ML20072F290

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Info on Reactor Vessel Matl Surveillance Program Brunswick Steam Electric Plant Unit 2
ML20072F290
Person / Time
Site: Brunswick Duke Energy icon.png
Issue date: 06/30/1994
From: Contreras G, Ranganath S
GENERAL ELECTRIC CO.
To:
Shared Package
ML20072F244 List:
References
NEDO-24157, NEDO-24157-R02, NEDO-24157-R2, NUDOCS 9408230276
Download: ML20072F290 (100)


Text

{{#Wiki_filter:& GE Nuclear Energy TechnicalServices Business General Electric Company,175 Curtner Avenue, San Jose, CA 95125 NEDO-24157 Revision 2 ClassI June 1994 INFORMATION ON REACTOR VESSEL MATERIAL SURVEILLANCE PROGRAM BRUNSWICK STEAM ELECTRIC PLANT UNIT 2 Prepared for Carolina Power and Light Company Prepared by. bb w G. W. Contreras, Senior Engineer RPV Integrity Approved by: S. Ranganath, Manager Structural Mechanics l l l I 9408230276 (740017 l L PDR ADOCK 05000324  ; P pop l

NEDO-24157 Revision 2 IMPORTANT NOTICE REGARDING CONTENTS OF tills REPORT PLEASE READ CAREFULLY This report was prepared by the General Electric Company (GE) solely for the use of Carolina Power and Light Company. The information contained in this report is believed by GE to be an accurate and tnie representation of the facts known, obtained or provided to GE at the time this report was prepared. The only undertakings of the General Electric Company (GE) respecting information in this document are contained in the contract between Carolina Power and Light and GE, as identified in the purchase order for this report and nothing contained in this document shall be construed as changing the contract. The use of this information by anyone other than Carolina Power and Light or for any purpose other than that for which it is iMended, is not authorized; and with respect to any unauthorized use, GE makes no representation or warranty, and assumes no liability as to the completeness, accuracy, or usefulness of the information contained in this document.

                                             - li -

NEDO-24157 Revision 2 CONTENTS Page 1

1.0 INTRODUCTION

1 2.0 RPV SUPPLIER AND SPECIFICATIONS 2 3.0 VESSEL BELTLINE MATER.IAL 2 3.1 Plate and Weld Locations 2 3.2 Plates / Forgings and Welds 6 3.3 Heat Treatment 7 3.4 Chemical Analyses 9 3.5 Tensile Properties (Unirradiated) 10 3.6 Fracture Toughness Properties (Unirradiated) 4.0 VESSEL MATERIAL SURVEILLANCE PROGRAM II 11 4.1 Plate Material 1I 4.2 Welds 11 4.3 Documentation 12

5.0 REFERENCES

APPENDICES A. As-built Fabrications Drawings A-1 B-1 B. Plate and Forgings CTRs C-1 C. Weld CTRs 1 D-1 l D. Weld Logs E. Thermal History Logs E-l F-1 l F. Surveillance Test Specimen Plan l l l l

                                           - iii -

NEDO-24157 Revision 2 l

1.0 INTRODUCTION

The original version of this report was issued in 1978. That report was furnished in response to a , request for information concerning the reactor vessel material surveillance program (Reference 1). l This revision contains several changes to report presentation and content. In order to make this report more complete, the bases information from which this summary was derived is contained in the appendices. In addition, for ease of use, the information has been reformatted to a more tabular format. And lastly, fluence, EFPY, and RTndt shift estimates were deleted. Since this information changes with time, it is more appropriate that this information be contained within reports specific to withdrawn surveillance capsules. l 2.0 RPV SUPPLIER AND SPECIFICATIONS The Bnanswick 2 RP,V was purchased from Chicago Bridge and Iron Company, Birmingham, Alabama (GE Purchase Order No. 205-H 1332, CB&l Contract No. 68-2472). The RPV is designed and constructed in accordance with the following codes and specifications: ~

a. ASNE Boiler and Pressure Vessel Code - Section III,1965 Edition and Addenda through Summer 1967 Addenda.
b. " Standard Requirements for Reactor Pressure Vessel", General Electric APED Specification No. 21 Al 100, Rev. O with Data Sheet 21 Al100AR, Rev.12.

I I I l

Revision 2 NEDO 24157 3.0 VESSEL BELTLINE MATERIAL 3.1 PLATE AND WELD LOCATIONS Materials in the RPV beltline region (as defined in 10CFR50, Appendix G, Section II) are identified below and are as shown in Figure 1. 3.2 PLATES / FORGINGS AND WELDS

a. All shell plate materialis S A-533-65 Gr. B., Class I; CB&I Specification MS-1, Rev.1; and provided by Lukens Steel Company, Coatesville, Pennsylvania.
b. Nozzles N16A and N16B material is A-508, Class II; CB&I Specification MS-2; and provided by Lenape Forge Division - Bonney Forge and Foundry Inc., West Chester, Pennsylvania.
c. Weld Materials and Process:

Coated Electrod_qs Flux Electrode Combinations Electrode: Filler Metal Type E8018G/NM Adcom INMM/Linde 124 RACO INMM/Linde 124 Trade Name: Alloy Rods E8018NM Adcom INMM RACOItaBf Supplier: Alloy Rods Co., Adcom Metals Co. Inc., - Reid-Avery Company Division of Chematron Corp., Atlanta, Georgia Baltimore, MD York, Pennsylvania Submerged Arc Submerged Arc Weld Process: Shielded Metal Arc 3.2.1 Lower Shell Course (Assembly Piece No.1200. Rine No 1) i (1) Plates (2)- 201 and 251 Piece No. ' Heat No. Slab No. 201 C4500 2 251 C4550 2

CH&f ASSE MBLY DHAWING Pc NO NO 1600 63 FINAL VESSE L ASSEMBLY 8200 12 SHE LL PL Af f ASSE MBL Y NO t HALF HING Pc Mk NO 200 PLATE PARI NO 208 - EXCLOOlNG NOZZLES AND NOZZLE WELDS 1200 33 SHELL PLATE ASSEMBLY NO 1 HALF HING Pc Mk NO 250 . PLATE PART NO 251 - EXCLOOING NOZZLES ANO NOZZLE WELOS 3300 14 SHELL PLATE ASSEMBLY NO 2 RING PLATE PART NOS 301 ANO 351 43 N16A/S NOZZLE ASSEMBLY - ASSEMBLY PART NO 302 TO N& 2 SHE4 L 6 SE AM OETAILS SE AMS F ANO G - SHELL VERTICAL SEAMS SE AM F G - SHELL GIRTH SE AM 7 SE AM BC FOR N16 NOZZLES VERT 6 CAL *

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2588 758 AZsMUTH 750 VEWL 0 G1 G2 (1300 ~ NO.1 RING) 's VE Ri tCAL SEAM Lb NUMSERS ARE CSal PART ANO ORAWeseG NUM8ERS UNLESS OTHERWISE DEF INED

                   ' REACTOR ASSEMSLY DRAWsNGGE 197RSO2 ELEV ATIONS ARE FROM VESSEL T Figure 1.        Brunswick             RPV Beltline Region Welds and Plates

Revision 2 NEDO-24157 (2) Vertical Seam Welds (GI and G2) (a) Coated Electrodes - Type E8018G/NM Reference Specification - S A-316 Traveler Heat No. laLNpm CB&I Wqld Snecs Card Set Seauence 08R481 3908A27A GRPI-Rev i 1200-R-12 6A (repair) 01R496 S925A27A GRPl-Rev i 1200-R 14/13 6A (repair) WPS-323-2F4F6 Rev 2 1200 2A (G1 root pass) WPS-323 2F4F6 Rev 1 1200 2B (G2 root pass) 82D913 D908A27A GRPl-Rev 1 1200-R-13 6A (repair) 88E081 F920A27A GRPl-Rev i 1200-R-19 6A (repair) 05R938 A020A27A GRP1-Rev i 1200-R-19 6A (repair) (b) Flux Electrode Combinations - Adcom/INMM-Type Linde 124 Heat No. Lot No. ILttn No CB&I Weld Spec. Traveler Card Set Seauence 3876 934 WPS-323-2F4F6, Rev. 2 1200 2 M,N,E.F S3986 3.2.2 Lower Intermediate Shell Course ( Assembly Piece No 1300. Rine 2) (1) Plates - 301 and 351 Piece No. Heat No Slab No. 301 C4489 1 351 C4521 2 (2) Vertical Weld Seams (F1 and F2) (a) Coated Electrodes - Filler Metal Type E8018G/NM Reference Specification - S A-316 Traveler Heat No. Lot No, CB&l Weld Spec. Card Set Sequence 977987 1802A27A WPS 3231F6 1300 SC & 5B 88E081 F920A27A GRP-1, Rev i 1450R26 6A 654W539 S823A27A GRP 1, Rev i 301-Rl/R2 6A/B, 6 (repairs) E916A27 A GRP-1, Rev i 1300-R4 6 601221 (b) Flux Electrode Combinations - Adcom/INMM - Type Linde 124 Heat No_. Lot No Run No CB&l Weld Spec. Traveler Card Set Sequence 934 WPS 323-lF6 1300 SF, P, G, Q S3986 3876 4-l

  . _ . . . _ _.                   ._                        _     = . _ . . .       .           ..       ..          _ - - . _ .

4 NEDO-24157 Revision 2 (3) Girth Weld Seam - FG - Assembly Piece No.1600 (a) Coated Electrodes - Filler Metal Type E8018G/NM Heat No. Lot No. CB&I Weld Spec _ Traveler Card Set Seauence C3L46C J020A27A WPS 323-2F4F6,Rev.2 1600 4A 432A2671 H019A27A WPS 323 2F4F6,Rev.2 1600 4A 662A746 h013 A27A GRP-1 Rev i 1600R-57 6A (b) Flux Electrode Combination - RACO INMM - Type 124 Heat No. Lot No Run No CB&l Weld Soec. Traveler Card Set Scauence 3932 WPS 323-2F4F6, Rev. 2 1600 4A 3P4000 (c) Overlay Seam Weld

                                 . Type:                                         E30915                      E308L-15
                                  . Trade Name:                                  Arcaloy 309 Lime            Arcaloy 308ELC Lime Supplier:                                     Alloy Rods Company Chemetron Corporation Iyps            Heat No Lot No.                       CB&I Weld Spec Traveler Card Set Secuence 8

E309-15 W73594 3 A922H5C GRP 2, Rev. 2 1600 R57 E308L-15 X47214 K019H2C GRP 2, Rev. 2 1600 R57_ 8 3.2.3 Nozzles N16A and N16B - Nozzle ( Assembly Piece No 302) to Shell (Assembiv Piece No.1300. Rine No 2) Forcines (1) Forgings I Nozzle Piece No Heat No Forcine No N16A 302 Q2QlVW 247P-3 A N16B 302 Q2QlVW 247P-3B (2) Nozzle to Vessel Weld Seam (a) Coated Electrodes Type E8018G/NM lieat No. Lot No. CB&l Weld Soec. Iraveler Card Set Seauence D908A27A WPS 303-lF4, Rev. l- 1300 23B&O& A-E,F - 82D913 E916A27A WPS 303-lF4, Rev. I 1300 23A-23E 4

                         -601221 S925A27A WPS 303-IF4, Rev. I                                1300                    23 A 23E,23N OIR496 D909A27A' WPS 303-IF4, Rev.~ l                              1300                    23 A-23 E, 23 N 85D766 l

Revision 2 NEDO-24157 3.3 HEAT TREATMENT 3.3.1 Plates and Test Soecimens All plates and test specimens were heated 1650 F 25 F, held I hr/in. minimum and water quenched for approximately 23 minutes. They were then tempered 1220 Filo F, held I hr/in minimum and air cooled. Plates were gas cut hot, stress relieved at i 150 F(+25/-50 F), held for 30 min /in. minimum and air cooled. Test specimens were stress relieved by heating within a rate of 72 F/hr to 1150 F(+25/-50 F), held for 50 hours, furnace cooled within a rate of 90 F/hr to 600 F and air cooled. CB&l reported the following heat treatment for the plates: 201 2.51 10_1 lil O&T 1650 F 5 hr 42 min 5 hr 50 min 5 hr 35 min 5 hr 45 min 1220 F 5 hr 45 min 5 hr 40 min 5 hr 35 min 6 hr 5 min Total Accumulative Stress Relief Time 1150 F 32 hr 55 min 32 hr 42 min 30 hr 28 min 30 hr 33 min The nozzle heat treatments were: 1675 F 25 F, I hr/in, air cooled 1560 F 25 F, I hr/in, water quench 1290 F 25 F, I hr/in, air cooled Tests stress relieved at i150 F 25 F for 50 hours i I 1 l l l l

Revision 2 NEDO-24157 3.3.2 Post. Weld Heat Treatment Location Temperature Duration Lower Shell Course 1100 F to 1175 F 22 hr 50 min Vertical Weld Seams GI and G2 Lower Intermediate Shell Course 1100 F to 1175 F 26 hr 23 min Vertical Weld Seams F1 and F2 Girth Seam Weld FG 1100 F to 1175 F 6 hr 10 min N16A/B Nozzle to Vessel Seams 1100 F to 1175 F 15 hr 43 min 3.4 CHEMICAL ANALYSES At the time of construction for these pressure vessels, the only requirements for chemical composition were those contained in the ASME material specifications (A533 Grade B for plate; and A233, A298, A316 or A371 for weld electrodes and rods). The elements reported in these specifications did not include copper (Cu). The available chemistry certifications are provided, but values for the copper contents of these materials are not directly available from these certifications. By tracing the heat numbers for the beltline plates and nozzle N16A/B forgings back to the suppliers (Lukens Steel and Lenape Forge, respectively), the copper contents for the plates and forgings were obtained. The ladle analysis for % Cu was measured and retained by the suppliers even though it was not required by the purchase specification. The copper content of the welds was provided by the supplier, though not required, except in the case of nozzle-to-vessel weld. Items marked N/R were not reported. l 1 1 i 7

Revision 2 NEDO-24157 (a) The chemical analyses for vessel beltline plate / forging material are as follows: Descrintion Plate Heat C &E S Qi 5 M @ Lower Shell 201 C4500-2 0.23 1.20 0.012 0.016 0.15 0.27 0.54 0.55 251 C4550-2 0.22 1.35 0.010 0.014 0.11 0.21 0.60 0.56 Lower Inter. Shell 301 C44891 0.25 1.40 0.007 0.016 0.12 0.27 0.'60 0.56 351 C4521-2 0.23 1.43 0.009 0.015 0.12 0.26 0.57 0.54 Nozzles N16A/B N16A/B Q2QlVW 0.21 0.75 0.010 0.015 0.16* 0.23 0.80 0.69 ladle 0.16 0.71 0.006 0.013 N/R 0.24 0.81 0.60 check

  • from product analysis (b) The chemical analyses for the vessel beltline welds are as follows:

Ie.it lie _at Lot No. C Mn E S Qi S M & Coated Electrodes - Type E8018G/NM AI396CX/CZ 08R481 J908A27A 0.04 0.93 0.019 0.016 0.02 0.37 0.87 0.52 AI380DX/DZ OIR496 S925A27A 0.05 1.11 0.020 0.017 0.02 0.48 0.92 0.54 5Z-3Z/5X 82D913 D908 A27A 0.063 1.06 0.009 0.018 0.03 0.39 0.80 0.45 A1304BX/Z 88E081 F920A27A 0.06 1.10 0.017 0.014 0.02 0.27 0.93 0.51 511 05R938 A020A27A 0.077 0 94 0.018 0.017 0.02 0.40 0 91 0.57 PT164S 977987 1802A27A 0.042 1.04 0.016 0.022 0.03 0.47 1.04 0.59 PT164N 654W539 S823A27A 0.041 0.95 0.015 0.020 0.04 0.38 1.09 0.58 AN239CX/Z 601221 E916A27A 0.041 1.05 0.018 0.015 0.03 0.35 0.88 0.49 875 C3L46C J020A27A 0.063 0.96 0.019 0.017 0.02 0.32 0.87 0.53 800 432A2671 H019A27A 0.057 1.22 0.019 0.014 0.04 0.44 1.08 0.51 WO No.11-D 662A746 H013 A27A 0.060 0.96 0.021 0.017 0.03 0.38 0.88 0.52 5Z-3Z/X 85D766 D909A27A 0.063 1.22 0.008 0.010 0.02 0.44 1.08 0.44 Flux Electrode Combinations - INMM Type Linde 124 PT200 S3986 3876 0.080 1.42 0.019 0.016 0.05 0.36 0.96 0.52 WO No.14-D 3P4000 3932 0.046 1.35 0.015 0.012 0 02 0.37 0.90 0.45 Nozzle to Vessel Overlay Seam - Type E309-15 M281C W73594 3 A922H5C 0.05 1.79 0.020 0.011 N/R 0.54 12.79 NR Nozzle to Vessel Overlay Seam - Type E308L-15 RQ-6474 X47214 K019H2C 0.03 1.69 0.02 0.02 N/R 0.72 9.26 N/R 8-

NEDO-24157 Revision 2 3.5 TENSILE PROPERTIES (UNIRRADIATED) Yield Ultimate Elongation Elates Heat No Slab No. Strenuth. ksi Strencth. ksi (% in 2 inches) C4500 2 63.8/63.0 89.4/89.9 25./28. Lower Shell Course C4550 2 70.1/68.9 94.1/94.5 22./22. 1 69.5/70.5 95.6/97.0 24./25. Lower Inter. Shell Course C4489 C4521 2 71.6/71.7 94.5/94.5 25./25. Nozzles N16A/B, (0) 69.0 88.65 22.5 Q2QlVW (180 ) 69.75 88.5 24.5 Forgings 247P-3 A,3B Yield Ultimate Elongation Weldj Heat No. .L_ot No. Streneth. ksi Strenuth. ksi (% in 2 inches) 08R481 J908A27A 80.5 90.5 28.0 Type E8018G/NM OIR496 S925A27A 84.0 92.5 26.0 82D913 D908A27A 78.0 86.5 28.0 88EO8i F920A27A 83.0 93.2 27.0 05R938 A020A27A 76.3 94.0 26.0 977987 1802A27A 71.2 85.1 26.0 654W539 S823A27A 74.0 84.1 28.0 601221 E916A27A 79.0 89.5 27.0 C3L46C J020A27A 80.4 91.0 26.0 432A2671 H019A27A 80.5 93.0 28.0 662A746 H013 A27A 80.0 91.0 26.0 85D766 D909A27A 82.5 90.0 28.0 3876 71.8 86.5 30.0 Adcom/INMM - Linde 124 S3986 3932 72.5 84.5 28.0 RACO/lNMM - Linde 124 3P4000 W73594 3A922H5C N/R N/R N/R E309-15 X47214 K019H2C N/R N/R N/R E308L-15 l I l l l

Revision 2 NEDO-24157 1 3.6 FRACTURE TOUGHNESS PROPERTIES (UNIRRADIATED) The Brunswick 2 reactor pressure vessel was ordered prior to the issuance of Appendix G, . I 10CFR Part 50. The ferritic pressure boundary material was qualified by drop weight testing for the shell plate and CVN testing for the weld material. Test results are shown in the followmg l tables. j Heat / Drop Weight Charpy Plates /Foruines Plates Slab NDTT Test Values Test Temnerature Lower Shell Course 201 C4500-2 +10 F or less 46,48,61 10 F  ; No.1200 251 C4550-2 +10 F or less 43,35,64 10 F Lower Inter. Shell 301 C4489-1 +10 F 38,45,38 10 F Course No.1300 351 C4521-2 +10 F 42,45,48 10 F Nozzle N16A/B (0 ) Q2QlVW +40 F 116,110,112 40 F (180 ) Q2QlVW +40 F 133,74,141 40 F Charpy Deltline Welds lleat Lot No. Test Values Test Temarature Type E8018G/NM 08R481 J908A27A 81,81,82 +10 F 01R496 S925A27A 62,64,68 +10 F 82D913 D908A27A 80,94,83,81,82 + 10 F 88E081 F920A27A 85,90,91 +10 F 05R938 A020A27A 66,84,86 +10 F 977987 3802A27A 105,109,73 +10 F 654W539 S823A27A 181,144,171 + 10 F 601221 E916A27A 107,108,108 +10 F C3L46C 1020A27A 35,39,40 +10*F 432A2671 H019A27A 31,31,33 + 10 F 662A746 H013 A27A 89,82,95 -20 F 85D766 D909A27A 87,69,73,71,75 +10 F Flux Electrode S3986 3876 46,51,49 + 10 F 3P4000 3932 97,95,88 +10 F  ; E309-15 W73594 3A922H5C N/R N/R E308L-15 X47214 K019H2C N/R N/R l l 1

                                           - 10 l
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1 1 Revision 2 NEDO 2415i  ! 1 1 4.0 VESSEL MATERIAL SURVEILLANCE PROGRAM 4.1 PLATE MATERIAL The plate material used in the surveillance program (Assembly 2613) was cut from piece 301, ! Heat C4489, Slab 1. The post-weld heat treatment of the plate specimen was at i150 F.(+25/- 50 F) for a total of 50 hours. Allinformation pertaining to the surveillance plate materialis contained in Section 3. 4.2 WELDS i CB&I files do not contain information on the weld material used in the surveillance program. The plate materialjoined by this weld was from piece 301, Heat C4489; Slab 1. CB&l performed the ' welding in accordance with the weld procedure in WPS-323-1-F6. The post-weld heat treatment of the welded piece was at i150 F(+25/-50 F) for a total of 50 hours. 4.3 DOCUMENTATION 2 A copy of the surveillance program drawings, and the surveillance test specimen preparation procedure No. STP-3 are attached to this report. V i

' ~ - - - - - ~ _ - - . - Revision 2 NEDO-24157

5.0 REFERENCES

1. Letter to Carolina Power & Light Company from A. Schwencer, USNRC, May 23,1977.

l l Revision 2 NEDO-24157 \ l l i I APPENDLX A i i As-Built Fabrication Drawing i 4 i t I

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NEDO.24157 Revision 2 1 APPENDIX Il Plate and Forgings CTRs l l i

                            . [3. l .

uuvise" copy 14 >4-ou - - LU:2N3 S"5L COfAPANY I .* Dart, 20-o8 me ' '1543 PURCHASER; cogg pam32o Chicago Bridge & Iron Co. TES7 CERT:r-ICATE Same 12 Jai.es

                                                           . C Thompson, Pur.Mgr                         mot osoir no.             cusio-en e.o.

Boyles, Ala. E.O. Box 277 2471-Sheet 1 GR 73168 Sa

                                                    'Birainchcu, Ala. 35202                               27474-3                                                                                   ,,

i- "to 2 s 1968 SPECIFICATION 5: MS-1 Rev. 1 Fbx. 80000 SA-533-% ar.s Class 1 Mod.by CB & I O.K. SheetJ1 of 2 ~ stuo test O.K. oxcesem ies, - C H E TA I C A L A N ALY SIS R R1gic procenn 5 Cu $i Ni Ca Mo V h A; MELI No. C Mn P l 012 016 27 54 -55 F.G. P.&V. I.P.Stce1 Electric C45m 23 1.20 Grair Size after stret s reli eved 0 -8 C4500-2 I PHY SIC AL PROPERTIES

                                                                                               '""                                             <*r^as                nae tur e                 oEscaIPTION 5'* *              " U"'
  • t. A. sun utu No. NO.
                                                                              "E'?

nu nm =2 - V-Notch +10"F. Annearanc e i I 25 l. 1-360 x 145-1/2 x 5-9/16" 2 638 894 l C4500 630 899 28 46 l48 g i ol 40% shear . 1 I La teral' exg>arlsion ijn inchre s

                                                                                                                                .03-      l.050 1 037                                          -

L l l N .D .T . is +J 0*F, o unde c. I I

                                                                                               ' I . p1     ccedul e TPC        -1     Eqv. 1 l Tect ed in' at cordar ce to                     C.B. E l           l Test location C.B.                      & I. MTP-1.                                                   l           l 7                                                                                                                                            l            l l                                                                                                                                            !            l
                                       !!oraogeneity test : atisct ctory.

1 se . - top mjddic olf plate Bend test st tisfac tory - Locat ion tr ansver ss thqn 1-1 / 2 inci es. Radit s of c ur va tt re le

                                                                                                                                                                                                          , CW l

f A .-MQ l Y l l r o.f,(y#; y ,,, We hereby certify the above figures are correct as contoir.ed in the records of the compon).

LUKENS STEEL COMPANY

  • fitt = 3
                          '                                                                                               DAf f .
               '                                                           (o At[$t i".;          39320
   '",""*'".                                                              TEST CERTIFICATE C   "5' G"' ' =                                      .

.2 Chicago Bridge & Iron Co. =>u orote no cusioute r o James C Thompson, Pur.Mgr. Same Boyles, Ala. 27474-3 2471-Sheet 1 . k# SPfCif fC Af TONS: - Same L Sheet #2 of 2 afND TE57 HOmaOGf{f{j - CHEMICAL ANALYSI5 Mo y to At a 5 Cu Si Ni Ca MELT NO C Mn P x c4500-2 PHYSICAL P R O P E R TIE S

                                                                                            ' '^ '$                                             DESCRIPTION
                                                    "",,   %tA        BHN MRT NO.                  ,            ,
                                                   +

1650*P ,- 25"F., hold 1 tr . perinc hl min. a nd W.Q. for 23 minut es . Plates and tests h eat *F,gdlO'F., held 1 hr. per inch min g and E ir cooled. Then tempered 1220 '

                                                                           +25 Plates gas cut hot and otress                    relieved 1150*F,         -50*Fl,       9 held; l1/2 hr. perinch min. and air cooled.

I

                                                                                                                        +2'i Tento stresa relieved b:r heat:_ng within a rate of'72* . perpr.                                          to ll50*F,-SD*F.,

perlhr. to 600*F.and air cooled. held 50 hrs ,and1'urnace cooled within a rate of 90' equirfmentslofMITeS-45208A. Produced in accordance with inspection syctem r I l l 1 1 I I I l l

                                                                                                                                                                         'f[
                                                                                                                                                             . i,..

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                                                                                                                                                                       ^ '
                                                                                                                                          " . T , '  ' '    ,

We hereby certify the above figures are correct as contained in the records of the company.

 ~
                                                                                                      -                            t   LUKENS STEE' COMPANY                                                        "

D A T E' F(JECHA5f R: - C0ATEi PA. _ Chicago Bridge & Iron Co. . TEST CERTIFICATE 12 James C. Thompson, Pur. Mgr. om onoie no cusiouse c o Same 27474-3 2471-Sheet 1 Boyles, Ala. . 5Ff CIFICATIONS: Same Addendum to Report 12-24-68 Sheet #3 9(NO TEU HOMOGENfifT IE$I ~ C H E MiC A L A ffA L Y S I 5 V is At 8 Cu Ni Ca Mo MELT NO. C Mu P 5 Sa n v

      ~
                                            '                                                                                    PH Y SIC AL PROPERTIES                                                                                                     'i 5 8                                                              % 9 A. SHN OE$CRIPTiON MEti NO.                                                   -
                                                                                                  'k.
                                                                                                   .s       ".N   ,~   2-1              I 24                                             l                Bottom Transverse c4500                                               2                                680             880                                     l Testa l             I l             i I             I I             i I             I 1              I I             I I             I I             I t

I I i I I I I I i 1 l l G a s...s,<.., J ,s. .s _ ,4 _ _ , _ , . m ,s. _ .,,s. < , ,. _ S=elseau

llovise f Copy 12. %-68 LU!CENS #"EL COMPANY COAL (f, PA. D320 DME. 10-22-68 '" 1543'

           *['                                                                                                           C " " "               baI Chicar,o Brldge & Iron Co.                                  TEST CEP.Tl?iCATE 12         J ar..c t, C. Thompson, Pur. M    6 r.   .1, o,ot e .e             cuuoute r o.                                   3""*                            ~

P.O. Box 277 Boyles, Ala. Birmingnau, Ala. 35202 27474-4 2471 Sheet 1 Mt 10468 LR SPECiftCATIONS: Fbx. 80000 31-533-65 .Cr. B Class 1 Mod by C.B. & I. MS-1 Rev. 1 %nt /! 1 nr ? eeno .est OJ. me* = ns 0.K. CHEMICAL ANALYSIS Ca Mo V ', %K m I dasic l'rocest; Mn P 5 Cu 5s Na Meli NO. C 22 1 35 010 014 21 60 56 F.b.P.V.I.P. Stee] Electric Gm 50 Grair Sizt after stret s relieved 8 C4550-2 PHYSICAL P P. O P E R T I E S W ACI5 NaCMe D E 5C RIP TIo N MELT NO. STAB y y 4 EN g ,,,, ggg V-Notch +10 F. Appearancc NO. um na I l 22 I i 1-360 x 145-1/2 x 5-9/16" C4550 2 701 941 64

                                             .945   22                           43 1         35 1           30% Shear 689                                                i           1

' Later al E:qiansiori in ir.ches

                                                                              .068 1.039 1.034                                         -                      .

l l . I l N .D.T. is -i lO'F. ar und er. i i - rocedt re TI C-1 Rdv. 1.1 Tested in a ccorcie nce tc C.B. & I. I 1 I i . Tests locat ion C. B. & 3 . MTP- 1 I I I 1  ! fiomogeneity test: .sati fa ctor y. l Locttion t ransvt rse - top niiddle lof pl te Bend test i atisfc ctory - I Radius of curvature 3 cas tilan 1 1-31/2 int hes. I a 'n-I l _

                                                                                                                                                                 ~

LUKENS STEEL MPANY - m'

  • ruscaA5te; comissvat s. e a. i,22o 04:r. g_n_g g C **G"" ' ,

Chicago Bridge & 1ron Co. TEST CERTIFICATE um o.oie to cosiooe. r o 2 Same Boyles, Ala. 27474-4 2471 Sheet 1 m ECIFICAilONS: Same . HOa*OGENfifY TE5I {hgg $? nf ? 8fND Ifst - C H E MIC AL A N A LY SIS V is At 8 5 Cu 5: Ni Ce Mo . MELI NO. C Mw P c o-2 PH Y SIC A L PROPERTIES

                                                                     % a A. SHN DE5CRIPTION Mf ti NO.           M'                                        ,

l 1

                                                               +

'lates and tests heated 1650'F. -25 *F., held 1 hr. der indh air min. and W.Q. for 22 minutes. ? hen temper ed 1220*F. 210*F., held 1 br. per inch mih. an cooled. cut hot and stress relieved ll 50*F. ,_ ., halld1/2 hr. per i nch min. 'lat a gas l l and D r coo led. +25*F. rate of 72*F. pelr hr. to ll50*F.

                                                                                                                                      -50*F.,

?osto stres s relieved by heating within a a 600 *F. a nd air cooled. rate of 90*gF . per hr. t told 50 hre . and furnace cooled witlhin a I l ion sy stein requigementq of MIL-I-45208A . 'roduced ir accordance with inspect I l - e g l 1 I I l i' l ' Ai$tf I i ' f l

     .    .     .... r .u  u.. r;,,,,,,,      ,,,, ce,,,c, ns enntnined in the records of the company.                   s,,,,,,,,,,,,,,                                       ,

LUKENS STEE6 JMPANY " " " coAYl5VltLE, PA. D AII: 8-27-69 -1 .; c ons cs,e-1 - I Chicago Bridge & Iron Co. TEST CERTIFICATE James C. Thompson,Pur. Mgr. Mitt CIDf R NO CtJ5fouta P O Same - 27474-4 2471 Sheet 1 Boyles, Ala.

                         'f CiflC ATIONS:

ame ooceneirv ns' Addendum _to_ Report 12-24-68

                                                                                                                                                                             ~

Sheet #3 -

                                                                                                                                                                                                                                         ~
                           ~.. eewo ses                                                                                               CHEMICAL C      Mn           P          5        Cu         5     Ni ~ ~A~A    Ce        LMoY S l 5 V   Te        At       8
                          ] ~ MELT NO                                                                                                                                                                                                     .-

Q PHY SIC AL PROPERTIES

                                                                                                                     % ttONG                                  ' "'                                            DE5CRIPTlON vis tD     itNshi                           BHN 3g ,,                                   % R A~

MELI NO. go ,74 ,7a, ,, rp . Bott " 2 673 905 24 Ts liS50 l l l I I I I I I I ~

                                 @                                                                                                                        l l

I i I l l I I I i l i I I I I I I I I I I I i ..

                                                                                                                                                                                                          ,  /7  me    e //7 -

l l _

                                                                                                         ~

f.hf, h L(

                                                                                    .        .      r-         . --.. - , renen;nad in the records of the company.                    ,,,,,,sn. ns,,uo                                     ,

Revised Copy 9-27-68 , r

                                                               -               LUKENS STEEL              )MPANY                                                '"'"-

rueC ASte: ce missutu. Pi. i,32o oa'e= 8-21-68 o 43 , C "5' ""- , TEST CERTIFICATE Chicago Bridge & Iron Co. Mitt ORDtt PO CU5tOMER P O Same y es, Ala. 27475-2 2471 Sheet 2 MB 72568 LR PECIFIC ATIONS: Rev. 1 Fbx. 80000 SA-533-65 Gr. B Class 1 Mod. by C.B. & I. MS-1, 1 erso tes' DK- "o-oc'"* '55' OK- _Sheat # Y nf' '>

  • CHEMICAL ANALYSIS MILT NO C MN P 5 Cu 5s No Ce Mo V Tr 4p & RedQmm
  ;44b                                                  016                  27        60                      56           F.G.F . V.] .P. St eel                 Electric 25       1.40            007 Grain Size after stress relieved 6-6 PH Y SIC AL PROPERTIES [fii C k,Lif g IMP AC15
                      $ lag      YtttD      itNSitt     % ftONG
                                                                   % 2 A.      SHN                                                                    OESCRfPTION Meli NO.        no         ,74         ,g        ,n    2,                     V-Notch -110'F.                Appearanco I            I 956         24                                  I            i                                    1-396 x 145-1/2 x 5-9/16" C4489              1         695 705            970         25                           38 1 45 1                 38 30% Shear i            I Lateral Ex11ansiod in ir ches
                                                                                    .030 1.036 l.034                                                                                     _
        @                                                                                     l            i l            l N.D.T. is 4 10'F.                                                                           l            l to C.B. &I. Pr ocedure TPC -1                     Revl. 1            l Tested in a ccorda nce                                                                      1            l             i I            i rest location C.E .            & I. MTP-1                                                  l            1 I            l lomogeneity test satisfactory                      .

l l Band test e atisfa ctory - Loca tion t ransvo rse - top Ididdle lof ple hes te Radius of curvature l ess tiqen 1- /2 inc .! , l l __ n_ i- . . .t , n . . nm. .. . ,,, ,.,,,,,,, ns enn,nined in the records of the company. - M, .

LUKENS STEEL MPANY _8-21-68 na no 1

                                                                                               ..,32o o*>r:

S 'C"^58 " = co ifsviu .

  • Chicago Bridge & Iron Co. TEST CERTIFICATE
  • Same 12 Jemea C Thompson, Pur.Mgr. uiu otote No cusiouie r o Boyles, Ala. -

27475-2 2471 Sheet 2 iCIFICATIONS: S me Sheet #2 of 2 . SENO !!$7 HOuOGENDN ff$1 - CHEMICAL Ni ANALYSIS Ce Mo V is At 8 C Mu P 5 Cu Se Mf ti NO. ~ ~ 9 - c4489-1 PH Y SIC A L PROPERTIES

                                                                                            '"'^ 5                                oesc,,,,,on uur No.

5j^ * "{ ",g'  ; " "", x. inn ^ l Pinto and testa neated 1650' P,+ 25'F., held I hr. prr g inch min. and W. Q. fo 23 minutes. Plat and tests were per inch yn. th;n tempered 12 20*F,g 10*F. , held I hr.  ; and cir co aled.  ; g P1ksgas cut ho t and stress relieved 1150*F, ffh*F.I, held i 1/2 hr. per inch min. and air cooled. g l I eved by heating within a rate of 72 F.per hr. Tasts st;rens peli cooled, withih a to 1150*F, _+5h* F. , held 50 haurs a nd turna ce rata of 90*F pe r hr. to 600* F. and mir g g requiementh Produced in accoraance with inspection system g g of MIL-I-45208A. l

                                                                                                                                                    'a T '

I I I I

 .       ..s _ ,.. ,, , ,. . _ . ,o,.<,       - -

_ , . ,s. ,.<o,e,o,,s. <o , ,. _ . , , o, ~ . ,pA . ,

                                                                                                                                                      ~

LUKENS STEEL )MPANY PuncnAsta: c ^nsmt r*. An 8-27-69 "" "o l. 3 C "5'o "'E- , Chicago Bridge & Iron Co TEST CERTIFICATE James C. Thorapson, Pur.Mgr. 8A'It ORDER NO <Usf0MitP O Same _ 2471 Sheet 2 Boyles, Ala. 27475-2 'E CiflC Af TON 5: une exentirv us' _ Addandum=ta= Report-9-27-68 Sheet =g3 - _ erno usi CHEMICAL A N ALY SIS C Mw P 5 Cu 5t He Ca Mo V Ti At _ B MELI NO

 ~
                                   '                                  PH Y SIC A L PROPERTIES DESCRIPTION MEti NO.

5 ' ' g

                                                                % R A.      BHN 24                                   I         I                  Bottom Transverse U89                      1           724      945                                         l         l                          Tests i         I I         I l        I e                                                                                 l l

l 1 1 I I I I I 3 I I I I I i l i I  ! I I I I l l n .

                                                                                                                                            ,  sn.

e

    ~
   , , . , _      -...,. ,, ese , ,;ee,es e,e <e,,e<, os coe,e;eea ; ,se ,e<e,as er ihe company.

c1/.'c9h 6%EwC .

Supplementury Copy 14-22-68 9,, 1, "M

                        .                                                 LUKENS STEI              OMPANY                                          ,,,,,'

PueCH ASE R: co,,,,y,t t ,, ,,_ ,,33 DATE: g_pl_gg ,34}

  • Chicago Bridge & Iron Co. TEST CERTIFICATE b uitt oaota to <ustoute e o Boyles, Ala.

27475-2 2471 Sheet 2 MB 72568 LR iPECif tCATIONS: SEND T1,7 HOWENEnft ff 51 CHEMICAL A N A LYSIS Mo V Te At 8 5 Cu 5t Ni Ca MELT NO. C Mw P (i PH Y SIC AL PROPERTIES 8

                                                                %eA        aHN DESCRIPTION utti NO.                      ,       ,

I I I I Drpp r Weight Te sts 1 I l l C4489 1 11est at 0*F. - Fdiled I i I g 21est at +20' F.- Pdssed i I I 2 lest at +50' F.- Pdssed I l i N.D.T. ic +10*N. l 3 I l I I I I I I I I k 0

    -s, sm.,4. ,s   -

s . ,;e...s .,. <.,,.<, ., <. ..; o ;. ,se ,e<.,as er ,se <. .,. a..._....,f***^*""'

R0 viced C-py 9-27-C

                                                                          .                                  LUKENS STEF* ".OMPANY                                                    ""~

PuiCsAdte, . co ,,,,y,,, _,,22o ^ 9-5-68 343 Chicago Bridf,o & Iron Co. TEST CERTIFICATE uitt osot n en custoute e o. 27475-3 2471 Sheet 2 MR 72968 LR Boyles, Ala. 8168 SPtClflC AflONS: SA-533-65 Gr. B Class 1 Mod. by C B & I MS-1 Rev. 1 Fbx. 80000 O.K . ,w,um ins, 0.K. Sheet g 1 of 2

            ,,no ,,s,                                                                                         _        .

M,4 P $ Cu 5s Na Ce Mo V is Et 1 Ra mi r. Pencema MELT HO. C 22 L.45 013 016 24 58 55 P.O.P . V.I .P. St eel Electric 0845 " " " " 23 L.43 009 015 26 57 54 c4521'. Gra Ln si se aft Br str ass relieved 38496-1 7-8 c4521-- 2 7-8 PHY SIC A L PROPERTIES DE5CRIPTION wtt No. 5t ^8 No.

                                                               'T um "E'

om

                                                                                 ' , ~2-' "      x n.A. BHN V-Notch +10'.F.                  Appearanc    e i          I 1          685         944     25                                          1          1                                1-360 x 145-1/2 x 5-9/16" 88496                                                                                                                                    40 30% shear

! 687 940 24 42 l 42 l l ,

'l .Later al.Explpnsionljin in ::hes l
                                                                                                                .035 i.034 l.028 I          I                                       "

j 1-C4521 2 716 945 25 l 717 945 25 42 i 45 i 48 30% Shear [ot1'l7L Latee l Expa,psion %n inc hes

                                                                                                                 .033 l.038 l.032 l         i j

N.D.T. is 4 10 F . rested in a ccorda nce to C.B. 4 1. Procedu re TPC-1 Rlpy . 1l

   'lest locati on C.B .8 1. MTP- 1 l          l llomogeneity test satisf actory .                                                                                          l          l ihnd test e stisfa ctory. - Location transverse
                                                                                                                - top          niddletof p1 ate l

i Rad,ius of curvat.ure less than 1-4/2 inches g ,7f_ [ [,,, We hereby certify the above figures are correct as contained in the records of the company.

                                                                                                                                                          ,,,,,, ,' Q_ .L i 1. v M ~ '- ~

I LUKENS STEEL COMPANY "" ~o ruecnAsEn: ' coArtsviu e ma o^"- 9-5-68 3 Chicago Bridge & Iron Co. TEST CERTertCATE , uitt cede R NO cusrOMER PO

 ' >-                                                                                                                                                       Boyles, Ala .

27475-3 2471-Sheet 2

    'ECIFiCATIONS:

a Some erso nsi ,omr~e.sv ns, t Sheet # 2 of 2 CHEMICAL ANALYSIS , C MN P $ Cu Sa Ni Ca Mo V is At B MELI NO.

  • J B6sd6-1 ,

J c4521-2 , J PH Y SIC A L PROPERTIES J

                                                                          "                                           ^

Meli NO. I  % 2 A. BHN DE5CRIPTION hr. p r incE'. mgn. J lat00 and tests heated 1650*P 125'F. , he ld 1 and W.Q. or 22 minutes. Plates and te sts were the n tern pered 1220* -10*F. held 1 hr. er inch mirt. and air cooled. latas gas out hot,and a tress relieved 115 0*F. held 1/2 h3 . per inch j ing.nd air cooled. +2 ,F. esto straso relieved by heatf.ng wii.hin a rate of 72 4 F. pe hr. 1,o 1150*F. -5 'F., eld 50 hrs , and furnace cooled within a rate of 90*P. per hr. to 600*F. and J ir cooled.  ;  ; Toduced in accordance uith inspect:.on system r equirementslofMIL-I-45208A. , j l l l l I I i 1 l _ We hereby certify the above figures are correct as contained in the records of the company. ,,, ,,, ys,,,

                                                                                                                                                                                             .).'

LUKENS STEEL COMPANY one no PueCHAste; van g_g7_gg

                                                                   ,                                       eoans         e ,.

3

  • C "" ""'
 .2         Chicago Bridge & Iron Co.                                                                   TEST CERTIFICATE                                                               ~

Jamea C. Diampsan, Pur.Mgr. uiu onoie re cusiodi e o. B es, m. ! 27475-3 2471 sheet 2

 #E Cif lC ATIONS:

lame i seNo us eoce~rin us Addendum to_ Report 9-27-68 sheet #3 - CHEMICAL ANALYSIS . Cs Mo V At 8 MELI NO . _C Ms P S Cu Se Ni To L PH Y SIC A L PROPERTIES w Mtli NO. 'N ",e,se" ,. p sea BHN OESCRIPTION NO nia 1 726 945 24 I I f ~ 18496 I I I Bottcus Transverse 2 956 25 I I J' Tests 24521 730 i  ! - 1 I I I V i I - a l I I I I i _ i i i i i I _ l l I I I I s

                                                                                                                !             I
                                                                                                                                                 ,-     .//  ,n    ,; ,,

We hereby certif y the above figures are correct os contained in the records of the company. ,,, ,,,,,, ,,,,[' 'v ' O i af s t

JPPlcant ry ~ Copy l'-22-68 ' LUKENS STEEL COMPANY rittNO part; PURCHA (R. ' CoAf tsvttt t9370 b3 c o"5'

  • TEST CERTIFICATE .

Chicago. Bridge & Iron Co. M8tt ORDie tO cUitUMii o Same 2471 Sheet 2 M 72968 LR Boyles, Ala. 27475-3 8168 SPECiflCAfiONS: T t Shset 4 2 of 2 GENO IE51 HonaOGENEITV IEst - CHEMICAL hNCaALYSIS Mo V Te At 3 M,4 P 5 Cu Ss Ni MELT NO. C

        \ _. .

l i PH Y SIC AL PROPERTIES OE5CRiPTION MELT NO. SI "' No-Yam um ess na -

                                                                                                       % R A.       BHN 1          I        -

1 I Dro p Weiz2t_Toats  ;  ; I I } c4521v 2 1 Test at -30* !r . ;Faileg y ,, I i l 1 Test at -10*F. ;Passepi , I I 1 Test at -10'F. q Faileg I 1 Test-at +10'F. g Passeh 1 Test at 410'F. Failed l 1 I

                                                                                                   .2 Test at 420 F .            q Passefi N.0 .T. i s+10'f.

i l i g I I .4 t'; o

                                                                                                                                                                  , ,,,, ,,,3

(, ./ / /

                                                                                                                                                                                                        / x;?/O We hereby certify the above figuies are correct as contained in the records of the company.
                                                             &Z.=;3 vS li "2_:.7                     / T.6:1L'6Z.J c/WSIOAf                                 go g ( h I-S-2m )

uooa. ,Fo,c. 5 .a<v ..c . ,gg DATE . July 3 3 . _ . _ __.__ 19 b0 MATERIAL TEST REPORT ig, no, ho68-8 Chicago Bridc<1 and Iron Cornany pu,chha s O, der No. Tan: P.O. B6250h-2h71U. contract 68 - e - pu, cruse, 2h71U C. I. Crais Co., Inc. g ,s,, a ,o, s o,oe, no. h9h9 ! oistributor f FCE.CHAH15 ATTACHED HE AT OR F O, ICING , d40 -~ HE AT T RE ATMENT VES NO ITEM PRODUCT SP E.C. CODE NO. NO. CTY,

                                                                                                                          ,2h7P-           675+ 25 F. 1 Er/in Air Cool                              I 2" Dia. Special t'elding Stubs per t             CIEI Spec.         Q2Q1W
  • 2 2 3A,38 560+ 25 F. 1 Er/in Water Quench Dwg. M13, Rev. 2 MS 2, Rev.3 ,
                                                                         .             of 5/8/68                            j             1290+ 250F.1 Hr/in Air Cool Tests stress relieved at:

(ASTM-ASC8-

                                                               ;d'>                    2) MS2, Par .                                      1150+ 25 F. for 50 hours 3.13.1                                                                                ,
                    .v I

CHEMICAL ANALYSIS ANO MECHANICAL PROPERTIES NDT REPORTS ATTACHEO

41. T. M. P. D. P. REMARKS F onGING HEAT MN P S $8 CR NI MO V NO. NO. C 80 .05 Ladle 1 I I 2 Dropw:ights - no
                                                .21     .75      .010      015 .23          .37                  69 2h7P-3A,             Q2Q1W                                                            .81          60        .03       Check                                                  break +500 F.

3B .16 .71 .Co6 013 .2h .36 Ferritic Grcin Si: 9 i (V Notch .: +h00 F, t eMPACT TESTS 8K.ynoa. e VtELO ELONG.% R.A. L AT E R A L E XP. (in ")  % SHE AM HEAT TEST T E NSIL E E NERGY (8s Ibs I FO ING PSE. t000 PS4.t000 in 2-*  % tl H.N. N O. NO. TEMP. 2h7P-3A, Q201W 116-100-112 .081 .07h .odo 90-80-95 o Roo:n Temp 88.65 69.0 22.5 66.5 3B 2h.5 69.5 133-7h-1hl .o85 .065 .c87 95-60-95 180 Room Temp 86.5 69.75

                      - CORP.ECTED TEST REIORT - Please destroy copy dated January 8,1969
                         'Tc hereby cartify the above results are correct and that all require-                                               f[- g g M[7 ments of above reformiced specifications and the purchase order have                                                  
                                                                                                                                                      ..a,,.,. %.4.e=.u. c P ,.,.,,,,,,,,.b,.,.,,,,,,,_,

been fulf111ed." .

94 11:45 usis sae;s e_. crav yzo too: Lennpa Forgo. Inc. l 1280 West Chostar Rd. West Chester. Pa. 19382 i

        ' arch 14. 1989 J Carolina Power & Light Co.

Box 1551 Raleigh, North Carolina 27802 Attn: Mr. Sam Grant

                      \
 .      Gentlemen.

The following information is being provided for your information and is applicable to Lenape Forge. Inc. Heat Codo Q2Q1V . A508-2 material melted by Sharon Steel Co. and received by Lenape Forge Inc. in June of 1988. Ladle Analysis: C Mn P S Si Cr Ni Mo Cu (Wt %) .21 75 .010 .015 .23 .37 .80 .89 Product Analysis .21 .75 .010 .014 .24 .37 .82 .89 .18 (Wt %) Drop Wt. Test Results Reported On Material Forged From Heat Code Q2Q1V. (Testing performed using P-3 specimens per ASTM E 208) Material Heat Treated Condition: s~ Normalized at 1850 F - cooled in air Austenitized at 1580 F - unter quenched Tempered at 1290 F - oooled in air Stress Relieved at 1150 F 30 Hrs. Drop weight test results: -20 F, -10 F, OF : Break 0 F +10 F '+10 F: No Break Please note. test results presented have been obtained by processing (forging and heat treating) starting stock selected from Lenape Forge Heat Code Q2Q1V. The above results are not intended to be used to certify any particular forgings in your possession. For specific forgings of concern, please refer to the applicable MTR (Material Test Report) supplied with forging shipment. Sincerely, 9 0.Tund R. Douglass Trout Plant Metallurgist

   ' w..

Revision 2 NEDO-24157 APPENDIX C Weld CTRs l l l l

              .C                                    i l

[' ALLOY RODS COWANY [- ^! k

  • D; hion or* Chemeleon Co*persoon 4.
                                                                                                                                                    $.             ( ':

r '

                                                                   Certi'icale of Analysis                                                                h..

Customer Order No. 3129..E 2130. bhicago Bridge f: Iron Co. 2700 Channel Ave.

                                                                                                                  . ...._.. Or d u N o .     .55990.._

Memphis, Tenn. P. O. M81808-69 -4824 ,49 62,5128 Shipped 11/7 /69.... _ _ _ . . . This rnaterici conforms to Specincotion S A_316.. _ _ . ._ Test No. AI 396 CX AI 396 CZ Ty p e _E. 8 018 G .. _ This electrode meets the requirements of Par. Trade None: Atom Arc S018NM N 511. 3 of ASME Section III Nuclear Code. Mechanical Tests 0 Diameter Sae: 5/32 Test specimen P. W. ht @ 1100 F, to 1150 r 2,250 Lbs. for 621/2 hrs. Lot Number: J908 A27 A Tensile Properties Heo Number: OSR481 Specimen Type . 505" UTS 90,500 Psi Carbon 04 YLP 80,500 Psi Mo"S c""c .93  % Elongation in 2 inches 28% Chroniv" Reduction of Area 72. 3% Nide! , g7 Impact Prope rtie s 5 *" .37 Specimen Type Charpy Vee Notch c ois re b: . , Test Tenpe rature Plus 10 F. To n'c k' Ft.-lbs. 81, 81, 8 2 Mel b C'"*" Laterial E.:pansion 59,58,63 i .52 */o She a r A rc a 70,70,70 Tungeen Coprc' 02 Othe r Tests Tit a niu m Concentricity 4% Pho:pbe vs 019 Moisture C 1800 F . O .14 % Sv!phu' We certify that the welded mate rial test Pl at 016 vonodium were subjected to the heat treatment as state lion in the attached report dated April 2,1969 of ferrite .

                                                                                        " Heat Treatment Cycle for Nuclear (ASME, Coda. "

This is to certih br.t the cri .ir.nl ceny of this tepert ha: Lcen prcperly sicncd an and nof:rized. SIC'C OI Pcuna. I SS The undersioned certif.es that tY.s report is COV"'T CI York 1 . correct and thet no signif cen' change hcs been rnode in any of the cicreents descr;r,cd Subscribed and sworn to befcre rne in the qual;f. cation opprovat this 14th dY' November W 69 AltOY RODS COMPANY c*,-..o, ce,,......, j / oi.;.:.,.

c. e..y,. .

3

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N995Ff P. bht

                                                                                                                                         ' A- ( ~r             -         -

BY -[- n My cornmissio. e mpires. 5/8/72 Witness ed by R. Stallman, Q. C. Engr. J. Harbold gy-.-s, 1

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APril 2e 1909 -

                                                                                                                                                            ' ALLOY RCOS CO:/?A-T O"-

COPICS: . Yora:. rE:ua.r:::,\:w, FROM: Ucat Treatment Cycic for Nuc1 car (AS JE) Eciler Code SUDJECT: Recorder Speedomai: H Round Chart Recorder Range 0 - 2 5 0 0' F. Prima:j E'ement Platinum - Platinum 10',', P.hodium Thermecoup1 Recorder Chart Speed One cycle - 24 hr Progrr m Duration - Star at . 12 5' F. + 5 0' F.

                                                                                                                      ~

Incrcr.se to 112 5' F. - in 4 hr (250' F/hr)

  • Maintain c.t- 112 5' F. +2 5* F. for C2-1/2 hr 600* F.
                                                                                                                      ~

G 100* F. per hr mn:: Decrease to Air Qacnch

  • Gear en Idotor Shaf t Unmarked Gear on Au::uia:/ Shrit "A" CP.m Cycle Tir.e 150 hv (cach Cam divis'.cn e 2 1/2 hr) ..

Percenr.gc of Time Ternp err.ture Tolerr.nc e Degrecs F. Degrees F. C t. m v

                                                          .       (hr)                                                                                                      3 O                                       125                          +50 375                                                 .           11 1                                                            ,

625 .

                                                                                                                                                                  .       10 2                     .

875

                                                                                                                                           - -                            28 3                     .

1225 '+25 38 4 1125

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alloy RODS COMPANY ( f,

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Certmcole of Analysis Customer Order No. - 3229 Chicago Bridg . Iron Co. 2700 Channel Ave. Order No. _.__56 3 3 5 Memphis, Tenn. P. O. M92204-3262 /3780 lO.l28).b3 Shipped This anoterial conforms to $pecification _SA.316. Test No. AI 380 DX AI 380 DZ Type __E_801.8G This electrode meits the requirements of Par. Trade Nome: Atom Arc 8018NM 'N 511.3 of ASME Section'III ~ ^ ' Nuclear Code. Mechanical Tests # ' Test Specimen P. W. @ 1100 F. to 1150 F. Diometer Size: 3 /16 5,250 Lbs. for 621/2 hrs. ~~ Tensile Properties tot Number: 5925A27A Heat Number: OlR496 Specimen Type . 505" - UTS 92,500 Psi , Carbon YLP 84,000 Psi 05 Manganese Te Elongation in 2 inches 26% 1.11 Chromium Reduetion of Area 71_4Te . NIO 'l .92 Impact Prope rties Smco" 48 Specimen Type Charpy Vee Notch Columbium Test Temperature Plus 10 F. Tantofsm Ft-Lbs 6 2,64,6 8 ' Molybdenum Lateral E epansion 49,48.54

                                           .54                                                                                                             l
                    . Tun g sten ToShear 40,50,50 Coppe'              02                                        Other Tes ts Tita niv rn                                                     - Concentricity 3Tg Phospherws                020                                           Moisture @ 1800 F . O .17 %

5viphv' We certify that the welded material test plates : 017 were subjected to the heat treatment as stated Vanadiw'" l'on in the attached report dated April 2,1969 of _' Ferrite

                                                                                         Heat Treatment Cycle for Nuclear (ASME)

Boiler Code. "

                                                                        .                         This'is to cortify that the original copy
                                     ~                                                             of this report has been properly' signed and notarized,
                                                       $$                                                    The undersigned certines that this report is rk                                                                  correct and that no signifcont change has been mode in any of the elements described
             $vbscribed and sworn to before me                                                               in the qualification opproval, this 19th             day of      November                19 69 ALLOY RODS COMPANY SEAL .                bfD            _g[_ , ,,,,,,,          .k[I                                .

u...y.ew My commisiion e pires, 3faf7z

                                                                                                              ,y     6 //g_,,,/,6 (

[J. Harbold ,

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         ,1                    OR            07. lCD(:ORRESPONDON(. _!
                                                                                                                                                                                                 . bm 
- Qr:5 DATE.* April 2,1969 'l TO*. -
                                                                                                                                                                                ' ALLOY RODS CO,'. IPA COPlES:

YoRd. PENNSYLVAmA : FROM: . Heat Treatrnent Cycle for Nuc1 car (ASME) Boiler Code -

SUBJECT:

Recorder Speedomax H Round Chart

       .                              Recorder Rango                                            0 - 2500' F.                                 l                              .                                              .

Primary Element Platinum - Platinum 107. Rhodium Thermocoup1 Recorder Chart Speed - One cycle - 24 hr ~ ' - Program Duration , Start at . 12 5' F. + 5 0* F. -- - Increase to 112 5' F. . in 4 hr (250' F/hr) . Maintain at 112 5' F. -F,,2 5' F. for 62-1/2 hr . Decrease to 600* F. @ 100* F., per hr =ax Air Quench , Gear on 3.totor Shaft Unmarked Gear on Auxilia:/ Shaft ,

                                                                                                 "A"                                                                                                             ,.

Cam Cycle Time 150 hr (cach Cam. division = 2-1/2 hr) Time Temperature Tolerar.c e ' Percentage of

                                                      . (hr)                                    Degrees F.                       Degrees F.                                                Camv O
  • 125 +50
                                                                                                                                    ~
                                                                                                                                                                        .                        3                       .'  -

I 11 1 . 375 1 .'.. .

                                                          '2                   .
                                                                                              -     625                                           .
                                                                                                                                                                                  ..           19 3                   -                     875 28 4                                     1125             *
                                                                                                                              ' +25"
                                                                                                                                   '~                      '

38 - 66-1/2 1125

                                                                                                                         ,                                                                     38 67-1/2                                  1025 34 68-1/2                                      925                          ...                                         .r -             30 825                                                                                       26 69-1/2                                                     ..
                                 .                       70-1/2                                      725     ,
                                                                                                                                   '~.              ,'    -

22 18

                         .                               71-1/2                                      625                ,        .

72 600 17

                                                                                   ' ' '*From this position on' Cam, subtract 3 /16", o o-
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                                  -                         Certi6cate of Analysis Chicago Bridge 8e Iron                                                Customer Order No.M30402-6 83262180 2700 Channel Ave.

Memphis, Tenn. Order No. _.....5 422L_ Shipped 4 /22 /69... This material conforms to Specincotion .. S A - 316_ . _ ... Test No. 5Z 3Z 5Z 5X Type E8016-G.._ Trade Nome: Atom Arc 8018NM This electrode meets the requirements of Par. N511. 3 of ASME, Section III, Nuclear Code. 0;ometer 5;re: 1/4 28,050 lbs . h. echanical Tests lot Nurnbe" D908A27A i Te st Specimens P. W . H.,T. at 1100 F. to Heat Number: 82D913 1 11500F, for 621/2 hours. Corb " .063 Tensile Properties Mongonese 1.06 Specimen Type: .505" O' Chromium UTS 86,500 N;ckel

                               .80                                                    YLP 78,000 Silicon         ,39                                                    To Elongation in 2 inches-28?o Columbium                                   i To Reduction of Area-72. 57o Tontolum Molybdenum                45                                         Impact Properties Tunguen                                                                   Specimen Type: Charpy Vee Notch Coppe'
                                .03                                                   Test Temperature Plus 10 0 F.

Titanium Foot-lb 80,94, 83, 81, 82 Phosphorus

                                .009 Lateral Expansion 76, 67, 68,63, 60
              $vlphur
                                .018 To Shear 60,60, 50, 50, 50 vanadium                                                            hher Tests Iron                                                                Concent ricity 4To Ferrite                                                                Moisture @ 1800 F 0. 09To We certify that the welded material test plates a

were subjected to the heat treatment as stated ir the attached report dated April 2 of " Heat Treat: Cycle for Nuclear (ASME) Boiler Code. State of I The undersigned certi6es that this report is SS C% d k*)* . correct and that no signi6 cont change hos been inade in ony of the elements described Subscribed and sworn to before me in the quali6colion opproval. this 20th day of May 19 69 ALLOY RODS COMPANY c.,, ... .. .a d . o;.i. ;. a e t cx , . ,.a S E A L q ,,. . . .._*W.. ._*_ . .. .. . , ' . .. . ._....I.... N re,y 7.uc ( A My commission empires: 5/8/72 BY s ...&

                                                                                                                                                     - 4 Witne s sed by R. Stallman. Q. C. Engr.
4. Harbold n-ir

(* ( a' p.n" 1 h TDR-OPPHCU CORRDSPONDENCE

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a TO: DATE: April 2,1960 ALLOY RODS COMPANY COPIES: 1 YORK, pef 1NSYLVANIA l FROM:

SUBJECT:

Heat Treatment Cycle for Nuclear (ASME) Boiler Code Recorder Speedomax H Round Chart Recorder Range 0 - 2 5 00* F. , Primary Element Platinum - Platinum 10% Rhodium Thermocouple ' Recorder Chart Speed One cycle - 24 hr I Program Duration Start at 12 5" F. + 50' F.

                                                                               ~

Increase to' 1125' F. in 4 hr (250' F/hr) Maintain at 112 5' F. + 2 5' F. for 62-1/2 hr Decrease to 600' F. _ @ 100' F. per hr rnax Air Quench Gear on Motor Shaft Unmarked Gear on Auxiliary Shaft "A"~ Cam Cycle Time 150 hr (each Cam division = 2-1/2 hr) Time Temperature Tolerance Percentage of (hr) Degrees F. Degrees F. C,am

  • 0 125 +50
                                                                                        ~
                                                                                                       . 3 1                    375                             . 11 2                    625                                 19 3                     875                                28 4                  1125               ~
                                                                                         +25               38 66-1/2                1125                                  38 67-1/2                1025                                  34 68-1/2                   925                                30 69-1/2                   825                                26            -

7041/2 725 22 71-1/2 625 18 72 600 17

                                                                  *From this position on Cam, subtract 3/16", or 6'l 4
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  • LLOY F,ODS COMPAllY r .- , ( ,

o,.n:.. .e c % o,.. c ,,,r ., ... .. ( Q ,, q, ,. , l s ( Certificole of Anclysis P.O. Chicago Bridge & Iron Custon.er Ouler No, .Mfbl0U -32b$r'3]SU 2700 Channel Ave. Memphis, Tenn. ... __. . _ _. Or d e r N o . .. S k45 . 5 hipped 8./ N.k.9 .- _ . . . - . . . _ This meter lof con forms to Soeciflcotion ._ ..3[.. .316... . . . Test No. AI 304 BX AI 304 BZ Type ..._. R 3013. G . _ . Atom Arc 8018 Nhi This electrode meets the requirements of Par. Trade Nome. N511.3 of ASME Section III Nuclear Code. oiemeier size: 1/8 Mechanical Tests 0 2,500 lbs . Test Specimen P.W. Ht @ 1100 F. to 1150 7. Lot Narnber: F920A27A for 621/2 hrs. Heat Nvenbar: 88 E081 Tensile Properties Specimen Type . 505" Co,Lon .06 UTS 93,200 Psi Mangoncie 1.10 YLP 83,000 Psi C hr omiu ni To Elongation in 2 inches 27% Nic k el ,93  % Reduction of Area 68. 3Tc Silicon .27 Impacts Properties Co h. m bie m Specimen Type Charpy Vee Notch ToMelum Test Temperature Plus 10 F. Ft. -lbs . 85, 90, 91 Mol y b d e n ..o .51 Tunguen Late ral Expansion 72, 67, 69

                                                                            % Shear              70, 80, 80 Ceprce           .02 Tironium Other Tests Pnospherus           .017                                            Concentricity 3%

Sviphur .014 Moisture @ 1800 F. .13 vanodive, We certify that the welded material test plates were subjected to the heat trec.cnent as stated iron in the attached report dated April 2,1969 of rer,ite

                                                                          " Heat Treatment Cycle for Nuclear (AShiE)

M i' io corti!v thd tha c.ri.;,:nal c,..,,,. cf th!: report ha Enn t.re,nrly .igned Boiler Code" tnd ra tirizad. Stoie c! penna

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                                           $$                                                        The undersigned certi6es that this report is CovMy of              York          I                                                                orre e and ther no signir. cont chor.gc H:s been mode in any of the elcraents describred
   $sbscribed end swo n to before me                                                                 in the qualiricofion opproval, th*: 7th            dey of August                          19 69 alloy F,ODS COMPANY

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April 2,1960 DATE. ' ' /.LLOY P.CCS CC..".?/. :. .. - TO- ' COFiES: Yom:. pct..NSny/s.w, FRO'.'; . Heat Treatment Cycle for Nuclear (ASME) Boiler Code SUDJCCT: Speedomax H Round Chart Recorder 0 - 2500* F. Recorder Rango Platinum - Platinum 1072 Rhodium Thermocouple Prin.ary Element Recorder Chart Speed One cycle - 24 hr Pro;p am Duration 12 5' F. + 50? F. Start at ~ in 4 hr (250' F/hr) 112 5' F. Increase to for 02-1/2 hr Maintain at 112 5' F. ~+2 5' F. 600* F. @ 100' F. per hr mnx Decrease to Air Qacnch Umnarked Gear on Motor Shaft Oct.r on Auxilic.:j Shaft "A" Cam Cycle Time 150 hr (cach C:un division u 2-1/2 hr) .. Tolcrtnc e Pere.cntage of Time To:nperaturo Degrecc F. Cc= o (hr) Degrees F. 3 125 +50

                                                                                                          ~

O ' 11 1 375 *- 10 2

                                                                                -    625                                      .           ,
                                                                                                                           -                         2S 3                           875
                                                                                                        ' +25                                        38 4                          1125                              ,
                                                                                                    '                                                 30 66-1/2                        1125                 

34 G7-1/2 1025 . 30 08-1/2 025 . 26 69-1/2 825 . 22 70-1/2 725 , 18 71-1/2 625 - # 17 72 600 ,

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                                                                                                                                 .f' CHEMETR0tl CORPORAT10ll I g,l[b           y m,e.u=,,...~u,c,u.,.m...~

t y Certificate of Analysis

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Chicago Bridge & Iron Customer Order No. __3430 2700 Channel Ave. Memphis, Tenn. Order No.511.44 _, P. O. M12170 3 -0416 - 30 Shipped 2.l.2 7_D.0 _ . _ , , This material conferrns to Specincotion SA..316 Test No. 511 Type E_8018G This electrode meets the requirements of Par Trade Name: Atom Arc 801SNM N511.3 of ASME Section III Nuclear Code. Mechanical Tests o o Diameter Size: 3 /16 Test Specimen P.W ht @ 1100 F. to 1150 F. 2,500 Lbs. for 621/2 hrs . A020A27 A Tensile Prope rties Lot Number: Hoot Number: 05R938 Specimen Type . 505" UTS 94,000 Psi Carbon 077 YLP 76,300 Psi Mongon e se .94 Elongation in 2 inches 26% Chromium Red. of Area 66. 7% Nickel .91 Impacts Properties Silicon 40 Specimen Type Charpy Vee Notch Columbium Test Temperature plus 10 F. Tontotum Ft-lbs. 66,84,86 Molybdenum 57 Lateral Expansion 54,67,66 Tungsten

                                            '                                  % Shear 80,90,90 Copper              02                                  Other Tests Titonium                                                   Concentricity 3%

Phosphorus 018 Moisture @ 1800 F. 0.16% Sulphu' .017 We certify that the welded material test plate - Yonodium we re subjected to th'e he at t reatment cycle as Iron stated in the attached report dated April 2, l' f"rif

  • of " Heat Treatment Cycle for Nuclear (ASME Boile r Code . "g g ,.,g,,.,..g.,,,,,,

of th:s r:;;ct; l,:: '.2 :n prc;;.l) d5r.cd and no!cri:cd. , , . State o' Penna ) The undersigned certines the! lhis report is j 55 Co< s v c r York ) correct and that no signiCcent change has been rnade in any of the efer ents described ' Subscribed and sworn to before rne in the qualiCcorion opproval, this 4th day of Ma r ch 19 70 . CHEMETRON CORPORATION ARC P dQDvC15 L' ASur a TL89 0 Oie >5 04 SEAL A ms. o M . .. ,. 4.e.n e: . - # rar.c i y y co _ i,, o e e.pi,es, New 12,4/72 or <' /d 44M d Harb d

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Csicaco Baloos & IRON COMPANY 1500 N SOTH 5 7. P. O SO x 7 /7, SIR MIN O M A M, A L, A S A M A 35202 TWx 810 733 3654 Western Union.WUX Area Coce: 205 595 1191 CERTIFICATE OF ANALYSIS-PURCHASE ORDER HU:iBER: MECHANICAL TESTS Tes t Number: PT164S Heat Treatment 1125/1150'F-50 Hours Type Electrode: E8018G Trade Name: Alloy Rods E8018NM Tensile Properties Di ame te r: 3/16"9 Type: .505"9 Lot Number: -J802A27A UTS 85,100 Heat Number: 977987 YLP 71,200

                                                                                                % Elongation in       2     i n ch es= 26.0 C__HEMICAL TESTS                                                         % Reduction of Area.-72.4 Carbon.         . . .              0.042                          - Impact Properties Manganese.                   . l iO 4                             Type: Charpy Vee Notch Chromium.                ..        0.03                               Orientation:Perpend. to Weld Direc-Nickel.         . . .             1.04                               Tes t Temperature -Plus 10*F Silicon.           . .            0.47                               Foot- lbs.105, 109, 73 4

Columbium. . ---- 1 Shear 60, 65, 45 Tantalum. .. .-__ Lateral Expansion 82, 84, 59 Molybdenum.. 0.59 Tungsten. .. ___. Copper. . .. 0.03 - Titanium. .. .... Phosphorus.. 0.016

    ~

Sulfur. . . . 0.022 Vanadium. .. ___. Iron. . . _ _ Schae f fler Ferri te. . ---- This material conforms to Section III of the ASME -CODE, , Paragraph N511.3 l l 1 CHICAGO BRIDGE AND !RON COMPANY Bi rmingh am Materi als Laboratory-By . t.- O AA 'l Date 4-/ 7 ~ b V In charge of Tes ting for Materials Evaluati v' " -- y' s r

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                                                               .                  ~ ALLOY , RODS COMPANY Olvis.2 of Chsmeer.e C.ep.e.eie.                                                               ,    ,/f i

Certi6 cote of Analysis - - - -

  ,                                                                                          ,;                            /
                                                                                                                                                                           '     B53011 2471/72W Post Weldin@pply Co.                                          . (,G .* C 6
  • I .i ' 4 .;[Ccy ,,,m.,< o, der No
                                                                                                                                                                                    ~ '~

4 F. U. D o H ill , 52240 1300 Seventh Ave. , North Order No. Birmingham, Alabama - ,. 10 /10 /6 8-

                                                                                                            .                              shipped This material conforms to Specification AWS A 5. 5-64T, ASTM 'A,316-64T Type Trade Nome,                Atom Arc 8018 NM                                                                     ;

oiameter s;2e, 3 /16 3 6 0 0 lbs . ------ - ------------ . Lot Number J802A27A ,C}W1601 ~ Heat Number 977987 F813A27A . Carbon .05 ' . Mongonese . 90 -  ; Chromium *, Nickel .95- l . 40 - j , Silicon Columbium  !' Tontolum , i Molybdenum .52 - . Tungsten Copper ,

      .                    Titanium Phesphorus                  .03                                              i Sulphur               .02                                         ,

Yonodium 01 i . Iron ,j , ferrite l - . 5' ate of Penna. 1

                                                                   $$                                  !                                      The undersigned certifies that this report l'
       .         County of               York                1
                                                                                                       !                                      correct and that no significant change hos -

i been mode in any of the elements described Subscribed and sworn to before me in the qualification opprovol. f thi' 9th doY of December M 68

                                                                                 -                                                             ALLOY R00$ COMPANY j              MI                                       *
                                                                                                                                                  ~ . e                       ~. .. .

SEAL

                                               'Y     ** e 0 L-                                                        .

N ,y e.ma , 4Y <- My commission espires (j 5/8/72 , f

(. W'LV CmcAc0 Baioce' & IRON COMPANY 1500 N. SOTH S T. P. O. Box 277 DIRM!N GH AM, ALADAMA 35202 TWX 610-733 3654 Western Union.WUX Area Coce 205 595-1191 CERTIFICATE OF ANALYSIS PURCHASE ORDER HUM 8ER: MECHANICAL TESTS Tes t Number: PT164N Heat Treatment ll25/ll50*F-50 Hou Type Electrode: E8018G . Trade Name: Alloy Rods E8018NM Tensile Properties 01ameter: 1/8"O Type: .505"O Lot Number: S823A27A UTS 84,100 Heat Number: 654U539 YLP 74,000

                                                            % Elongation in        2    inches =28%

CHEMICAL TESTS *  % Reduction of Area.=75%

                                                                                ~

Carbon. . . 0.041 Impact Properties Manganese. 0.95 Type: Charpy Vee Notch Chromium. . 0.02 Orientation:Perpend, to Weld Direc Nickel. . . 1.09 Tes t Temperature Plus 10*F Silicon. . 0.38 Foot- lbs. 181-144-171 Columbium. ._____  % Shear 100-80-100 Tantalum. .._____ Lateral Expansion 88-89-95 Molybdenum.. 0.58 Tungsten. .. ____ . Copper. . . 0.04 Titanium. .. ____ Phos ph orus . . 0.015 Sulfur. . . 0.020 Vanadium. . 0.020 Iron. . ____ Schae f fler Ferri te. .

       *Per L-248 This material conforms to Section III of the ASME CODE, Paragraph N511.3 CHICAGO BRIDGE AND IRON COMPANY Bi rmingh am Ma terials Labora tory By       4'e . - C  h/M-/          Date 4 69 In i:harge of Tes ting for Materials Evaluati
                                                                                          ,/*i            .'

ll e . * .' o

MY ( ALLOY RODS COMPANY om.ie. t c . ..,.. c.,,.,elie. (' .p Certif,icate of Anolysis

                                                                       .           j, .*         .
                                                                                                                         .s                                                                 ..N Post Welding Supply Co.                           / > ,'            ,

r % f,; Custernu Ordu No. l B53011-2471/72W ,,, , p,~O~ Bos 2111 , u Order No. . 5.ZZAD 1300 Seventh Ave. , North _ _ . B.irmingham, Alabhma 10 /10 /6 8 Sh.ipped This material conforms lo $pecificationAWS

                                                                                                                            ..        A .5.         5 64T, ASTM A 316-64T ,,.'

TYPE Trade Nome, Atom Arc 8018 NM , olometer sizer 1/8 1000 lbs. i- '

  !             LotNumber:                 5823A27A                                  l                                                                               . .                          .

Heat Number: 654W539 j b

                                                  /
   -                   Carbon             .05                                                               .                                              -
                                          .90 f Mongonese
    .                Chromium Nickel           .95 /                                                     -

i silicon .40 / , t

    .               Columbium                            ,

t Tantolum - Molybdenum .52 / 8 Tungsten Copper , Tita nium Phosphorus 01 j , + Sulphur .02 I i Vonodium .01 i s Iron I Ferrite

                $ lote of          Penna.           )                                                                                       The undersigned certi6es that this report in County of           York            )                                   ,l                                           ,       correct and that no significant change hos :
                                                                                                                         '     .        ' been made in any of the elements described :
                                                                                            !                                                la the qualincotion opproval.

Subscribed and sworr. to before me ~ this 9th d'Y 'I December If 68 .

                                                                                                                                           ' ALLOY RODS COMPANY                                                       l
                                  ,3 i
  • ow.i .I ch...w.a ce,p. .ii.a U ' ' - -

SEAL

                              <                    ,s., s ,,,o.                                                            .

nY A f- - 7~,l

                                                                                                                                                                                           ~
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My commlision empires: 5/8/72- / . . .. $. , l

( ghQ/ i' ' ALLOY RODS COMPANY

                                                     .....;.. . c,. .. c.,, m..                                              x Certi6 cote of Analysis                                        /

Customer order Np. M10102. 6.812.61480 l Chicago Bridge 8e Iron ' i 1500 North 50th St. Order No. 54810._. l Birmingham, Ala.

                                                                                    $ hipped       5 /27 /6c)

I This material conforms to Specification __SA-316 Test No. AN239CX AN239CZ Type __E.8.018 G This electrode meets the requirements of Par. Trade Nome: Atom Arc 8018NM N511. 3 of ASME Section III, Nuclear Code. Diameter size: 5/32 2,300 lbs. Mechanical Tests 0 Test specimen P.W,H.T. at 1100 F. to 1150 F lot Numbert E916A27A - Heat Number: 601221 for 621/2 hrs. Tensile Properties

                                         ^

Carbon ,041 Specimen Type, .505" , UTS 89,500 Psi Mongonese 1.05 YLP 79,000 Psi Chromium -

                                                                       % Elongation in 2 inches 27%

Nickel 88 72.7 % silicoa .35  % Reduction of Area Columbium Impact Properties Tor tolum Specimen Type Charpy Vee Notch Test Temperature Plus 10 F. Molybdenum ,49 Ft. Ibs .107,108,108 Tung sten Lateral Expansion 78, 66, 80 Copper ,03

                                                                       % Shear 80, 80, 80 Tiionium Other Tests Phosphorus               .018                                    Concentricity 3%
            $wiphur             015                                                                 12 ~

Vonodium Moisture @ 18009F. I" We certify that the welded material test plates s I'"I' ' subjected to the heat treatment as stated in the attached report dated April 2 of " Heat Treatmen Cycle for Nuclear (ASME) Boiler Code." le f Penna, i The undersigned certifies that this report is 55 County of York I correct and that no significant change has been made in any of the elements described in the qualification approval, Subscribed and sworn to before me this 12th day of Jt.ne 19 69 [e ALLOY RODS COMPANY o,...m. .. c,. . .... c . .. .. p'h' , SEAL k , . , . .~  ; sy / . My commission espires: 5/8/72 , str2 + . . A w. - n Stallman. Q. C. Engr. [ ,

                                                                                                                                     )
                       . . . -    -            -    _.                  - .    -..        ..~_        -_ -.-               .-       . .-.

s- * , s ,. . ,, . ,. il mly

a. . .

gem omca copaspoxnaxca .

                                                                                                                        +,.3 DATE.*

Apru 2,1000 7 70- * . ALLOY RO.75 CC.'/.P/,NY COPIES: YORK PE;;tiSYLVli.'il,*. FROM:

SUBJECT:

Heat Treatment Cycle for Nuc1 car (ASME) Boiler Code Recorder Speedoma:: H Round Chart Recorder Range 0 - 2500* F. Prirc.ary Element Platinum - Platinum 10% Rhodium Thermocouple Recorder Chart Spcod One cycle - 24 hr Pro;; ram Durr. tion Start at 12 5' F. + 50' F. . Increase to 1125* F. in 4 hr (250' F/hr) Maintain at 112 5' F. +25* F. for 62-1/2 hr Decrease to 600* F. @ 100 F. per hr me.:.: Air Quench Gear on Motor Shrft Unmarked Gear on Au :iliary Sheft "A" Cten Cyc1c Time 150 hr (each Cam division = 2-1/2 hr) Time Temperaturo Tolerance . Percentage of (hr) Degrecs F. Degreca F. Cam

  • 0 125 +50 3
                                                                                      ~

1 375 11 2 025 , 19 3 875 - 28 4 1125- +25 38

                                                                                      ~

66-1/2 1125 38 1025 34 67-1/2 925 30 08-1/2 825 26 09-1/2 725 22 70-1/2 , 625 16 71-1/2 72 600 17

                                                                *From this position on Cam, sub: r.ct 3 /16", o:[
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                                -                           CHEMETRON CORPORAfl0N anc prooucts meanuractumac omsrou

[. Certificate of Analysis y 24897 l Chicago Bridge 8e Iron Customer order No. I 2700 Channel Ave. Order No. 61999 Memphis, Tenn. Shipped 12/4/70 This material conforms to Specification _ASME_S A_31,6 Type _E801BG Test No. 875 This electrode meets the requirements of l Atom Arc 8018NM Par N511.3 of ASME Section III Nuclear Code. Trade Nome Mechanical Tests j Test Specimen PW ht @ 1100 F. to 1150 F. Diameter Site: 7/32 l 10, 500 Lb s . for 621/2 hrs. Tensile Properties Lot Number: J020A27A Specimen Type .505" Heat Number: C3L46C UTS 91,000 Psi - YLP 80,400 Psi Carbon 063 Elongation in 2 inches 26% Mongonese .96 Chromium Red. of Area 64.1% Impact Properties Nickel .87 Specimen Type Charpy Vee Notch

                  $ilicon             .32                                       Test Temp plus 10 F.

Columbium Tantotum Ft. Lbs. 35,39,40 Lateral Expansion 34,39, 39 Molybdenum .53 Tungsten

                                                                                 % Shear 60,60,60 Copper                  02                                     Other Tests Concentricity 4%

Titanium Phosphorus 019 , Moisture @ 1800 F. O.15% We certify that the . welded material test plate Sulphur 017 were subjected to the heat tre;atment cycle as Yonodium Iron stated in the attached report da ed April 2, Ferrite 1969 of " Heat Treatment Cycle for Nuclear s (ASME) Botter Code." This is to certify that th: crigi .al ce ' of this report has been pro;orly sigr; and notorized. Penna. ) The undersigned certif:ei that this report is: Store of $$

                                                                                                  ,or,ect and that no significant change hos; County of           York                )

been mode in any of the elementi describec: in the qualiflcolion opproval, Subscribed and sworn to before me thi$ 3rd, d Y of December 19 70

                      /
                                              /
                                                           ////

f' ,J '***n//'J / @-

                                                                                ^

CHEMETRON CORPORATION ARC P400WCis unsur actwo 8G Divis-Q= lc'

           $ eat    J .f w 'aop' 's,
                                  ?-

N d}' .iory Mi.e -

                                                                                                                                   /

3Y # ' 8%-- --- ' My commission expires: 5/8/72 R. R. Bloom

pc-5 Y e enoovers wa,u, evu m a o asi ^] l\-7_ To Carli0 cots of Analysis , 4033 Chicago Bridge & Iron Co. Customer Order No. 2700 Channel Ave. Order No. 61685 Memphis , Tenn. P.O. M72102041630 9/25/70 Shipped This material conforms to Speci6cotion __AS.ME S A 316 J Type .E_8018C, Test No. 800 This electrode meets the requirements of Par. N511. 3 of ASME Section III Nuclear Code. Trade Nome: Atom Arc 8018NM Mechanical Tes.ts o o Test Specimen PW ht @ l100 to 1150 F for Diameter size: 1/8 621/2 Hrs. 2,500 Lbs. Tensile Properties tot Number: H019 A27 A SPecimen Type .505"

            ' Heat Numbers                        432 A 2671                                   UTS 93,000 Psi /

YLP 80,500 Psi Carbon .057 / Elongation in 2 inches 28% M Mongonese 1.22 # Red of Area 72.6% Chromium . Impact Properties Nickel 1.08 / Specimen Type Chgrpy V Notch Silicon 44 - Test Temp plus 10 F.' Columbium Ft . Lb s . 31, 31, 33 . Tontolum Lateral Expansion 30, 32, 30 Molybdenum . 51 /  % Shear 30,30, 30 Tungsten copper .04 / Other Tests Concentricity 4'*g Moisture @ 1800 F 0.18% Titanium - Phosphorus 019 / . We certify that the welded material test plates Sulphur 014 / were subjected to the heat treatment cycle as Vonodium stated in the attached report dated April 2,196; Iron of " Heat Treatment Cycle for Nuclear (ASME) ferrite s Boiler Code . " , This is to cortify that the original copy; of this report has beon properly signeci t and notarized. . . . . i

                                                                                                                                                                     ~

State of ' Penna. 1 The undersigned certi6es that this report is SS York I correct and that no signi6 cont change hos County of been made in any of the elements described in the quali6cotion opproval. Subscribed end sworn to before me - thi' d"Y 'I October 19 70 l- 27th CHEMETRON CORPORATION ARC PMooucT s M ANUF ACTQHineG olyf 5fQN

                                                                                                                                                 ')

M'ge ,- .' g SEAT h w M '.n ..r ,ai,s

                                                           '                                                        sy ,    A,.          [                  M      b l                My commission empires: 73 j4773 G. W. Folcome r III                   g L

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             .                 CHICAGO BRIDGE & IRON COMPANY P. O. DOX 13300           MEMPHIS. TENNESSEE 30113 cot s47 CERTIFICATE OF NJALYSIS Purchase Order Number: M72102041630' MECHANICAL TEST RESULTS
      ' Test Number:           WO #11-D                              Heat Treatment 1100-1150*F for
                                                        .                .                     62 1/2 Hrs
 , Type Electrode: E8018NM                                         Tensile Properties (CTR)

Trade Name: Atem Arc 8018NM Type: .505 Electrode Diameter: 5/32 UTS 91,000 PSI Lot Number: H013A27A YLP 80,000 PSI Heat Number: 662A746  % Elongation in 2 _inche s = 2 6 % Flux Batch Nu-ber:  % Reduction of Area = 70. 5 % CHEMICAL TEST RESULTS ( CTR) Impact Properties - Carbon........ .060 Type: Charpy Vee Notch Manganese..... .96 - Orientation: l,to Weld Direction Test Temperature -20*F Chromium...... Foot - Lbs. 89, 82, 95 Nickel........ .88

                                            .38                       % Shear                   45, 40, 65 Silicon.......

Lateral Expansion 69, 64, 68 Colu-biuta. . . . . Tantalum...... Molybdenum.... .52 Tungsten...... This material conforms to SECTION Copper........ .03 III of the ASME CODE, Paragraph N511.3 l Titanium...... , Phosphorus.... .021 . l Sulfur........ .017 Vanadium...... ' h Ib (g

                 . Iron..........

Schacffler Ferrite..

                                          .                   CHICAGO BRIDGE & IRON COMPANY BY         )          wm               DATE $    -

0! $ /?R 7 fi v' l \

(.H ElliEI R 0 ff (.vit 90 R Ai j U N ~ ' A *' ,-

                                                              *'             AIC 'e80uC.d WAmuf Actu2tNG OtvistoM                                          ,

CertiGeore of Analysis c y ,,,, , , o, der No. 4033 Chicago Bridge & Iron ' 2700 Channel Ave. 61685 Order No. Memphis, Tenn. P. O. M72102041630 9/25/70

                                                                                                                    $ hipped This material conforms to specification                AS M_E S A 316 Test No. 792                                Type _ E_80J8G 1                                                                                                 This electrode :.neets the requirements of Par Atom Arc 8018NM                                 N511.3 of. ASME Section III Nuclear Code.

Trade Name: Mechanical Tests Test Specimen PW ht @ 1100 to 1150 F. for Diometer size: 5/32 621/2 Hrs. 5,000 Lbs. tot Numbert H013A27A Tensile Procerties

      ,                                                                                          Specimen Type . 505" Heat Number:                  662A746                                         UTS 91,000 Psi                                 -

YLP 80,000 Psi Carbo" .060 / B Elongation in 2 inches 26% Mongon'$* .96 / \0@OO Red. of Area 70.5% Chromium Impact Properties Nickel 88

                                                          /                                       Specimen Type Charpy V Notch Silicon               .38                                             Test Temp plus 10 F.                                  ~

Columbium Ft. Lbs 35, 38, 47 Tantorum

                                                   ,32 /                                          Lateral Expansion 35, 31, 43 Molybdenum ToShear 50,50, 50 Tungsten Copper                  ,03     /                                      Other Tests Concentricity 4%

Titanium Phosphorus 021 / Moisture @ 1800 F. 0.16% We certify that the ' welded material test plat : Sulphur 017 / were subjected to the heat treatment cycle a: Vonodium stated in the attached report dated April 2, E fron of " Heat Treatment Cycle for Nuclear (ASM - Ferrite , Boiler Code." This is to certify that the crisinal cop of this report h.ss b:en properly signc) and notarized. . . Sto k of Wea.  ! The undersigned certif;es that this report i;

                ' County of                 York               I                                                       correct and that no signincont ch:nge hc!

been mode in any of the elements descrii:e Subscribed and sworn to before me

                                                                                                              ,, , In the qualification opprovol, this 27th               day of    Oct.                               1970 a

g c CHEMETRON AAc CORPORATION Peo0wcIs pamu,actwainG oivi6 JN .r

                                                                                  - hd             <-

SEAL _ManowYN . .,, /' e.vi. O 7 1

g. 7~~/? ) ' ,/ " -'ffma,'I!/T m;

{ My comm,a,s,on enotres 12/4/77 G. W. Folcome r !!!

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(s ALLOY RODS COMPANY 1 o..w ,. .e cn...u.. c.,,.,..... / /

                                         -                           Certi6 cote of Analysis M30403-68 3J62s SO Chicago Drldga 8.t iron                                           Customer Order No.

2700 Channet Ave. Me rr phi s . T nn. Order No.5447 3. 54.74 Shipped 48 2d/b9 ,, This material conforms to $peciEcotion ..,5[.-316 _ re st No. 5.' 3 4 5 ' 3N Typ. .% 3.0 L1..G. rhis electrode meets the requirements of Par. Trade Name: Atom Arc 3013NM N511.3 of A3MI. Section III. Nuctent Co12. . Diameter Size: 7/32

5. 000 lbs. h'e chante n i Te 4t i o 090?A27A Te st Spacimen i P. '.'. . H. T. at 1130 7. to tot Number:

Heat Number: 95 3766 1150 F. for 621/2 houri. Tonsile Properti o Carbon .063 1,22 Specimen rype: .505" O Mca90aese c,iromium ej r'; 90,000 p3t Nickel 1.03 YLP 32. 500 PJL 9 :tongation in 2 inches 2b'7 Sibcoa .44 Columbium C Heduction of / rea-63.6L Tantolum Molybdenum ,48 I-. 9:.et Proorrtiu ; Tu n g s'e a Jpecimen rype: Charpy Ve Notch rest Temperature Plu .10 F. Coppe- .02 Foot -lbr . 37. 69. 73. 71, 75 Toonium unteral _Npan.sica 52. 70. 56, 54. 57 phosphorus .003 1eihear 60.40, 40, 50, 53

                    $ulphur             .010 vanodium                                                             Other rests l'on                                                     %      Concentricity 4f.

Moi 4ture 1300 F. O. I2fc f er'ik u e certify that the .."aldel material tast plate s were suyectad to the heat treatment a s stated in the attached report datad Aprl! ; of "icat Treatment Cycla for Nuct:ar (/SM :) Boller Cod : State of Penna.

                                                )

The undersigned certi6ei that this report is I correct and that no signincont change has

             ""'t                   York been mode in any of the elements described Subscribed and sworn to before me
                                                                                                         ;n ih, quai;nca,,an app, oval.

l this 20th day of May 19 69 l alloy ROD $ COMPANY , y - o....... .e ca...u. c.,,.,..... l e

         $E AL .._. _

a' _ ,, _ &

                                               ~...,, ,. m                                                              ,

8Y - -, -. b , My commission empires: 5/8/72 /J. Harbotd ,, 7 ', I V itne a e ed by R. Staltman. Q. C. Engr.

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    '                                                                                                                 D
          ' INTER - OFFICE CORRESPONDENCE W.

TO: DATE: April 2,1969 ALLOY RODS COMPANY COPIES: YORK, PENNSYL.VANIA FROM:

SUBJECT:

Heat Treatment Cycle for Nuclear (ASME) Boiler Code i e Recorder Speedomax H Round Chart Recorder Range 0 - 2 500* F. Primary Element Platinum - Platinum 10% Rhodium Thermocouple

 -                           Recorder Chart Speed                 One cycle - 24 hr Program Duration Start at                              12 5' F. + 50' F.
                                                                               ~

Increase to ' 112 5' F. in 4 hr (250' F/hr) Maintain at 112 5' F. +25' F. for 62-1/2 hr Decrease to 600* F. @ 100' F. per hr max Air Quench Gear on Motor Shaft Unmarked Gear on Auxiliary Shaft "A" Cam Cycle Time 150 hr (each Cam division = 2-1/2 hr) Time Temperature Toleranc e Percentage of (hr) Degrees F. Degrees F. C am

  • 0 125 +50
                                                                                      ~

3 1 375 . 11 2 625 19 3 875 28 4 1125 -

                                                                                       +25                   38 66-1/2        1125                                     38 67-1/2        1025                                     34 68-1/2          925                                    30 69-1/2          825                                    26 70-1/2          725                                    22 71-1/2          625                                    18 72              600                                    17
                                                                 *From this position on Cam, subtract 3/16", or 6%!
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UllICt! CtKSIL:5 CC':FO.1ATIoll I. ' P . O . E c.': 550, !!icce.ra Fallc,  !!.Y. CiRTIFICATE OF ACCET'TA'?C$ IliSPTUTIO;! Shipper flo.s 027092 Shipped to: Chicago P. ridge and Iron Company . Quantity Shipp:d: 84,000 lb. 2700 Channel Avenue Date Shipped: 3-24-69 Memphis, Tennessee . Your Ordsr !!o.: A.22S4 9 RSFORT OF TE3T3 0F GRADE 124 UNICI:GLT UELDII:3 COM?OSITION Identificatien cf Material Testeds Grado 124 , Size 20 x 150 _, Lot. s q 7c, _, Run 934 .. . ,. This certifies that the Valding Ccmposition identified above has been-tested fcr conto:ning to spoeifications as fcilows: Sizing: ,20 Mesh Minus 150 Mnh 1.3% 3.5% 2.5% 10.05 SiO2 Ca0 Al 023 Unifor:ity: 21.114 14.50*. 32.07?. 29-38% 18-23'. 11-17'. Lower lina gives spe:.ification limits -  : ingle valu:: at: ::.xi .= . State of !!r.. York County of !!iagara ,,

                                                                                                                       }

f .- , Sworn to before me this

                                                                                                 -  , ( h/ 76 Materials 41ality - Zle .tric Weltng ;

19th y of Decenber _, 9 69 6 n~ef_ . I L. h _.e A -

                                            . . . . .    . . . .    ..    . >., ,,7/                                                     ,

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L. Adcom Metn is Compa ny. I s u:.

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February 4, 1969 m , r a c. w 2., . s. A 1 L. A . T A CCC,.4Ji,. s0ggg, Chicago. Bridge & Iron DATE SHIPPED: 1-17-69 SHIPPED TO:

                                              .            P.O. Box 277 Birmingham, Ala. 35202 867 CUSTOMER ORDER #B52815-2471/72U                                           ADCOM ORDER #

Gentlemen: . , , We horeby certify that material referred to conforms to the phystcal an-f tests as follows and is in accordance with specifications. Consisting ef 60-7Ce coils 14 Material Marked 3/16" 1MMM t I St C r- Mo Va Heat C Mn P S Ni -

                                                                            .010         .012     .07        1.07       .010         .oo S-3986                    16      1.97 Al           Ti          Cu
                                                  .006                      .05
                              ~                                                                                                                          ,r.       '

Y.S. Elon. Pro.St. R c:<.v. el t l'

7. S . ,
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gy p;t': .. Ott*7 3. S'at* JI ' W 2

                                   .w ssen C. p.st 5 .'1') d,19 U.-

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c - ( r , e-C1ncacO Bluoas & IRON COMPANY

  • 1000 N DOTH S T. P. O. DOX 2 TI. O HI M IN G H A M. A L. A U /s M A 3 0 ;t 0 2
  • TWX 010.'133 3054 Western Umon.WUX Area Code: 200 003 1191 J' ICIRT'I F5C AT E O F Atl AL Y S I S- -- - - - - -

PURCllASE ORDER tlu:4 Belt: MECHANICAL TESTS Tes t. Ilumbe r: PT#200-Sinqle Mire lleat Treatmen t!i2-1/2 hours 01125/ll5 : Type Electrode: Adcom Inmm/l.inde 124 Trade Name: Adcom I nmm '.li re Tensile Properties At Room Temperatu: Di ame te r: 3/16"U Type: 0.505"J Lot Number: Run !!934 For I inde 124 UTS 36,500 lle a t Number: S-3986 YLP 71,000

                                                                                          % Elongation in                    2           inches" 30.0p CHEMICf.L TESTS                                                             % Reduction of Area. = 68.6%

Carbon. . .. 0.080 Impact Properties llanganese. 1.42 Type: Charpy Wg flotch Chromium. .. 0.07 Orientation: J. 'leid

                                                                                                                                 .           Di rection Tes t Temperature                      Plus        10*F Nickel.         . ..           0.96
Silicon. . . 0,36 Foot- lbs. 40-S1-49 Columbium.  % Shear 40-40-40 Lateral Expansion 38-44-43 Tantalum. ..

Molyb de n um. . 0.52 Tungsten. .. Copper. . .. 0.05 Titanium. .. Phosphorus.. 0.019 Sulfur. . .. 0.016 Vanadium. ., , Iron. . Schae f fler Ferrite. . This material conforms to Section !!! of the ASME CODE, Paragraph N511.3 CHICAGO BP.lDGE AND 1R0tl CO MP Ally Bi rmingh am Materials Lab oratory Uy ogpt /? h/?/?Y Date f */2.- $ ? i n ch a rg e oTT es ti ng f o r Iia t o ri a fs .E v a l u a .

                                                                                                                                                        */:

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THE EID- AVERY COMPANY f DATE: April 13s 197 ' BAL TIMORE, 00NDAL K, MARYL ANO QUALITY ASSURANCE TEST RgPQR,T,

  • am gjgpgfS.TENE. E SHIPPED: 2/23/71 Chicas;o 3 ridge & Iron Co. SHIPPED TO:

SOLD TO: 2700 Channel Avenue P. O. Box 13308 38113 / Apg } g g7f Memphis, Tennessee P.O N O:- P. O. NO.- lt30502-0416-30 HE AT NO. SPECIFIC ATlON: TYPE LOT NO. POUNOS SIZE ITEM 6M coils ' 3Nooo I' 24,185 3/16 anoo 1=! '~------.... __ 2 3 4

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WELD MET AL / I CHEMICAL NALYSIS OF PRE O p VA CR Ni MO l CU MN I

                                            'P          ~S I
                                                                   /SI ITEM           C
                                                                                                        .48        .02           .005
                                                                  .09          .05         .97
                         .11     1.86       .007     .Cid 2

I 3 4. 5, 6. ADDITIONAL TEST RESULTS V us (<jl

                                                                                                                     %                 /

( l certif y the chemicol anotysis and physical Stote of. or mechonicol test results reported above meet the specifications on the described City M _ day Subscribed ono sworn to before me this moteriot and ore correct os contoinedynj of 19 the records of the company. -,p Narnrv Public

( u (' CHICAGO BRIDGE & 1RON COMPANY l P. O. DOX 13300 MCMPHla. TENNESSEE 30113 f CERTIFICATE OF ANALYSIS oot o4y.33 l Purchase Order Number: M80502-0416-30 MECHANICAL TEST RESULTS M20504-0416-30 , Test Nu.mber: W.O. #14D (Single Wire) Heat Treatment ll50*F +25* -50'F i for 62 1/2 Hours l Type Electrode: RACO IN:'.M/Linde 12 4 . . Tensile Properties (20 x 150) Flux Trade Name: RACO IN!@l , Type: .505"d

                                                       ~

Electrode Diameter: 3/16" UTS 84,500

                                                                                                                          )

Lot Number: --- YLP 72,500 ' Heat Number: 3P4000  % Elongation in 2 inches = 28% Flux Batch Number: ot 2

                                                                        % Reduction of     Area =      69.3%

CHEMICAL TEST RESULTS Impact Properties , I Carbon........ .046 Type: Charpy Vee Notch 1 Manganese..... 1. 3'5 Orientation: l to Weld Direction Chromium...... .04 Test Temperature +10'F Foot - Lbs. 97, 95, 88 Nickel........ .90

                                     .37                                % Shear               80, 80, 70                  l Silicon.......

Lateral Expansion 85, 82, 64 Columbium..... Tantalum...... Molybdenum.... .45 Tungsten...... This material conforms to SECTION Copper........ .

                                      .02                 III of the ASME CODE, Paragraph N511.3 Titanium......

j Phosphorus.... .015 Sulfur......... .012 Vanadium...... Iron.......... Schacffler Ferrite.. p[+\ CHICAGO BRIDGE & IRON COMPANY ar Y. . nnsO DATE d,m&MA7f/ -

                                                                                                                 /

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( T-615-613

                      ;                    (
  • UNIOff CARBIOE CORPORATION

(' l I Llh0E OlVISIOil P.O. Box 66, tilagara Falls, llew York 14302 . CERTIFICATE OF ACCEPTA!1CE INSPECTION Shipper's No.: 066919A

       . Shipped to:       Chicago Bridge and Iron                               & e. n           Quantity Shipped: 75,000 lbs.

d',Date Shipped: 2-17-71 2700 Channel Avenue Memphis, Tennessee 38113

                                                                                    %,[ hip',gg/ '~ D
                                                                                 ' [8                                        N vi Your Order tio.: B-1000                                                                /8/7 N

121 Util0tittELT WEL0lt!G C0ttPOSITI0tt

 -                        REPORT 0F TESTS OF GRADE
                                                                                           , Size 20 x 150 identification of tiaterial Tested - Grade 124 Lot 3932              , Run 989                 _.

This certifies that the Velding Composition identified above has been tested for conforming to specifications as follows: . t 20 itesh Hinus 150 Mesh Sizing: 0% 6.1% 2.5%

                                                                            -                           10%

Unlformity: , SIO Ca0 Al.0, P

                                                                                                                          .s 2-20.21*                             11.01%         0.010%
                                                       ~33,06%_
                                        .               29-38%                       18-23%                             11-17%         0.0254,/

Lower line gives specification limits - single values are maxinun. State of llcw York County of fliagara Sworn to before me this 19th day of Februarv , 19 71 L

  • Op%Sv /*d444fr Consumabics quality'- Electric ..dtcing
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                                                ,               \           ALL'OY RODS COMPANY f*                                                        oi.i.... ., ca...:,.. c.,,.,.....

Certificate of Analysis Chicago Bridge & Iron Co. Customer Order No. .B11.L503 -?411/12 P. O. Bov277 T- r- i Birmingham, Ala* Order No. . Shipped 3 /17 /69 , , , , , , , _ , , . This material conforms to Specincotion - Type E 309 -15 This test material conforms to specification Trade Name: Arcaloy 309 Lime

                                                      .                                                 SA 298 (ASME Section II PartA) and to Diameter site                        3 /16                                                      paragraph N-511,3 ASME Code Section III 4,080 lbs.

Lot Number: 3 A922H5C Heat Number: W73594 e Carbon 05 Mongonese t,79 Chromium 23,51 Nidel 12,79 Silico" .54 Columbium Tontalum Molybdenum Tun g ste n Copp.r Titanium

Phosphorus .020
                    $w!phur                  ,O}}

Yonodium 4 fron ferrite 7 y' This is to certify that the original copy of this report has been properly signed

                                                                                                             - and notatized.

J 5 tate of ' Penna. 1

                                                              $$                                                        The undersigned certi6es that this report is County of                   York               I correct and that no signincont change hos been 'mede in any of the elements described                     ;

Subscribed and sworn to before me in the e.golification approval. ' this 23rd day of June 19 b9 ALLOY RODS COMPANY q / oi,i ;.. .# ch...v.. c.,e...n..

           $ tat                 l$.W Yk Ad                              8.             f?.
                                                         ...ry r se My commission empires:                       5/8/72 8Y ^          -
                                                                                                                                                    --    4-               - - -

Witne s sed by, R. Stallman, Q. C. Engr. Ha rbold 7[ (

G. .. . (, . (.

                                                  ; CmCAGO Brunas & IRON COMPANY
                                                     ,p.o. sox 13 a o s , MEupMis. TENNESSEE Ss113 CERTIFICATE OF ANALYSIS                                                                                            .

set on.ov i Puychasa Order Number: B111503-

                        ~ ~ ~ ~ ~ ~ ~ "

MECHANICAL TEST RESULTS 24.71/72 ,

              'T#9t Numbgr; M281C                                                            . ,

Heat Treatment . Type Elc9tF949: E309-15 (S A-29 8) i' Tensile Properties TF549 Na597 Alloy Rods Co. . - yyp ] 5199tF94g Diameter: 3/16" -

                                                                                                                               ,,            -gg                                                    .

L9% Nymbgy; 3A922H5C g , Etat Numbgy; W73594, l'

                                                                                                                                     .. . 4 Elongation in                                               inches =

Flu patsii uttmber: c,. , t Reduction of Area - CffEH!eAL TEST RESULTS Impact Properties Cgybgn,,,,,,,. Type: Charpy Vee Notch

                      ,Manygnesg,,,..                                                                             ,';    -

Orientation: ,,to Weld Direction g)1rgPLium,,,,'.. ,.

                                                                                                                               '                Teat Temperature Wighgl , , , , , , , . -

Foot - Lbs. SilI999,eerr.. 4 Shear , gelumbium,,,.. , Lateral Expansion Ta!)talum , , , , . . '". Molybdenne,.. - . E9D99t9 Drier.. ' This material conforms to SECTION C9PP9Fe erer..

                                                                                                      '"jII of the ASME CODE, Paragraph N511.3 Titgnium,,,...                                                                        ,                                                               ,             ,   ,

PhosPh9Fus,... . ', fulfur.,,,,... . Vanadigm,,,... , IF9Beeeeeere.. . , Schaefflor rerrite.. CHICAGO BRIDGE.& IRON COM N cobalt.ttt,....

                                                               .090                             ,

1 BY I, . tC.- DATE May 14, 1070 f'

=!
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                                        .i CHEMt1RON CORPORAil0W                                                                            ,
                                                                                                                         .e      e .. m.a.. .. e .                                                                       l Certhoto of Analysis               -

Chicago Drtdge 8: tron Ced+a.e orde, He. 24897 2700 Channel Ave. Memphis. Tenu _ %g 61999 s'

                                                                                                                                            +

6Mpped 12/4/70

                                                                                                                                                                                                        ~ ~

TW meievlet eeafeems to speciAcetion SMC SA 298 Par N511.3 Section III

                                                                                        .            Test No. RQ-6474                      yyp, _ EJ081s.15 These electroiles conform to ASME specification Trede Neme'                             . --Arcaloy 308ELC Lime                                                                                                       ]

SA 298, type E308L 15 and were tested in j

                                          , th.ee., stiei                                        3/16                                     accordance with the requirements of Par                                        1 4,000 Lbs.                               N511.3 of ASME Section 111 Nuclear Code, los H beri                                K019H2C m.it w i                                          X47214                                   We ce rtify that this material is in ' compliance
                                                                                                                                        ~with Appendix IX Section !!!. ASME Code.

Cerb.a 03 (1968 Edition) mape a.ee 1.69 Che adv. t9,15 *

                                               .                       . . Nickel               9.26                                                                                                                 = l siscoa                 72 Colvmbiv.                                                                                                              *                              ' l Temok=

h!,bdeawee . Teagsten i

                                         .. _. . . C* P P                                                                                                                                                              l Thea3wn Phosp herv'                       .02                                                                                                                    l SwlPhw'                 02 Yeao d.wm

, treni  ! Thli is to < artify that the original copy fc'he 6% 'l thl8 'eP*rt hn beeri property sisned Cobat t .19 and rioteria.d. -

                                     -- ---Sicie o f                                 Penna.                  I    g g            ,,      g,             , g,        , ;,

Covaty of York I c ,,eci end e i a, e af.c o a t osa he been made in oar of the ele **als desuibed 3.,becri%ed ead e een to before me in the q,etWee'on oppre,st, this 3rd, der et De ce mbe r M 70 ,

                                                                                                                            '                               CHtM                 R                              .

me ese.rIRO.N..C..O.c

                                                                                                                                                                     .<is          v ; e is. POR AT.. ION..

ital P 7' G t. m My comminica e s p ,e 5/8/72 R. R. Bloom

                                                                                                               . . . . .                     . .       s..                     ~.

4

Revision 2 NEDO-24157 APPENDIX D Weld Logs

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l Revision 2 NEDO-24157 APPENDIX F Surveillance Test Specimen Plan t

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U C'.Cid f' f l0 '4 _ 4 SURVEILLAt1CE TEST SPECIMEN PREPARATION PLAN TilIS PLAN APPLIES TO THE THREE (3) REACTORS FOR Ct.ROLIN A POW COMPANY, CONTRACT NUMBERS 68-2471/72/73. V9h

  • s 1.O G CN r.PJ,L INSTRUCTIONS 1.1 All final cutting shall be done by machining.

eru of utmost importance. 1.2 Specimen marking and mark orientation In c,Tse of a mistake , or if uncertain about the marking on a blank, DO NOT use it for a finished specimon. 1.3 Material must be us'cd cautiously since there is no replacement material. 0 C 1.4 Material to be heat treated at 1150 F plus'25 F or minus 50 F ( for a total of 50 hours, lu.ss any heat treating time aftcr tempe ri ng . 2.0 SllIP".LWT INSTRUCTIONS 2.1 Arrange each group of like specimens in serial order so they will remain in serial order during shipment. 2.2 Adequately crate or box spucimens for protection during shipme CU$T 01.'.E R AP PH 0V AL Approved September 4, 1969 by Eugene O'Connor. Received from G.E. ER #S939 dated 9-8-69, VPF #2478-291-1 e er k 0* no se o are ai r o o, o f pigt j r. f aon m.u no og r cn e r 6 o i.o.<p n og oc .o

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___films-of -the welded secms in the surveillance test plates and 4 contes of all mecc11urgical data and docu:r.ents 2.3 (Certified Test Reports) including Oravingu T-5 through T-13, nendcstructive test of plate, heat t r e c.tmen t re co r c. s a r,<.i 1.ox as the test s pe c :.me ns . M reports chall be packed in the 2. E.u r> hove rc.ctall,trgical data and N Two renroducib]c prints of documents shall be submi t te: . by mai l v/i _hin five days of the ship"1.cnt. The coverin .- letter chall include the date / of .h i pree n t , the route and 011 ship:,.r.g documents. 3.0 ll A F !: :!r.TAL MA" !qI AL 3.1 The basu natal shall be taMn filom Tc.s t Plate marked (2607), which shall be cut. f r,om shcil Plate nrmrknd (301), as .<hown on Drawing T-5. P i r. t c (J01) is.a , lute opposite the Active Puel Z on c. in the Core Regi<'n. . 3.2 Te r, t P la tc- (2007), Drawing T-5, sh<til be given a stress relief in aceutdance with paragrapl. 1.4 to cioulate the of strcss rel:.cf ( of the Core Regior. Plate., ( 3 01 a nd 3 '.21 ) . X-rays the weld must be sent to the cus tc:r.e r (sce p7ragraph 2.3). 4.0 117. rs ' . !'CTAI,

                                 .                TEST PLATE Sl'IPPCD TO GF"EPAL El.I:CTMIC 4.1               Stencil bi:sc metai Tes t Pla te tsarked (2630) cut from shc11                             -

Plate mathed (301) as follcus: (Use symbols at least 1/4" high) G.E. DASE NLTAL M3LL ROL?.I?:C DTEECTION lli.AT NU.:DElt Si,AD NUMHrit CONTRACT NU.1 DER Documento shall he upplied to General P.lectric showing the source, chtmintry and all heat treatment of the plate. 4.2 The abovo Test Plate marked (2610) shall be shipped to

          ,-                                General C]ectric.

1 s

SURVC'LLANCE TEST f*'* C ]

           '                                                                                                   enec ~ ": p o r n A n m o ::

i _ _m - ev. u ,, _ y tt,t. m L i?L tci Pic C o n A:.y _ _ , _ _ , ,

                                                                                                             ""#AUW           STP-3
                     , , _ ,JQ.1 J,I N G._lUd!' R !!!' C T. r!. . B.ELC'l.Q3___                              a ^o a No. 3    -or  15      i r.. A oc                                               . .                                  __

oArt 7-21-69 l A w. u ou _ , _ J'

                                                       ~                             ~~     ~ ~
                                    ~~

nevisiou ,,o. l n ne e r io" _. l l 3 .[ l 5.0 DASU MCT/.L TEST PI ATC USED DY Cl!ICACO BRIDGC r. IRON TO t'!.EE DA:;( .LWAL MCC!: A.:IC AL 'fi".S A' SfE'I52"?), Plate (2607) cut from shcIl Plato (301) shall be used T-7 to make 4A Mechanical Test Specimens required by Drawings T-6, and k T-8. 6.0 L! ACC ?'.r:TliL Cl?/inPY CPECI'1 ENS 6.1 Specimen Requirements G'.l.1 Prepare the Charpy II.' pact Specime.ns in accordance with Drawings Y-6 and T-7. - 6.1.2 The specimens shall Le taken from 1/4 thickness pocitien in the ple".c. The long axis of the specimen sheill be t A ;..U . L ' n t.h pi u . rolling directicn.

                                            'I he n::cc!          '-  re'-              -
                                                                                          ;' C )

p>f nd i <:ula r to the original .Le i . w. - .- W: -  :- be creat mll ed by ( , t l.c ac i t.u ; . t i o'. o. t h. - . 0 .c 't i ngs on the spectr en blinik s . 6.2 Specim.cn Prcparation , 6.2.1 Power bar.d sou t'io (2) 2 1/2" x 5 5/8" x 12" sub-blocks and stencil them U:'.C-A and tim',2 B as indicated on Drawing T-6. 6.2.2 Finish machinc entire sido to be marked and stencil cach speciton blank location as shown on Drawin3 ~'-7 g beforo dividing the sub-blocks into slabs and s p curen 1 blanks. The top of the markin1 symbols are perpendicular to the original plate surface; thereforc. the top of the three digits will indicate the notched side of the upociman as shown in Detail D. 6.2.3 Power band saw the Dt:C-A sub-block into ninctcen (19) 1/2" x 2 1/2" x 5 5/8" slabs, as indicated by Detail A-6.2.4 Power hand saw the P:C-B sub bicch into 1/2" x 2 1/2" x 5 5/8" slabs, as indicated by Detail D. The remainder of this sub-block shall be stored. 4-

           -        . . _     _   -      . . - . -       . ~.-              --      .                      - --

T~ l Svavnzux:ct rze: ry8

    '/
                                             -(

S PEC D'C:: ?P ?TsRAT:n! ,.

                 ,]       {                                                                                        -

[* ~ 7 PLA'l Sj 'Oi' STP-3 omw ,,_rgi;g t l'LrcTnic cO:'n.wy pact No. 4 cr 15 o...,o uc t ,, ,82I Lit.'G b'ATCR t'UC L E/s!! PCACTOS 7-21-69 oATc a s s c u uv< _ Atvisio N wo, 1 O C5C hip T IO N .__

 .(

6.2.5 Machine both 5 5/0" x 2 1/2" .00r$yrfaces of each slab to a thickness of 0.400" +0 - 6.2.6 Power band saw the 2 1/2" x 0.400" x 5 5/8" slabs into specimen blanks as shown in Detail C. ' 6.2.7 1achine both 2 1/2" x 0.400" nyrfaces of cach specir.en to a thickness of 0.400" + OL'S -0

                                                                                  ,    as indicated in Detail D.

6.2.8 Place O fty-threc ( 5,3 ) specimen blanks (2k'l t11rouah 2MJ.for 68-2471; 361,,through 3XJ,, for 68-2472 ; SL6 through StiT and JAl thrcuch Jr.Y for 68-2473) in separate serially marked cnvelopes and preparc them in accordance with the following paragraphs t 6.2.8.1 through 6.2.8.7. ( 6.2.8.1 Machinc and finish grind the 2 1/2" x 0.400" surfaces to a 'thickness of .394", as i'ndicated *

  • in Detail E. Place cach blank .in its serially marked individual envelopo for further processing.

6.2.8.2 Mark with pen, an arrow on the notch side of the specimen blanh (indicating the proper mark orientation). Soc Detail E. 6.2.8.3 Finish unmarked end of each specimen in accordanco with Detail F, and return speci.en to its' envelope. 6.2.8.4 Romark the designated marked end of cach finished specimen with its corresponding envelopo serial number if its original mark is destroyed. Start with the lowest marked cnvelope and proceed serially. 6.2.8.5 Finish the specimen in accordance with Detail F 4  %,, [

SURVCILLA:'CE TEST P l (n! . J S P PC I".f:M P RE P A T'.'m o:( [/ \ y, q w p I. 3.t.! a wr - ,. m .i t

                                                                                                                                                 '";fN$N'                  STP-3
       \,          . cw '-         . , D i '.11.1L.;C'EELC .CC D A !

r, ec tr ,n n r _.c p,,, s'Act wo. 5 or15

rwoouci . _i
oIf r r 1;f.+ __

o AT c 7-21-09 mow ,_ ,J,'~ - oce,ctm ner4 _,, nevmos No. 1

                                                                                  -                . - , .                 -m              -               -

u...2...s----,-- o 6.2.8.6 1001 dimensionally inspect, cican and dip cuch specimen in " Dip. Scal Plastic" DS 300 Clear, or equal. NN G.2.8.7 Packaue fi f ty-three (53) specimens in

         '                                                                          accordio. o with chip'nont instructions, Paragraph 2.0 cf thia plan. The specimens l

shall bc. nent to iencral Cicctric's Plant ' i at San . lone, Ca1ifornia. 6.2.9 Extra specimens are to be placed in serially marked envelopeu and ret .ined by CinI for possibic dimensional ro]ects. In tiw casos where catra specimens arc not provided, dimonaicnal rejec a: will be discarded and , 3 their mark numbc.rs vill Lc u.;cd on replacement specimen = taken irm the c : r co .maturial . Caro must a be tahr.r. 90 ir.:cr proper rp.,cimen orientation and I source. 7.0 A *, - ._ .M -"._T. M. . ., ..T

5_1.E_ .. _F...t , ". _'s..

7.1 Spc.;/im .n Kr..;itiru d.s , i 7.1.1 Prepare the tenuiju cpccimens in accordance wit'1 ' Drawingc T-6 and T-8. 7.1.2 The specitnans shall be tak.cn f rom 1/4 thickness f

positionn in the plate. Thu long axes of the specimens shall bu parallel 1.o the plate rolling direct.t.on.

7.2 Specimen Preparation 7.2.1 Power band sau onn (1) 3 1/2" x 5 5/8" x 12" sub-block and stencil it imT as indicat.ed on Drawing T-6. 7.2.2 Stencil cach spoein'en blank location as shown on Drawing T-8 before dividiner the sub-block into slabs

s. and specimen blanks.

7.2.3 Power hand sau the 3 1/2" x 5 5/8" x 12" sub-bloc). into ton (10) 5/C" x 3 1/2" x 5 5/8" slabs, as i indicated by Detail A. i l i.

                                      .      - . .             .      .--.w--.~           - .:-._..-.--                                             .-        . . - . .    --.        ,-

l'~'/ 7 T,.7 '( l SURVCIL'P.h'CC TEs7 S P EC I".CM P PIP APM; .3 f, [ , PL 76' b,_d

                                                                         '"k"2 ANN '    FTP-3
                ,_   _G E : M & I L E C 2'f M C*TAMY b .Iica sucr         qqI. LING wit t_EJ NUCLEAR _FE/.CTOR              pact No.

o A r t __,, 6 or 15 7-21-69 as wouv oncmrtios acvistos No. 1 k 7.2.4 Power band saw the ten (10) 5/8" x 3 1/2" x 5 5/8" slabs into specimen blanks, as shown in Detail B. 7.2.5 Place fourteen (14) specimen blanks ( 33 l through 3'3'X p fp,r 60-2471; SJ1 through SJK for 68-2472; 625 through

    \

62T for 68-2473) in separate serially marked envelopes and preparc then in accordance with the following paragraphs 7.2.5.1 throu;h 7.2.5.4. 7.2.5.1 Finish each specimen in accordance with Detail D, Drawing T-8 and return it to its envelopc. . 7.2.5.2 ncmark one end of cach finished specimen with its corrcoponding onvolope serial nu.ber if its original mark is destroyed. Start with the lo,; cst marked envelope and proceed serially. k 7.2.5.3 100% dimensionally inspect, clean and dip each specimen in " Dip Seal Plastic"'CS 300 Clear, or equal. 7.2.5.4 Package fourteen (14) specimens in accordance with shipment instructions, Paragraph 2.0 of this plan. The spccinens shall be sent ' to General Electric's Plant at San Jose, California. 7.2.6 Extra specimens arc to be placcd in serially marked envelopes and retained by CBLI for possibic dimensional ( rejects. In the cases where extra specimens are no:

                                    ' furnished, dimensional rejects will be discarded and their mark nunbors will be used on replacement specimens taken f rom the extra inatcrial provided.

Care must be taken to insuro proper specimen

        ,                            orientation and sourec.

l r

        /.

[ l

                      ^                                                                                                          t              SURVEILLlJ:CE Tz37

((D yl l

                          'l j                                                                                                             ,, sPnCImm no rr Apf Ie :

( - ptAN

        .- _ _ . _ d v"t o       , ___ .C L;: Elm n rc" 7 c c~ ipr n'                                                                          '" f#d7 '          FTP-3 s? t t(* f ta p,  p  AC';O p,                                                       P AGE NO.        7     cr     15 P R 0 0 U '., f    _,   SQT!.T*!C W Af'n g AT E           7-21-69 S S $ E v ut. f                        .          ..

O C $ C ni f' f '0 4 ngvision so,1

       - .r         .

0.0 WELD & !! EAT AFFECTED ZONE MATERIAL 8.1 The wcld and heat affected zone metal shall be taken from Plate marked (2608), cut from shc11 Plate marked (301), b with a contral wold which longitudinal weld. is cimilar to the reactor vessel (Sce Drawing T-5) . 8.2 Test Plato (2608), Drawing T-5, shall be given a stress relief in accordance with Parngrat li 1.4 to simulate the stress relief of the Core Region Plates (301 and 351). X-rays of the wcld must be sent to the customer (See ,

                                                                                      -                                                                                    l Paragraph 2.3).

l 9.0 WCLDUD ".' CST PLATE Sl:IPPED TO GENCRAL ELECTRIC  ! 9.1 Stencil welded Test Plato marked (Use symbols (2609) eut from 1/4" at least shellhigh)Plate marked (301) as follows: G .E. HELD METAL MILL ROLLI!!G DIRI:CTION 1 HEAT NU:1BP.R  ! SLAB NUMBER l CO" TRACT MUMBER Documents shall be supplied to General Electric showing the source, chemistry and heat treatment of the plate. 9.2 The above wolded test Plate marked (2609) shall be shipped to Gonoral Electric in accordance with Paragraph 2.0. 10.0 WCLD):D TEST PLAT!: U3ED DY CllICACO BRIDGE & IROM TO mal:E WELD AND llUAT AFFECTCO ZONU ".CCl!/ 5ICAL TEST Sl';;C lMl:ND 10.1 Plate (2600) cut from shcll Plate (301) shall be used to make the Mechanical Test Specimens required by Drawings T-9 through T-13. 10.2 Test Plate (2608) shall be cut into four (4) control blocks (Stencil all excess material as indicated on Drawing T-9. (_ and control blocks as indicated) N

                '-                  '; i                                                                                                                   ./ SURVC?LLANCC TEST i'
                     /
                                        .l                                                                                                                           FPCCTMEM i)REFAPAT'OM

[ f p t, Aa; - w __ --o

                                                                                                                                                                  "" Wif "              STP-3
g. cuen Gjg;Jg AL 1;LECTRIC COMPANY o^oc No. 8 _o r 15 nnonuct _,

BOILING WATER NUCLEAR RCACTOR 7-21-69

                                                             -                                                                                                    ontc assc u ni. y         ,

acvisioN No. 1 ocscaiatioN J ] 11.0 WELD METAL CHARPY SPECIMENS (WC) 11.1 Specimen Requirements - 11.1.1 Prepare the Charpy Impact Specimens in accordance with Drawings T-9 and T-10. 11.1.2 The long axis of the npccimen shall be perpendicular to the wcld direction and parallel to the plate surface, with the middle of the specimen at the mid-plane of the weld as shown in Drawing T-10. The notch shall be perpendicular to the plate surface. 11.2 Specimen Preparatio'n 11.2.1 Powcr band saw the central weld section 5 1/2" x 5 S/8" x 2 1/?.", marked WC, with the weld center plane at the center of the ucld block indica.:d in Dntail B, Drnwiny T-9, 11.2.2 Finish machinc ent ito sjda Lo 1c marked and stencil each specit.a blank lecction us shown on Drawing T-10 before dividing Lho central wcld section.into slabs and specimen blanks. The top of the marking sy:-bols are on a linc perpendicular to the plate surface: thereforc, the top of the three digits will indicate the notched side of the specimen as shown in Detail D, i Drawing T-10. T!!IS IS VCRY IMMRTANT. 1 11.2.3 Power band saw the 5 1/2" x 5 5/8" x 2 1/2" wcldx ) ' control block (WC) into ninc (9) 1/2" x 5 5/8" 2 1/2" slabs. 11.2.4 Machine both 5 5/8" x 2 1/2" surfaces of(Drawing each slab T-10, to get a thichness of 0.400" go05". Detail B). 11.2.5 Power band saw the nino (9) 5 5/8" x 0.400" x 2 1/2" slabs into specimen blanks. j 11.2.6 Machine both 2 1/2" x 0.400" .9urfaces of cach ' specimen to a thickncas of 0.400" +0.005", as indicated in. Detail C, Drawing T-10 l f l

I SUPNCILLANCE TES';' 7 , ~ ~]

                               '                                                                                                                                                     SPECI"C': P P P P ts: 'Tn :

t 6- = a . PLA:' i o w. n gigren rf ar mic co 2 :t' ".?dt,-l ' ST?-3 ( nosuct F.U L 1MG _ luc t' Nuc! ?2f ? " "o') a AGE No. 9 or '5 assr u ou - oATE 7-21-69 ossempTeos atvision No.1

          - _ - - - -                                                   ; --- ~

J 11.2.7 Place fifty-throc ( 5,3 ) specimen (2P'l through 2UJ f o r 6 0 - 2 4,7,1 ; 3 /,1* through 3', D6 blanks for 68-2472; SMU through SUD for 68-2473) in separate serially marked envolopes and prepare them in accordance with the following Paragraphs 11.2.7.1 through 11.2.7,0. 11.2.7.1 Machino and finish grind the 2 1/2" x 0.40C" surfaces to a thic}.noss of .394", as indicatcc' in Detail D, Drawing T-10. Place cach blank in its serially marked individual.anvelora for further processing. l'l.2.7.2 rinish grind the unmarked end as indicated I in Detail D, Drawing T-10. f 11.2.7.3 Mark with pen, an arrow on the notched side of the specimen blanV, per Octail D, Drawing ) ( T-10. Remark the derignated end of each blank with its corresponding envelope I number if its original mark is desercyed. Use the arrow to orient the mark number properly. 11.2.7.4 rinish the specimen in accordance with Detail E, Drawing T-10. , 11,2.7,5 100% dimnnnionally inspect, clean and dip , the specimens in " Dip Seal Plastic" DS 300 l Clear, or equal, for p otection against runt and mechanical damage. Package fifty-thrco (53) specimens ir. f 11.2.7.6 accordance with shipment instructions, Paragraph 2.0 of thbi plan. The speci.eas . shall be cent to General Clactric at San Jose, California. l l *

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