ML20072F286

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Info on Reactor Vessel Matl Surveillance Program Brunswick Steam Electric Plant Unit 1
ML20072F286
Person / Time
Site: Brunswick  Duke Energy icon.png
Issue date: 06/30/1994
From: Contreras G, Ranganath S
GENERAL ELECTRIC CO.
To:
Shared Package
ML20072F244 List:
References
NEDO-24161, NEDO-24161-R01, NEDO-24161-R1, NUDOCS 9408230275
Download: ML20072F286 (113)


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      &                                                      GE Nuclear Energy Technical Services Business General Electric Company,175 Curtner Avenue, San Jose, CA 95125 NEDO-24161 Revision i ClassI June 1994 INFORMATION ON REACTOR VESSEL MATERIAL SURVEILLANCE PROGRAM BRUNSWICK STEAM ELECTRIC PLANT UNIT 1 Prepared for Carolina Power and Light Company Prepared by:           M       b Jdue G. W. Contreras, Senior Engineer RPV Integrity Approved by:       /         G       <dc i

S. Ranganath, Manager Structural Mechanics 9408230275 940817 PDR ADOCK 05000324 P PDR l

Revision i NEDO-2416I IMPORTANT NOTICE REGARDING CONTENTS OF Tills REPORT i i PLEASE READ CAREFULLY ] i This report was prepared by the General Electric Company (GE) solely for the use of Carolina Power and Light Company. The information contained in this report is believed by GE to be an accurate and true representation of the facts known, obtained or provided to GE at the time t report was prepared. The only undertakings of the General Electric Company (GE) respecting information in this document are contained in the contract between Carolina Power and Light and GE, as identified  ; in the purchase order for this report and nothing contained in this document shall be construed as changing the contract. The use of this information by anyone other than Carolina Power and Light or for any purpose other than that for which it is intended, is not authorized; and with respect to any unauthorized use, GE makes no representation or warranty, and assumes no liability as to the completeness, accuracy, or usefulness of the information contained in this document. 1 i F

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Revision 1 NEDO-24161 CONTENTS Pagg

1.0 INTRODUCTION

1 2.0 RPV SUPPLIER AND SPECIFICATIONS 1 3.0 VESSEL BELTLINE MATERIAL 2 3.1 Plate end Weld Locations 2 3.2 Plates / Forgings and Welds 2 3.3 Heat Treatment 6 3.4 Chemical Analyses 7 3.5 Tensile Properties (Unirradiated) 9 3.6 Fracture Toughness Properties (Unitradiated) 10 4.0 VESSEL MATERIAL SURVEILLANCE PROGRAM 11 4.1 Plate Material 11 4.2 Welds 11 4.3 Documentation 11 5.0 IEFERENCES 12 APPENDICES A. As-built Fabrications Drawings A1 B. Plate and Forgings CTRs B-1 C. Weld CTRs C-1 D. Weld Logs D-1 E. Thermal History Logs E-1 F. Surveillance Test Specimen Plan F-1 1

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Revision 1 NEDO 24161

1.0 INTRODUCTION

The original version of this report was issued in 1978. That report was furnished in response to a request for information concerning the reactor vessel material surveillance program (Reference 1). This revision contains several changes to report prescatation and content. In order to make this report more complete, the bases information from which this summary was derived is contained in the appendices. In addition, for ease of use, the information has been reformatted to a more tabular format. And lastly, fluence, EFPY, and RTndt shift estimates were deleted. Since this information changes with time, it is more appropriate that this information be contained within reports specific to withdrawn surveillance capsules. 2.0 RPV SUPPLIER AND SPECIFICATIONS The Brunswick 1 RPV was purchased from Chicago Bridge and Iron Company, Birmingham, Alabama (GE Purchase Order No. 205-H1332, CB&l Contract No. 68-2471). The RPV is designed and constmeted in accordance with the following codes and specifications:

a. ASME Boiler and Pressure Vessel Code - Section III,1965 Edition and Addenda through Summer 1967 Addenda.
b. " Standard Requirements for Reactor Pressure Vessel", General Electric APED Specification No. 21 A1100, Rev. O with Data Sheet 21 Al100AR, Rev.12.
                                             -l.

Revision 1 NEDO-24161 3.0 VESSEL BELTLINE MATERIAL 31 PLATE AND WELD LOCATIONS Materials in the RPV beltline region (as defined in 10CFR50, Appendix G, Section 11) are identified below and are as shown in Figure 1. 3.2 PLATES / FORGINGS AND WELDS

a. All shell plate material'is SA-533-65 Gr. B., Class I; CB&l Specification MS-1, Rev.1; and provided by Lukens Steel Company, Coatesville, Pennsylvania.
b. Nozzles N16A and N168 material is A-508, Class II; CB&l Specification MS-2; and provided by Lenape Forge Division - Bonney Forge and Foundry Inc., West Chester, Pennsylvania.
c. Weld Materihls and Process:

Coated Electrodes Flux Electrode Combinations Electrode: Filler Metal Type E8018G/NM Adcom INMM/Linde 124 Trade Name: Alloy Rods E8018NM Adcom INMM Supplier: Alloy Rods Co., Adcom Metals Co., Inc. Division of Chematron Corp., Atlanta, Georgia York, Pennsylvania Weld Process: Shielded Metal Arc Submerged Arc 3.2.1 Lower Shell Course (Assembly Piece No.1200. Ring No.1) (1) Plates (2) . 201 and 251 Piece No. Heat No. Slab No. 201 C4535 2 251 C4550 1 ) i l CB&l ASSE MBLY DR AWING Pc NO. NO. 1600 63 FINAL VESSEL ASSEMBLY 1200 12 SHELL PLATE ASSEMBLY NO.1 HALF RING - Pc Mk NO 200 PLATE PART NO. 201 - EXCLUDING NOZZLES AND NOZZLE WELDS 1200 13 SHELL PLATE ASSEMBLY NO.1 HALF RING - Pc Mk NO 250 PLATE PART NO. 251 - EXCLUDING NOZZLES AND NOZZLE WELDS 1300 14 SHELL PLATE ASSEMBLY NO. 2 RING  % PLATE PART NOS. 301 AND 351 43 N16A/B NOZZLE ASSEMBLY - ASSEMBLY PART NO. 302 TO NO.2 SHELL 6 SE AM DETAILS SEAMS F AND G - SHELL VERTICAL SEAMS SEAM FG - SHELL GIRTH SE AM 7 SEAM BC FOR N16 NOZZLES VERTICAL SEAM F2 F1

  • H 300 - M 2 RING) -1990 AZIMUTH 160 3460 ^
                                                                                  ^                        ^

ELEV eseSTRuneENTATION

                                                                       -------                    - - - - - - - -                         3846n.                  - NOZZLE NIS
                                                                                                                      -                  362SSin.                 - TAF
  • PLATE PLATE E NO. E SEAM FG
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                                                                                         -                      -                        208 SS&n.                - SAF*

PLATE PLATE NO. 251 NO. 201 a AZIMUTH 750 2560 750 VERTICAL Gl G2 (1200 - NO.1 RING) VESSE L 0 s SEAM NUMBERS ARE CSSI PART AND DRAWING NUMBERS UNLESS OTHERWISE DEFINED Li

  • REACTOR ASSEMSLY ORAWING GE 197R602 ELEVATIONS ARE FROM VESSEL T Figure 1. Brunswick RPV Beltline Region Welds and Plates

Revision 1 - NEDO-24161 (2) Vertical Seam Welds (G1 and G2) (a) Coated Electrodes - Type E8018G/NM Reference Specification - SA-316 Traveler Heat No. Lot No. CB&l Weld Spec. Card Set Secuence 649T273 1726A27A WPS 323-IF6, Rev. I 1200 3B & 3C (root pass) 601221 E916A27A WPS 203 2F4, Rev. 0 1200-Tl C-1 (weld femp. lugs) 601221 E916A27A WPS 323-2F4F6, Rev. I 1200 2A (G1 and G2 fit up) 88E081 F920A27A GRP-1 Rev. I 1200 R13 6 (repair to GI) (b) Flux Electrode Combinations - Adcom/INMM-Type Linde 124 Heat No. Lot No Run No. CB&I Weld Soec. Traveler Card Set S.eauence S3986 3876 934 WPS 323-lF6, Rev I 1200 3F & 3G WPS 323-2F4F6, Rev. 2 3P & 3Q 3.2.2 Lower Interinediate Shell Course ( Assembly Piece No.1300. Ring 2) (1) Plates - 301 and 351 Piece No. Heat No Slab No. 301 C4487 1 351 B8496 1 (2) Vertical Weld Seams (F1 and F2) (a) Coated Electrodes - Filler Metal Type E8018G/NM Reference Specification - S A-316 Traveler IdeatN2 tot No

                        -                       C_B&l Weld Soec.                 Card Set Seauence 977987       J802A27A        WPS 323-1F6                      1300        7 (1st layer of root pass) 649T273 1726A27A             WPS 323-IF6                      1300        7 (1st layer of root pass)

(b) Flux Electrode Combinations - Adcom/INMM - Type Linde 124 I.raveler Heat No. Lot No. Run No. CB&l Weld Spec. Card Set Seauence i S3986 3876 934 WPS 323-lF6 1300 9J,101, 9K,10K

Revision 1 NEDO-24161 (3) Ring Repairs - Assembly Piece No.1300, Ring No. 2 Coated Electrodes - Filler Metal Type E8018G/NM Heat No. Lot No. Traveler Card Set Secuence 08T401 F821A27A 1300-R3 6-ABCD GRP-1 977987 J802A27A 1300-R2 6-A, B GRP-1 654W539 5823A27A 1300-RI 4C , (4) Girth Weld Seam - FG - Assembly Piece No.1600 (a) Coated Electrodes - Filler Metal Type E8018G/NM Lot No, CB&I Weld Soec. Traveler Card Set Seauence Heat No. 662A746 H013 A27A WPS 323-2F4F6,Rev.4 1600 3A-421A6811 H010A27A WPS 323-2F4F6,Rev.4 1600 3A GRP-1, Rev. I 1600R-54 6A 411A3531 H004A27A WPS 323-2F4F6,Rev.4 1600 3A GRP-1, Rev. I 1600R-54 6A 401Z9711 A022A27A WPS 323-2F4F6,Rev.4 1600 3A GRP-1, Rev. I 1600R-54,55,56 6A (b) Flux Electrode Combination - Adcom INMM - Type 124 Heat No Lot No. Run No. CB&l Weld Spec _ Traveler Card Set Seauence IP4218 3929 989 WPS 323-2F4F6, Rev. 4 1600 3A 3.2.3 Nozzles N16A and N16B - Nozzle (Assembly Piece No 302) to Shell (Assembly Piece No.1300. Rine No 2) Forgings (1) Forgings Nozzle Piece No. Heat No. Forcine No N16A 302 Q20iVW 247P-4A N16B 302 Q2QlVW 247P-4B (2) Nozzle to Vessel Weld Seam (a) Coated Electrodes - Type E8018G/NM Heat No Lot Nom C B & l W eld S oec Traveler Card set 'Seauence 1802A27A WPS 303-1F4 1300 285,F,N,O 977987 WPS 303-lF4 1300 28E,F,N,O l 649T273 1726A27A 650X006 J807A27A WPS 303 1F4 1300 28E F,N,O i l [

Revision 1 NEDO-24161 (b) Overlay Seam Weld Type: Type E309-15 E308L-15 Trade Name: Arcaloy 309 Lime Arcaloy 308 ELC Lime Supplier: Alloy Rods Company Alloy Rods Company Iyg Heat No. Lot No. CB&I Weld Spec. Traveler Card Set Sequence E309-15 W73594 3A922H5C WPS 103-lF5 1300 32A and 32B E308L-15 65298L 2A923H2C WPS 103-lF5 1300 32A and 32B 3.3 HEAT TREATMENT 3.3.1 Plates and Test Specimens All plates and test specimens were heated 1650 F 25 F, held I hr/in. minimum and water quenched for approximately 23 minutes. They were then tempered 1220 F!!0 F, held I hr/in minimum and air cooled. Plates were gas cut hot, stress relieved at i 150 F(+25/-50 F), held for 30 min /in. minimum and air cooled. Test specimens were stress relieved by heating within a rate of 72 F/hr to 1150 F(+25/-50 F), held for 50 hours, fumace cooled within a rate of 90 F/hr to 600 F and air cooled. CB&I reported the following heat treatment for the plates: 201 251 301 351 O&T 1650 F 5 hr 35 min 5 hr 35 min 5 hr 35 min 5 hr 40 min 1220 F 5 hr 35 min 5 hr 35 min 5 hr 35 min 6 hr 40 min Total Accumulative Stress Relief Time 1150 F 36 hr 48 min 39 hr 18 min 34 hr 16 min 31 hr 23 min The nozzle heat treatments were: 1675 F125 F, I hr/in, air cooled 1560 F 25 F, I hr/in, water quench 1290 F 25 F, I hr/in, air cooled Tests stress relieved at i150 F 25 F for 50 hours. P' Revision 1 NTDO-24161 3.3.2 Post-Weld Heat Treatment Location Temperature Duration Lower Shell Course 1100 F to 1175 F 25 hr 33 min Vertical Weld Seams Gl and G2 Lower Intermediate Shell Course 1100 F to 1175 F 27 hr 23 min Vertical Weld Seams F1 and F2 Girth Seam Weld FG 1100 F to 1175 F 6 hr 15 min N16A/B Nozzle to Vessel Seams 1100 F to 1175 F 15 hr 30 min 3.4 CHEMICAL ANALYSES At the time of construction for these pressure vessels, the only requirements for chemical composition were those contained in the ASTM material specifications (A533 Grade B for plate; and A233, A298, A316 or A371 for weld electrodes and rods). The elements reported in these specifications did not include copper (Cu). The available chemistry certifications are provided, but values for the copper contents of these materials are not directly available from these certifications. By tracing the heat numbers for the beltline plates and nozzle N16A/B forgings back to the suppliers (Lukens Steel and Lenape Forge, respectively), the copper contents for the plates and forgings were obtained. The ladle analysis for % Cu was measured and retained by the suppliers even though it was not required by the purchase specification. The copper content of the welds was provided by the supplier, though not required, except in the case of nozzle to vessel weld. Items marked N/R were not reported. l

Revision 1 NEDO 2416I (a) The chemical analyses for vessellaeltline plate / forging material are as follows: Descriotion Plate Heat C Mn P S Cy Si N_i Mg Lower Shell 201 C4535-2 0.23 1.28 0.012 0.015 0 12 0.24 0.58 0.54 251 C4550-1 0.22 1.35 0.010 0.014 0.11 0.21 0.60 0.56

                                                                                          ~

Lower Inter. Shell 301 C4487-1 0.23 1.50 0.010 0.015 0.12 0.27 0.56 0.57 351 88496-1 0.22 1.45 0.013 0.016 0.19 0.24 0.58 0.55 Nozzles N16A/B N16A/B Q2QiVW 0.21 0.75 0.010 0.015 0.16* 0.23 0.80 0.69 ladie 0.219 0.63 0.006 0.025 N/R 0.24 0.84 0.72 check

  • from product analysis.

(b) The chemical analyses for the vessel beltline welds are as follows: e 31 I_e. lig.a.1 a Lot No. C Mn P S Cy Si N_i Mo Coated Electrodes - Type E8018G PT164X 649T273 1726A27A 0.048 1.12 0.017 0.023 0.02 0.52 1.00 0.59 AN239CX/Z 601221 E916A27A 0.041 1.05 0.018 0.015 0.03 0.35 0.88 0.49 A1304BX/Z 88E081 F920A27A 0.06 1.10 0.017 0.014 0.02 0.27 0.93 0.51 PT164S 977987 J802A27A 0.042 1.04 0.016 0.022 0.03 0.47 1.04 0.59 PT146B 08T401 F821A27A 0.047 0.93 0.016 0.025 0.02 0.38 0.90 0.52 PT164N 654W539 S823A27A 0.041 0.95 0.015 0.020 0.04 0.38 1.09 0.58 WO No. Il-D 662A746 H013 A27 A 0.060 0.96 0.021 0.017 0.03 0.38 0.88 0.52 771 421 A6811 H010A27A 0.057 1.16 0.020 0.016 0.03 0.50 0.89 0.46 770 411 A3531 H004A27A 0.066 1.13 0.018 0.017 0.02 0.51 0.96 0.47 519 401Z9711 A022A27A 0.057 1.I5 0.021 0.017 0.02 0.39 0.83 0.48 PT164W 650X006 3807A27A 0.052 0.95 0.020 0.023 0.03 0.40 0.96 0.56 Flux Electrode Combinations - Adcom/INMM Type Linde 124 PT200 S3986 3876 0.080 1.42 0.019 0.016 0.05 0.36 0.96 0.52 569C IP4218 3929 0.085 1.43 0.010 0.015 0.06 0.39 0.87 0.45 Nozzle to Vessel Overlay Seam - Type E309-15 W73594 3 A922H5C 0.05 1.79 0.020 0.011 N/R 0.54 12.79 N/R Nozzle to Vessel Overlay Seam - Type E308L-15 ) RQ4997 65298L 2A923H2C 0.04 1.83 0 020 0.02 N/R 0.72 9.71 N/R 1 l l 1 4 Revision 1 NEDO-24161 3.5 TENSILE PROPERTIES (UNIRRADI ATED) Yield Ultimate Elongation Ejlates Heat No. Slab No. Strength. ksi Strenuth. ksi (% in 2 inchg.s) Lower Shell Course C4535 2 68.1/67.7 92.1/91.6 24.0/23.0 C4550 1 66.9/66.8 91.5/91.I 24.0/26.0 Lower Inter. Shell Course C4487 1 64.6/65.1 89.0/89.1 24.0/26.0 B84% 1 68.5/68.7 94.4/94.0 25.0/24.0 Nozzles N16A/B, Q2QlVW (0 ) 78.0 97.25 21.0 Forgings 247P-4 A,4B (180 ) 73.0 94.5 20.0 Yield Ultimate Elongation Welds Heat No. Lot No. Strenuth. ksi Strength. ksi (% in 2 inches) Type E8018G/NM 649T273 1726A27A 73.5 88.3 25.5-601221 E916A27A 79.0 89.5 27.0 88E081 F920A27A 83.0 93.2 27.0.. 977987 J802A27A 71.2 85.1 26.0 08T401 F821A27A 68.1 80.6 29.5 654W539 S823A27A 74.0 84.1 28.0 662A746 H013 A27A 80.0 91.0 26.0 421A6811 H010A27A 72.0 84.0 27.0 411 A3531 H004A27A 71.5 84.5 29,0 40IZ9711 A022A27A 76.0 91.5 28.0 650X006 J807A27A 66.0 80.0 28.0 Adcom/lNMM - Linde 124 S3986 3876 71.8 86.5 30.0 1P4218 3929 78.5 92.5 27.0 E309-15 W73594 3A922H5C N/R N/R N/R E308L-15 65298L 2A923H2C N/R N/R N/R 9

Revision 1 NEDO-24161 3.6 FRACTURE TOUGHNESS PROPERTIES (UNIRRADIATED) The Brunswick I reactor pressure vessel was ordered prior to the issuance of Appendix G, 10CFR Part 50. The ferritic pressure boundary material was qualified by drop weight testing for the shell plate and CVN testing for the weld material. Test results are shown in the following tables. Heat / Drop Weight Charpy Beltline Plates /Forginas Plates Slah NDTT Test Values Test Temperature Lower Shell Course 201 C4535-2 +10 F or less 45,38,46 ft-lbs 40 F No.1200 251 C4550-1 +10 F orless 50,41,47 fl-lbs 10 F Lower Inter. Shell 301 C4487-1 +10 F 41,26,46 R-lbs 10 F Course No.1300 351 B8496-1 +10 F 42,42,40 ft-lbs 10 F Nozzles N16A/B 0 Q2QlVW +40 F 38,39,41 ft-lbs 40 F 180 Q2QlVW +40 F 31,25,44 fl-lbs 40 F Charpy Beltline Weld.s lie _;11 Lot No. Test Values Test Temp _erature Type E801SG/NM 977987 J802A27A 105,109,73 + 10F 662A746 H013A27A 89,82,95 -20 F 401Z9711 A022A27A 98,99,104 +10 F 411A3531 H004A27A 60,60,68 +10 F 421A6811 H010A27A 88,92,93 +10 F 08T401 F821A27A 117, 116.5, 115.5 +10 F , 654W539 S823A27A 181,144,171 +10 F 650X006 3807A27A 89,93,97 +10 F 649T273 1726A27A 81, 67, 81.5 +10 F 601221 E916A27A 107,108,108 +10 F 88E081 F920A27A 85,90,91 +10 F Flux Electrode, Adcom/lNhBI S3986 3876 46,51,49 +10 F 1P4218 3929 94,91,90 +10 F E309-15 W73594 3A922H5C N/R N/R 1 E308L-15 65298L 2A923H2C N/R N/R l l i i

l l Revision 1 NEDO-24161 l I 4.0 VESSEL MATERIAL SURVEILLANCE PROGRAM 4.1 PLATE MATERIAL The plate material used in the surveillance program (Assembly 2613) was cut from piece 301, Heat C4487, Slab 1. The post-weld heat treatment of the plate specimen was at 1150 F (+25/- 50 F) for a total of 50 hours. All information pertaining to the surveillance plate materialis contained in Section 3. 4.2 WELDS The weld material used in the surveillance program was fabricated using Adcom Heat No. S3986 (INMM) Linde No.124 Flux Run 934. The plate materialjoined by this weld was from piece 301, Heat C4487, Slab 1. CB&I performed the welding in accordance with the weld procedure in WPS-323-1-F6. The post-weld heat treatment of the welded piece was at 1150 F(+25/-50 F) for a total of 50 hours. All information pertaining to the surveillance weld material is contained in Section 3. 4.3 DOCUMENTATION A copy of the surveillance program drawings, and the surveillance test specimen preparation procedure No. STP-3 are attached to this report. Revision 1 NEDO-24161

5.0 REFERENCES

l 1

1. Letter to Carolina Power & Light Company from A. Schwencer, USNRC, May 23,1977.

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1 Revision 1 NEDO 24161 l APPENDLX B Plate and Forgings CTRs en l l

                      - B                                                 1 l

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                                                                                                                                                            ' ~ " " " "
  • MI* g.k.68 '"
  • 1543 "

< * * ~ " COAtilvetit

                                                                                                                                          * * * ' ',PA,99320                                                                                            W
                               ~
  • PURCHAs(se
  • Chicago Bridge & Iron ~ Co.

TEST CE".~lFICATE

                                                                                                                                                                                                                         - 'SEl* s    d?               \

autt osois se. cu m e'"- Same ~ 12 '. James C Thompson, .Pur.Mgr. ' Boyles, Ala. P.O. Box 277 27474-4 2471-Sheet 1 Mn 72368 Sa , e a rmingham, Ala. 35202 O N SP(CifDCAlloNs. SA-533-65 Gr.B Class 1 Mod. by C.B. a I. Ms-1, nev. 1, Fbx. 80000 - i' . O.K..- O. K. ..- - Sheet #1 of 2 3r. o oce,*.se wie see in

                                                                                                          - -                CHE MIC AL ANc. ALYSIS                                 y      a     4.          .                nruiu Emo.

i c., s. u. u. u e 5 . unr uo. c - F.G P. &V I.P.S cel L Electrio 24 58 54 23 1.28 012 015 - . C4535 ' f' , .  :

                                                      # t.-                                                                                                                                                                                                 -  +

v1 .. ias e rliev id 7 -8 f m

                                   "                                                                    .                             Gr ain si te aft er str                                                                                 .
                               ,'                                                                                            PHYSIC AL PROPERTIES                                   __ _ i '. u n aas  = sta=a amicaos Appearance                     3esCearieou una                  *                   "'A
  • V-Notch +40*P. -
                                              *' "0-                         *eo.     '.a *
                                                                                         "       .     ,,, 2 .

l l-

                                                                                                                                                                                                                                                         ~
                                                                                                                                                ~             "

1-360 x 145-1/2 x 5-9/16" 2 681 921 24 g i 46 30fehear

                                         ~c4535                                                  916      23                               45        l33            l 677                                                                                             ~                               '

Lateral expar.s Lon inlinche i 038 g.038 g.034 [ M.D.T. $s +20 'F. or 115XE5ffY?Y3 under. ,

  • g 151E. -

l I)14)IMEIRILtITEEIIIX111 I I  ;

                                                                                                                    ?ro$ed are T ?C-1                Fev. 1l
                                     - Tested in accord ince to C.B. &

I.

                                                                                                                                        .   .          l.             l l                                                                                                               -

[ l Test locatLon C. 3. Es I . NTP 't i *- l I ' l l . Homogene1t r test, satis Eactdr r _ l

                        ~

l y transv yree - top middle lof plite , Bend test satisf actory - In cation curva ture lens than 1-jt/2 inehes Radtus of - l 1 l l i

  • I I e e j
  . _ _ _ _ _ _ - _ ___                          ~~ ~- ~ - - - - - - _

a a. one. 9-4 68 '" ~ 15813 I counou.,i. C***'** rueCHA$(9. . l' Chicago Bridge #s Iron Co.

                                               ~                                           TEST CERTIFICATE cuuomia e o.

Y

             .                                                          me oeces en                                                            Same                                  '-

J i 12,Jamde C Thompeon, Pur.Mgr. Boyles, Ala. 27474-4. 2471-Sheet 1

                                                                                                                                                                           '=.

snCW.CAIOe$. . Sheet #2 of 2

      -          same                       ou    no t

CHE MICu.AL ANALY5t$

                 .. o i.u                                                                                                                n.        e c,           ua   v s.

s q. s. c m e ma no ,

        . c4535-2        .

w

  .      i-                                                                   -

PHY SIC AL PROPERTIES '"' " pescatrreon u a A. n unt ho. Sj *E[

                                                  ",{        [ ",

l l

                                                                    +                       I hr. 'pe r heate i 1650'F-2 5* F. , 1 eld 3 teet s werelg Plates     and   tes te inch min. and W. 2. fog 23 mi lukee.

Plat sa an

                                                             , held 1 br. per Lnch mLn.

l g then tempe red 12 ?O*F,- 10* F. g J l and air co<>1ed. - 45 t l stree s reli eved I l50*F,-50* F), helg1 - Platee cae cut h>tmin. and and ' g al F cool id. g F. , 1/2. t!r. pc r inch Ling wt tt.in a rat eofof90 7 h*F. pyr f hr. to 1150* F , [ 5O Testa etre se rel Leved ay hea F. pe:r hr. to

                               ?. and furna
e coo 8ed wi thin a rate m 3 .

held 50 hr air ce;oled.

                                                                  -                                    g             g
  • 600*F. and  ; 1 inspeo tion a retem requi rement s of MIL-I-45208 L. -

Produced i 1 acco rdance with I I l l a' w - t l ,, I I L4 We hereby cert.fr the atme figuies are correct as contoined in the secords of the company.

                                                                                                                                                                                                                                               -----------..a<s...

ruscumsta. - ^'"""' 8-27 69

                                                                                                                                                                                                                                                                                                           '"5"*'-

543

  • Chicago Bridge & Iron Co. TEST CERTiflCATE Same 12 James C. Thompson, Pur. Hgr. === oeos = .<>. couo e ,o Boyles, Ala.

27474-4 2471-sheet 1

                                            . sncascarms.                                                                                                                                                                                                                        -

Same Addendum to Report 12-24-68 Sheet # 3

                                                                        ,,,,,3,           m.,,,,,,,

CH E MICm AL ANALYSIS c. u. i y v. a. s c a e i s cg s. wu no i i w 4 k PHY SIC AL PROPERTIES '" oe sceirison , , wu wo. "g "f "E ', 'y'. =si - I i l Botton Transverse 873 26 I Tests ! c4535 2 638 l l i i I . 1 I I i ' l I I I

                                                                             .                                                                                                                                                                            I             I                                                                                                                                      ,

I I i I - i i  ! I l ! v I I I I

                                                                                                                                                                                                                                    ~

l l < I I I I I I . 9

                                                                                                                                                                                                                                                                                                                                ~
                                                                                                                                                                                                                                                                                                                                  ~
  • AZ we hereby cers.ly the obove f%wes are correct as contained in the records of the company.

ruecpAsrt. Luimu :,icut t.uavwANT cou n u u.,* m a ea'<< 9-13-68..

                                                                                                                                                                                                                                    -1543-         (g)

TEST CERTIFICATE

                                                                                                                                                                                            ' ""'""'/..                                                .

Chicago Br,idge /d Iron Co. ans oeoes no. cuuoi ta e o. same. .M e SEP *'. 31968 James C. Thompsdn, Pur. Ngr. 22 Boyl*#' P.O. Box 277 27474-4 2471 Shoot 1 hR 83168 LR - . Birmingham, Ala. 35202

  • SetCifeCAltoN5.

Rev. 1 c1 1 Mod. by CB &I. MS-3, f5x. $0000 ' B ' . SA-533-65 0.K '.Gr.' o.ocewa mi O.K. Sheet # 1 of 2 d nuoint i CHE MIC AL A N A L Y SIS Pa c i e Pr n ca .m ia N. Cs I Ma V _ iie .'.- 4 r.J e utt: No. c un P $ , Sa

                                                                                                                                                                                                                      ..,'.       i. '       l~ '

1 . ., ,.- , y P.G.T . V.2 .P. Stoel Electric 21 60 56 C4550 . ' .. 22 - ;- 1.32 .'01c. 014' Grain size after stress re11oved 7-8 , C4550-1 P H 'I S I C A L PROPERTIES' naccWU

                                                                                                =n=                        ,,,-

ia**as D E $ C E1e fION met No. S'^e 'ga , ny ,,, V-tfotch v,10*F. Appea r:.nct

                                                                 *-           c                        2-                                                                                                                                                        l I             1.-

1 669 915 24 I i 1-33 x 145-1/2 x 5-9./16" c4550 26 50 1 41 l 47 30% shuar 668 911 J

                                                                                                                          .                         I Lateral Expansion in 2 a'chos
                                                                                                                                       .041 l .036l.037 l             1
                                             !! . D .T . ir    cif t.ni'.

1-'r.tetr. .,'.mirfxrYhr'f X'.01X3 MI i ,i Drnp2%%1rN.h.K Tested in a corda ice to C.D. " I. J.credu;o tG-1 . v. 1. I I 11TP-L. l l' w Test locacian.C.L. & I. a llomoger.sity test catia rkit.t or yl.

                                                                                                                   ~-
                                                                                                                                                                 -l f    1,1r ctory - Loca% ion t t'                    ant.'tepo -           tur. 34tddle p/2 inc!.e Bend teac .Qt.isf.*                            .Radtas of curvathra 1 osa ti;pn 1-11l                                             aos.    .

l g l J 1 I _ f_. f.i n * % J!bHj W}/m .

04 . 9-13 68 tatt egg. l}4) ,( y-FUSCHASit. I

                                                                       ~ ~ * *comiiseur
                                                                               ** * * * * ~ ~ '. F A ime TEST CERTIFICATE
                                                                                                                              ' " ' " ' '                                  g Chicago Bridge & Iron Co.                  == o.oie no             (usio.ee '                                              Eame boyles, Ala.

12 27474-4 2471 bheet 1

     ~$rtCitsCAffoN1.
  * ,           ba:ee o oce     s,                        Sheet f 2 of 2                                                                                               -
             . res:

C H 5~id I C A L A N A L Y so 515 V is As a

                                                                        $s      He            Ce Mes      F        5         Ce Mtti HO.      C c4550-1 i                                                                                                                                 ,

1 v .

                                                                                                                                                                       ~

l-PHY SIC AL PROPERTIES DESCaaPTioH, e I'"" #w 96 8 A. BMN *- Mill NO.  % I I W.Q. for 23 minutes. 1650' F. 4

                                                       -25  *F. , hold 3 hr. per inqh min. erand                 inch   mi n. aniair cooled.

Plates and tests heatec 1220'F. 110'F., lheld N hr. p . Plates and tests were then tccapered 42)*H. I

                                                                                -$u M. helq 1/2 t r. per inc h min. and air cooled.

Plates gas cut het and strese relieved 1150*F. of 7 'F. pqr hr. to 1150'F, nd air cooled. hk, Tects strot s relieved ty heat ing within a rate of 901F. pen hr. to 600*F. e held 50 hre . and furnaco cooled within a rate I I L-S-45208t with inspect ion sy stem requigementaq of M3

        '                accor   dance Produced ir                                                                     !          l l          l I         l                                                                          l V                                                                                          l          1                                                                         i I
                                                                    -                      1 l          l P/
                                                                                                                                                                   l
          .                                                                                 I         i i          I
                                                                                                                                            /    D           /)

I t

                                                                                                                                              '?
  • O kh 4 > '

We hereby censify the above figuees are correct os contained in the records of the company.

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1543 Ps)RCH A$1 R. couisuis,e. w,a o*ii. 7-:5-68 Chicano Drldne & Iron Co. TEST CERTIFICATE couomen e o. Same h2s_ 12 Jamee C. Thompson, Pur. Mgr. =m osoinec. ' Boyles, Ala. P.O. Box 277 27475-2 2471 Sheet 2 MB 71368 LR Birmingham, Ala. 35202 . SPfCthCATIONS. Gr. B Class 1 Mod. by C . B . &. I . MIXE MS-1, Rev. 1 Fbx. 60000 O SA-533-65 , D erre irs: 0.K. .o ociw use O.K . Sheet i 1 of 2 ~ CHE MIC AL A N A L Y_ SsoI S Basic Process

n. c. v r er s g m r s ce s.

urir uo c Y 57 F .O .I . Y .] .P. St eel Electric .E 23 1.50 010 015 27 56 C4487 ' f V 6- 7 Orain Size afte r stre ss rel ievec PHY5tC AL P R O PE RTIE S Fracture ,,,c,,,,,og *

                                                                                                 'a'act$
                                                        = st**             .
                ,g-              sian I   =ge    'ag=e 2-
                                                                  ,,(

Y-Not ch 41C 'F. Appnarant e wo. . . l l 1 I I i 1-396 x 145-1/2 x 5-9/16" 646 890 24 46 30f, Shear C4487 1 651 891 26 41 1 26 l

  • l l Lateral Expansioq in ir chea
       '                                                                          .024 l.034 l.030 l                               i l                                l N.D.T. is         -

10'F. I I

a. I . F rocedu re TI C-1 llor. 1 l Tested in s e cordiince to C.B. l l '

l Test location C.I . a. I . MTP- 1. l V l l satisfactory l l  ! Homorenalty test . , l 1 I' !

                                                - Loco tion t ransve ese -

top nliddle lof plo to Bend test e atisfr ctory J ess titan 1- /2 inc hes. Radius of curvature W eby certify the obove figuies are correct as contoined in the records o'

                                                                                                   ' company.                                                                                                                               ,,, , d , M k        .       .
                                                                                                                                                                                                 '"'1543
                                                                                                                                ~
                               * ^ " ' * *
  • c.ai sIk s[,iS,$ ' out- 7-25-68  ?

Chicago Bridge & Irun Co. TEST CERTIFICATE 12 James C Thoppson, Pur.Mgr. ou o.oi. e cusioLie , o ( (u ' .\ 38** 1 bi O Dox 277 Ala. 35202 2471 Sheet 2 toyles, Ala. riningham, 27475-2 l specnications. Same Sheet /2 of 2 Of t3D 1t%I **0aaOGENEW ttit CHE MIC A L A N ALY SIS - y is At 3 5 Cu a sa He ce Mo M[tl No C Mee P I c4487-1 1 PHY $1C AL PROPERTIES

                                                                                                                                   ""^'"                                          o e s c.i,r io u .

l unti ex). *g ',{ "E' ','""*, u . a. - Plates and teste heate s 1650* F,I 25* F. , neld 1 hr. per

                               *nch min, and W. Q. for 23 m1 2utes. Plate s and tests were ;

then tempe red 12 ?O'F,1 10*F. , held I hr. per Lnch mLn. anf air cooled , g l eved I L50*F,h*F, heli Plates Ene cut b>t and stres s reli

d.

1/2 hr. pe e inch min. .ind ai r cool  ; g t rat e of 7 *F. p er hr. l Testa stre agpelLeved ay hea ting w Lthin :e co.31ed w thin t rate 50 hr s, and furna to 1150*F,

                                                            ,,5 f*F,, held I

of 90*F. p er nr. to 60)* F. g g Pruduced 1 1 acco rdance with Lnspec tion s.rstem requihements l j of MIL-I-4 5208A. , g  ; i i . i 1 i l l ((k

w. s.. .s, . .,, ,, ,s. . . . . .. . , _, ., _,.m.a m ,s. . . o, .. . s. _-,. , _ . ,

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                                                                                                                                                                                                         " J-5-68 1543       (.oQ Chicago Bridge A. Iron Co.                                            TEST CERTIFICATE if.                                                                                           unt otDtt HO.                 cu% Outa t o Same
                           %;' *                                    12                                                                            2471 Sheet 2                      MR 72968 LR                 Boyles, Ala.

27475-3 8168 W+ . setcwicAnons. *

                              /f                             '                                     Cr. B Class 1 Mod. by C B E I MS-1 Rev. 1 Fbx. 80000 p'                                              SA-533-65
                                                                                                       -u             O.K.                                                                            Sheet f I of 2 hib'                          N*
                                                                            .. nsi      :0.K.

C HE MIC AL A U A L Y S 15

c. v + * *
                                                                  '       meni no.            c        u       e         s       a          s.            u.                       un                                              Saei M rw ash a

3L ! 58 55 F.G.I . Y.] .P. Steel Electrio B8496)-f' 22 1 45 013 016 24 a e a a y ! C4521 1.43 009 015 26 57 54 23 e' I Grain size after stress relieved V Bc496-1 - 7-8 l-C4521-2 , 7-8 . PH Y SIC AL PROPERTIES

                                                                                                                      ==                                             w acii              Fracture                      , , g g , , , , , g ,,

wg , smaa 'g* "y ,,, m V-Notch +10*F. Anocarance

                                                                                             *0-        ==     ==     ='>-                                                                    -

l i ' 944 25 l l 1-360 x 145-1/2 x B8496 1 685 40 30% Shear 687 940 24 42 l 42 l

                                                                    "                                                                                            I             i
  • Lateral Expansioq in iriches
                                                                    -                                                                                 .035 1034 l .028 l             l                                            a s                                                            25 C4521.               2         716      945                                               l              l 48 30% Shear                     v i        g y '?

717 945 25 42 l 45 l

                                                                          ,,, g          )                                                                        I Later1 Expqnsionlin inchee I
                                                                                                                                                      .033 l.038 l .032 l             I l
                                                                     , N.D.T. is 410*F.

l ' i 5 1. Frocedu re TFC-1 May, 1l Tosted in o ccordence to C.B. l Test loc a t. ion C.1- .& I. MTP- 1 l llomogeneity test satisfa ctory . transversa - top ptiddlq of plate l l

                                                                                                                                                                                                                                                   'f"*s d'

l Bend test ratisfa ctory. - Location

                                                                                         !          i             Rad lus of curvature less t4han 1-11/2 ir;ches

( ebr cert'ly the above f gures one correct as contoined m the secords c company. , , , , _ , gh ft/

                                                                                                                                                                        . the company.                 ,,,,,, iiu ,
                                                                                                                             * ~ - --' a *d 'a 'h* Co
                  , o, c,,,., ,                                                                         co.. w . . . ..                        ...

8-27-69 '"' " 1543

                                                                                                                                               "'C'                                             '

i' 12

                        - Chicago Dridge as Iron Co.                                          TEST CERTiflCATE                                                                           (U sg} 

James C. Thompson, Pur.Mgr. ==t e o . .*>

                                                                                                           ~

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                    '          " 'r r.ori ty <:crt.ify t.ho abwe results ero correct :nd that                                                                                          till require-                               *' Y,e. .eW M.". ((,' em4.M
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                     <94   11:45   *ET919 345 2520      CP&L/NED                             - @ 002 Lonape Forgo. Inc.

1280 West Chester Rd. West Chester. Pa. 19382

            ! arch 14. 1989
    %./Carolina Power & Light Co.

Box 1551 Raleigh, North Carolina 27802 Attn: Mr. Sam Grant

       . Gentlemen.

The following information is being provided for your information and is applicable to Lenape F.orge. Inc. Heat Code Q2Q1V . A508-2 material melted by Sharon Steel Co. and received by Lenape Forge Inc. in June of 1988. Ladle Analysis: C Mn P S Si Cr Ni Mo Cu (Wt %) .21 .75 .010 .015 .23 .37 .80 .69 Product Analysis .21 .75 .010 .014 .24 .37 .82 .89 .18 (Wt %) Drop Wt. Test Results Reported On Material Forged From Heat Code Q2Q1V. (Testing performed using P-3 specimens per ASTM E 208) Material Heat Treated Condition: s" Normalized at 1850 F - cooled in air Austenitized at 1580 F - water quenched Tempered at 1290 F - cooled in air Stress Relieved at , 1150 F 30 Hrs. Drop weight test results: -20 F, -10 F, OF  : Break 0 F, +10 F. +10 F: No Break l Please note, test results presented have been obtained by processing (forging and heat treating) starting stock selected from Lenape l Forge Heat Code 92Q1V. The above results are not intended to be used to l certify any particular forgings in your possession. For specific forgings I of concern, please refer to the applicable MTR (Material Test Report) supplied with forging shipment. l Sincerely, R.0.T& R. Douglass Trout Plant Metallurgist

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l l Revision 1 NEDO-24161 l

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I APPENDLX C Weld CTRs

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Certificote of Analysis

                                         -            Post Welding Supply Co.                                             co ,,,,, o, der No.                                      10722 1300 Seventh Ave. , North                                                                                                    g, g, 9            gg jf Birmingham, Alabama, 35233                                                                            o, der No.                   < W' Shipped                                  5/15/68                         .

This rnoteriot conforms to Speci6cotien Para. N511 S,cetion 111 ASME .. Test #RO-4651 Type Trade Nome: Atom Arc 8018NM . Diameter sice, 7/32" 40 Lbc. - . 1726A27A Lot Number: - ,

             ' Heat Numbers b49I273
                                                                                                                                                                 ' {l 07 Carbon
  • Mongonese 'b
  • IO ,
       .               Chromium
                                                                                                                                                            '  I ' -

Nickel * + 91 ^ ' *

                                                      '* 44 Silicon                                                                                                             ,

Columbium Tantolum , 55 .,' Molybdenum Tungsten Copper Titanium . Phosphorus 02 '- Sulphu, 02 *

                                                                        +

Vonodium .

  • Iron ..-

Ferrite

                                                                                                                                                                 ,t-State of                           Penna.)         55            ,

The undersigned certi6es that this report In County of York ) correct and that no signi6 cont change has

                                                            *             '                                                      been mode in any of the elements desuibed
                    $ubscribed and sworn to before me                                                                     ',"In the quali6colion opproyo!.

thi 20th day of May 168 . ALLOY RODS COMPANY 04,1.; . o...eren c.,p.,.i;..

                                                                               /                                                                                                                                  '
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1 te.. ,',. . My commission expires: 5/0/72 ,,. , _. , ,y . ' tC _ (&#. ' A. Almoney m

idblat:lRUff LViirVidiidis~

                                                                                                      ~
  • A2c *1oouc.4 MAssuractuetNG omsioM

( Certi6 core of Analysis c . cys,,m , o, der No. 4033 Chicago Bridge & Iron - 2700 Channel Ave. ' 61685 Memphis , Tenn. Order No. P. O. M72102041630 9/25/70

                                                                                               $ hipped This materief conforms to specincotion            AS M_E S A 316 Test No. 792                           Type _ _E_80L8_G This electrode meets the requirements of Par Trade Name:           Atom Arc 8018NM                           N511.3 of ASME Section III Nuclear Code.

Mechanical Tests Test Specimen PW ht @ L100 to 1150 F. for Diameter Sizer 5/32 5,000 Lbs. 621/2 Hrs. tot Number: H013A27A Tensile Procerties Specimen Type ..505" Heat Number: 662A746 UTS 91,000 Psi - () YLP 80,000 Psi Carbon 060 /' b-Elongation in 2 inches 26% Mongonese .96 / 10 2d10 Red, of Area 70.5% Chromium Nickel 88

                                         /                                  Impact Properties
                                         /                                  Specimen Type Chgrpy V Notch Silicon       .38                            .

Test Temp plus 10 F. ~ Columbium Tantorum Ft. Lbs 35, 38, 47 Lateral Expansion 35, 31, 43 Molybdenum .S2 /  % Shear 50,50, 50 Tungsten Copper .03 Other Tests Concentricity 4% Titanium Phosphorus .021 / Moisture @ 1800 F 0.16% We certify that the welded material test plate Sulphur .017 / were subjected to the heat treatment cycle as Yonodium stated in the attached report dated April 2, l' fron of " Heat Treatment Cycle for Nuclear ( ASME Ferrife ' Boiler Code. " This is to certify that the otit nal i copy el this report has b:en proper!y signec - and notorized. -

            $1ote of         R nna.          )                                                    The undersigned certines thot this report is County of        York            )                                                    correct and that no signi6 cont chenge hos
  • been mode in any of the elements descri:ed
                                                                                                  ]n ghe qualincotion opproval.

Subscribed and sworn to before me , , , day I Oct. 1970 7 this 27th

                                                                                                                                              '/

CHEMETRON CORPORATION / anc raooucis waav8*c'wa iaG om6'" ;

            $EAL .      < anna.x cY. ...., .d e.DW-.

f W.-- r/? rf

                                                                                                              -- )-'-' fe /m '.*

My commission expires: 12/4/72

                                                                                                                                         ..'W

[ ,- G. W. Folcome r III

                                                                                          ,                                                 f!) L V

(~ f l CmcAGO Baroos & IRON COMPANY l 1500 N. SOTH S T. P. O. D O X 27 7. SIR MIN O M A M. AL AD A M A 35202 TWX 8tO-733 3654 Western Union-WUX Area Coce; 205 595-1191 CERTIFICATE OF ANALYSIS h 7- WG 2-MECHANICAL TESTS PURCHASE ORDER NUMBER: Tes t .. umber: PT164X Heat Treatment il25/ll50*F-50 Hout: Type Electrode: E8018G (JA'J/'l Tensile Properties Trade Name: Alloy Rods E8018NM Type: 505"O 01ameter: 7/32"0 UTS 88,300 Lot Number: 1726A27A YLP 73,500 Heat Number: 649T273  % Elongation in 2 i n ch es= 25. 5% CHEMICAL TESTS

                                                                     % Reduction of Area.=71.2%

Carbon. . . 0.048 Impact Properties Manganese. 1.12 Type: Charpy Vee Notch 0.02 Orientation:Perpend. to Weld Direct Chromium. . Tes t Temperature -Plus 10* F Nickel. . . 1.00 Foot- lbs. 81, 67, 81.5 Silicon. . . 0.52  % Shear 60, 45, 55 Columbium. . ---- Lateral Expansion 65, 66', 63 Tantalum. .. ---- Molybdenum.. 0.59 Tungsten. .. ---- Copper. . . 0.02 Titanium. .. __-- Phosphorus.. 0.017

             . Sulfur.    .  .

0.023 Vanadium. . . Iron. . Schae f fler Ferri te. . This material conforms to Section III of the ASME CODE, m Paragraph N511.3 CHICAGO BRIDGE AND IRON COMPANY Birmingham Materials Laboratory By , fo u O /lM __ 0 a t e '/ -/ I-C 9 d In charge of Tes ting for Rate,ri als Evaluati 62242:7YO 9-F70 Bf& lD

( ( .

                         . CHICAGO BRIDGE & 1RON COMPANY P.O. BOX 13308             MEMPHIS. TENNESSEE 38113 oot sci.

CERTIFICI$TE OF ANALYSIS MECHANICAL TEST RESULTS . Purchase Order Nu.ber: M72102041630* WO #11-D Heat Treatment 1100-ll50*F for

    ' Test Number:              .                                      .                           62 1/2 Hrs Type Electroc. e: E8018NM                                  Tensile Properties (CTR)

Trade Name: Atem Arc 8018NM Type: .505 Electrode Diameter: 5/32 ,UTS 91,000 PSI Lot Number: H013A27A YLP 80,000 PSI Heat Number: 662A746  % Elongation in 2 inche s = 26 % Flux Batch Number:  % Reduction of Area = 70. 5% CHEMICAL TEST RESULTS ( CTR) Impact Properties - Carbon........ .060 Type: Charpy Vee Notch , Manganese..... .96 - Orientation: L to Weld Direction Test Temperature -20*F Chromium...... Foot - Lbs. 89, 82, 95 Nickel........ .88

                                                                                      '~
                                        .38                         % Shear                         45, 40, 65 Silicon.......

Lateral Expansion 69, 64, 68 Colu.bium..... Tantalum......

                                        .52 Molybdenum....                                      ,

Tungsten...... This material conforms to SECTION Copper........ .03 III of the ASME CODE, Paragraph N511.3 Titanium...... , Phosphorus.... .021 . Sulfur........ .017 Vanadium...... N f q ', IN 9

              . Iran..........

Schacffler Ferrite..

                                      .                      CHICAGO BRIDGE & IRON COMPANY O!      d /96; BY I / hm                            __DATE
                                                                                                      <          'n
                                                                                                                   /

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                                                                                   ,e CarcAoO Biuoos.& IRON COMPANY
  • 1000 N SOTH S T. P. O D O X 2 T/. Ulf 4 MIN G H A M, A L, A D A M A 3U202 TWX 810 733 3054 Western Union-WVX Area Code: 203 000 1191 CERTIFl(ATE OF ArtALYSIS PURCilASE ORDER llU:iBER: 14E Cil AN I C AL TESTS T es t. !!umbe r: PT #200-Si nql e '.!i re lleat TreatmentG2-1/2 hours 01125/115 Type Electrode: Adcom Inmm/tinde 124 -

Trade Name: Adcom I n mm 'cli re Tensile Properties At Room Temperatu Di ame te r : 3/16"g Type: 0.505") Lot Number: Run #934 For i inde 124 UTS 36,500 lleat Number: S-3986 YLP 71,000

                                                                       % Elongation in 2                 inches" 30.0C CilDil C AL T E STS                                          % Reduction of Area. = 68.6%

Carbon. . . . 0.080 Impact Properties llang a ne s e . 1.42 Type: Charpy We tiotch Orientation: 3t 'leid Di rection Chromium. .. 0.07 . Nickel. . . . 0.96 Tes t Temperature Plus 10*F Silicon. . . 0.30 Foot- lbs. 40-51-49 47 a Columbium. .  % Shear 40-40-40 Tantalum. .. Lateral Expansion 38-44-43 liolybdenum. . 0 52 Tungsten. .. Copper. . .. 0.05 Titanium. .. Phosphorus.. 0.019 Sulfur. . .. 0.010 , Vanadium. .. Iron. . Schae f fler Fe rri te. . This material conforms to Section til of the ASME CODE, Paragraph N511.3 CHICAGO BRIDGE AND IRON C0t4 pally Bi rmi ngh am '4a te ri al s L ab o ra to ry B y, 7 o 4./P 8/P '/ Date f /2.- 6 7 I n ch a rg e oT T e s t i n g f o r iia t e ri ~f~s E v a l u a . \ L

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                                                                     -          Adcom Met.n Is Compa ny, I m:.
                                      .           .-              .:            . -,. .       ~ ',.~.~ ~: 7= :.~. : ~ ~:              ** * * ~= =. ~.~.~.~~ r T ~. 7 =~.': T ~.~ ' ' * ** ; ' " ~ ~ ~~~ -

February 4, 1969

                     +

v , i n a u , x. e , : s. . .

                               ..                                                                  -                                                                          Awaura oce ma..          o. tic Chicago. Bridge & Iron                                                  DATE SHIPPED: 1-17-69 SHIPPED TO:
                                                                         -             P.O. Box 277 .

Birmingham, Ala. 35202 867 CUSTOMER ' ORDER #B52815-2471/72U ADCOM ORDER #

                                                                                                                                          .           e,.

Gentlemen: . We hereby certify that material referred to conforms to the physical and tests as follows and is in accordance with specifications. Consisting of6 0-7C# coils 14 Material Marked 3/16" 1NMM i

      ?

Mo ', Mn P S St Ni C r-Heat C

                                                                                                                                              .07              1.07     .010            .Y 16         1.97                 .010            .012 S-3986 Al
  • Ti Cu
                                                                            .006                                  .05                                                                                            (
                                                  ~
7. S . Y.S . Elon. ,

Pro $i.- Roexv. ell [ .'.d r/ m y Pete. 0te rs, c' ate at t.:r: e , v

                              -                      ,say :nman.swcn E.7p.:e5 Jay *!,1973/                             , .,
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                   ,                     \.      UNIG!! C/K91L3 COL:F03ATI0t!
                   ',                 P. O. Eor. 550, !!irce.ra Fe.11% !! . Y .                                   ~

CLRTIFICATE CF ACCEFT.C.CN II:SPFUTIO;! Shipped to: Chicago Bridge and Iron Company Shipper lio.: 027092 Quantity Shipped: S4,000 lb. 2700 Channel Avenue Date Shippad: 3 24-69 Memphis, Tennessee . Your Orde.r fio.: A.22S4 o REFORT OF TE3TS OF GRADI 124 UNI 0illELT UELDII:0 ColPOSITION Identificatien of Material Te:ted: Grade 124 ,, Size 20_x 150 ., Lot. 1976 _, Run 934 _. . ,. This certifies that the Welding Ccmposition identified abo te has been tested fer conforming to specificaticas as fcllows: Sizing: 20 Mesh Mir.us 150 Mnh

1. 3f. 3.5%

2.5% 10. 0 '. SiO2 Ca0 A1 073, Uniformity: 32.07'. 21.11*. 14.50** 29-385 18 - 2 3'. , 11-17*. Lower lins gives spe:.ificatica limits - ci.gle valu:: :.r : r.:.:d=c. . State of !!c.u York County of !!iagara -

                                                                                                    ..   ,        ,)    ,
                                                                                                       ,/ M          T Sworn to before :r.e this                                                Materials Qaality - Ele:.tri:                 ' c i~.:.ni i.

19th y of Decenber _, 9 69 6 n~/ l L J eA' l

                                            . . , . .       ..     .   . .. u y/

N

                                                                                                                                       / :

C}{EMETRON CORPORATION

                                                                  .. = ,, . r.c.... , . _ ..o .

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  • Certificate of Analysis custome, o, der No. 3440 Chicago Bridge 8c Iron 2700 Channel Ave. 57744 Memphis, Tenn. Order No.

P. O. M12170 3 -0416 -30 Shipped 2B7/70 This material conforms to Specification SA_316 Test No. 519

                                            -'                                  . Type E 10.1A G This electrode meets the requirements of Par Trade Name:            Atom Arc 8018NM                              N511.3 of ASME Section III Nuclear Code.

Mechanical Tests # Test Specimen P.W. ht @ 1100 F. to 1150 F. Diameter Size: 1/4 20,700 Lbs. for 621/2 hrs, A022A27A Tensile Propertie s . tot Number: *. Heat Number: 401Z9711 Specimen Type . 505" - UTS 91,500 Psi

                                    .057                                           YLP 76,000 Psi Carbon Mongonese           1.15                                              Elongationin 2 Inches 28%

Chromium Red, of Area 71. 8% Impact Properties

                                                                                           ~

Nickel 83 Silicon .39 Specimen. Type Charpy Vee Notch coivmbium Test Temperature plus 10 F'. Tantotum

                                                                                   . Ft-lbs . 98,99,10 4 Molybdenum              .48                                            Late ral Expansion 70,69,73
  • Tungsten  % Shear 80,70,80 Copper 02 Other Tests Titanium Conc entricity. 4%

Phosphorus 021 Moisture @ 1800 F.O.15% Sulphur .,017 We certify that the welded material test platt Yonadium were subjected to the heat' trea: ment cycle as l'*" stated in the attached report dated April 2,1 Ferrite of " Heat Treatment Cycle for Nuclear ( ASME. Boile r Co de . "g, ;, g g, .. . . .g g.. g ,,..,,. of ins r:;:.t != Unit PtG~d/ C90*d and no'crized. , , State of Penna. 1 The undersigned certifies that this teocit is County of York ) correct and that no signitcent c* cage Fos been mode in any of the elements descr bed Subscribed and sworn to before me in the qualification opproval. this . 4th doy of March 19 70 CHEMETRON CORPORATION . anc enoovets n.amusicruams oms.c-SEA c,wus < I . , .

u. ., e.w.< ,y c _A BY MI'X f My commiss*on expire 12 /4/7 2 J. Harbold ,.
                                                                                                                                                     ]

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N DAT E.

  • April 2,1969 .
                                                                                                                                                                                                                                                                   * /.LLOY RO S CO.'/.?ANY
      - TO:                                                                                                                                                                           -                               .

CO?lCS: YORfs. Pi.fiNSYLY/,til A

     ~ ROM:                                                                                                                                                                                                                                                                                  .

Heat Treatment Cycle for Nuclear (ASME) Doilcr Code ijECT: - i Speedomax H Round Chart Recorder 0 - 2 50 0' F. Recorder Range Platinum - Platinura 10% Rhodium Thernoccuple Primary Element One cycle - 24 hr Recorder Chart Speed .

                                                                                                                                                                                                                                                                         ~~

Program Duration .. 12 5' F. + 50? F. 7-Start at . 1125' F.

                                                                                                                                                                                             ~

in 4 hr (250' F/hr) Increase to 112 5' F. ~+25' F. for 62-1/2 hr Maintain at @ 1006 F. per hr mrx 600* F. Decrease to Air Quench . Un: narked

           .                                 Gear on hiotor Shaft                                                                                                         "A"
                    -                        Gear on Au:dliary Shaft                                                                                                                                                                                                                                                                                        .      ;

Cam Cycle Time 150 hr (cach Cm division a 2 1/2 hr) . Percente.ge of Tolertne c - l Tirne Temperature Cnm *  ! Degrecs F. Degrees F.

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                                                                                                                                                                                                                           +50                          .

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1500 N SOTM ST. P. O DOX 2/7 BIR MIN O M A M. A L, A D A M A 35202 TWX 810-733-3654 Western Union.WUX Area Code. 205 595-1191 CERTIFICATE OF ANALYSIS PURCHASE ORDER NUMBER: MECHANICAL TESTS Tes t Number: PT1645 Heat Treatment 1125/1150* F-50 Hours Type Electrode: E8018G Trade Name: Alloy Rods E8018NM Tensile Properties Diameter: 3/16"9 Type: .505"9 Lot Number: J802A27A UTS 85,100 Heat Number: 977987 YLP 71,200

                                                            % Elongation in 2              i n ch es= 26.0 CHEMICAL TESTS                                           % Reduction of Area.-72.4 Carbon. . .    . 0.042                        Impact Properties Manganese.       . 1,04                             Type: Charpy Vee Notch Ch romi um.   .. 0.03                             O ri e n t a ti on :P e rp en d . to Weld Direct Nickel. . . .       1.04                              Tes t Tempera ture -Plus 10* F Silicon. . .        0.47                              Foot- lbs.105, 109, 73 Columbium.       .  ----                              1 Shear 60, 65, 45 Tantalum. ..       ____                              Lateral Expansion 82, 84, 59 Molybdenum..       0.59 Tungsten. ..        ....

Copper. . .. 0.03 - Titanium. .. ..._ Phosphorus.. 0.016 Sulfur. . .. 0.022 Vanadium. .. ___. Iron. . .___ Schaef fler Ferri te. . This material conforms to Section III of the ASME CODE, Paragraph N511.3 CHICAGO BRIDGE AND IRON COMPANY Bi rmingh am Materials Laboratory By . ,'e ' . - I' AP/1-/ D a t e N-/ 7 - (- 9 In charge of Tes ting for Materi als Evaluati

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                                                         .          / ALLOY RODS COMPANY                                                                                 , gd #
                '              -                                    \    oivi.w et cm.                    .r  c.<;.cs.i..                 \                        ,

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                                                           -              Certi6 cole of Anolysis j                         l                                          /, , - - - -- - s :

Post Weldin@pply Co. .I(,6 l C6 ' '. .. 4 I[('cyg,,,,, o, der No. B 53011-2471/72W

                                                                                                                                                                  ~
                                                                                                                                                                          '~~A P. u. box]Ill 1300 Seventh Ave. , ' North                        *
                                                                                                                            -                         . Order No.       52240 Birmingham, Alabama
                                                                                                                            $ hipped 10 /10 /6 8 This material conforens to Specification AWS A 5. 5-64T, ASTM' A 316-64T Type                                                            .

Trade Name: Atom Arc 8018 NM , Diameter size: 3 /16 3 6 0 0 lb s . - -- - - - - - - - - - -- - - - -- - - Lot Number: J802A27A 422W1601 Heat Number: 977987 'F8[3 A27A , Carbon .05 ' -

                                              . 90 -

Mongonese Chromium  ; '

                                                                                     'l Nick el           .95 /
                                              . 40 -

Silicon j Columbium  !- To r.f olu m , Molybdenum .52 ,, l' Tungsten Copper ,

       .                 Titanium                                                                                                                                                         .,

Phesphorus .03 i Sulphur .02 Vonodium .01 i fron ,j , i Ferrite  ; l n l Stone of Penna. 1 55 t The undersigned certifies that th; report is . County of York I

                                                                                            !                                 correct and that no significant chon9e ho' I                                 been made in any of the elements described Subscribed and sworn to before me                                      ,f                                      in the qualification opprovol.

thi' 9th doY 'i December 19 6$  ; I l ALLOY RODS COMPANY oi,i.i .e c6... .. c.,,.,.n..

                $EAl ,                      'T         '                NS My commissica empires' tY       r 5/8/72                                    g

[J. Harbold

                                                                                                                                                                                     ~

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                 ,       CWCAGO BRIDGE & IRON COMPANY 15 00 N. SOTH S T. 68. O- SOX 277 DIR MIN O M A M. ALASAMA 35202 TWX 810 733 3654 Western Union-WUX Area Code. 205 595-1191 CERTIFICATE OF ANALYSIS PURCHASE ORDER NUMBER:                               MECHANICAL TESTS Test Number: PT164W                                Heat Treatment ll25/1150* F-50 Hou:

Type Electrode: E8018G Trade Name: Alloy Rods E8018HM Tensile Properties Diameter: 1/4"9 Type: .505"0 Lot Number: J 80 7 A27 A UTS 80,000 Heat Number: 650x006 YLP 66,000

                                                                      % Elongation in         2 inches =28.0i CHEMICAL TESTS                                         % Reduction of Area.         =73.8%

Carbon. . 4.052 Impact Properties Manganese. .0.9.5 Type: Charpy Vee Notch Chromium. . 0.03 Orientation:Perpend. to Weld Di rec. Nickel. . 4.96 Tes t Temperature -Plus 10* F Silicon. . . 0.40 Foot- lbs. 89, 93, 97 Columbium. .----  % Shear 55, 55, 55 Tantalum. ..---- Lateral Expansion 64, 74, 75 Molybdenum..'.56 0 Tungsten. ..---- Copper. . . 0.03 Titanium. ..---- Phosphorus. 0.020 Sulfur. .

                                  . 0.023 Vanadium.      ..----

Iron. . Schaef fler Ferrite. . ---- This material conforms to Section III of the ASME CODE,

       .s .        Paragraph N511.3 CHICAGO BRIDGE AND IRON COMPANY                              l Bi rmingh am Materi als Lab ora tory d                                                    By       4 s -# hX*df              D a t e #/ / 7
  • d 9 In charge of Tes ting for Rate, rials Evaluat'
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                                                                                                                                                                                                                                                                   , M ')..
                                                                                                                                                                                          ,'(

[ AltdY miiu. it cm.RODS .i,e. c,y,m,;u CCMPANY Aj v Certi cale of Analysis . 7: '('- -.s.,';- . 53011-2471/

                                                                                                                                                                                                                                            ', . . . %')                72W Pos          Ve ding Supply Co.                                                             .

Customer Order No. ,

                                                                                                                                                                                                                                                        - .       . .e 1300 Seventh Ave. , North                                                                                     .

Order No. 52240 Birmingham, Alabama

                                                                                                                        .                                           sh;pped                                         10/10/68 AWS 5 5. 5 64T, hSTM A 316-64T This material conforms to $peci6cotion                                                                  '
  • t . ,

Type __

    - -                                     Atom Arc 8018 NM.                                                                             l                    .                        .

Trade Nome .

                                                                                                                                           '-                                                                                                                     .            lg
r ,

Diameter sire, 1,/4 I

                                                                                                                                                                                                                                                                        ,,l 10,700 lbs ,                                     l Lot Number:                    J807A27A                                                                                                                    '

N.. , ." Heat Number 650X006 ',

  • I
  • i , 3 Co, ton 05 - . *
     ^

Mangei..se .90 / , Chrernium ' Nick el .95 ' 40 Y

                               $ilicon                                                                                                        f
  • Columbium ,.

Tonforum ' ' Molybdenum . 52 / ' Tungsten

                                                                                                                                     ..s   ~

i s Copper . l Titanium Phosphorus .02 . Sulphur 02 , Vonodium .01 .

                                                                                                                                                  ,s'                                                                  .

Iron *

                                                                                                                                                                                  .                                                                                                           l Ferrite                                                                                                             i                                                                                                                                         l
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                 . Store of              Penna.          I                                                                                           I.'
                                                                                                                                                     '                       The undersigned certines that this report is
                                                                                                                                                                                                                                                                                              )

County of York ) l

                                                                                                                                                      ' , .' correct 1

been madeand in anythat of the noelements significant described lc

                                                                                                                                                      '                       In the qualincolion opproval.
                    $wbscribed and sworn to before me                                                        '

8! this 9th day of Dec embe r If 68 .

                                                                                                                                                       !                     ' ALLOY RODS COMPANY i                    . ei,s.t.. .t ch. . .                                    c.,,.,.u..
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5 eat . ' 8C!l.'l D&C4 .

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8Y' - l~'~ ##'f ' My commission espires' 5/8/72 i

                                                                                                                                                                                        /J. Harbold                                                                                ,.-

( . ( CHEMETRON CORPORATION e...uc r i mu,.c t v .,o e... .. Certificate of Anolysis Cvitomer orde, No, 4033 Chicago Bridge & Iron Co. 2700 Channel Avenue o, der No. _61685 Memphis , Tenn, P. O. M7 21020416 30 $ hipped 9_L25 /70 This material conforms to $pecification _6SME. SJ _316 Test Ne, 770 Type 18018.G This electrode meets the requirements of Pa N511.3 of ASME Section III Nuclear Code. Trade Nome: Atom Arc 8018NM Mechanical Tests Test Specimen PW ht @ 1100 to 1150 F. fo r Diomeier size, 3 /16 621/2 Hrs, 5,000 Lbs . Tensile Properties _ - tot Numberi goo 4A27A

                                                                        $Pecimen Type .505" HootNumbe4             4tl A 3531                                UTS 84,500 Psi YLP 71,500 Psi Carbon         .066 '                                    Elongation in 2 inches 29%

Monsonese 1.13 - Red, of Area 72.5% Chromium t D 'D ' Impact Properties Nickel .96 " specimen Type Chagpy V Notch

                 $aicon         . 51 -                                    Test Temp, plus 10 F.

Columbium Ft. Lbs. 60,60,68 - Tentalum Lateral Expansion 51, S2,54 Mofybdenum .47 '

                                                                          % Shear 60,50, 60 Tungsten Copper           02 #                                    Other Tests Concentricity 4Q Titanium Moisture @ 1800 F. 0.l?%

We certify that the welded mateiial test plat Phosphorus .018'

                 $v!phur         .017 /                                    were subjected to the heat treatment cycle Vonodium                                                     stated in the attached report dated April 2.

Iron of " Heat Treatment Cycle for Nuclear ( AS.\ Ferrite i Boile r Code." This is to certify that N orioine! Ct of this repost has been preocr!y si and riotarized. , Slote of Penna. ) The vndersigned cernfe, that fMs recort l ce,,ec, and shot no sign fccet choase e Cova ty of York been mode in any of the eivmeM6 erscrio in the qualiCcohon opprovol.

          $vbscribed and sworn to before me                                            

Octobe r M70 th18 27th dof of r

                                                                                                 .C..H.C.

oo_ METR,ON. e . .. CO.R.Po.

                                                                                                                               ... m. AT y'                                                                 *
           $tAL m            w T [ n .. . , ,...s u e
                                                                                                                        /

My comminion e.pires: 12/4/72 / G. W. Folcome r I!! (*, r

                                                                                                                            ,V        b
        . . _~       .                      -    -                             .                           -

4.. a (. f. CHIcAco Baioos' & IRON COMr>ANY 1500 N. 5OTH S T. P. O. S O X 277, DIR MIN O M A M. ALABAMA 35202 TWX S10 733 3654

                                      ,                                                              Western Union.WUX Area Code 205 595-1191 CERTIFICATE OF ANALYSIS PURCHASE ORDER NU;4BER:                                MECHANICAL TESTS Test Number: PT164N                                      Heat Treatment        ll25/ll50*F-50 Hou Type Electrode: E8018G
    ,              Trade Name: Alloy Rods E8018N:4                     Tensile Properties Diameter: 1/8"g                                          Type:     .505"9
                     . Lot Number: $823A27A                                 UTS 84,100 Heat Number: 654U539                                  YLP 74,000                       _              .
                                                                            % Elongation in           2    inches =28%

CHEMICAL TESTS *  % Reduction of Area.=75%

                                                                                                   ~

Carbon. . . 0.041 Impact Properties Manganese. 0.95 Type: Charpy Vee Notch Chromium. . 0.02 Orientation:Perpend._ to Weld Direc: Nickel. . . 1,09 Tes t Temperature Plus 10*F

  .                Silicon.       .

0.38 Foot- l b s . 181 - 14 4- 171 Columbium. ......  % Shear 100-80 100 Tantalum. ..... . Lateral Expansion 88-89-95 Molybdenum.. 0.59 Tungsten. . . . . . . . Copper. . . 0,64 Titanium. .. .._. Phosphorus. *0.015 Sulfur. . . 0.020 Vanadium. . 0.020 Iron. . .... Schaef fler Ferrite. . ----

                   *Per L-248 This material conforms -to Section III of the ASME CODE, Paragraph N511.3
            ,                                               CHICAGO BRIDGE AND IRON l COMPANY Bi rmingh am Materials Laboratory By /

4'e . - D / M -/ Date 9-47-69 In i;harge of Tes ting for liaterials Evaluati

                                                                                                               ,/'t              4?

d;

                                                                                                                   ~

l- , 9. l

            *        *                                                                                                                                                                             /J/ y w .u. ,cm....,e.ROD

(' ALLOY c.,,e . .. 5 CO.MPANY

                                                                                                                                       ,                        (-                             p Certificate of Anolysis                                                                              ,,.....
l. 4 .

es ( h

                                                                                                      '     ' ~

J g, der No. . b."2471/72W post Welding Supply Co.

                          ~                            "~             /  '        ,-

c,,,,,,,, Fi .O. Bcd 211I 1300 Seventh Ave. , North - Order No. 322.40 B.rmingham, Alabhma i 10 /10 /6 8

                                                                                                                                           $h.opped This mater of conforms to $pecification f f. A 5. 5-64T, ASTM A 316
                                                                                        -                                                                                                            ,. 64T Type                                                                                 .

Trade Name, Atom Arc 8018 NM , 1/8 Diometer size . 1000 lbs'. ,

  !               tot Number:                      S823A27A                          I                                                                                    .   .

654W539 Heat Number: ' 1 . I 4

   .,                        Carbon                .05 '                                                            .

Mongone,e .90 .

                       - Chromium Nicker             .95 7                                                                    .i
                                                   .40 '                                                                       l Silicon                                                                                                                                                                        .
    .                  Columbium                                 .

Tontalum Molybdenum .52 / { Tungsten Copper , Titanium . Phosphorus 03 ' Sulphur 02  ! i Yonodium 01 > I* ' Iron l Ferrite State of Penna. I The undersigned certifies that this report 18' ss County of York ) ,; 1 , correct and that no significant change hos

                                                                                                                                               ' been made in any of the elements described
                                                                                               !                                                  in the qualification opproval,
                    $vbscribed and sworr. to before me                                                                                                                      ^                                '

this 9th d'Y 'I December II 6d '

                                                                                                                                                 ' AltOY RODS CbMPA.NY
                                           ,3
. ~ ,i.. . t c, , . .. c .,, ... ,i..
                                         /                                                                        _
                                                               ' Mu. < 'W SEAL                      /.[WN *.i.,y~

Y b r/G / , ( w U My commim.on empire 5/8/72 ./ l

                                                                                                                                                         /*J. Harbold                                          1
        .                                                                                                                          80 -3 # 7o Q)W CQ p Q'~

(r.HEMETRON

                                                            \

CORPORAT10N uc emuess muune,tuxiuc oivision ( Certificate of Anolysis 4033 Customer drder No. Chicago Bridge & Iron Co. ' 2700 Channel Ave. Order No. 61685 Memphis, Tenn. P.O. M72102041630 $ hipped _ 9/25/70 ASME SA 316 This material conforms to Specincotion Type E 8018G Test No. 771 This electrode meets the requirements of Par. N511.3 of ASME Section III Nuclear Code. Trade Name: Atom Arc 8018NM Mechanical '"e s ts

                                                 '                                  Test Specimen PW ht @ 1100 to 1150 F. for Diameter Size                 7/32 2,350 Lbs.                                     621/2 Hrs.

Tensile Propertiess

         ' tot Number:               H010A27A Specimen Type . 505" Heat Number                   421A6811                                       UTS 84,000 Psi y                                    YLP 72,000 Psi Carbon              057 Elongation in 2 inches 27%

Mongonese 1.16 ' Re'd. of Area 72. 3% Chromium j Impact Properties Hicke! 89 , Specimen Type Charpy V Notch Silicon 5 0

                                                                                     . Test Temp plus 10 F.                      .

Columbium Ft Lbs . 88, 9 2, 93 Tantotum j Lateral Expansion 71, 78, 77 Molybdenum .46 7ungsten j

                                                                                      % Shear 80,90,90 coppe'            .03                                             Other Tests D " "I"
  • Concentricity 4%

g Phosphorus .020

                                                                                  . Moisture @ 1800 F. 0.16%
                                                    '                                 We certify that the welded material test plate Sulphur            .016"                                          were subjected to the heat treatment cycle as .

Yonodium stated in the attached report dated April 2,1( Iron ' of " Heat Treatment Cycle for Nuclear ( ASME:

     -                 I' "I'
  • s Boiler Code." This is to certify thet the original ceoy of this report has been properly signed and notarized. . _

The undersigned certines shot th;s repert i. State of Penna. ) SS Correct and that no signintent c,henge ho County of York i been made in any of the elements cescoce( In the qualiGcotion opprovoi. Subscrit ed and sworn to before me 19 70 this 27th day of Oct. CHEMETRON CORpCRATION s "% j Atc P AODuC7 5 Wahuf aciu *O D.vsa { mWf

                                                             /_. <_2.,c s SEAL <                                          r a..       , /"
                                                                                                          ,y ' g         l ' M c, G M u....,

y ycommi,sion e., ires, ' 12/4/72 O. W. Folcomer Ilt;

e ' (

                  ~

b " ALLOY RODS COMPANY f/ oi.;.4. o os.,,,e. c.,m. /[# \ Certificate of Analysis / Chicago Bridge &c Iron Customer Order k. M30A02-6.81262480 f l 1500 North 50th St. 5A810,_, Order No.

                                                      ~

Birmingham, Ala. Shipped 8i/27/63 j I This molerial conforms to Specification SA 3L6 l I Test No. AN239CX I AN239CZ Type __E801.8. G i l This electrode meets the requirements of Par. [ Trade Nome: Atom Arc 8018NM N511.3 of ASME Section III, Nuclear Code. Diameter site: 5/32 2,300 lbs. Mechanical Tests 0 Test specimen P.W.H.T. at 1100 F, to 1150 F : lot Number: E916A27A Heat Number: 601221 for 621/2 hrs. - Tensile Properties Carbon ,041 Specimen Type, .505" UTS 89,500 Psi Mongonese 1.05 YLP 79,000 Psi Chromium Nickel , gg  % Elongation in 2 inches 27% ~

                                                                 % Reduction of Area           72.7 %

Saicea .35 Columb;um Impact Properties Tortolum Spt cimen Type Charpy Vee Notch Molybdenum Test Temperature Plus 10"F.

                          ,49 Tungsten Ft. l os .107,108,108 Lateral Expansion 78, 66, 80 Copper            03 Tiio nium
                                                                 % Shear 80, 80, 80 Phosphorus           .018                                Other Tests                                                    i sulphu' Concentricity 3%

015 0 l Yonodium Moisture @ 1800 F 12 3" We certify that the welded material test plates w l J Fenite subjected to the heat trettment as stated in the attached report dated April 2 of " Heat Treatmen Cycle for Nuclear (ASME) Boiler Code." l State of Penna. I The undersigned certi6es that this report is I g g correct and that no signi6 cont chonge has been mode in any of the elements described

   $wbscribed and sworn to before me                                             in the quali6cotion approval.

this 12th day of Jt.ne 39 b9 [O alloy ROOS COMPANY

                                                                                  .......t......c_......               g
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                                   #4...,y PeMit A se& 7 L 8Y                   '[              -

my commission ..pi,eii 5/8/72 Witnessed by R. Etallman, Q. C. Engr.

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[Nt0R - O?P5CU CORRESPOND 0NCE -

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DATE: /,pril 2,1900 . TO: . ALLOY ROSS COMP /.NY COPlES. YORK. PEi;t.SYLY/dilA FROM: ,

SUBJECT:

Heat Treatment Cycle for Nuclear (ASME) Boiler Code w Recorder Speedomm: H Round Chart Recorder P9nge 0 - 2500* F. Priraary Element Platinum - Platinum 10% Rhodium Thermocouple Recorder Chart Spcod One cycle - 24 hr l Program Durr. tion Start at . 125' F. + 50' F. , Increase to 1125' F. in 4 hr (250' F/hr) . Maintain at 112 5' F. +25' F. for 62-1/2 hr Decrease to _ 600' F. @ 100* F. per hr mcx Air Quench Gear on Motor Shrft Unmarked ' Gear on Au :lliary Shan "A" Ce.m Cycle Time 150 hr (cach Cam division = 2-1/2 hr) Time Temperaturo Tolerance - Percentage of (hr) Degrecs F. Degrecs F. Cam 0 125 +50 3 0 ~ 375 11 1 G25 19 2 , 3 875 28 . 4 1125 +25 38

                                                                        ~

1125 38 60-1/2 34 67-1/2 _1025 30 08-1/2 925 825 26 69-1/2 22 70-1/2 725 18  ; 71-1/2 625 600 17 l 72

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1 i Po:st Welding Supply Co. Customer Order No. ..U1391(.:.kjll/ll.VI , P. O . B o x Zllt 52240 1100 Snventh Ave. , North . Order No. 13irtuinghatu, Alab:una f 10 /l0/68 Shipped AWS A 5. 5-64T, ASTM A 316-64T. This material conforms to Specification i t.

                                                                                       -Type Trod, Nom,,                Atom Arc 8018 NM                                                                                      .

o;o m.,,, $;,e: 5 / .M --------------------- 3 0 50 lb'.s .

    . tot Number                 F821A27A                          S817A27A   .

HeatNumber: 08T401 . 650W4'p 8

                                              ^

Carbon .05 ,

                                                                          ,l Mongoness                    . 90 '                                                                                                       ,

Chromium l ' Nickel .95 / ' Silicon .40 / ^ Columbium l , i Tantolum , Molybdenum .52.~ Tungsten Copper j Titanium l Phosphorus . O '! Sulphur 02 Yonodium 01 lron feirite i

            "              EC""8-                                                                           The undersigned ceiliGet that this report is County of             Y ork            l                                                               correct und that no signi6 cont change ho8 been mode in any of the elements described in the quali6collon oPProval*

Subscribed and sworn to before ene this 9th doF of Dec embe r W 68 ALLOY A005 COMPANY g- . . o,...... ., o . . . m. c... e.,. .

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4 U NA .. My commission empires: 5/8/72 "Y ^

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~ r , gtW CHIcAco Bnicos & IRON COMPANY 1500 N. SOTH S T. P. O. B O X 2 '7 7. B I R M I N O M A M. ALADAMA 35202 TWX 810-733-3654 Western Umon-WUX Area Code: 205 595-1191 CERTIFICATE OF ANALYSIS PURCHASE ORDER NUMBER: MECHANICAL TESTS Test Number: PT146B Heat Treatment 1125/ll50* F.50 Hour Type Electrode: E8018G Trade Name: Alloy Rods ES018NM Tensile Properties 01 ame te r : 5/32"O Type: .505"O Lot Number: F821A27A UTS 80,600 Heat Number: 08T401 YLP 68,100

                                                                     % Elongation in         2    i n ch e s= 29. 5 %

CHEMICAL T_ESTS  % Reduction of Arga.=72.0 Carbon. . . 0.047 Impact Properties Manganese. . 0.93 Type: Charpy Vee. Notch Weld Ch romi um. . 0.02 Grientation: Perpendicular to Dire Nickel. . . 0.90 Tes t Temperature Plus 10'F Silicon. . . 0.38 Foot. Ibs. 117, 116.5 115c5 Columbium. . ....  % Shear 65, 60, 70 Tantalum. .. .... Lateral Expansion 73, 75, 87 Molybdenum.. 0.52 Tungsten. .. .... Copper. . . 0.02 Titanium. .. Phosphorus.. 0.016 Sulfur. . . 0.025 Vanadium. . . . . . Iron. . S ch ae f fle r Fe rri te . ....- This material conforms to Section III of the ASME CODE, Paragraph N511.3 CHICAG0 BRIDGE AND IRON COMP ANY Bi rmingh am Materi als Lab ora tory By lN O 9-In charge of Tes tingd'/ for_Materials _ O a t eEva V '/ I_S ! l

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O R M ANUFACTuntR$ OF TECHNIC ALLY CONTROLLEO we.te -

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                          ])                                                                                                                    ST AIN LE SS STE EL. NIC KE L. M ON EL. iNC ONCL. tNC ON CL s
    ,3               ,,_ ..           . -.;                                                                                                 LOW ALLOY STECLS. WCLDING ALLOV S. LOW M E DlWM. Het g e ... s - . b4 jg]                                 COMBUSTION ENGINEElllNG. INC.

WIRE oR AWING PLANT 845 AT BE AVER RUIN RoAo P. O. Bo x 20!.0S ATLANTA. GEORGIA 30329

.                    custexE xs oRos a No.                                    suon oRoe R No.                   I        o A TE s aines o X>5bh<                                                  965-3 I                                seteiricATioN I

9-17-70 1 P .O.# t1-309190416-20 - 1 i MARKED: SHIPPED 9 90 iTE,PA CONSISTING OF 175 02 to P. O. Box 13308 3716" Type INMM Memphis , Tennessee 38113 Welding Wir e a L_

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             ,                GENTLEMEN:

WE HEREBY CERTIFY THAT MATERIAL. REFERRED TO AEOVE CONFORMS TO THE AND CHEMICAL TESTS AS FOLLOWS AND IS IN ACCORDANCE WITH SPECIFICATIONS:. HEAT C. j f.in. Si. ' t S. ' l l P. ' i Cr. Ni. ' Cv. ' f.'g. i Fe. l Al. WGO '.18 11.901.070 .013 .008 l T6. Cb. + Ta. l Me" i i e i

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I I i i  ; t i ITEM l TENSILE STRENGTH YlELD STRENGTH ELON. l l GRAIN S!ZE l ROCKWELL SHEAR 1  ! l 118,400 P.S . I. 1 I .' i

                                                                                                                                              ,                         i J                                                                                                                                                                                                              ~

YOU R20Uc5TED THIS IIAPORTANT INFORIA ATION. va'Nruiv veun. j cor.icusTion EncisEERiNc.isc. Ncr3 v 17 1 _ M _.

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Avr oRizeo o[,iew. 0L6f> PLE ASE GIVE TO YOUR PURCH ASING AGGNT. . le'

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                                                  .       CERTIFICATE OF ANALYSIS                                             oos e47.:r.it Purchase Ord,er Number: M30919                              MECHANICAL TEST RESULTS M60913 Test Number 569C Tandem Wire                                      Beat Treatment il50*F + 25'-50*F for d21/2 Hours Type Electro.de: Adcom 1NMM/Linde 124 Tensile Properties (20 x 150) Flux                                                                             '

Trade Name Adcom 1NMM Type: 505"# . Electrode Diameters 3/16 trrs 92,500 Lot Number --- - YLP 78,500 - Heat Number: 1P4218  % Elongation in 2 inches = 27% I 9 Flux Batch, Number: Lot t Reduction of Area = 65.4% CHEMICAL TEST RESULTS , Impact Properties Carbon......... 085' Type: Charpy Vee Notch Mangane se . . . . 1,4 3 , orientation: 1 to. Weld Direction , Chromiura. . . . . . .07 Test Temperature +10*F y Nickel........ .87 , Foot - Lbs. 94, 91, 90 Silicon......*. .39  % shear 98, 95, 95

                                 ~

i,I . Columbium..... Lateral Expansion 58, 66, 77 Tantalum...... Molybdenum.... .45 -

  • Tungsten......
                                                             .             T is material conforms to SECTION Copper........      .06          -      III of the ASME CODE, Paragraph N511.3 Titanium......

Phosphorus.... .010' .

                    . Sulfur........      .015                                                ,

Vanadium...... Iron.......... Schaeffler Ferrite.. pHICAGO BRIDGE & IROK COMPANY DY hh DATE 10-16-70 7

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                                     ' 'j CmCAGO Emnes                                                                 & IRON COMPANY MEupMis. TENNESSEE 3 e 113
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CERTIFICATE OF ANALYSIS . Sot w7 sii pgychase drder Number: B111503- MECHANICAL TEST RESULTS

                     ~ ~ ~ - - - ~ '

2471/72 ,

       'gggt Nympgy; M281C                                               _
                                                                                  .-                        '.                    Beat Treatment                                    .

Type Elggtypse: E309-15 (SA-29 8) "' Tensile Properties - TFg(g MaMg; Alloy Rods Co., , yype ElestF94g pigmater: 3/16" ' , , ' , UTs - E4% NWBb9F; 3A922H5C , y.gp , ,

                                                                                  ^

Ettt pgmpgy; W73594, , I'

                                                                                                                    , . . . 4 Elongation in                                inches =

Flu Betsh Number: - -

                                                                                                                          ,          4 Reduction of Area =

Impact Properties CHEMIeAL TEST RESULTS CAFb9n,,,,,,,. Type: Charpy vee Notch Mgr,gggggg,,,..

                                                                                                         ',-                         Orientation: _ to Weld Direction ghygmium,,,,..                                               .

Test Temperature s , Niek91, , , , , , , . ' , Foot - Lbs. Sil199n,,,,,,.  ; ,

                                                                                                                                      % Shear                                                       ,

gglymbium,,,.. , Lateral Expansion

                                                                                            ~

Tantglgm,,,,.. , Mglybdgnus,,.. . Tynggten,,,,.. This material conforms to SECTION

                                                                                          .*5II of the ASME CODE, Paragraph N511.3
                                                                                                                                          ~

09PP9Freerr,+- Titanium,,,... , - Ph99Ph9F9F, - ,, ggifur,,,,,... , Vanadium,,,... . IF90er,este, . - E9hB9ff19.r Ferrite..

                                                                                                       ** CHICAGO BRIDGE.& IRON COMPANY
                                                              .090 gghalt,,,.,...                                                                                                       ,

f DATE May 14. 1970 BY ,

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                                                             \       ALL'OY RDDS COMPANY                             \.                                                             l i

e' o;,iii.a .t ch....,.. c.,,. . ...  ; Certificate of Anolysis Chicago Bridge & Iron Co. Customer Order No. . Bill 50 3 -232HI2 P. O. Box 277 Birmingham, Ala. __ o, der No. . shipped 3 /17 /69 This material conforms to Specification Type E 309 -15 This test material conforms to specification Trade Name: Arcaloy 309 Lime i SA 298 ( ASME Section II PartA) and to Diameter Size: 3 /16 Paragraph N-511. 3 ASME Code Section III 4,080 lbs. tot Number 2 3A922H5C Heat Number: W73594 Carbon .05 Mongonese 1,79 Chromium 23.51 Nidel 12.79 Silicon .54 l Columbium I Tontalum Molybdenum Tungsten l Copper I Tita nium , Phosphorus .020 l Sulphur .011 Vonodium fron Fenite 77r This is to certify that the original copy of this report has been properly signed and notarized, i 1 I

                                                                                                                                                                               -1 State of                 Penna.             1 55                                                   The undersigned certifies that this report is                   ;- !
               ""'#       '          YOYh              '       .

correct and that no significant change hos I been mode in any of the elements' described l Subscribed and sworn to before me in the qualification opproval, this 23rd dOY CI - June 19 69 ALLOY RODS COMPANY oi i.i.a .e ch. .. e,.. c.,e.,..... f') SEAL h h' ?N O &...., Y ra a Y h $$!

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Witne s s e d by, R. . Stallrrian, Q. C. Engr.

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                                                            . .LLOY RODS COMPANY                                  ,
                                                              @visiaa of Chsmstrea Ctepsrctesa                                                           f l

Certificate of Analysis Chicago Bridge & Iron Co. Customer Order No. Bill 503 -2471/ 72 P.O. Box 277 Birmingham, Ala. Order No. _ _, Shipped 3.Bl.lM This material conforms to Specification Test No. RQ-4997 Test No. RQ-5004 Type 7308L.d5 Trade Nomer Arcaloy 308 ELC Lime This test mateiial conforms to specification

                                          '                                        SA 298 (ASME Section II Part A) and to Diameter Sim               3 /16                                            paragraph N-511. 3 ASME Code Section III.

900 lbs. 5. 220 lbs. Lot Number: 2A923H2C A922H2C Heat Number: 65298L 65278L Carbon ,o4 ,04 Mongonese 1.83 1.86

 .            Chromium         20,41                         20.40 Nickel 9.71                          9.60 Silico"          .72                           .74 j             Columbium Tontolum Molybdenum Tungsten Copper Tita nium Phosphorus
                                   .02                           .02 Sulphu'             02                          .02 Vonodium This is to certify that the original copy Ferrite          g y,                          BTe                       of this report has been properly signed and notarized.

Store of Penna. ) The undersigned certifies that _ this report is SS County of York ) , correct and that no significont change has been mode in any of the elements desenbed Subscribed and sworn to before me in the qualincotion approval, this 23rd day of June 19 69 ALLOY RODS COMPANY

                     ,'                                                                             o;.i.;.. .t ch...t,.. c.,,.,.i..a
         $ eat                   !V          ~....,.....

b]$$l b My commission expires: 8Y A

  • 5/8/72 f - r.

Witnes sed by R/ Stallman Q. C. Engr. J. Ha rbold g

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                   -                                    ( LLOY RODS COMPANY o..w. ., c im .,. c,.,r.. ..e,

[ /p ' , c,, ,. , ! , 0 Certificate of Anclysis P.O. Chicago Bridge & Ir " Customer Order No.* M"b.120(dj64.r'3760 2700 Channel Ave. Memphis , 'Tenn. . . . . . . . . . . . . - Order No, 5540! Shipped 8 / 5 /6,9,._ This material conforms to Specincotion . ...S A.-316 . Test No. AI 304 BX AI 304 BZ Type .E.3013 -G Trade Nome: Atom Arc 8018 N,M This electrode meets the requirements of Par. N511.3 of ASME Section III Nuclear Code. Diameter Size; 1/8 Mechanical Tests 2,500 lbs. Test Specimen P.W. Ht @ 1100 F, to 1150 F, tot Number: F920A27A for 621/2 hrs. Heat Number: 88 E081 Tensile Properties Specimen Type . 505" Carbon .06 UTS 93,200 Psi Mongonese 1.10 YLP 83,000 Psi Chromium  % Elongation in 2 inches 27% N!ctol .93  % Reduction of Area 68.3% Silicon 27 Impacts Properties Columbium Specimen Type Charpy Vee Notch Tontelvm Test Temperature Plus 10 F. Ft. -lbs . 8 5, 90, 91 Molybdenum .51 Tungsten Late ral Expt.nsion 72, 67, 69 02  % Shear 70, 80, 80 Connr T;tonly n Other Tests Pnci.che us 017 Concentricity 3%

               $vlphur            .014                                    Moisture @ 1800 F. .13 vanodium We certify that the welded material test plates were subjected to the heat tree.: ment as stated                                           ;

iron rer,iie in the attached report dated April 2,1969 of

                                                                       " Heat Treatment Cycle for Nuclear (ASME)
                   '8M I. to co.-tif y ih9 tha c,ric!nsl ee py cf thb report hc2 bnn r ro.*ntly .isned             Boiler Code" l

t.nd nctcri:.ad. l l l State cf Penna. I

                                               $$                                              The undersigned cer Mes that this repert is                         l County of          York           I                                                    correct end that no signif con' cheic h 5
                                                  .                                            been modo in any of the elen:ents describ;c                         j Subscribed cnd swo.n to before me                                                      in the quahncolion opproval.                                        l this 7th          dcy of August                       19 69 7                                      ALLOY RODS COMPANY f                                         0;. mea .# c%e..... c.,r.......
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Nol.'y P.bhe 3

                                                                                                                             /l                       - f My ecmmission capires:           5/8/72                                                 BY @. ...                 .CI_ !T .e         !.i. ' 3.E _.

Witnes sed by R. Stallman, O. C. Engr. J . Ha rbold

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a aN7 .. .c,,.. Q 'N '.f')- 7. .Ns9s. e. .q. I N.t,*,"'*: 13 s ^ as t ,, r;. a v. ~ 9;.. DATE: April 2,1960 ' /,LLOY iiODS CC.".?AN' 70- ' COPIES: YORK. pet;h$YLVANIA FROM: . Heat Treatment Cycle for Nuclear (ASME) Boiler Code

SUBJECT:

Speedomax H Round Chart Recorder Recorder Range 0 - 2500* F.

           .                                                                                                   Platinum - Platinum 10% Rhodium Thermocouple Primary Element Recorder Chart Speed                                                   One cycle - 24 hr                                                                    .

Program Duration .. Start at 12 5* F. + 50? F. 112 5' F. in 4 hr (250' F/hr) Increase to' for 02-1/2 hr Maintain at 1125' F. +25' F. 600* F. @ 100' F. per hr mra: Decrease to Air Quench . Gear on Motor Shaft Unmarked Gear on Auxiliar/ Shaft "A" Cam Cycle Time 150 hr (cach Co.m division = 2-1/2 hr) .. Percent:.ga of Temperature - Tolcrcnc e Time Degrecc F. Cam * (hr) Degrees F. *

                                                                                                                                                +50                                                      3 0                                            125                      ~

11 1 375 '

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625 .

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30 60-1/2 1125 -

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34 07-1/2 1025

                                                                                                                                                                                        .               30 08-1/2                                          025                          ,

26 69-1/2 825 22 70-1/2 725 . 18 71-1/2 625 , ' 17 73 600 . e

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                                                                                                                                                                                                   .M

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                                                                                            '                                                                                                          \

CERTWIC ATION REV C B 41 Aie DATEIN-7/ CUSTOMER QATE CODE DAT L DWG  ! 4 i

l l Revision 1 NEDO-24161 I 1 APPENDIX F Surveillance Test Specimen Plan

                                            - F- t -

1 J

T.URVEIL' ANCE TEST

     ~ r:7,fC.C"')
                                                                                      */'
                                             ,      .                                  ( '

Si'ECIMEN PREPA?;.? ION

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                                 !             \.3 I!

PLAN

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GCMERAL UL1:CTRIC COMPliNY ' " LEON' STP-3 e c.r.it n PAGCNO. I OF 15 encou,T BO[bhMGWATMRNUCLEARRCACTOR OATE 7-21-69 Asscuoi.y REVi$10N NO. I o csc.mr'rioy 4 SURVEILLANCE TEST SPECIMEN PREPARATION PLAN TilIS PLAN APPLIES TO THC THREE (3) REACTORS FOR CAROLINA POWER AND LIGHT COMPANY, CONTRACT NUMBERS 68-2471/72/73; b+ . 1.0 GENERAL _ INSTRUCTIONS 1.1 All final cutting shall be donc by machining. 1.2 Specimen marking and mark orientation arc of utmost importance. In cTse of a mistake, or if uncertain about the marking on a blank, DO NOT use it for a fi'nished specimon. 1.3 Material must be us'cd cautiously since there is no replacement material. 1.4 Material to be heat treated at'1150 F plus 25 F0 or minus 50 0F ( for a total of 50 hours, less any heat treatitig time after tempering. 2.0 SilIPMUNT INSTRUCTIONS . 2.1 Arrange each group of like s,nricimens in serial order so they will remain in serial order during shipment. 2.2 Adequately crate or box specimens for protection during shipme..t 1 CUST01.tER APPROVAL Approved September 4. 1969 by Eugene O'Connor. Received from G.E. ER #S939 dated 9-8-69, VPF #2478-291-1 l t . (' aro ne o lp av l c a ' C( !: on on os os om aro cn,.e to on ei o I

               ;                 o:e.s              i ~ r.       cn           .on  cw      i.m, oc ce v       o      u. o        u,.r
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                      ~ ""                                     ,(.                                             h 'UlWEILLANCE T:s?

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                                 \     .,

Sl'rCT"rN P7EPl.PATW: (I . ...(1)j '

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                                       )                                                                           PLAN e uu uu .
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                               .... G L'!!1:1'.AL 3LEC'P"1 F & " " ?dLY._ _....

Pact No. 2 or 15 enonoci __,DQUd1W 11 ATE _jUtf;WR P, lect,gn oAtt 7-21-69 A w v.s a y , ,_, , [ 1 AEVISION NO. DL $Cl41P T inn _ ar-sen. r. .m-r- . =. ars=:summm.r--.- m - _ _ . - - a.ma_. i C 2.3 The X-ray films of the welded scams in the surveillance test plates and 4 copies of all metallurgical data and documents including Drawingu'T-5 through T-13, (Cortified Test Reports) of plate, heat treatment recorcia and nondestructivo test M 5 reports shall be l'acked i n the seen ho.s: as the test speci:. ens. Two reproducib3c prints of above metallurgical data and documents shall be submitted by mai1 within five days of the shipNent. The coverinj letter chall include the date of chipment, the route and all shipping documents. / ! 3. 0

  • liASI: :!CTAL MATERIAL 3.1 The base natal shall be tahan f' rom Tcist Plate marked (2607),

which shall.bo cut fr,om shcIl Plato-ru'.rknd (301), as shown on Drawing T-5. Plnto (301) is,a plato opposite the Active ruel Zonc in the Coro Region. shall be given a stress _ relief

                                                                                                               ~

3.2 Ten t Pla tc' (2007), Drawing T-5, y in accordancer with paragraph 1.4 to cinulate the strcss relief of the Core Region Plater. (301 and 351). X-rays of the weld must be sent to the custc:r.or (sce paragraph 2. 3) . . 4.0 117,CC t' ETA;, TEST PLATE SI:1PPED TO GFMEPAL El.CCTRIC 4.1 Stencil base meta) Tes t Plato marked (2630) cut from shcIl Plate marhad (301) as follcus: (Use symbols at least 1/4" high) G.E. DASE METAL M3 LL ROLL.I!!G D.TRECTION III:hT NU:: DER . S1,hD NUMilrR CONTRACT NU.'1BER Documento shall hi> rupplica to General Ulcetric showing the i sourec, chemistry and all heat treatment of the plate.

                 -4.2                     The above Test Plate marked (2610) shall be shipped to Goncral Electric.

1 61

r"' ,'D "7 *( SURVEILLANCE TEST

       /

_ .t u i:s SPEC T tir N P 9 EPA R ATIo'; w n - :u,i PLAN

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                                                                              ~

Dr sCRil'ison _ _ REVISION NO. 3 ___mm,..__..-- .

                                                               .       m _ .-         -

(/ 5.0 DASE METAL TEST PLATE USED BY Cl!ICACO BRIDGE r. IRON TO MAKE DA8;. .i.'sTAL MECl: AMICAL Ti'S r SPECJ NU!,Q Plate (2607) cut from shcll Plate (301) shall be used to make f.s Mechanical Test Specimens required by Drawings T-6, T-7 and

        .                      T-8.

6.0 BASE .**i:TAL CIINTLPY SPECI'iEMS 6.1 Specimen Requirements 6'.l.1 Prepare the Charpy Itapact Specimens in accordance with Drawings T-6 and T-7. 6.1.2 'The specimens shall be taken from 1/4 thickness pocition in the p3cte. The long axis of the specimen shall be t:.in.11 1 in t.h. s plat.a rolling direc tion. The npoc! : m- re'*- -

                                                                          <hii ) k ,m pendi<:ular to the s                                       original ; . Le t.u . ! .. ::u: , :. e - :> be cont.colled by the orica ; . ti u. o- i n.       .<f .m ". ings on the specir en blanks.                                                            .

6.2 Specimen Pn.paration , 6.2.1 Power bar.d saw two (2) 2 1/2" x 5 5/8" x 12" sub-blocks and stencil them 13!C-A and 1010 B as indicated on Drawing T-6. 6.2.2 Finish machinc entire sido to bc marked and stcncil cach specimen blank location an shown on Drawing T-7 beforo dividing the nub-blocks into slabs and spaci:.cn ( blanks. The top of the markirn symbols are perpendicular to the original plate surface; therefore, the top of the three digits wi11 indicate the not.ched side of the specimen as shown in Detail D. 6.2.3 Power band saw the Bl:C-A sub-block into ninctcen (19)

     .                                      1/2" x 2 1/2" x 5 5/8" slabs, as indicated by Detail A.

6.2.4 Power band saw the P!:C-B sub-bicek into 1/2" x 2 1/2" x 5 5/8" sjabs, as indicated by Detail D. The remainder of this sub-block shall be stored.

                                                   .~

e

                                                                            } SURVEILLANCE TEST            21j
  ' [',r--) " '"~ 7   a     .
                                          *{                               (
                     ,j       V                                                SPECIMEN 'REPARA"'m!-       .
                             .J-                                               PLAN ou t. a  _,J g1; GAL PLFcTnIr ro*mANv                           "1JKM'         STP-3 F...o uc t ,, ,BQI_ LING h'ATER NUCLEAP. REACTOR                        PAGENO.      4   Cr   15 OATE         7-21-69 A 55EM DL Y __                '

ncvision so. 1 oc5cumrion --

  .q 6.2.5    Machine both 5 5/8" x 2 1/2" nyrfaces of each' slab to a thickness of 0.400" +.005-0 t

6.2.6 Power band.saw the 2 1/2" x 0.400" x 5 5/8" slabs into specimen blanks as shown in Detail C. 6.2.7 Nachine both 2 1/2" x 0.400" nyrfaces of each specimen ' to a thickness of 0.400" +.005-0

                                                                         ,    as indicated in Detail D.

6.2.8 Place fifty-three (53) specimen blanks (2M1 thrnuck 2MJ_ for 68-2471; 361,,through 3XJ,,for 65-2472; SL6 through SMT and JAl through JAY for 68-24F3) in separate serially marked envelopes and prepare them in accordance with the following paragraphs 6.2.8.1 through 6.2.8.7. A 6.2.8.1 Machinc and finish grind the 2 1/2" x 0.400" surfaces to a thickness of .394", as i'ndicated

  • in Detail E. ' Place cach blank in its serially marked individual envelope for further processing.

6.2.8.2 Mark with pan, an arrow on the notch side of the specir.1cn blanh (indicating the proper mark orientation). See Detail E. . l 6.2.8.3 Finish unmarked end of each specimen in , accordance uith Detail F, and return speci.en ' j to its' envelope, 6.2.8.4 Remark the designated marked end of cach finished specimen with its corresponding envelope serial number if its original mark is destroyed. Start with the lowest marked envelope and proceed srrially. l 6.2.8.5 Finish the specimen in accordance with Detail F.

                          .                                                                                  d

1 1

                                                                                 '                                   <l y                   

( SUPNCILLAMCE TEST I

          ,I          . i,                                                             SPFCIMP.M PREPARATIOM_         j "w [ -,d                                                                      PIAN                           !

tI g , e .y , . ,3;p:g 3 g g g g g,.gpAny .. .uuont 0 0 i . i .n o STP-3 3 buonoci ._.I;oILTnc_,tyarn ytcr m nr w mn. _ P^c.c wo, 5 orl5 i m r.e.n in. y - DATc 7-21-69 ' nc.,cnir Ticu Revision NO. 1 um. m- .. .. . i 6.2.8.6 1001 dimensionally inspect, clean and dip each specimen in " Dip Scal Plastic" DS 300 Clear, or equal. 6.2.8.7 Packagc fi f ty-three (53) specimens in accord o,cc with chip'nort instructions, Paragraph 2.0 cf this plan. The specimens shall be nent to i.cncral Electric's Plant at San Jose, California. 6.2.9 Extra specimens are to be placed in serially marked envelopes and reteined by Cl3sI for possible dimensional rejects. In the casos where ext.ra specimens are not provided, dimensional reject.n will be discarded and their mark numbers vill ha u:;cd on replacement specimenn taken from the c': r ce material . Care must be takcr. to incrc proper roecimen orientation and source. s 7.0  % , m'T AL T ' :S U.E' 91 " *:S 7.1 Spccim.o Rt.;alre 2l s 7.1.1 Prepare the tenulle cpecimens in accordance with Drawingc T-6 and T-8. 7.1.2 The specitncns shall be tat.en from 1/4 thickness positionn in the plate. Thu long axes of the specimens shall be parallcl to the plate rolling direction. 7.2 Specimen Preparation 7.2.1 Power band saw onn (1) 3 1/2" x 5 5/8" x 12" sub-block and stencil it DMT as indicat.ed on Drawing T-6. 7.2.2 Stencil cach specimen blank location as shown on Drawing T-8 beforo dividinq the sub-block into slabs N. and specimen blar.hs. 7.2.3 Power band saw the 3 1/2" x 5 5/8" x 12" sub-block into ten (10) 5/8" x 3 1/2" x 5 5/8" slabs, as indicated by Detail A. 4

w. ,

1

I"'/ 7 G ' (~

                                                                                .I SURVEILLT.NCE TEST SPECIMEN PRCPARATr.,N
          % ,___J                                                                    PLAN                                      l Outn .,____GE:EllAL FTIcTP Tc co'ipMy                          "OVu?n"         STP-3                ,
       >\ ,suct            , BO_I_ LING WATER NUCLEAR REACTOR                     PAGENO.      6    Or 15                     I assewouv                                                                   oATE           7-21-69                  ,l DESCMPTION                                                                   REVi$10N NO.

+ - ,-um - I (

  • 7.2.4 Power band saw the ten (10) 5/8" x 3 1/2" x.5 5/8" slabs into specimen blanks, as shown in Detail B.

7.2.5 Place fourteen .(14) specimen blanks (351 throu,gh 35K g' fo,r 68-2471; 5J1 through SJK for 68-2472; 625 through

       \                                  62T for 68-2473) in separate serially marked envelopes and prepare them in accordance with the following
                                         ' paragraphs 7.2.5.1 through 7.2.5.4.

7.2.5.1 Finish each specimen in accordance with 5 Detail D, Drawing T-8 and return it to its envelopo. .

                                                                                                                         ?

7.2.5.2 Romark one end of cach finished specimen I: with its corresponding onvelope serial nu-ber

 .                                                      if its original mark is destroyed. Start with the lowest marked envelope and proceed                       2 serially.                                                         '
          '                                                                                                               5 7.2.5.3       100% dimensionally inspect, clean and dip                        j each specimen in " Dip Seal Plastic"'DS 300 Clear, or equal.                                                 J: -

7.2.5.4 Package fourteen (14) specimens in accordance , with shipment instructions, Paragraph 2.0 of this plan. The specimens shall be sent , to General Electric's Plant at San Jose, i: California. 7.2.6 Extra specimens arc to be placed in serially marked envolopes and retained by CD&I for possible dimensional rejects. In the cases where extra specimens a're not

                                         ' furnished, dimensional rejects will be discarded and their mark numbers will be used on replacement specimens taken from the extra material provided.

Care must be taken to insure proper specimen

           -                             orientation and source.

l . i h l

 ~.                                           _ = - - _                      - ...- ~ .- -.                        -     - - . - . - . ~ - , ~                .

[ (' SURVEI LLA'.'CE TIST

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o~l .'Il r sg SPECIMTT PPEFAP).TIo;; d PLAN-um". .C CILH AL ELI'cTrTc COMPA"Y ""2SfN' CTP-3 . psonuct _ _ 13OILTHC 11ATrn wctr:An pgACTog PAGE NO. 7 or 15 Assrvoty . oATc 7-21-69 otsenirrioN -- nevisiow wo._1 a (,-rw , 0.0 WELD & llEAT AFFECTED ZONE MATERIAL 8.1 The wold and heat affected zone metal shall be taken from Plate marked (2608), cut from shcIl Plate marked (301), h with a contral wold which is similar to the reactor vessel longitudinal weld. (Sce Drawing T-5). 8.2 Test Pl' ate (2608), Drawing T-5, shall be given a stress relief in accordance with Paragraph 1.4 to simulate the stress relief of the Core Region Platos (301 and 351). X-rays of the weld must be sont to the customer (See Paragraph 2.3). - 9.0 WELDED TEST PLATE S!!IPPED TO GENERAL ELECTRIC 9.1 Stencil wolded Test Plato marked (2609) cut from shell Plate marked (301) as follows: (Use symbols at least 1/4" high) s G.E. UELD METAL MILL ROLLING DIRI:CTIOO - HEAT NUMBER SLAD UUMDER CONTRACT NUMBER Documents shall be supplied to General Uloctric showing the source, chemistry and heat treatment of the plate. 9.2 The abovo welded test Plate marked (2609)-shall be shipped to Gonoral Electric in accordance with Paragraph 2.0. 10.0 WELDMD TEST PLATI: USED DY CHICAGO BRIDGE & IRO!! TO mal'E WELD AND llEAT AFFECTED 7,ONE MCCl!ANICAL TEST SPECIMUN", 10.1 Plate (2G00) cu t from shcIl P] ate (301) shall be used to make the Mechanical Test Specimens required by Drawings T-9 through T-13. 10.2 Test Plate (2608) shall be cut into four (4) control blocks

             ,                     as' indicated on Drawing T-9.                                     (Stoncil'all excess material s                           and control blocks as indicated) 4.

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           \.   ,cuen                GJH{!)l'AL ELECTRIC COMPANY                                   92vVEN'           STP-3 encoucT           ,

BOILING WATER NUCLEAR RCACTOR pace No. 8 or 15 asscu nt y , care 7-21-69

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otsemptioN __ acvislON NO. 1 2 11.0 WELD RETAL CHARPY SPECIMENS (WC) 11.1 Specimen Requirements b 11.1.1 Prepare the Charpy Impact Specimens in accordance with Drawings T-9 and T-10. 11.1.2

                                                ~

The long axis of the npocimen shall be perpendicular to the wcld direction and parallel to the plate surface, with the middle of the specimen at the mid-plane of the weld as shown in Drawing T-10.

       .                                                The notch shall be perpendicular to the plate surface..

11.2 Specimen Preparation 11.2.1 Power band saw the central weld section 5 1/2" x 5 5/8" x 2 1/2", marked WC, with the weld center

     . s plane at the center of the ucld block indicated in Detail B, Drawing T-9.

11,2.2 Finish machino enLiro $J00 Lo 1.c marked and stencil each specim.a blank location as shown on Drawing T-10 beforc dividing Lho central wcld section into slabs and specimen blanks. The top of the marking symbols are on a lino l'orpendicular to the plate surface; therefore, the top of the thrco digits will indicate the notched side of the specimen as shown in Detail D, Drawing T-10. TilIS 1 VERY IMPORTANT. 11.2.3 Power band saw the 5 1.2" x 5 5/8" x 2 1/2" ucid control block (WC) into nino (9) 1/2" x 5 5/8" x 2 1/2" slabs, 11.2.4 Machine both 5 5/8" x 2 1/2" surfaces of each slab to get a thickness of 0.400" +3005". (Drawing T-10,. Detail D). . 11.2.5 Power band saw the nine (9) 5 5/8" x 0.400" x 2 1/2" slabs into specimen blanks. 11.2.6 Machine both 2 1/2" x 0.400" surfaces of each

                                                                                                              .005", as specimen to a thickness of 0.400" +9 indicated in. Detail C, Drawing T-lD
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  • T* STP-3 PHonuct gQ1Lj,];1G_lGTER NUci . 3 P3c'*'O R PAGENO, 9 OF 15 ASSEM OL Y
  • OATE 7-21-69 DESCRIPTION REVi$lON NO. 1 a

11.2.7 P,1, ace fifty-threc ( 5,3 ) specimen (2P'l through 3AK through 3b, 6-for blanks68-2472; 2,UJ for 60-24,7,1; SMU through SUD for 68-2473) in separate serially marked envelopes and prepare them in accordance with the following Paragraphs 11.2.7.1 through ' 11.2.7.6. 11.2.7.1 Machine and finish grind the 2 1/2" x 0.400" surfaces to a thickness of .394", as indicated in Detail D, Drawing T-10. Place cach blank in its serially marked individual.cnvelope for further processing. 11.2,7.2 rinish grind the unmarked end as indicated 1 in Detail D, Draving T-10. 11.2.7.3 Mark with pen, an arrow on the notched side of the specimen blank per Detail D, Drawine

i
    'q                                                       T-10. Remark the designated end of each blank with its corresponding envelope number if its original mark is destroyed.

Use the arrow to ori.ent1the mark number properly. , 11.2.7.4 rinish the specimen in accordance with Dctail E, Drawing T-10. , 11,2.7.5 100% dimonnionally inspcet, clean and dip the specimens in " Dip Seal Plastic" DS 300 Clear.. or equal, for protcetion against runt and mechanical damage, i 11.2.7.6 Package fifty-threc_(53) specimens in accordance with shipment instructions, Paragraph 2.0 of thin plan. The specimens shall be sont-to General Electric at San Jose, California. kw  %.

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RcvisioN No. 1 ocscniPTioN . C4 11.2.8 Extra specimens are to be placed in serially marked envelopes and retained by CD&I for possible dimensional rejects. In the cases where extra specimens are not furnished, dimensional rejects will be discarded and their mark numbers will be used on replacement specimens taken from the extra material provided.

                               . Care must be taken to insure proper specimen orientation and source.

12.0 WELD METAL TENSILE SPECIMEMS_ 12.1 Specimen Requirements . 12.1.1 Prepare the weld metal tensile specimens in accordance with Drawings T-9 and T-11. 12.1.2 The long axes of the specimens shall be parallel to the length of the wcld and parallel to the top surface ( of the plate. T h .: guye ler.uth be of wcld deposii wetal only. of the specimens shaJ.1 The threaded ends of the specimens m y,inelode base metal. 12.2 Specimen Preparation 12.2.1 Power band saw the contral wcld section 14 3/8" x 5/8" x 5 5/8" per Detail A, Drawing T-9. 12.2.2 Mark the top of the contral weld section sub-block WT (1.4 3/8" x 5/8" x 5 5/8") with 4 arrows to indicate the location of the mark number and power band saw it into four (4) 3 1/2" x 5/G' x 5 5/8" slabs per Detail A, Drawing T-ll. 12.2.3 Stencil cach specimen blank location per Detail B, Drawing T-ll, beforc dividing the slabs into specimen blanks. 12.2.4 Power band saw the four (4) slabs into specimen blanks as indicated in Dctail B, Drawing T-ll, and place each fn its envolepc.

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SPECIl'E : PP.EPARATICN

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    .       .stuoty                        -

REVi$lON NO. I oEscNiaTiON s (\ 12.2.5 Place thirtcen ,(13) specimen blanks (321 through 3'dJ for 68-2471; 5JM through 5KA for 68-2472; 62U through 63D for 68-2473) in separate scrially marked envelopes and prepare them in accordance with the following Paragraphs 12.2.5.1 through 12.2.5.5. ( 12.2.5.1 Mark with pen, an arrow on the top side of the specimen blank (indicating the proper marking orientation - see Detail C,

                                             .                             Drawing T-11) and finish the blank ends to obtain the proper specimen length.

(See Detail- D, Drawing T-ll). 12.2.5.2 Remark the designated marked end of each specimen with its corresponding envelope serial number if its original mark is destroyec Uce the marked arrow to orient the mark number pr.rerly. . Start with the lowest ( marked envelope %d proceed serially. 12.2.5.3 Fininh ench specir.+: in accordance with Detail D, Drawing T-ll. 12.2.5.4 100% dimensionally inspect, clean and dip each specimen in " Dip Seal Plastic" DS 300 Clear, or equal. 12.2.6 Extra specimens are to be placed in serially marked envelopes and retained by CB&I for possible dimensional rejects. In the cases where extra specimens are not furnished, dimensional rejects will be discarded and ( ' their mark numbers will be used on replacement specimens taken f rom the extra material provided. Care must be taken to insure proper specimen orientation and sourcc. (

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      . T o u t. '*       G D rRAL et"cTRTr cmtpA':Y P4cE NO. 12   or 15 PAOouCT                 POILING WATER NUCLEAR REACTOR                                 7-21-69 oArc A 5$C M OL Y ncvisio n wo. 1 a .senseTioN                                                                                         ~.

13.0 llr.AT AFFECTED ZONE CHARPY SPECIMENS 13.1 Specimen Requirements 13.1.1 Prepare the Charpy Impact Specimens _in accordance with Drawings T-9 and T-12. 13.1.2 The long axis of the specimen shall be perpendicular to the length of the wcid and parallel to the top surface of the plate. The radius of the notch of the specimen shall be at the edge of the weld. The axis of the notch shall be perpendicular to the original plate surface. The notch orientation shall be controllbd by the marking orientation. 13.2 Specimen Preparation 13.2.1 Power band saw the central weld section 5 1/2" x s 5 5/8" x 4", marked HAC, por Detail C, Drawing T-9.

                                                                               ~

13.2.2 Stoncil each specimen blank location before dividing the contral weld section into slabs and specinen blanks. The top of the marking symbols are on a line perpendicular to the plate surface and thus the top of the three digits will indicate theDrawing notched side of the specimen as nhown in Detail D, T-12. THIS IS VERY IMPORTANT. to locate 13.2.3 Lightly acid etch both 5 5/8" x 4" surfaces the heat affected zone of cach specimen blank to be made from the slab. 13.2.4 Power band saw the 5 1/2" x 5 5/8" x 4" weld control block, marked (HAC), into seven (7) 1/2 " x 5 1/ 2 " x 4 " slabs, as shown in Detail A, Drawing T-12. i 13.2.5 Machineboth51/2"x4"surfgggsofcachslabto 0

   \                                    got a thickness of 0.400" [3             ,

13.2.6 Power band saw the seven (7) slabs into specimen blanks. 13.2.7 Machine both 4" x 0.400" surfaces of cach specimen to a thickness of 0.400" +0- .005", as indicated in Detail C, Drawing T-12. 4

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i SPECIMEN PREPARATION L% e PLAN
           *sTouta ,         [:f$;JugAr. Pr.Prmn Tr rn'tpANY                     "7 sew '           STP- 3 c.couct              noT r Tnn entra Muripan nnarmon                     pAos No.       13    or         15 A S SE M UL. Y                                                           DATE           7-21-69 oEsenmTioN                                                                A EV15 ton NO. 1 sC                            23.2.8 P1, ace fifty-threc (53) specimen,, blanks (2Y1 through 3,2J for 68-24~1; 3D7 through 3JY for 68-2472; 5UE through 624 for 68-2473) in separate serially marked envelopes and preparc them in accordance with Paragraphs 13.2.8.1 through 13.2.8.4.

13.2.8.1 Machine and finish grind the 4" x 0.400" surfacca to a thickness of .394", as indicated in Detail D, Drawing T-12. Place cach blank in its serially marked envelope for further processing. 13.2.8.2 Mark with p'en, an arrow on the notched side of the specimen to indicate the location df the marking series and remark the designated end of each blank with its corresponding onvelope mark number if its original mark is destroyed. Use the marked arrow to orient the mark number A properly. . 13.2.8.3 Pipich the pe. i:rc n in accordance with Detail E, Drawing T-12. 13.2.8.4 100% dimensionally inspcet, clean and dip the specimens in " Dip Seal Plastic" DS 300-Clear, or equal, for protection against rust and mechanical damage. Package fifty-threc (53) spccinens in accordance with shipment instructions, Paragraph 2.0  ! of-this plan. The specimens shall be sent to Gonoral Electric's plant at San Jose, ( California. 1 13.2.9 Extra specimens are to be placed in serially marked envelopes and retained by CD&1.for possible dimensional rejects. In the cases where extra specimens are not furnished, dimensional rejects will be discarded and their mark-numbers will be used on replacement specimens taken from the extra material provided. Care must be taken to insure proper I specimen orientation and sourec. l 1

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TN Y ~i SURVEILLANCE TEST - SPECIMEN PP. EPA!u7r g b2- -- __m PLAN

          'OMi " _    GM;;; PAL FLECTnTc rnW Any                   "JMOT          STP-3 D AGE NO. 14   OF 15 e ,.so uc t    ___ Hor tTMn MATrn mrr. van nr Ar mn            oArg         7-21-69 45scuot y ,

DESCRIPTION REVISION NO.1 of \ 14.0 HEAT AFFECTED ZONE TENSILE 3PECIMENS 14.1 Specimen Requirements YA 14.1.1 Prepare .the Heat Affected Zone Tensile Specimens in accordance with Drawings T-9 and T-13. 14.1.2 The long axes of the specimens shall be perpendicular to the length of the wold and parallel to the top surface of the plate. The center of the specimen shall be in the Heat Affected Zonc adjacent to the edge of the weld metal. 14.2 Specimen Preparation 14.2.1 Power band saw the 2 7/8" x 5 5/8" x 5" central weld section, marked (HAT), withithe wcld center plane located as indicated in Detail D, Drawing T-9. Stencil the sub-block (HAT) as shown on Drawing T-9. 14.2.2 Stencil each specimen blank l'ocation as shown on Drawing T-13 before dividing the sub-block into slabs and specimen blanks. 14.2.3 Lightly acid etch both 5 5/8" x 5" surfaces to locate the Heat Affected Zone of each specimen blank to be mado from the slab. 14.2.4 Power band saw six (6) 5/8" x 2 7/8" x 5" slabs as shown in Detail A, Drawing T-13. i

    '                   14.2.5    Power band saw specimen blanks from the six (6) slabs as indicated in Detail B, Drawing T-13.

14.2.6 Place thirtoon (13) specimen blanks (351 through 35J for 68-2471; SND through SL3 for 68-2472: 63E through 644 for 68-2473) in separate serially marked envelopes and preparc them in accordance with Paragraphs 14.2.6.1 through 14.2.6.5. I I

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4 SURVCILLA'.JCE TEST

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14.2.6.1 Mark uith pen, an arrow on the top side of I the specimen blank to indicate the proper marking orientation and finish the blank ends obtaining the proper specimen length.

   ~                                             (See Drawing T-13) .

14.2.6.2 Remark thc'dosignated marked end of each specimen with its corresponding envelope serial number, if its original mark is destroyed. Start with the lowest marked envelope and proceed serially. 14.2.6.3 Finish each specimen in accordance with

                                                 ' Detail E, Drawing T-13.

14.2.6.4 100% dimensionally inspect, clean and dip. each specimen in " Dip Seal Plastic" DS 300 Clear, or equal. 14.2.6.5 Package thirtoon (13) specimens in accordance with shipment instructions, Paragraph 2.0, of this plan. The specimens shall be sent to General Electric's plant at San Jose, California. 14.2.7 Extra specimens are to be placed in serially marked envelopes and retained by CB&I for possible dimensional rejects. In the cases where extra specimens are not furnished, dimensional rejects will be discarded and their mark numbers will be used on replacement specimen taken from the extra material provided. Care must be taken to insure proper orientation and source.

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