method Result Units Difference %
16-6795-2 11 /22/2016 Suspended Solids SM 25400 11. mg/L 1% Acceptable Duplicate 16-6795-2 11 /22/2016 Suspended Solids Dup. SM 25400 12. mg/L 1%
Rec 16-6795~2 11/22/2016 Suspended Solids SM 25400 <3. mg/L 1% < 5% of Average
Abalone Coast Analytical, Inc. Order #: 16-7041 141 Suburban Rd, Ste C-1 San Luis Obispo CA, 93401 OatefTime
\
Rec'd: 12/1/16 1335 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWTP
~~Contact:~~
Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP Sample# Sample Description Date I Time Analysis Method Result MDL RL Oil Factor Units Completed
-1 Decant Arm 12/1/16 0846 Suspended Solids SM 2540 D. 23. 2.57 3. 1 mg/L 12/05/16
\
-2 Decant Arm 12/1 /16 *0900 Settleab)e Solids SM 2540 F. <0.1 0.1 1 mUL 12/01/16 SUB Oil & Grease Report Completion date: 12/6/16 Reviewed: ~~~~~~~~~~~~~~~~~
Amanda Smith, Lab Director Definitions:
mUL =milliliters per liter (ppm) mg/L = milligrams per liter (ppm)
MDL= .Method Detection Limit RL = Reporting Limit ND = Analyte NOT DETECTED at or above MDL QA/QC Results Description Run Date Test Method Result Units Difference %
16-7077-1 12/5/2016 Suspended Solids SM 25400 7. mg/L Acceptable Duplicate 16-7077-1 12/5/2016 Suspended Solids Oup. SM 25400 8. mg/L Recovery 12/5/2016 Suspended Solids SM 25400 Rec 105%
Blank 12/5/2016 Suspended Solids SM 25400 <3. mg/L ~ 5% of Average
Abalone Coast Analytical, Inc. Order #: 16-7133 141 Suburban Rd, Ste C-1 San Luis Obispo CA, 93401 .Date/Time Rec'd: 12/6/16 1329 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWTP
~~Contact:~~
Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP Sample# Sample Description Date I Time Analysis Method Result MDL RL Oil Factor Units Completed
-1 Decant Arm 1216/16 0831 Suspended Solids SM 2540 D. 5. 2.57 3. 1 mg/L 12/08/16
-2 Decant Arm 12/6/16 0900 Settleable Solids SM 2540 F. <0.1 0.1 1 mUL 12/06/16 SUB Oil & Grease Report Completion date: 12/13/16 Reviewed:.
~~~~~~~~~~~~~~~~~
Amanda Smith, Lab Director
~~Definitions:~~
mUL = milliliters per liter (ppm) mg/L = milligrams per liter (ppm)
=
MDL Method Detection Limit
=
RL Reporting Limit ND = Analyte NOT DETECTED at or above MDL QA/QC Results Description Run Date Test Method Result Units. Difference %
16-7131-1 12/8/2016 Suspended Solids SM 25400 3.7 mg/L Acceptable Duplicate 16-7131-1 12/8/2016 Suspended Solids Dup. SM 25400 3.8 mg/L Recovery Suspended Solids SM 25400 Rec 103%
Blank 12/8/2016 Suspended Solids* SM 25400 <3. mg/L < 5% of Average
Abalone Coast Analytical, Inc. Order#: 16-7309 141 Suburban Rd, Ste C-1 San Luis Obispo CA, 93401 Date/Time Rec'd: 12/13/16 1422 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWTP
~~Contact:~~
Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP Sample# Sample Description Date I Time Analysis Method* Result MDL RL Oil Factor Units Completed
-1 Decant Arm 12/13/16 0916 Suspended Solids SM 2540 D. 20. 2.57 3. 1 mg/L 12/15/16
/
-2 Decant Arm 12113/16 0930 Settleable Solids SM 2540 F. <0.1 0.1 1 mUL 12/13/16 SUB Oil & Grease Report Completion date: 12119/16 Reviewed:
Amanda Smith, Lab Director Definitions:
mUL = milliliters per liter (ppm) mg/L = milligrams per liter (ppm)
=
MDL Method Detection Limit
=
RL Reporting Limit
=
ND Analyte NOT DETECTED at or above MDL QA/QC Results Description . Run Date Test Method Result Units Difference %
16-7304 12/15/2016 Suspended Solids SM 25400 26. mg/L Acceptable Duplicate 16-7304 12/15/2016 Suspended Solids Dup. SM 25400 26. mg/L Recovery 12/15/2016 Suspended Solids SM 25400 Rec 100%
Blank 12/15/2016 Suspended Solids SM 25400 <3. mg/L < 5% of Average
Abalone Coast Analytical, Inc. Order #: 16-7429 141 Suburban Rd, Ste C-1 San Luis Obispo CA, 93401 Date/Time Rec'd: 12/19/16 1315 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWTP
~~Contact:~~
Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP Sample# Sample Description Date I Time Analysis Method Result MDL RL Oil Factor Units Completed
-1 Decant Arm 12/19/16 1141 Suspended Solids SM 2540 D. 5. 2.57 3. 1 mg/L 12/22/16
-2 Decant Arm 12/19/16 0810 Settleable Solids SM 2540 F. <0.1 0.1 1 mUL 12/19/16 SUB Oil & Grease Report Completion date: 12/2]/16 Reviewed:
Amanda Smith, Lab Director Definitions:
mUL = milliliters per liter (ppm) mg/L = milligrams per liter (ppm)
MDL= Method Detection Limit RL =Reporting Limit ND = Analyte NOT DETECTED at or above MDL QA/QC Results Description Run Date Test Method Result Units Difference %
16-7453-1 12/22/2016 Suspended Solids SM 25400 9. mg/L Acceptable Duplicate 16-7453-1 12/22/2016 Suspended Solids Dup. SM 25400 9. mg/L Recovery 12/22/2016 Suspended Solids SM 25400 Rec 94%
Blank I
/ 12/22/2016 Suspended Solids SM 25400 <3. mg/L < 5% of Average
/
Abalone Coast Analytical, Inc. Order #: 16- 7557 141 Suburban Rd, Ste C-1 San Luis Obispo CA, 93401. Date/Time Rec'd: 12/27/16 1343 Phone: 595-1080 Fax:'595-1080 Diablo Canyon WWTP
~~Contact:~~
Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP .
Sample# Sample Description Date I Time Analysis Method Result MDL RL Oil Factor Units Completed
-1 - Decant Arm 12/27/16 0840 Suspended Solids SM 2540 D. 6. 2.57 3. 1 mg/L 12/29/16
-2 Decant Arm 12127/16 0855 Settleable Solids SM 2540 F. <0.1 0.1 1 mUL 12/27/16 SUB Oil & Grease -
Report Completion Date: 1/3/17 Reviewed: ~~~~~~~~~~~~~~~~~
Amanda Smith, Lab Director Definitions:
mUL = milliliters per liter (ppm) mg/L = milligrams per liter (ppm)
MDL= Method Detection Limit RL =Reporting Limit ND = Analyte NQT DETECTED at or above MDL QA/QC Results Description Run Date Test Method Result Units Difference %
16-7584-1 12/29/2016 Suspended Solids SM 25400 8. mg/L Acceptable
.J Duplicate 16-7584-1 12/29/2016 Suspended Solids Dup. SM 25400 8. mg/L Recovery Suspended Solids SM 25400 Rec 100%
Blank 12/29/2016 Suspended Solids SM 25400 <3. . mg/L < 5% of Average
Client Sample Results Client: PG&E Corporation TestAmerica Job ID : 160-20450-1 Project/Site: Diablo Canyon Power Plant Client Sample ID: 001F OWS 4TH QTR 2016 COMPOSITE Lab Sample ID: 160-20450-1 Date Collected: 12/14/16 10:00 Matrix: Water Date Received: 12/19/1611:00 Method: 245.1 - Mercury (CVAA)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
[ Mercury --~ N~D - .2 - 0.-08-0 -ug-/L_ _ _ 12/23/16 09:44 12/23/16 16:53 - - 1 Client Sample ID: 001H U-1CDRS4TH QTR 2016 COMPOSITE Lab Sample ID: 160-20450-2 Date Collected: 12/14/16 10:00 Matrix: Water Date Received: 12/19/16 11:00 Method: 245.1 - Mercury (CVAA)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
[ Mercury ND -~o ~.2= 0 -~o .=
08=0 ug~/L_ __
12/23/16 09:44 12/23/16 16:57 - - 1 Client Sample ID: 001H U-2 CDRS 4TH QTR 2016 COMPOSITE Lab Sample ID: 160-20450-3 Date Collected: 12/14/16 10:00 Matrix: Water Date Received: 12/19/16 11:00 Method: 245.1 - Mercury (CVAA)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
[ Mercury --~ N=o 0.20 -~o .=
08~0 -ug~/L___ 12/23/16 09:44 12/23/1617:00 - - 1 Client Sample ID: 001 L U-1 SGBD 4TH QTR 2016 COMPOSITE Lab Sample ID: 160-20450-4 Date Collected: 12/14/16 10:00 Matrix: Water Date Received: 12/19/16 11:00 Method: 245.1 - Mercury (CVAA)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
[ Mercury - - - - , -N=o -~o~.2= 0 -~o .=
08=0 -ug~/L___ 12/23/16 09:44 12/23/1617:03 - - 1 Client Sample ID: 001L U-2 SGBD 4TH QTR 2016 COMPOSITE Lab Sample ID: 160-20450-5 Date Collected: 12/14116 10:00 Matrix: Water Date Received: 12/19/16 11:00 Method: 245.1 - Mercury (CVAA)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
[ Mercury - - - - , -N=o 0.20 -~o .=
08=0 -ug~/L___ 12123116 09:44 12123/1617:07 - - 1 Client Sample ID: 001D LRW 4TH QTR 2016 COMPOSITE Lab Sample ID: 160-20450-6 Date Collected: 12/14/16 10:00 Matrix: Water Date Received: 12/19/16 11 :00 Method: 245.1 - Mercury (CVAA)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Oil Fae
[ Mercury --~ N=o -~0~ . 2~
0 -~0 .~
08~0 -ug-/L_ __ 12/23/16 09:44 12/23/16 17:10 - - 1 TestAmerica St. Louis Page 11 of 13
Client Sample Results Client: PG&E Corporation TestAmerica Job ID: 160-20449-1 ProjecUSite: Diablo Canyon Power Plant Client Sample ID: 0010 LRW 4TH QTR 2016 COMPOSITE Lab Sample ID: 160-20449-1 Date Collected: 12/14/16 10:00 Matrix: Water Date Received : 12/19/16 11:00 Method: 200.8 - Metals {ICP/MS)
Analyte Resu lt Qualifier RL MDL Unit D Prepared Ana lyzed Oi l Fae Silver 0.12 J 1.0 0.10 ug/L 12/28/1 6 10:36 12/28/1 6 16:53 - - 1 Cadmium 0.22 J 0.50 0.043 ug/L 12/28/16 10:36 12/28/16 16:53 1 Chromium 3.0 2.0 1.0 ug/L 12/28/16 10:36 12/28/16 16:53 Copper 2.9 J 5.0 0.50 ug/L 12/28/16 10:36 12/28/16 16:53 Nickel 1.8 J 5.0 0.40 ug/L 12/28/16 10:36 12/28/16 16:53 Lead 0.81 0.30 0.060 ug/L 12/28/16 10:36 12/28/16 16:53 Zinc 59 20 2.8 ug/L 12/28/16 10:36 12/28/1 6 16:53 B
TestAmerica St. Louis Page 11 of 13
BABCOCK Laboratories, Inc.
The Swndard of Excellence far Over I00 Years Client Name: Diablo Canyon Power Plant Analytical Report: Page 2 of 6
~~Contact:~~
Clint Gans Project Name: Diablo Canyon Power Plant-Closed Address: 4340 Old Santa Fe Road Project Number: NPDES - Avila Beach, CA San Lu(s Obispo, CA 93401 Work Order Number: B6J0983 Report Date: 20-0ct-2016 Received on Ice (YIN): Yes Temp: 3 °C Laboratory Reference Number /
86J0983-01 Sample Description Matrix Sampled Date/Time " Received Date/Time Intake Liquid 10/04/16 09:55 10/11/16 9:15 Analyte(s) Result RDL *.MDL Units Method Analysis Date Analyst .Flag Nutrients Ammonia-Nitrogen 0.19 0.10 0.048 mg/L ~M4500NH3H 10/14/~6 14:29
sll i-mailing location p 951 653 3351 CA ELAP No. 2698 P.0 Box 432 6100 Quail Valley Court F 951 653 1662 EPA No. CA00102 Riverside, CA 92502*0432 Riverside, CA 92507*0704 www.babcocklabs.com NELAP No. OR4035 LACSD No. 10119
, BABCOCK Laboratories, Inc.
The Sta.ndard efExcellence for Over I 00 Years Client Name: Diablo Canyon Power Plant Analytical Report: Page 3 of 6
~~Contact:~~
Clint Gans Project Name: Diablo Canyon Power Plant-Closed Address: 4340 Old Santa Fe Road Project Number: NPDES - Avila Beach, CA San Luis Obispo, CA 93401
_Work Order Number: 86J0983 Report Date: 20-0ct-2016 Received on Ice (YIN): Yes Temp: 3 °C Laboratory Reference Number B6J098J Sample Description Matrix Sampled Date/Time Received Date/Time Discharge Liquid 10/04/16 10:07 10/11/16 9:15 Analyte(s) Result RDL MDL Units Method Analysis Date Analyst Flag Nutrients .-
Ammonia-Nitrogen 0.15 0.10 0.048 mg/L SM4500NH3H 10/14/16 14:29 sll mailing location p 951 653 3351 CA ELAP No. 2698 P.O Box 432 6100 Quail Valley Court F 951 653 1662 EPA NQ. CA00102 Riverside, CA 92502*0432 Riverside, CA 92507-0704 www.babcocklabs.com NELAP No. OR4035 LACSD No. 10119
January 17, 2017 Mr. Clint Dans PG&E- Diablo Canyon Power Plant 9 Miles NW Avila Beach Avila Beach, CA 93424
~~Dear Mr. Gans:~~
We are pleased to present the enclosed bioassay report. The test was conducted under guidelines prescribed_ .in Guidelines for Performing Static Acute Fish Bioassays in Municipal aiid Industrial Waste Waters as provided to us by Frederic R. Kopperdahl, Fish and Wildlife Water Pollution Control Laboratory, Department of Fish and Game.
All acceptability criteria were met and the concentration-response was normal. This is a valid test. " Results were as follows:
CLIENT: PG&E~ Diablo Canyon Power Plant SAMPLE I.D.: Discharge 001- Acute DATE RECEIVED: 20 Dec - 2016 ABC LAB. NO.: PGE1216.194 ACUTE ABALONE SURVIVAL BIOASSAY LC50 = I 00 % Survival in 100 % San1ple
~~TUa = 0.00~~
~~TU(a) Is calculated by: log(% Mortality)/1.7 Laboratory Director 29 north olive st. ventura, ca 93001 (805) 643 562 l Www.aquabio.org~~
CETIS Summary Report Report Date: 17 Jan-17 09:21(p1 of 1)
Test Code: PGE1216.194 112-3260-1887 96 Hour Red Abalone Survival Aquatic Bioassay & Consulting Labs, Inc.
Batch ID: 20-5802-7777 Test Type: Survival (96h) Analyst:
Start Date: 21 Dec-16 09:51 Protocol: Kopperdahl (1976) ) Diluent: Laboratory Seawater Ending Date: '25 Dec-16 08:24 Species: Haliotis rufescens Brine: Not Applicable Duration: 95h Source: Cultured Abalone Age:
Sample ID: 16-5318-9222 Code: PGE1216.194 Client: Pacific Gas & Electric Co.
Sample Date: 20 Dec-16 10:45 Material: .
Sample Water Project: Toxicity Testing Receipt Date: 20 Dec-16 15:10 Source: Bioassay Report Sample Age: 23h (5.8 °C) Station: Discharge 001- Acute Slngle Comparison Summary Analysis ID Endpoint Comparison Method P-Value Comparison Result 16-0980-0849 96h Survival Rate Equal Variance t Two-Sample Test 1.0000 100% passed 96h survival rate 96h Survival Rate Summary Cone-% Code Count Mean 95% LCL 95% UCL Min Max Std Err Std Dev CV% %Effect 0 N 2 1.0000 1.0000 1.0000 1.0000 1.0000 0.0000 0.0000 0.00% 0.00%
100 2 1.0000 1.0000 1.0000 1.0000 1.0000 0.0000 0.0000 0.00% 0.00%
96h Survival Rate Detail Cone-% Code Rep 1 Rep 2 0 N 1.0000 1.0000 .-
100 1.0000 1.0000 96h Survival Rate Binomials Cone-% Code Rep 1 Rep 2 I; 0 N 10/10 10/10 100 10/10 10/10 000-189-126-0 CETIS TM v1 .9.2.6 Analyst: ~ QA:
CETIS Analytical Report Report Date: 17 Jan-17 09:21 (p 1 of 2)
Test Code: PGE1216.194 J .12-3260-1887 96 Hour Red Abalone Survival Aquatic Bioassay & Consulting Labs, Inc.
Analysis ID: 16-0980-0849 Endpoint: 96h Survival Rate CETIS Version: CET1Sv1 .9.2 Analyzed: 16 Jan-17 17:31 Analysis: Parametric-Two Sample Official Results: Yes Batch ID: 20-5802-7777 Test Type: Survival (96h) . Analyst: /
Start Date: 21 Dec-16 09:51 Protocol: Kopperdahl (1976) Diluent: Laboratory Seawater Ending Date: 25 Dec-16 08:24 Species: Haliotis rufescens Brine: Not Applicable Duration: 95h Source: Cultured Abalone Age:
Sample ID: 16-5318-9222 Code: PGE1216.194 Client: Pacific Gas & Electric Co.
Sample Date: 20 Dec-16 10:45 Material: Sample Water Project: Toxicity Tesling Receipt Date: 20 Dec-1615:10 Source: Bioassay Report Sample Age: ~3h (5.8 °C) Station: Discharge 001- Acute Data Transform Alt Hyp Comparison Result Angular (Corrected) C>T 100% passed 96h survival rate Equal Variance t Two-Sample Test Control vs Cone-% Test Stat Critical DF P-Type P-Value Decision(a:5%)
Negative Control 100 0 2.92 2 CDF 1.0000 Non-Significant Effect ANOVA Table .
Source Sum Squares Mean Square "DF F Stat P-Value Decision(a:5%)
Between 0 0 1 65540 1.5E-05 . Significant Effect Error 0 0 2 Total 0 l 3
96h Survival Rate Summary Cone-% Code Count Mean 95% LCL 95% UCL Median Min Max .Std Err CV% %Effect 0 N 2 1.0000 1.0000. . 1.0000 1.0000 1.0000 1.0000 0.0000 0.00% 0.00%
100 2 1.0000 1.0000 1.0000 1.0000 1.0000 1.0000 . 0.0000 0.00% 0.00%
Angular (Corrected) Transformed Summary Cone-% Code. Count Mean 95% LCL 95% UCL Median Min Max Std Err CV% %Effect 0 N 2 1.412 1.409 1.415 1.412 1.412 1.412 0 0.00% 0.00%
100 2 1.412 1.409 1.415 1.412 1.412. . 1.412 0 0.00% 0.00%
96h Survival Rate Detail Cone-% Code Rep 1 Rep 2 0 N 1.0000 1.0000 100 1.0000 1.0000 Angular (Corrected) Transform.ad Detail Cone-% Code Rep 1 Rep 2 0 N 1.412 1.412 100 1.412 1.412 96h Survival Rate Binomials Cone-% Code Rep 1 Rep 2 0 N 10/10 10/10 100 10/10 10/10 000-189-126-0. CETIS' v1.9.2.p Analyst: \_,.-..1'"\. aA:._..__L_
CETIS Analytical Report Report Date: 17 Jan-17 09:21 (p 2 of 2)
Test Code: PGE1216.194 I 12-3260-1887 96 Hour Red Abalone Survival Aquatic Bloassay & Consulting Labs, Inc.
. Analysis ID: 16-0980-084 9 Endpoint: 96h Survival Rate CETIS Version: CET1Sv1.9.2 Analyzed: 16 Jan-17 17:31 Analysis: Parametric-Two Sample Official Results: Yes Graphics 1.0 l.OE+oO
~~0 0.9 0.8 11 7.SE--01~~
~ 0.7
-~ 0.6
.c 0.5 5.0E--01
"'"' 0.4
. 0.3 2.SE--01 0.2 0.1 O.OE+OO .....__ _ _ ___,__.____,__ _.....__ __.._ __,
a.a ON 100 *l.5 -1.0 --0.S 0.0 0.5 1.0 1.5 Conc.. 0/o Ran kits 000-189-126-0 CETIS' v1 .9.2.6 Analyst: _ _ \~c~.A~ QA:___* r_.1_
/
CETIS Measurement Report Report Date: 17 Jan-17 09:21 (p 1 of 1)
Test Code: PGE1216.194 J 12-3260-1887 96 Hour Red Abalone Survival Aquatic Bioassay & Consulting Labs, Inc.
Batch ID: 20-5802-7777 Test Type: Suivival (96h) Analyst:
start Date: 21Dec-1609:51 Protocol: Kopperdahl (1976) Diluent: Laboratory Seawater Ending Date: 25 Dec-16 08:24 Species: Haliotis rufescens Brine: Not Applicable Duration: 95h Source: Cultured Abalone Age:
Sample ID: 16-5318-9222 Code: PGE1216.194 Client: Pacific Gas & Electric Co.
Sample Date: 20 Dec-16 10:45 Material: Sample Water Project: Toxicity Testing Receipt Date: 20 Dec-1615:10 Source: Bioassay Report Sample Age: 2~h (5.8 °C) Station: Discharge 001- Acute Dissolved Oxygen-mg/L j Cone-% Code Count Mean 95% LCL 95% UCL. Min Max Std Err Std Dev CV% QA Count 0 N 10 7.91 7.609 8.211 7.4 8.6 0.1329 0.4202 5.31% 0 '
100 10 7.75 7.484 8.016 7.3 8.3 0.1176 0.3719 4.8% 0 Overall 20 7.83 7.645 8.015 7.3 8.6 0.08829 0.3948 0 (0%)
pH-Units Cone-% Code Count Mean 95%.LCL 95% UCL Min Max Std Err Std Dev CV% QA Count 0 N 10 7.42 7.354 7.486 7.3 7.5 -- 0.02906 0.09189 1.24% 0 100 10 7.49 7.366 7.614 7.3 7.8 0.05467 0.1729 . 2.31% 0
~~overall 20 7.455 7.39 7.52 7.3 7.8 0.03118 0.1395 1.87% .o (0%)~~
Salinity-ppt Cone-% Code Count Mean 95% LCL 95% UCL Min Max Std Err Std Dev CV% QA Count*
0 N 10 34 34 34 34 34 0 0 0.0% 0 100 10 34 34 34 34 34 0 0 0.0% 0
~~.Overall 20 34 34 34 34 0 0.00% 0 (0%)~~
Temperature-°C j
Cone-% Code Count Mean .95% LCL 95% UCL Min Max Std Err Std Dev CV% QA Count 0 N 10 14.53 14.5 14.56 14.5 14.6 0.01527 0.04828 0.33% 0 100 10 14.54 14.5 14.58 14.5 14.6 0.01632 0.05161 0.35% 0 Overall 20 14.54 14.51 14.56 14.5 14.6 0.01094 0.04894 0.34% 0 (0%)
Dissolved Oxygen-mg/L Cone-% Code 2 3 4 5 6 7 8 9 10 0 N 8.6 8.6 7.4 7.5 7.6 7.7 8 8 7.7 8 100 8.3 8.3 7.4 7.3 7.5 7.5 8 7.7 8 7.5 pH-Units Cone-% Code 2 3 4 5 6 7 8 9 .10 0 N 7.5 7.5 7.5 7.4 7.5 7.5 7.3 7.4 7.3 7.3 100 7.8 7.8 7.4 7.4 7.5 7.4 7.5 7.4 7.4 7.3 Salinity-ppt Cone-% Code 2 3 4 5 6 7 8 9 10 0 N 34 34 34 34 34. 34 34 34 34 34 100 34 34 34 34 34 34 34 34 34 34 Temperature-°C Cone-% Code *, 1 2 3 4 6 7 -s 9 10 0 N ' 14.6 14.6 14.6 14.5 14.5 14.5 14.5 14.5 14.5 14.5 100 14.5 14.5 14.6 14.6 14.5 14.6 14.6 14.5 14.5 14.5 000-189-126-0 CETIS' v1 .9.2.6 Analyst: \ .... j\.. QA:_l_
January 17, 2017
('
Mr. Clint Gans PG&E- Diablo Canyon Power Plant 9 Miles NW Avila Beach Avila Beach, CA 93424
~~Dear Mr. Gans:~~
We are pleased to present the enclosed bioassay report. The test was conducted under guidelines prescribed in Short-T_erm Methods for Measuring the Chronic Toxicity of Effluents and Receiving Waters to West Coast Marine and Estuarine Organisms, EPA-R-951136. "All acceptability criteria were met and the concentration-response was nom1al.
This is a valid test. " Results were as follows:
CLIENT: PG&E- Diablo Canyon Power Planj:
SAMPLE l.D.: Discharge 001 DATE RECEIVED: 20 Dec - 2016 ABC LAB. NO.: PGE1216.195 CHRONIC ABALONE LARVAL DEVELOPMENT BIOASSAY NOEC= 100.00 %
TUc 1.00 EC25 = >100.00 %
,EC50 >100.00 %
You~et~~1~"\ ___,___....
Sco~son Laboratory Direct-0 29 north olive st. ventura, ca 93001 (805) 643 5621 www.aquabio.org
CETIS Summary Report Report Date: 17 Jan-17 09:21(p1 of 1)
Test Code: PGE1216.195 I 06-6646-9526 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Batch ID: 03-7513-0511 Test Type: Development Analyst:
Start Date: 20 De'c-16 15:31 Protocol: EPN600/R-95/136 (1995) Diluent: Laboratory Seawater Ending Date: 22 Dec-16 15:30 Species: Haliotis rufescens Brine: Not Applicable Duration: 48h Source: Cultured Abalone Age:
Sample ID: 14-9573-1426 Code: PGE1216.195 Client: pacific Gas & Electric Co.
Sample Date: 20 Dec-16 10:45 Material: Sample Water Project: Toxicity Testing Receipt Date: 20 Dec-16 15:10 Source: Bioassay Report Sample Age: Sh (5.8 °C) Station: Discharge 001- Chronic Multiple Comparison Summary Analysis ID Endpoint Comparison Method NOEL LOEL TOEL TU PMSD ./
03-6078-9719 Proportion Normal Steel Many-One Rank Sum Test 100 > 100 n/a 1 1.96%
Point Estimate Summary Analysis ID Endpoint Point Estimate Method Level % 95% LCL 95% UCL TU .j 03-3140-6330 PropOrtion Normal Linear Interpolation (ICPIN) ECS >100 n/a n/a <1 EC10 >100 n/a n/a <1 EC15 >100 n/a n/a <1 EC20 >100 n/a n/a <1 EC25 >100 n/a n/a <1 EC40 >100 n/a n/a <1 EC50 >100 n/a n/a <1 Test Acceptability TAC Limits Analysis ID Endpoint Attribute Test Stat Lower Upper Overlap Decision 03-3140-6330 Proportion Normal Control Resp 0.982 0.8 >> Yes Passes Criteria 03-6078-9719 Proportion Normal Control Resp 0.982 0.8 >> Yes Passes Criteria Proportion Normal Summary Cone-% Code Count Mean 95% LCL 95% UCL Min Max Std Err Std Dev CV% %Effect 0 N 5 0.9820 0.9658 0.9982 0.9600 0.9900 0.0058 0.0130 1.33% 0.00%
10 5 0.9940 0.9829 1.0000 0.9800 1.0000 0.0040 0.0089 0.90% -1.22%
18 5 0.9940 0.9829 1.0000 0:9800 1.0000 0.0040 0.0089 0.90% -1.22%
32 5 0.9900 0.9776 1.0000 0.9800 1.0000 0.0045 0.0100 1.01% -0 ..81%
56 5 0.9820 0.9716 0.9924 0.9700 0.9900 0.0037 0.0084 0.85% 0.00%
100 5 0.9920 0.9758 1.0000 0.9700 1.0000 0.0058 0.0130 1.31% -1.02%
Proportion Normal Detail Cone-% Code Rep 1 Rep 2 Rep 3 Riip 4 Rep 5 0 N 0.9900 0.9900 0.9600 0.9800 0.9900 10 1.0000 0.9900 1.0000 0.9800 1.0000 '
18 0.9900 1.0000 1.0000 0.9800 1.0000 32 0.9800 0.9900 1.0000 0.9800 1.0000 56 0.9900 0.9800 -0.9700 0.9800 0.9900 100 1.0000 0.9900 0.9700 1.0000 1.0000 Proportion Normal Binomials Cone-% Code Rep 1 Rep 2 Rep 3 Rep4 Rep 5 0 N 99/100 99/100 96/100 98/100 99/100 10 100/100 99/100 100/100 98/100 100/100 18 99/100 100/100 100/100 98/100 100/100 32 98/100 99/100 100/100 98/100 100/100 56 99/100 98/100 97/100 98/100 99/100 100 100/100 99/100 97/100 100/100 100/100 000-189-126-0 CETIS' v1 .9.2.6 Analyst: \..,...J\ QA:
CETIS Analytical Report Report Date: 17 Jan-17 09:21(p1of2)
Test Code: PGE1216.195 I 06-6646-9526 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Analysis ID: 03-6078-9719 Endpoint: Proportion Normal CETIS Version: CETISv1 .9.2 Analyzed: 16 Jan-17 17:21 Analysis: Nonparametric-Control vs Treatments Official Results: Yes Batch ID: 03-7513-0511 Test Type: D~velopment Analyst:
Start Date: 20 Dec-16 15:31 ,Protocol: EPA/600/R-95/136 (1995) Diluent: Laboratory Seawater Ending Date: 22 Dec-16 15:30 Species: Haliotis rufescens Brine: Not Applicable Duration: 48h *Source: Cultured Abalone Age:
Sample ID: 14-9573-1426 Code: PGE1216.195 Client: Pacific Gas & Electric Co.
Sample Date: 20 Dec-16 10:45 Material: Sample Water Project: Toxicity Testing Receipt Date: 20 Dec-16 15:10 Source: Bioassay Report Sample Age: 5h (5.8 °C) Station: Discharge 001- Chronic Data Transform Alt Hyp NOEL LOEL TOEL TU PMSD Angular (Corrected) C>T 100 > 100 . n/a 1.96%
Steel Many-One Rank Sum Test Control vs Cone-% Test Stat Critical Ties OF P-Type P-Value Decision(a:5%)
Negative.Control . 10 35 16 2 8 Asymp 0.9979 Non-Significant Effect 18 35 16 2 8 Asymp 0.9979 Non-Significant Effect 32 31.5 16 2 8 Asymp 0.9757 Non-Significant Effect 56 26 16 2 8 Asymp 0.7237 Non-Significant Effect 100 34.5 16 8 Asymp 0.9969 Non-Significant Effect Test Acceptability Criteria TAC Limits Attribute Test Stat Lower Upper Overlap Decision Control Resp 0.982 0.8 >> Yes Passes Criteria ANOVA Table Source Sum Squares Mean Square OF F Stat P-Value Decision(a:5%)
Between 0.01499 0.002998 5 1.563 . 0.2083 Non-Significant Effect Error 0.0460239 0.0019177 24 Total 0.0610139 29 Distributional Tests )
Attribute Test Test Stat Critical P-Value Decision(a:1%)
Variances Bartlett Equality of Variance Test 1.087 15.09 . 0.9552 Equal Variances Variances Levene Equality of Variance Test 0.3727 3.895 0.8623 Equal Variances Variances Mod Levene Equality of Variance Test 0.09167 4.248 0.9925 Equal Variances Distribution Anderson-Darling A2 Normality Test 1.969 3.878 <1.0E-37 Non-Normal Distribution Distribution D'Agostino Kurtosis Test . 0.901 2.576 0.3676 Normal Distribution Distribution D'Agostino Skewness Test 1.767 2.576 0.0773 Normal Distribution Distribution D'Agostino-Pearson K2 Omnibus Test 3.933 9.21 0.1399 Normal Distribution Distribution Kolmogorov-Smirnov D Test 0.2954 0.1853 3.4E-07 Non-Normal Distribution Distribution Shapiro-Wilk W Normality Test
0.8618 0.9031 0.0011 Non-Normal Distribution Proportion Normal Summary Cone-% Code Count Mean 95% LCL 95°/o UCL Median Min Max Std Err CV% %Effect 0 N 5 0.9820 0.9658 0.9982 0.9900 0.9600 0.9900 0.0058 1.33% 0.00%
10 5 0.9940 0.9829 1.0000 1.0000 0.9800 1.0000 0.0040 0.90% -1.22%
18 5 0.9940 0.9829 1.0000 1.0000 0.9800 1.0000 0.0040 0.90% -1.22%
32 5 0.9900 0.9776 1.0000 0.9900 0.9800 1.0000 0.0045 1.01% -0.81%
56 5 0.9820 0.9716 0.9924 0.9800 0.9700 0.9900 0.0037 0.85% 0.00%
100 5 0.9920 0.9758 1.0000 1.0000 0.9700 1.0000 0.0058 1.31% -1.02%
000-189-126-0 CETIS' v1.9.2.6 Analyst:_\~..,,_f\.._ QA:_J_
CETIS Analytical Report Report Date: 17 Jan-17 09:21 (p 2 of 2j Test Code: PGE1216.195 I 06-6646-9526 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Analysis ID: 03-6078-9719 Endpoint: Proportion Normal CETIS Version: CET1Sv1 .9.2 Analyzed: 16 Jan-17 17:21 Analysis: Nonparametric-Control vs Treatments Official Results: Yes Angular (Corrected) Transformed Summary Cone-% Code Count Mean 95% LCL 95% UCL Median Min Max Std Err CV% %Effect 0 N 5 1.442 1.387 1.497 1.471 1.369 1.471 0.01987 3.08% 0.00%
10 5 1.492 1.441 1.544 1.521 1.429 1.521 0.0186 2.79% -3.49%
18 5 1.492 1.441 1.544 1.521 1.429 1.521 0.0186 2.79% -3.49%
32 5 1.474 1.417 1.531 1.471 1.429 1.521 0.02056 3.12% -2.22%
56 5 1.439 1.4 1.478 1.429 1.397 1.471 0.01413 2.20% 0.20%
100 5 1.486 1.418 1:553 1.521 1.397 1.521 0.02433 3.66% -3.04%
Proportion Normal Detail Cone-% Code Rep 1 Rep 2 Rep 3 Rep4 Rep 5 0 N 0.9900 0.9900 0.9600 0.9800 0.9900 10 1.0000 0.9900 1.0000 0.9800 1.0000 18 0.9900 1.0000 1.0000 0.9800 1.0000 32 0.9800 0.9900 1.0000 0.9800 1.0000 56 0.9900 0.9800 0.9700 0.9800 0.9900 100 1.0000 0.9900 . 0.9700 1.0000 1.0000 Angular (Corrected) Transformed Detail Cone-% Code Rep 1 Rep2 Rep 3 Rep4 Rep 5 0 N 1.471 1.471 1.369 1.429 1.471 10 1.521 1.4 71 1.521 1.429 1.521 18 1.471 1.521 1.521 1.429 1.521 32 1.429 1.471 1.521 1.429 1.521 56 1.471 1.429 1.397 1.429 1.471 100 1.521 1.471 1.397 1.521 1.521 Proportion Normal Binomials Cone-% Code Rep 1 Rep 2 Rep 3 Rep4 Rep 5 0 N 99/100 99/100 96/100 98/100 99/100 10 100/100 99/100 100/100 98/100 100/100
, 18 99/100 100/100 100/100 98/100 100/100 32 98/100 99/100 1901100 98/100 100/100 56 99/100 98/100 97/100 98/100 99/100 100 100/100 99/100 97/100 100/100 100/100 Graphics i.o F E!=i 0.075 0.9 0.050 0 0
-.; 0.8
§ 0.025 0 0.7 z
c
~ 0.6 0.000 0
~~e-... 0.5~~
0.025 0.4 0.3 *0.050 ***
0.2 *o 0
-O.o75 0.1 0.0 .___ _..1.__ __J.__ __ , __ __....L._ __ _ ._ __ _ J "
-0.100 L----L--'---.l__...l._ _,___,__...I._ _j__.L___I ON 10 18 56 100 *2.5 *2.0 *1.5 *1.0 -0.5 o.o 0.5 1.0 1.5 2.0 2.5 Conc- 0/o Rankits 000-189-126-0 CETIS ' v1 .9.2.6 Analyst: \_,..J'\_. r_
aA: __ _
1
CETIS Analytical Report Report Date: 17 Jan-17 09:21 (p 1 of 2)
Test Code:
~~PGE1216. 195 J 06-6646-9526 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.~~
Analysis ID: 03-3140-6330 Endpoint: Proportion Nom1al CETiS Version: CET1Sv1 .9.2 Analyzed:* 16 Jan-17 17:21 Analysis: Linear interpolation (ICPIN) Official Results: Yes Batch ID: 03-7513-0511 Test Type: Development Analyst:
Start Date: 20 Oec-16 15:31 Protocol: EPA/600/R-95/136 (1995) Diluent: Laboratory Seawater Ending Date: 22 Dec-16 15:30 Species: Haliotis rufescens Brine: Not Applicable Duration: 48h Source: Cultured Abalone Age:
Sample ID: 14-9573-1426 Code: PGE1216.195 Client: Pacific Gas & Electric Co.
Sample Date: 20 Dec-16 10:45 Material: Sample Water Project: Toxicity Testing Receipt Date: 20 Dec-16 15:10 *Source: Bioassay Report
~ample Age: 5h (5.8 °C) Station: Discharge 001- Chronic Linear Interpolation Options X Transform Y Transform Seed Resamples Exp 95% CL Method Linear Linear 0 280 Yes Two-Point Interpolation Test Acceptability Criteria TAC Limits Attribute Test Stat Lower Upper Overlap Decision Control Resp 0.982 0.8 >> Yes Passes Criteria Point Estimates Level % 95% LCL 95% UCL TU 95% LCL 95% UCL EC5 >100 n/a n/a <1 n/a n/a EC10 >100 n/a n/a <1 nla n/a EC15 >100 n/a n/a <1 n/a n/a EC20 >100 n/a n/a <1 n/a n/a EC25 >100 n/a n/a <1 n/a n/a EC40 >100 n/a n/a <1 n/a n/a EC50 . >100 n/a n/a <1 n/a n/a Proportion Normal Summary , Calculated Variate(A/B)
Cone-% Code Count Mean Min Max Std Err Std Dev CV% %Effect A B 0 N 5 0.9820 0.9600 0.9900 0.0058 0.0130 1.33% 0.0% 491 500 10 5 0.9940 0.9800 1.0000 0.0040 0.0089 0.90% -1.22% 497 500 18 5 0.9940 0.9800 1.0000 0.0040 0.0089 0.90% -1.22% 497 500 32 5 0.9900 0.9800 1.0000 0.0045 0.0100 1.01% -0.81% 495 500 56 5 0.9820 0.9700 0.9900 0.0037 0.0084 0.85% 0.0% 491 500 100 5 0.9920 0.9700 1.0000 0.0058 0.0130 1.31% -1.02% 496 500 Proportion Normal Detail Cone-% Code Rep 1 Rep 2 Rep 3 Rep4 Rep 5 0 N 0.9900 0.9900 0.9600 0.9800 0.9900 10 1.0000 0.9900 1.0000 0.9800 1.0000 18 0.9900 1.0000 1.0000 0.9800 1.0000 32 0.9800 0.9900 1.0000 0.9800 1.0000
' 56 0.9900 0.9800 0.9700 0.9800 0.9900 100 1.0000 0.9900 0.9700 1.0000 1.0000 Proportion Normal Binomials Cone-% Code Rep 1 Rep 2 Rep 3 Rep 4 ,Rep 5 0 N 99/100 99/100 96/100 98/100 99/100 10 100/100 99/100 100/100 98/100' 100/100 18 99/100 100/100 100/100 98/100 100/100 32 98/100 99/100 100/100 98/100 100/100 56 99/100 98/100 97/100 98/100 99/100 100 100/100 99/100 97/100 . 100/100 100/100 000-189-126-0 CETIS' v1.9.2.6 Analyst:_........,.,_--..._ QA:__L
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CETIS Analytical Report Report Date: 17 Jan-17 09:21 (p 2 of 2)
Test Code: PGE1216.195 I 06-6646-9526 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Analysis ID: 03-3140-6330 Endpoint: Proportion Normal CETIS Version: CETISv1 .9.2 Analyzed: 16 Jan,17 17:21 Analysis: Linear Interpolation (ICPIN) Official Results: Yes Graphics 1.0 0.9 0.8
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0.3 0.2 0.1 0.0 0 20 ~o 60 80 100 Conc* 0/o 000-189-126-0 CETIS' v1 .9.2.6 Analyst: \____ ['-* QA:_~f_.1_
CETIS Measurement Report Report Date: 17 Jan-17 09:21 (p _1 of 2)
Test Code: PGE 1216.195 I 06-6646-9526 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Batch ID: 03-7513-0511 Test Type: Development Analyst:
.Start Date: 20 Dec-1615:31 Protocol: EPA/600/R-95/136 (1995) Diluent: Laboratory Seawater Ending Date: 22 Dec-16 15:30 Species: Haliotis rufescens Brine: Not Applicable Duration: 48h Source: Cultured Abalone Age:
Sample ID: 14-9573-1426 Code: PGE1216.195 Client: Pacific Gas & Electric Co.
Sample Date: 20 Dec-16 10:45 Material: Sample Water Project: Toxicity Testing Receipt Date: 20 Dec-16 15:10 Source: Bioassay Report Sample Age: Sh (5.8 °C) Station: Discharge 001- Chronic Parameter Aeceptabil.ity Criteria TAC Limits Parameter Min Max Lower Upper Overlap Decision Salinity 34 34 32 36 Yes Passes Criteria Temperature 13 14.2 14 16 Yes Below Criteria Dissolved Oxygen-mg/L ,,---
Cone-% Code Count Mean 95% LCL 95% UCL Min Max Std Err Std Dev CV% QA Count 0 N 2 6.8 4.259 9.341 6.6 7 0.2 0.2828 4.16% 0 10 2 6.75 2.303 11.2 6.4 7.1 0.35 0.495 7.33% 0 18 2 6.8 2.988 10.61 6.5 7.1 0.3 0.4243 6.24% 0 32 2 6.8 2.988 10.61 6.5 7.1 0.3 0.4243 6.24% 0 56 2 6.65 2.203 11.:1 6.3 7 0.35 0.495 7.44% 0 100 2 6.9 1.818 11.98 6.5 7.3 0.4 0.5657 8.2% 0 Overall 12 6.783 . 6.564 7.003 6.3 7.3 0.09987 0.346 5.10% 0(0%)
pH-Units Cone-% Code Count Mean 95% LCL 95% UCL Min Max Std Err Std Dev CV% QA Count 0 N 2 7.55 6.915 8.185 7.5 7.6 0.05 0.07071 0.94% 0 10 2 7.6 6.329 8.871 7.5 7.7 0.1 0.1414 1.86% 0 18 2 7.6 6.329 8.871 7.5 7.7 0.1 0.1414 1.86% 0 32 2 7.65 7.015 8.285 7.6 7.7 0.05 0.07071 0.92% 0 56 2 7.65 7.015 8.285 7.6 7.7 0.05 0.07071 0.92% 0 100 2 7.65 7.015 8.285 7.6 7.7 0.05 0.07071 0.92% 0 Overall 12 7.617 7.564 7.67 7.5 7.7 0.0241 0.08348 1.10% 0(0%)
Salinity-ppt Cone-% Code Count Mean 95% LCL 95% UCL Min Max Std Err Std Dev CV% QA Count 0 N 2 34 34 34 34 34 0 0 0.0% 0 10 2 34 34 34 34 34 0 0 0.0% 0 18 2 34 34 34 34 34 0 0 0.0% 0 32 2 34 34 34 34 34 0 0 0.0% 0 56 2 34 34 34 34 34 0 0 0.0% 0 100 2 34 34 34 34 34 0 0 0.0% 0 Overall 12 34 34 34 34 34 0 0 0.00% 0 (0%)
Temperature-°C Cone-% Code Count Mean 95% LCL 95% UCL Min Max Std Err Std Dev* CV% QA Count b N 2 14.2 14.17 14.23 14.2 14.2 0 0 0.0% 0 10 2 14 11.46 16.54 13.8 14.2 0.2 0.2828 2.02% 0 18 2 13.85 9.403 18.3 13.5 14.2 0.35 0.495 3.57% 0 32 2 13.75 8.032 19.47 13.3 14.2 0.45 0.6364 4.63% 0 56 2 13.7 7.347 20.05 13.2 14.2 0.5 0.7071 5.16% 0 100 2 13.6 5.976 21.22 13 14.2 0.6 0.8485 6.24% 0 Overall 12 13.85 13.55 14.15 13 14.2 0.1357 0.47 3.39% 0(0%)
000-189-126-0 CETIS' v1.9.2.6 Analyst: 1 0 A., QA:_L
CETIS Measurement Report Report Date: 17 Jan-17 09:21 (p 2 of 2)
Test Code: PGE1216.195 I 06-6646-9526 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Dissolved Oxygen-mg/L Cone-% Code 1 2 0 N 7 6.6 10 7.1 6.4 18 7.1 6.5 32 7.1 6.5 56 7 6.3 100 7.3 6.5 pH-Units Cone-% Code 2 0 N 7.6 7.5 10 7.7 7.5 18 7.7 7.5 32 7.7 7.6 56 7.7. 7.6 100 7.7 7.6 Salinity-ppt Cone-% Code 2 0 N 34 34 10 34 34 18 34 34 32 34 34 56 34 34 100 34 34 Temperature-*c Cone-% Code 2 0 N 14.2 14.2 10 13.8 14.2 18 13.5 14.2 32 13.3 14.2 56 13.2 14.2 100 13 14.2
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000-189-126-0 CETIST" v1 .9.2.6 Analyst: _ ___._,__ QA: _ __
CHAIN OF CUSTODY RECORD Client: Project Name/Number: Anal~sis Pacific Gas & Electric Co Toxicity Testing Address: Project Mgr:
9 Miles NW Avila Beach Merrie Johnson Avila Beach, Ca. 93424 P.O.# ~
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(;V\r-v\-\J Temperature upon sample receipt: degrees C Aquatic Bioassay and Consulting Labortories 29 N. Olive Street Ventura, Ca. 93001 Phone: (805) 643-5621 Fax: (805) 643-2930
aquatic b1oassay consulting laboratories, inc CHRONIC ABALONE DEVELOPMENT BIOASSAY DATE: 20 December 2016 STANDARD TO XI CANT: Zinc NOEC= 32.00 ug/l EC25 = 39.04 ug/l EC50= 46.65 ug/l Yours]~~ '
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Laboratory Dite..Q.tor 29 north olive st. ventura, ca 9300 J. (805)_ 643 5621 www.aquabio.org
CETIS Summary Report Report Date: 17 Jan-17 09:21 (p 1 of 1)
Test Code: ABS122016 I 20-9773-27.52 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Batch ID: 07-0829-0131 Test Type: Development Analyst:
Start Date: 20 Dec-16 15:30 Protocol: EPA/600/R-95/136 (1995) Diluent: Laboratory Seawater Ending Date: 22 Dec-16 15:30 Species: Haliotis rufescens Brine: Not Applicable Duration: 48h Source: Cultured Abalone Age:
Sample ID: 20-6479-5531 Code: ABS122016 Client: Internal Lab Sample Date: 20 Dec-16 15:30 Material: Zinc Project: REF TOX Receipt Date: Source: Reference Toxicant SamplerAge: n/a Station: REF TOX Multiple Comparison Summary Analysis l,D Endpoint Comparison Method NOEL LOEL TOEL TU PMSD ./
16-3945-2315 Proportion Normal Dunnett Multiple Comparison Test 32 56 42.33 4.7%
Point Estimate Summary Analysis ID Endpoint Point Estimate Method Level µg/L 95% LCL 95%.UCL TU ./
00-2927-(383 Proportion Normal Linear Interpolation (ICPIN) EC5 32.96 30.12 33.8 EC10 34.48 33.04 35.32 EC15 36 34.7 36.86 EC20 37.52 36.32 38.45 EC25 39.04 37.9 40.03 EC40 43.61 42.44 44.87 EC50 46.65 45.28 48.13 Test Acceptability TAC Limits Analysis ID Endpoint Attribute Test Stat Lower Upper Overlap Decision 00-2927-1383 Proportion Normal Control Resp 0.976 0.8 >> Yes Passes Criteria 16-3945-2315 Proportion Normal Control Resp 0.976 0.8 >> Yes Passes Criteria 16-3945-2315 Proportion Normal NOEL 32 << 56 No Passes Criteria 16-3945-2315 Proportion Normal PMSD 0.04701 << 0.2 No Passes Criteria Proportion Normal Summary Conc-µg/L Code Count Mean 95% LCL 95% UCL Min Max Std Err Std Dev CV% %Effect 0 N 5 0.9760 0.9593 0.9927 0.9600 0.9900 0.0060 0.0134 1.37% 0.00%
"18 5 0.9740 0.9598 0.9882 0.9600 0.9900 0.0051 0.0,114 1.17% 0.20%
32 5 0.9580 0.9214 0.9946 0.9100 0.9800 0.0132 0.0295 3.08% 1.84%
56 5 0.1880 0. 1108 0.2652 0.1000 0.2600 0.0278 0.0622 33.09% 80.74%
100 5 0.0560 0.0000 '0.1287 0.0000 0.1500 0.0262 0.0586 104.58% 94.26%
180 5 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 100.00%
Proportion Normal Detail Conc-µg/L Code Rep 1 1' Rep.2 Rep 3 Rep 4 Rep 5 0 N 0.9900 0.9600 0.9700 0.9700 0.9900 18 0.9700 0.9600 0.9800 0.9700 0.9900 32 0.9500 0.9100 0.9700 0.9800 0.9800 56 0.2600 0.2300 0.1900. 0.1000 0.1600 100 0.1500 0.0700 0.0200 0.0000 0.0400 180 0.0000 0.0000 0.0000 0.0000 0.0000 Proportion Normal' Binomials Conc-µg/L Code Rep 1 Rep 2 Rep 3 Rep 4 Rep 5 0 N 99/100 96/100 97/100 97/100 99/100 18 97/100 96/100 98/100 97/100 99/100 32 95/100 91/100. 97/100 98/100 98/100 56 26/100 23/100 19/100 10/100 16/100 100 15/100 71100 21100 0/100 4/100 180 0/100 0/100 0/100 0/100 0/100 000-189-126-0 CETIS ' v1 .9.2.6 Analyst: 'c.A., QA: rrtss i.,
CETIS Analytical Report Report Date: 17 Jan-17 09:21 (p 1 of 2)
)
Test Code: ABS122016 I 20-9773-2752 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Analysis ID: 16-3945-2315 Endpoint: Proportion Normal CETIS Version: CETISv1 .9.2 Analyzed: 16 Jan-17 17:12 Analysis: Parametric-Control vs Treatments Official Results: Yes Batch ID: 07-0829-0131 Test Type: Development Analyst:
Start Date: 20 Dec-16 15:30 Protocol: EPN600/R-95/136 (1995) Diluent: Laboratory Seawater Ending Date: 22 Dec-16 15:30 Species: Haliotis rufescens Brine: Not Applicable Duration: 48h Source: Cultured Abalone Age:
Sample ID: 20-6479-5531 Code: ABS122016 Client: Internal Lab Sample Date: 20 Dec-16 15:30 Material: Zinc Project: REF TOX Receip~ Date: Sour,ce: Reference Toxicant Sample Age: n/a Station: REF TOX Data Transform Alt Hyp NOEL LOEL TOEL TU PMSD Angular (Corrected) C>T 32 56 42.33 4.70%
Dunnett Multiple Comparison Test Control vs Conc-µg/L Test Stat Critical MSD DF P-Type P-Value Decision(a:5%)
Negative Control 18 0.1636 2.305 0.118 8 GDF 0.7427 Non-Significant Effect 32 0.9339 2.305 0)18 8 CDF 0.4091 Non-Significant Effect 55* ( 1g.15 2.305 0.118 8 CDF 4.5E-07 Significant Effect 100* 23.7 2.305 0.118 8 CDF 4.5E-07 Significant Effect Test Acceptability Criteria TAC Limits Attribute Test Stat Lower Upper *overlap Decision Control Resp 0.976 0.8 >> Yes Passes Criteria NOEL 32 << 56 No Passes Criteria PMSD 0.04701 << 0.2 No Passes Criteria ANOVA Table Source Sum Squares Mean Square DF F Stat P-Value Decision(a:5%)
Between 7.06636 1.76659 4 271.5 <1.0E-37 Significant Effect Error 0.130129 0.0065065 20 Total 7.19649 24 Distributional Tests Attribute Test Test Stat Critical P-Value Decision(a:1%)
Variances Bartlett Equality of Variance Test
6.698 13.28 0.1527 Equal Variances Variances Levene Equality of Variance Test 1.777 4.431 0.1730 Equal Variances Variances Mod Levene Equality of Variance Test 2.089 4.8g3 0.1331 Equal Variances Distribution Anderson~Darllng A2 Normality Test 0.47 3.878 0.2512 Normal Distribution Distribution D'Agostino Kurtosis Test 1.157 2.576 0.2474 Normal Distribution Distribution D'Agostino Skewness Test 0.109 2.576 0.9132 Normal Distribution Distribution D'Agostino-Pearson K2 Omnibus Test 1.35 9.21 0.5092
~~Normal Distribution I~~
Distribution Kolmogorov-Smirnov D Test 0.1348 0.2018 . 0.2800 Normal Distribution Distribution Shapiro-Wilk W Normality Test 0.9639 0.8877 0.4964 Normal Distribution Proportion Normal Summary Conc-µg/L. Code Count Mean 95% LCL 95% UCL Median Min Max Std Err CV% %Effect 0 N 5 0.9760 0.9593 0.9927 0.9700 0.9600 0.9900 0.0060 1.37% 0.00%
18 5 0.9740 0.9598 0.9882 0.9700 0.9600 0.9900 0.0051 1.17% 0.20%
32 5 0.9580 0.9214 0.9946 0.9700 0.9100 0.9800 0.0132 3.08% 1.84%
56 5 0.1880 0.1108 0.2652 0.1900 0.1000 0.2600 0.0278 33.09% 80.74%
100 5 0.0560 0.0000 0.1287 0.0400 0.0000 0.1500 0.0262 104.58% 94.26%
180 5 0.0000 0.0000 0.0000 0.0000 0:0000 0.0000 \ 0.0000 100.00%
000-189-126-0 CETIS' v1.9.2.6 Analyst: lv\_ . QA:_l_
CETIS Analytical Report Report Date: 17 Jan-17 09:21 (p 2 of 2)
Test Code: ABS122016 I 20-9773-2752 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Analysis ID: 16-3945-2315 Endpoint:* Proportion Normal CETIS Version: CETISv1 .9.2 Analyzed: 16 Jan-1717:12 Analysis: Parametric-Control vs Treatments Official Results: Yes Angular (Corrected) Transformed Summary Conc-µg/L Code Count Mean 95% LCL 95% UCL Median Min Max Std Err CV% %Effect '
0 N 5 1.421 1.363 1.479 1.397 1.369 1.471 0:02093 3.29% 0.00%
18 5 1.412 1.364 1.461 1.397 1.369 1.471 0.01732 2.74% 0.59%
\ 32 5 1.373 1.288 1.459 1.397 1.266 1.429 0.03083 5.02% 3.35%
56 5 0.4439 0.341 0.5469 0.451 0.3218 0.5351 0.03708 18.68% 68.76%
100 5 0.2117 0.04884 0.3747 0.2014 0.05002 0.3977 0.05868 61.96% 85.10%
180 5 0.05002 0.05001 0.05003 0.05002 0.05002 0.05002 0 0.00% 96.48%
Proportion Normal Detail Conc-µg/L Code Rep 1 Rep 2 Rep 3 Rep 4 Rep 5 0 N 0.9900 0.9600 0.9700 0.9700* 0.9900 18 0.9700 0.9600 0.9800 0.9700 0.9900 32 0.9500 0.9100 0.9700 '0.9800 0.9800 r
.J 56 0.2600 0.2300 0.1900 0.1000 0.1600 100 0.1500 0.0700 0.0200 0.0000 0.0400 180 0.0000 0.0000 0.0000 0.0000 0.0000 Angular (Corrected) Transformed Detail Conc-µg/L Code Rep 1 r Rep 2 Rep 3 Rep 4 Rep 5 0 N 1.471 1.369 1.397 1.397 1.471 18 1.397 1.369 1.429 1.397 1.471 32 1.345 '1.266 1.397 1.429 1.429 56 0.5351 0.5002 0.451 0.3218 0.4115 100 0.3977 0.2678 0.1419 0.05002 0.2014 180 0.05002 0.05002 0.05002 0.05002 0:05002 Proportion Normal Binomials Conc-µg/L Code Rep 1 Rep 2 Rep 3 Rep 4 Rep 5 0 N 99/100 96/100 97/100 97/100 99/100 18 97/100 96/100 98/100 97/100 99/100 32 95/100 91/100 97/.100 98/100 98/100 56 26/100 23/100 19/100 10/100 16/100 100 15/100 71100 2/100 0/100 4/100 180 0/100 0/100 0/100 0/100 0/100 Graphics 1.0 r 0.9 E353
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000-189-126-0 CETIS' v1 .9.2.6 Analyst: ~QA:\ ---
CETIS Analytical Report Report Date: 17 Jan-17 09:21 (p 1 of 2)
Test Code: ABS122016 I 20-9773-2752 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Analysis ID: 00-2927-1383 Endpoint: Proportion Normal CETIS Version: CETISv1 .9.2 Analyzed: 16 Jan-17 17:12 Analysis: Linear Interpolation (ICPIN) Official Results: Yes Batch ID: 07-0829-0131 Test Type: Development Analys.t:
Start Date: 20 Dec-16 15:30 Protocol: EPA/600/R-95/136 (1995) Diluent: Labor<i'tory Seawater Ending Date: 22 Dec-16 15:30 Species: Haliotis rufescens Brine: Not Applicable Duration: 48h Source: Cultured Abalone , Age:
Sample ID: 20-6479-5531 Code: ABS122016 Client: Internal Lab Sample Date: 20 Dec-16 15:30 Material: Zinc Project: REF TOX Receipt Date: Source: Reference Toxicant Sample Age: n/a Station: REF TOX Linear Interpolation Options X Transform Y Transform Seed Resamples Exp 95% CL Method Linear . Linear 0 280 Yes Two-Point Interpolation Test Acceptability Criteria TAC Limits Attribute Test Stat Lower* Up.per Overlap Decision Control Resp 0.976 0.8 >> Yes Passes Criteria Point Estimates Level µg/L 95% LCL 95% UCL EC5 32.96 30.12 33.8 EC10 34.48 33.04 35.32 EC15 36 34.7 36.86 EC20 37.52 36.32 38.45.
EC25 39.04 37.9 .40.03 EC40 43.61 42.44 44.87 EC50 46.65 45.28 48.13 Proportion _Normal Summ~ry Calculated Variate(A/B)
Conc-µg/L Code Count Mean Min Max Std Err Std Dev CV% *i.Ettect A B 0 N 5 0.9760 0.9600 0.9900 0.0060 0.0134 1.38% 0.0% 488 500 18 5 0.9740 0.9600 0.9900 0.0051 0.0114 1.17% 0.2% 487 500 32 5 0.9580 0.9100 0.9800 0.0132 0.0295 3.08% 1.84% 479 500 56 5 0.1880 0.1000 0.2600 0.0278 0.0622 33.09% 80.74% 94 500 100 5 0.0560 0.0000 0.1500 0.0262 0.0586 104.60% 94.26% 28 500 180 5 0.0000 0.0000 0.0000 0.0000 0.0000 100.0% 0 500 Proportion Normal Detail Conc-µg/L Code Rep 1 Rep 2 Rep 3 Rep 4 Rep 5 0 N 0.9900 0.9600 0.9700 0.9700 0.9900 18 0.9700 0.9600 0.9800 0.9700, 0.9900 32 0.9500 0.9100 0.9700 0.9800 0.9800 56 0.2600 0.2300 0.1900 0.1000 0.1600 100 0.1500 0.0700 0.0200 0.0000 0.0400 180 0.0000 0.0000 0.0000 0.0000 0.0000 Proportion Normal Binomials Conc-µg/L Code Rep 1. Rep 2 Rep 3 Rep 4 Rep 5 0 N 99/100 96/100 97/100 97/100 99/100 18 97/100 96/100 98/100 97/100 99/100 32 95/100 91/100 97/100 98/100 98/100 56 26/100 23/100 19/100 10/100 16/100 100 15/100 71100 2/100 0/100 . 4/100 180 0/100 0/100 0/100 0/100 0/100 000-189-126-0 CETIS' v1.9.2.6 Analyst:* lr~ QA: f
CETIS Analytical Report Report Date: 17 Jan-17 09:21 (p 2 of 2)
Test Code: ABS122016 I 20-9773-2752 Red Abalone Larval Development Test Aquatic Bloassay & Consulting Labs, Inc.
Analysis ID: 00-2927-1383 Endpoint: Proportion Normal CETIS Version: CET1Sv1.9.2 Analyzed: 16 Jan-17 17:12 Analysis: Linear lnterpolati.on (ICPIN) Official Results: Yes Graphics 1.0 0.9 0.8
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0.1 0.3 0.2 0.1 o.o 0 20 40 60 80 100 120 t<O 160 180 I' Conc-µg/L 000-189-126-0 CETIS"' v1 .9.2.6 Analyst: v-.)'- QA:.__ ~--
CETIS Measurement Report Report Date: 17 Jan-17 09:21 (p 1 of 2)
Test Code: ABS122016 I 20-9773-2752 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Batch ID: 07-0829-0131 Test Type: Development Analyst:
Start Date: 20 Dec-1615:30 Protocol: EPA/600/R-95/136 (1995) Diluent: Laboratory Seawater Ending Date: 22 Dec-16 15:30 Species: Haliotis rufescens Brine: Not Applicable Duration: 48h Source: Cultured Abalone Age:
Sample ID: 20-6479-5531 Code: ABS122016 Client: Internal Lab Sample Date: 20 Dec-16 15:30 Material: Zinc Project: REF TOX Receipt Date: Source: Reference Toxicant Sample Age: n/a Station: REF TOX Parameter Acceptability Criteria TAC Limits Parameter Min Max Lower Upper Overlap Decision Salinity *, 34 34 32 36 Yes Passes Criteria Temperature 14.2 14.2 14 16 Yes Passes Criteria Dissolved Oxygen-mg/L Conc-µg/L Code Count Mean 95% LCL 95% UCL Min Max Std Err Std Dev CV% QA Count 0 N 2 6.8 4.259 9.341 6.6 7 0.2 0.2828 4.16% 0 18 2 6.85 2.403 11.3 6.5 7.2 0.35 0.495 7.23% 0 32 2 6.85 . 2.403 11.3 6.5 7.2 0.35 0.495 7.23% 0 56 2 6.85 2.403 11.3 6.5 7.2 0.3,5 0.495 7.23% 0 100 2 6.85 2.403 11.3 6.5 7.2 0.35 0.495 7.23% 0 180 2 6.85 2.403 11.3 6.5 7.2 0.35 0.495 7.23% 0 Overall 12 6.842 6.622 7.061 6.5 7.2 0.09959 0.345 5.04% 0(0%)
pH-Units Conc-µg/L Code Mean 95% LCL 95% UCL Min Max Std Err Std Dev CV% QA Count 0 N 2 7.55 6.915 8.185 7.5 7.6 0.05 0.07071 0.94% 0 18 2 7.55 6.915 8.185 7.5 7.6 0.05 0.07071 0.94% 0 32 2 7.55 6.915 8.185 7.5 7.6 0.05 0.07071 0.94% 0 56 2 7.55 6.915 8.185 7.5 7.6 0.05 0.07071 0.94% 0 100 2 7.55 6.915 8.185 7.5 7.6 0.05 0.07071 0.94% 0 180 2 7.55 6.915 8.185 7.5 7.6 0.05 0.07071 0.94% 0 Overall 12 7.55 7.517 7.583 7.5 7.6 0.01508 0.05222 0.69% 0 (0%)
Salinity-ppt Conc-µg/L Code Count Mean 95% LCL 95% UCL Min Max Std Err Std Dev CV% QA Count 0 N 2 34 34 34 34 34 0 0 0.0% 0 18 2 34 34 34 34 34 0 0 0.0% 0 32 2 34 34 34 34 34 0 0 0.0% 0 56 2 34 34 '34 34 34 0 0 0.0% 0 100 2 34 34 34 34 34 0 0 0.0% 0 180 2 34 34 34 34 34 0 0 0.0% 0 Overall 12 34 34 34 34 34 0 0 0.00% 0(0%)
Temperature-°C Conc-µg/L Code ,Count Mean 95% LCL 95% UCL Min Max Std Err Std Dev CV% QA Count 0 N 2 14.2 14.17 14.23 14.2 14.2 0 0 0.0% 0 18 2 14.2 14.17 14.23 14.2 14.2 0 0 0.0% 0 32 2 14.2 14.17 14.23 14.2 14.2 0 0 0.0% 0 56 2 14.2 14.17 14.23 14.2 14.2 0 0 0.0% 0 100 2 14.2 14.17 14.23 14.2 14.2 0 0 , 0.0% 0 180 2 14.2 14.17 14.23 14.2 14.2 0 0 0.0% 0 Overall 12 14.2 14.2 14.2 14.2 14.2 0 0 0.00% 0(0%)
000-189-126-0 CETIS' v1.9.2.6 Analyst: \...../\ QA:___.__r_
CETIS Measurement Report Report Date: 17 Jan-17 09:21 (p 2 of 2)
Test Code: ABS122016 I 20-9773-2752 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Dissolved Oxygen-mg/L Conc-µg/L Code 1 2 0 N 7 6.6 18 7.2 6.5 32 7.2 6.5 56 7.2 6.5 100 7.2 6.5 180 7.2 6.5 pH-Units Conc-µg/L Code 2 0 N 7.6 7.5 18 7.6 7.5 32 7.6 7.5 56 7.6 7.5 100 7.6 7.5 180 7.6 7.5 Salinity-ppt Conc-µg/L Code 2 0 N 34 34 18 34 34 32 34 34 56 34 34 100 34 34 180 34 34 Temperature-*c Conc-µg/L Code 1 2 0 N 14.2 14.2 18 14.2 14.2 32 14.2 14.2 56 14.2 14.2 100 14.2 14.2 180 14.2 14.2 p
000-189-126-0 CETIS' v1.9.2.6 Analyst: 'c (\.. QA: {
ALS Group USA, Corp.
dba ALS Environmental Analytical Report Client: Pacific Gas and Electric Company (PG&E) Service Request: Kl612743 \
Project: NPDES Annual Date Collected: 10119116 Sample Matrix: Ocean Water Date Received: 10/20/16 Analysis Method: 335.4 Units: mg/L Prep Method: Method
Basis: NA Cyanide, Total Date Date Sample Name Lab Code Result MRL MDL Dil. Analyzed Extracted Q Influent Kl612743-001 ND U 0.010 0.0009 10/24/1612:11 10124116 Discharge 001 . Kl612743-002 ND U 0.010 0.0009 10/24/16 12: 11 10/24/16 Method Blank K1612743-MB ND U 0.010 - 0.0009 10/24/16 12:11 10/24/16 7
~~Printed 10/2612016 3:30:55 PM~~
~~Superset~~
~~Reference:~~
16-0000397706 rev 00 Page 13 of 47
ALS Group USA, Corp.
dba ALS Environmental Analytical Report Client: Pacific Gas and Electric Company (PG&E) Service Request: Kl612743 Project: NPDES Annual Date Collected: 10/19/16
Sample Matrix: Ocean water Date Received: 10/20/16 Mercury, Total Prep Method: METHOD Units: ng/L Analysis Method: 1631E Basis: NA Test Notes:
Dilution Date Date Result Sample Name Lab Code MRL MDL Factor Extracted Analyzed Result Notes Influent Kl612743-001 0.5 0.06 10/24/16 10/25/16 0.34 J Discharge 001 Kl612743-002 0.5 0.06 10/24/16 10/25/16 0.47 J Method Blank Kl612743-MB1 0.5 0.06 10/24/16 10/25/16 ND Method Blank Kl612743-MB2 0.5 0.06 10/24/16 10/25/16 ND Method Blank Kl612743-MB3 0.5 0.06 . 10/24/16 10/25/16 0.093 J Kl612743ICP.ACI *Sample 11122116 Page No.:
Page 20 of 47
ALS Group USA, Corp.
dba ALS Eoviroomeotal Analytical Report Client: Pacific Gas and Electric Company (PG&E) Service Request: Kl612743 Project: NPDES Annual Date Collected: 10/19/16 08:15 Sample Matrix: Ocean Water Date Received: )0120116 08:30 Sample Name: Influent Basis: NA Lab Code: Kl612743-001 Total Metals Analysis Anall'.!e Name Method Result Units MRL MDL* Dil. Date Anall'.zed Date Extracted Q Arsenic 200.8 1.31 ug/L 0.50 0.03 1 11/14/16 10:42 11103/16 Cadmium 200.8 0.052 ug/L 0.020 0.003 1 11/14116 10:42 11/03/16 Lead 200.8 0.077 ug/L 0.020 0.004 1 11/14/16 10:42 11/03/16 Silver 200.8 0.018 J ug/L 0.020 0.004 1 11/14/16 10:42 11103/16 Titanium 200.7 ND U ug/L 2.0 0.4 1 11/18116 15 :51 10/31/16 j
I Printed 11122116 2:49:59 PM Superset
~~Reference:~~
Page 25 of 47
ALS Group USA, Corp.
dba ALS Environmental
Analytical Report Client: Pacific Gas and Electric Company (PG&E) Service Request: K1612743 Project: NPDES Annual Date Collected: 10/19/16 08:25 Sample Matrix: Ocean Water Date Received: 10/20/16 08:30 Sample Name: Discharge 001 Basis: NA l
Lab Code: K1612743-002 Total Metals Analysis Anall:'.!;e Name Method Result Units MRL MDL Dil. Date Anal;rzed Date Extracted Q Arsenic 200.8 1.28 ug/L 0.50 0.03 1 11114116 10:46 11/03/16 Cadmium 200.8 0.044 ug/L 0.020 0.003 1 11/14/16 10:46 11103/16 Lead 200.8 0.056 ug/L 0.020 0.004 ~ 11114116 10:46 11103/16 Silver 200.8 ND U ug/L 0.020 0.004 1 11/14/16 10:46 11103/16 Titanium 200.7 ND U ug/L 2.0 0.4 1 11/18/16 15:58 10/31/16 Printed 11/22/16 2:49:59 PM Superset Ref~rence:
I Page 26 of 47
ALS Group USA, Corp. dba ALS Environmental Analytical Results Client: Pacific Gas and Electric Company (PG&E) Service Request: Kl612743 Project: NPDES Annual Date Collected: 10/19/2016 Sample Matrix: Ocean water Date Received: 10/20/2016 Polychlorinated Biphenyls,(PCBs)
Sample Name: Influent Units: ug/L Lab Code: Kl612743-00I Basis: NA Extraction Method: EPA 3535A Level: Low Analysis Method: 8082A Dilution Date Date Extraction Ana.lyte Name Result Q MRL MDL Factor Extracted Analyzed Lot Note Aroclor 1016 ND U 0.20 0.0094 10/26/16 10/29/16 KWG1609785 Aroclor 1221 ND U 0.39 0.0094 10126116 10129116 KWG1609785 l
Aroclor 1232 ND u 0.20 0.0094 10126116 10/29/16 KWG1609785 Aroclor 1242 ND U 0.20 0.0094 10/26/16 10/29/16 KWG1609785 Aroclor 1248 ND U 0.20 0.0094 10/26/16 10/29/16 KWG1609785 Aroclor 1254 ND U 0.20 0.0094 10/26/16 10/29/16 KWG1609785 Aroclor I 260 ND U 0.20 0.0094 10/26/16 10/29/16 KWG1609785 Control Date Surrogate Name %Rec Limits Analyzed Note Decachlorobiphenyl 83 36-113 10/29/16 Acceptable Comments:
Printed: 11/02/2016 13:01 :44 Form IA- Organic Page 1 of u:\Stealth\Crystal.rpt\F orm I mNew.rpt Merged SuperSet
~~Reference:~~
RRI93462 Page 36 of 47
ALS Group USA, Corp. dba ALS Environmental Analytical Results Client: Pacific Gas and Electric Company (PG&E) Service Request: K1612743 Project: NPDES Annual Date Collected: 10/19/2016 Sample Matrix: Ocean water Date Received: 10/20/2016 Polychlorinated Biphenyls (PCBs)
Sample Name: Discharge 001 Units: ug/L Lab Code: K1612743-002 Basis: NA Extraction Method: EPA3535A Level: Low Analysis Method: 8082A Dilution Date** - Date Extraction Analyte Name Result Q MRL MDL Factor Extracted* Analyzed Lot Note Aroclor 1016 ND U 0.20 0.0094 10/26/16 10/29/16 KWG1609785 Aroclor 1221 ND u 0.39 0.0094 10/26/16 10/29/16 KWGI609785 Aroclor 1232 ND U 0.20 0.0094 10/26/16 10/29/16 KWGI609785 Aroclor 1242 ND u 0.20 0.0094 10/26/16 10/29/16 KWGI609785 Aroclor 1248 ND U 0.20 0.0094 10/26/16 10/29/16 KWG1609785 Aroclor 1254 ND u 0.20 0.0094 10/26/16 10/29/16 KWGI609785 Aroclor 1260 ND U 0.20 0.0094 10/26/16 10/29/16 KWGI609785 Control Date Surrogate Name %Rec . Limits Analyzed Note Decachlorobiphenyl . 77 36-113 10/29/16 Acceptable Comments:
Printed: 11102/2016 13:01:47 Fonn I A - Organic Page 1 of u:\Stealth\Crystal.rpt\Form I mNew.rpt Merged SuperSet
~~Reference:~~
RRl93462 Page 37 of 47
ALS Group USA, Corp. dba ALS Environmental Analytical Results Client: Pacific Gas and Electric Company (PG&E) Service Request: Kl612743 Project: NPDES Annual Date Collected: 10/19/2016 Sample Matrix: Ocean water . Date Received: 10/20/2016 Semi-Volatile Organic Compounds by GC/MS Sample Name: Influent Units: ug/L Lab Code: K1612743-00I Basis: NA Extract~on Method: EPA 3520C Level: Low Analysis Method: 8270D Dilution Date Date Extraction Analyte Name Result Q MRL MDL Factor Extracted Analyzed Lot Note Phenol ND U 0.50 0.063 10125116 11101116 KWG1609692 2-Chlorophenol ND U 0.50 0.054 10125116 11/01/16 KWG1609692 2-Methylphenol ND U 0.50 0.11 10/25/16 11/01/16 KWG1609692 4-Methylphenolt ND u 0.50 0.12 10/25/16 11101/16 KWG1609692 2-Nitrophenol ND U 0.50 0.063 10125116 11/01/16 KWG1609692 2,4-Dimethylphenol ND U 4.0 2.2 10/25/16 11/01116 KWG1609692 2,4-Dichlorophenol ND U 0.50 0.047 10/25/16 11101116 KWG1609692 4-Chloro-3-methy lpheno 1 ND u 0.50 0.037 10125116 11101/16 KWG1609692 2,4,6-Trichlorophenol ND u 0.50 0.0.58 10125116 11101116 KWG1609692 2,4,5-Trichlorophenol ND U 0.50 0.031 10125116 11101116 KWG1609692 2, 4-Dinitrophenol ND U . 4.0 0.17 . 10125116 11101116 KWG1609692 4-Nitrophenol ND U 2.0 0.28 1. 10/25/16 11101116 KWG1609692 I
2-Methyl-4,6-dinitrophenol ND u 2.0 0.025 . I 10/25/16 11/01116 KWGJ609692 Pentachlorophenol ND U 1.0 0.34 1 10125116 11/01/16 KWG1609692 Control Date Surrogate Name %Rec Limits Analyzed Note 2-Fluorophenol 73 34-118 11/01116 *Acceptable Phenol-d~ 73 39-109 11101/16 Acceptable 2,4,6-Tribromophenol 97 35-132 11/01116 Acceptable r
t Analyte Comments 4-Methylphenol This analyte cannot be separated from 3-Methylphenol.
Comments:
Printed: 11/02/2016 15:31:20 Form IA- Organic Page 1 of u:\Stealth\Crystal.rpt\Fonnl mNew.rpt Merged SuperSet
~~Reference:~~
RRl93484 Page 42 of 47
ALS Group USA, Corp. dba ALS Environmental Analytical Results Client: Pacific Gas and Electric Company (PG&E) Service Request: Kl612743 Project: NPDES Annual Date Collected: 10/19/2016 Sample Matrix: Ocean water Date Received: 10/20/2016 Semi-Volatile Organic Compounds by GC/MS Sample Name: Discharge 001 Units: ug/L Lab Code: Kl612743-002 Basis: NA Extraction Method: EPA 3520C Level: Low Analysis Method: 8270D Dilution Date Oate Extraction Analyte Name Result Q MRL MDL Factor Extracted Analyzed Lot Note Phenol ND U 0.49 0.063 10/25/16 11101116 KWGl609692 2-Chlorophenol ND U 0.49 0.054 10/25/16 11101/16 . KWGl609692
, 2-Methylphenol ND U 0.49 0.11 10/25/16 11101/16 KWG1609692 4-Methylphenolt ND u 0.49 0.12 10/25/16 11101/16 KWG1609692 2-Nitrophenol ND U 0.49 0.063 10/25/16 11/01/16 KWG1609692 2,4-Dimethy !phenol ND U 3.9 2.2 10/25/16 11101/16 KWG1609692 2,4-Dichlorophenol ND u . 0.49 0.047 10/25/16 11/01116 KWG1609692 4-Chloro-3-methylphenol ND U 0.49 0.037 10/25/16 11/01116 KWG1609692 2,4,6-Trichlorophenol ND U 0.49 0.058 10/25/16 11/01116 KWG1609692 2,4,5-Trichlorophenol ND U 0.49 0.031 10/25/16 11/01116 KWG1609692 2,4-Dinitrophenol ND U 3.9 0.17 10/25/16 111011{6 KWG1609692
(
4-Nitrophenol ND\U 2.0 0.28 10/25/16 11101116 KWG1609692 2-Methyl-4,6-dinitrophenol ND U 2.0 0.025 10/25/16 11101/16 KWG1609692 Pentachlorophenol ND U 0.97 0.34 10/25/16 11101116 KWG1609692 Control Date Surrogate Name %Rec " Limits Analyzed Note 2-Fluorophenol 79 34-118 11101116 Acceptable Phenol-d6 79 39-109 11101116 Acceptable 2,4,6-Tribromophenol 89 35-132 11/01/I 6 Acceptable t Analyte Comments 4-Methylphenol This analyte cannot be separated from 3-MethylphenoL Comments:
Printed: 11102/2016 15:31:24 Fonn IA - Organic Page 1 of u:\Stealth\Crystal.rpt\Form I mNew.rpt Merged SuperSet
~~Reference:~~
~~RRl93484 Page 43 of 47~~
~~BABCOCK Laboratories, Inc.~~
Tu 5imiilmd of facellen(e for Ovrr 100 tears Client Name: Severn Trent Services Analytical Report Page 2 of 3 Contact Jim Wysong Proj~ct Name: Diablo Canyon Plant - Annual Address: 320 Beta Ct Sludge Project Number: PG&E Diablo Canyon WWfP Arroyo Grande, CA 93420 Report Date: o4-Nov-2Q16 Work Order Number: B6J1712 Rea:ived on la: (YIN): Yes Temp: 5 °C Laboratory Reference Number B6J1712-01 Sample Oescription Matrix Sampled Date/Time ReceiVed Datemme
Sludge Holding Tank Sludg~ 10/17/19.10:30 10/18116 10:30 Analyte(s) Result RDL IVIDL Uriits Method Analysis Date Analyst Flag Anions Nitrate as N ND 2jo 110. mg/kgdfy EPA300.0 10/26/16. 21 :48 deb N_WEX Aggregate Properties pH 7.0 1.0 . 1.0 pH Units SM4500H+B 10/20/16 22:30 gv Solids To~I SOiids 9600 400 300 mg/L SM2540B 10120116 14:30 .cmr Nutrients Ammonia-Nitrogen 7300 2100 1000 mg/Kg*~fy SM4500NH3H 10/19/16 13:19 sU N_WEX Kjeldahi Nitrogen 76000 21000 21000 mg/kg dry EPA351.2 10/25/16 23:12 jina Total Phosphorus 26000 510 260 mgiKg*dry EPA6020 1oi25116 13:03 met M~tals arid Metalloids; EPA $W846 Series Boron 180 100 2.6 mg/kg dry EPA6010B 10125116 20:22 kya cadmium. 1.6 1.0 0.63 mg/kg dry EPA6020 10125/16 16:23 mel Total Chromium 9.4 1.0 0:81 mg/kg dry EPA.6020 10125/16 16:23 niel Copper 430 1.0 0.78 mg/kg dry EPAS020 10/25i16 16:23 niel Lead t.1 5.0 ' 0.29 mg/kg dry EPA6020 10125116 16:23 mel Mercury 0.23 0.10 0:049 mg/kg dry EPA 7471A 10/24/16 12:42 kya Nidcel 11 1.0 0.48 mg/kg dry EPA6020 10125/1616:23 mel Zinc 740 5.0 1.7 mg/kg dry EPA6Q2.0 10/25/16 16:23 mel CalifOmia Waste Extraction Test (Title 22 sec. 66261 Apx II); lnorganics ..
eoi>per 0.062 2.5 .0.0058 mg/L EPA 6020AANET 11/02/16 19:39 mel J mailing lqcation p 951 653 3351 CA ELAP No. 2698 P.0Box432 6100 Quail V:alley Court F 951 653 1662 EPA No. CA00102 Riverside, CA 92502--0432 Riverside, CA 92507*0704 Www.babcocklabs.rom NELAP No. OR4035
BABCOCK Laboratories, Inc.
1/ie Standwd ~f Euellence]or Om 100 fears Client Name: Severn T~nt Servic:eS Analytical Report Page 2 of 3 Contact Jim Wysong Project Name: Diab lo Canyon Plant-- Annual Address: 320 Beta.Ct Sludge Project Number: PG&E Diablo Canyon WWTP, Arroyo Grande, _CA 93420 Avila Beach CA Report Date: 11-Nov-2016 Work Order Number: B6K0212 Received on Ice (Y/Jlf): Yes Temp: 6 °C Laboratory Reference Number B6K0212-01 Sample Description Matrix Sampled Datemme Received Datemme Oil & Grease - PG&E Diablo Canyon WWTP, Avila Sludge 11/01/16 09:25 11/02/16 9:09 Beach CA
. Analyte(s) Result RDL M.DL Unl1s Method Analys~ Date Analyst Flag Solids Totai Solids 1.0 0.10 0.10 % SM2540G 11/04/16 09:30 sll Aggregate Organic Gompaunds Oil & Grease (HEM) ND 9.7 9,7 %dry EPA9071B 11/10/1611:3o krv mailioc hcation p 9l_il 653 3351 CA ELAP No. 2698 P.0Box432 6100 Quail Valley Court F 951653 1662 EPA No. CA00102
~rside, CA 92\)02*0432 Riverside, GA 92507'.0704
~~www.babcocklabs.com NELAP No. OR4035~~

DCL-2017-500, Discharge Monitoring Report for Fourth Quarter 2016

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