Text

Unit 1, Form a - Application for Nondomestic Permit Under Missouri Clean Water Law
	ML24354A190
Person / Time
Site:	Callaway
Issue date:	12/19/2024
From:	; Ameren Missouri, Union Electric Co
To:	; Office of Nuclear Reactor Regulation
Shared Package
ML24354A188	List: ML24354A190; ULNRC-06912, Unit 1, NPDES Permit Renewal Application;
References
	ULNRC-06912
	Download: ML24354A190 (1)
	v • d • e

Attachment to ULNRC-06912 109 Pages to follow Form A - Application for Nondomestic Permit Under Missouri Clean Water Law

I-rl L

({/j MISSOURI DEPARTMENT OF NATURAL RESOURCES WATER PROTECTION PROGRAM FORM A - APPLICATION FOR NONDOMESTIC PERMIT UNDER MISSOURI CLEAN WATER LAW FORAGENCY USE ONLY CHECK NUMBER DATE RECEIVED FEE SUBMITTED PLEASE READ ALL THE ACCOMPANYING INSTRUCTIONS BEFORE COMPLETING THIS FORM.

SUBMITTAL OF AN INCOMPLETE APPLICATION MAY RESULT IN THE APPLICATION BEING RETURNED.

IF YOUR FACILITY IS ELIGIBLE FOR A NO EXPOSURE EXEMPTION:

Fill out the No Exposure Certification Form (Mo 780-2828): https://dnr.mo.qov/forms/780-2828-f.pdf

1. REASON FOR APPLICATION:

Va.

nb nc.

!d This facility is now in operation under Missouri State Operating Permit (permit) 1yg - 0098001, is submitting an application for renewal, and there is p proposed increase in design wastewater flow. Annual fees will be paid when invoiced and there is no additional permit fee required for renewal.

This facility is now in operation under permit MO -

is submitting an application for renewal, and there is a proposed increase in design wastewater flow. Antidegradation Review may be required. Annual fees will be paid when invoiced and there is no additional permit fee required for renewal.

This is a facility submitting an application for a new permit (for a new facility). Antidegradation Review may be required. New permit fee is required.

ThisfacilityisnowinoperationunderMissouriStateoperatingPermit(permit)Mo_-andisrequestinga modification to the permit. Antidegradation Review may be required. Modification fee is required.

2. FACILITY NAME Ameren Missouri Callaway Energy Center TELEPHONF NUMBER WITH AREA CODE 31 4-31 5-3035 ADDRESS (PHYSICAL) 8315 County Rd 459 ctry Steedman STATE MO ZIP CODE 65251

3. OWNER NAME Union Electric Company d/b/a Ameren Missouri TELEPHONE NUMBER WITH AREA CODE 31 4-31 5-3035 EMAIL ADDRESS cgiesmann@ameren.com ADDRESS (I\i]AILING) 1901 ChouteauAveMC602 CITY St. Louis STATE MO ZIP CODE 63166-6'149

4. CONTINUING AUTHORIW NAME SAME AS OWNER TELEPHONE NUMBER WTH AREA CODE EMAIL ADDRESS ADDRESS (MAILING) ctry STATE ZIP CODE

5. OPERATOR CERTIFICATION NAME SAME AS OWNER CERTIFICATE NUMBER TELEPHONE NUMBER WITH AREA OOIJE ADDRESS (MAILING)

CITY SIAII ZIP CODE

6. FACILITY CONTACT NAME Timothy Neterer TITLE Chemistry Manager TELEPHONE NUMBER WTH AREA CODE 314-21 0-3835 E-MAIL ADDRESS tneterer@ameren.com

7. DOWNSTREAM LANDOWNER(S) Attach additionalsheets as necessary NAIVIE Michael J&JobyLBrower ADDRESS 10200 State Route 94 CITY Portland STATE MO ZIP CODL 65067

8. ADDITIONAL FACILITY INFORMATION 8.1 Legal Description of Outfalls. (Attach additional sheets if necessary.)

For Universal Transverse Mercator (UTM), use Zone 15 North referenced to North American Datum 1983 (NAD83) 001 1/4 1/4 Sec T

R County UTM Coordinates Easting (X):

Northing (Y):

002 1/4 1/4 Sec T

R County UTM Coordinates Easting (X):

Northing (Y):

003 1/4 1/4 Sec T

R County UTM Coordinates Easting (X):

Northing (Y):

004 1/4 1/4 Sec T

R County UTM Coordinates Easting (X):

Northing (Y):

Include all subsurface discharges and underground injection systems for permit consideration.

8.2 Primary Standard Industrial Classification (SIC) and Facility North American Industrial Classification System (NAICS) Codes.

Primary SIC and NAICS SIC and NAICS SIC and NAICS SIC and NAICS

9. ADDITIONAL FORMS AND MAPS NECESSARY TO COMPLETE THIS APPLICATION A.

Is this permit for a manufacturing, commercial, mining, solid/hazardous waste, or silviculture facility? YES NO If yes, complete Form C.

B.

Is the facility considered a Primary Industry under EPA guidelines (40 CFR Part 122, Appendix A) : YES NO If yes, complete Forms C and D.

C.

Is wastewater land applied?

YES NO If yes, complete Form I.

D.

Are sludge, biosolids, ash, or residuals generated, treated, stored, or land applied?

YES NO If yes, complete Form R.

E.

Have you received or applied for any permit or construction approval under the CWA or any other YES NO environmental regulatory authority?

If yes, please include a list of all permits or approvals for this facility:

Environmental Permits for this facility:__________________________________________________

F.

Do you use cooling water in your operations at this facility?

YES NO If yes, please indicate the source of the water: ___________________________________________

G.

Attach a map showing all outfalls and the receiving stream at 1 = 2,000 scale.

10. ELECTRONIC DISCHARGE MONITORING REPORT (eDMR) SUBMISSION SYSTEM Per 40 CFR Part 127 National Pollutant Discharge Elimination System (NPDES) Electronic Reporting Rule, reporting of effluent limits and monitoring shall be submitted by the permittee via an electronic system to ensure timely, complete, accurate, and nationally consistent set of data. One of the following must be checked in order for this application to be considered complete. Please visit https://dnr.mo.gov/env/wpp/edmr.htmfor information on the Departments eDMR system and how to register.

- I will register an account online to participate in the Departments eDMR system through the Missouri Gateway for Environmental Management (MoGEM) before any reporting is due, in compliance with the Electronic Reporting Rule.

- I have already registered an account online to participate in the Departments eDMR system through MoGEM.

- I have submitted a written request for a waiver from electronic reporting. See instructions for further information regarding waivers.

- The permit I am applying for does not require the submission of discharge monitoring reports.

MO 780-1479 (04-21) 6(($77$&+('6+((7 4911 221113

Missouri River

1I. FEES Permit fees may be paid by attaching a check, or online by credit card or eCheck through the JetPay system. Use the URL provided to access JetPay and make an online payment:

For new permits: https://maoic.collectorsolutions.com/maqic-ui/payments/mo-natural-resources/591

12. CERTIFICATION I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.

NAME AND OFFICIAL TITLE (TYPE OR PRINT)

Fadi Diya, Senior Vice Pres. & Chief Nuclear Operator TELEPHONE NUMBER WTH AREA CODE 573-823-6531 SIGNATURE fu^ffi DATE SIGNED t2ltl lzozY

8.1 Legal Description of Outfalls 001 NE 1/4 NE 1/4 Sec 14 T 46N R 8W Callaway County 002 NW 1/4 NW 1/4 Sec 13 T 46N R 8W Callaway County 003 SW 1/4 SW 1/4 Sec 13 T 46N R 8W Callaway County 007 SW 1/4 SW 1/4 Sec 13 T 46N R 8W Callaway County 009 NW 1/4 NW 1/4 Sec 5 T 46N R 8W Callaway County 010 SW 1/4 SW 1/4 Sec 12 T 46N R 8W Callaway County 011 NW 1/4 SE 1/4 Sec 12 T 46N R 8W Callaway County 012 NE 1/4 NE 1/4 Sec 11 T 46N R 8W Callaway County 014 NE 1/4 NE 1/4 Sec 14 T 46N R 8W Callaway County 015 SE 1/4 SE 1/4 Sec 11 T 46N R 8W Callaway County 016 NW 1/4 NW 1/4 Sec 13 T 46N R 8W Callaway County 017 SE 1/4 NE 1/4 Sec 14 T 46N R 8W Callaway County 018 SE 1/4 NE 1/4 Sec 14 T46N R 8W Callaway County 100 NW 1/4 NW 1/4 Sec 5 T 45N R7W Callaway County Note: The location of Outfalls 002 and 016 is described at the connection to the plant discharge line. The location of Outfall 001 is described from the Discharge Monitor Tanks.

L Fv1 MISSOURI DEPARTMENT OF NATURAL RESOURCES WATER PROTECTION PROGRAM, WATER POLLUTION CONTROL BRANCH FORM C - APPLICATION FOR DISCHARGE PERMIT _ MANUFACTURING, COMMERCIAL, MINING, SILVICULTURE OPERATIONS, AND STORMWATER GENERAL INFORMATION (PLEASE SEE INSTRUCTIONS) 1.0 NAME OF FACILITY Ameren Missouri Callaway Energy Center

,1,1 THIS FACILITY IS OPERATING UNDER MISSOURI STATE OPERATING PERMIT (MSOP) NUMBER:

MO-0098001 1.2 IS THIS A NEW FACILITY? PROVIDE CONSTRUCTION PERMIT (CP) NUMBER IF APPLICABLE.

1.3 Describe the nature of the business, in detail. ldentify the goods and services provided by the business. lnclude descriptions of all raw, intermediate, final products, byproducts, or waste products used in the production or manufacturing process, stored outdoors, loaded or transferred and any other pertinent information for potential sources of wastewater or stormwater discharges.

Steam Electric Power Plant (Nuclear)

FLOWS, TYPE, AND FREQUENCY 2.0 Attach a line drawing showing the water flow through the facility. lndicate sources of intake water, operations contributing wastewater to the effluent, and treatment units labeled to correspond to the more detailed descriptions in item B. Construct a water balance on the line drawing by showing average and maximum flows between intakes, operations, treatment units, evaporation, public sewers, and outfalls. lf a water balance cannot by determined (e.g, for certain mining activities), provide a pictorial description of the nature and amount of any sources of water and any collection or treatment measures.

2.1 For each outfall (1) below, provide: (2) a description of all operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water, stormwater runoff, and any other process or non-process wastewater, (3) the average flow and maximum flow (put max in parentheses) contributed by each operation and the sum of those operations, (4) the treatment received by the wastewater, and (5) the treatment type code. Continue on additional sheets if necessary.

'1. OUTFALL NO

2. OPERATION(S) CONTRIBUTING FLOW; INCLUDE ALL PROCESSES AND SUB PROCESSES AT EACH OUTFALL

3. AVERAGE FLOWAND (MAXIMUM FLOW), INCLUDE UNITS.

4. TREATMENT DESCRIPTION

5. TREATMENT CODES FROM TABLE A 001 Radwaste Treatment System*

0.075 (0.093) MGD Discharge 2J,1Q,2K,4A

1) Boron Recycle 0.001

2) Equipment Drains 0.0002 3)Primary Floor Drains 0.0013 4)Laundry/Hot Shower 0.0002 5)Polisher Regen Waste 0.008 6)Secondary Floor Drains 0.0093 7)Steam Generator Blowdown 0**

002 Cooling Tower Blowdown 6.41 (12.6) MGD Discharge 2F,44 003 Water Treatment Plant Waste**

0.36 (1.6) MGD Sedimentation 1U,4C Attach additional pages if necessary MO 780-1s14 (02-19)

Page I of 13

MO 780-1514 (02-19)

Page 2 of 13 2.2 INTERMITTENT DISCHARGES Except for stormwater runoff, leaks, or spills, are any of the discharges described in items 2.0 or 2.1 intermittent or seasonal?

Yes (complete the following table)

No (go to section 2.3)

1.

OUTFALL NUMBER

2. OPERATION(S) CONTRIBUTING FLOW

3. FREQUENCY

4. FLOW C. DURATION (in days)

A. FLOW RATE (in mgd)

B. TOTAL VOLUME (specify with units)

A. DAYS PER WEEK (specify average)

B. MONTHS PER YEAR (specify average)

1. MAXIMUM DAILY

2. LONG TERM AVERAGE

4. LONG TERM DAILY

3. MAXIMUM AVERAGE 2.3 PRODUCTION A. Does an effluent limitation guideline (ELG) promulgated by EPA under section 304 of the Clean Water Act apply to your facility? Indicate the part and subparts applicable.

Yes 40 CFR_________

Subpart(s) ________

No (go to section 2.5)

B. Are the limitations in the effluent guideline(s) expressed in terms of production (or other measure of operation)? Describe in C below.

Yes (complete C.)

No (go to section 2.5)

C. If you answered yes to B, list the quantity representing an actual measurement of your maximum level of production, expressed in the terms and units used in the applicable effluent guideline and indicate the affected outfalls.

A. OUTFALL(S)

B. QUANTITY PER DAY C. UNITS OF MEASURE D. OPERATION, PRODUCT, MATERIAL, ETC.

(specify) 2.4 IMPROVEMENTS A. Are you required by any federal, state, or local authority to meet any implementation schedule for the construction, upgrading, or operation of wastewater treatment equipment or practices or any other environmental programs which may affect the discharges described in this application? This includes, but is not limited to, permit conditions, administrative or enforcement orders, enforcement compliance schedule letters, stipulations, court orders, and grant or loan conditions.

Yes (complete the following table)

No (go to 2.6)

1. IDENTIFICATION OF CONDITION, AGREEMENT, ETC.

2. AFFECTED OUTFALLS

3. BRIEF DESCRIPTION OF PROJECT

4. FINAL COMPLIANCE DATE A. REQUIRED B. PROJECTED B.

Optional: provide below or attach additional sheets describing water pollution control programs or other environmental projects which may affect discharges. Indicate whether each program is underway or planned, and indicate actual or planned schedules for construction. This may include proposed bmp projects for stormwater.

12 0.075 Cooling Tower Bypass 3.2 1.3 12 016 Radwaste Treatment 3.5 001 52 D/yr 1.0 0.093 See Attachment C, Description of 180 D/yr Intermittent Flows

122

MO 780-1514 (02-19)

Page 3 of 13 2.5 SLUDGE MANAGEMENT Describe the removal of any industrial or domestic biosolids or sludges generated at your facility. Include names and contact information for any haulers used. Note the frequency, volume, and methods (incineration, landfilling, composting, etc) used. See Form A for additional forms which may need to be completed.

DATA COLLECTION AND REPORTING REQUIREMENTS FOR APPLICANTS 3.0 EFFLUENT (AND INTAKE) CHARACTERISTICS (SEE INSTRUCTIONS)

A. & B. See instructions before continuing - complete one Table 1 for each outfall (and intake) - annotate the outfall (intake) number or designation in the space provided. The facility is not required to complete intake data unless required by the department or rule.

C. Use the space below to list any pollutants listed in the instructions section 3.0 C. Table B which you know or have reason to believe is discharged or may be discharged from any outfall not listed in parts 3.0 A or B on Table 1. For every pollutant listed, briefly describe the reasons you believe it to be present and report any analytical data in your possession.

1. POLLUTANT

2. SOURCE

3. OUTFALL(S)

4. ANALYTICAL RESULTS (INCLUDE UNITS) 3.1 Whole Effluent Toxicity Testing A. To your knowledge, have any Whole Effluent Toxicity (WET) tests been performed on the facility discharges (or on receiving waters in relation to your discharge) within the last three years?

Yes (go to 3.1 B)

No (go to 3.2) 3.1 B Disclose wet testing conditions, including test duration (chronic or acute), the organisms tested, and the testing results. Provide any results of toxicity identification evaluations (TIE) or toxicity reduction evaluations (TRE) if applicable. Please indicate the conclusions of the test(s) including any pollutants identified as causing toxicity and steps the facility is taking to remedy the toxicity.

3.2 CONTRACT ANALYSIS INFORMATION Were any of the analyses reported herein, above, or on Table 1 performed by a contract laboratory or consulting firm?

Yes (list the name, address, telephone number, and pollutants analyzed by each laboratory or firm.)

No (go to 4.0)

A. LAB NAME B. ADDRESS C. TELEPHONE (area code and number)

D. POLLUTANTS ANALYZED (list or group)

Republic Waste Services hauls and landfills the sludge removed from the cooling tower basin. Normally 400 cubic yards of sludge is hauled off once every 36 months.

Asbestos Cooling Tower Fill material 002 Trace amounts Strontium, Zirconium Fission & Activation products 001 mg/day

Annual Whole Effluent Toxicity (WET) tests are conducted in accordance with permit conditions. The last test was conducted in October 2024 and a report was issued November 2024. All WET tests in the past 5 years have passed with no additional issues.

Pace Analytical Services, LLC 2231 W. Altorfer Drive Peoria, IL 61615 800-752-6651 See Attachment E, NPDES Sampling & Analysis

4.0 STORMWATER 4.1 Do you have industrial stormwater discharges from the site? lf so, attach a site map outlining drainage areas served by each outfall. lndicate the following attributes within each drainage area: pavement or other impervious surfaces; buildings; outdoor storage areas; material loading and unloading areas; outdoor industrial activities; structural stormwater control measures; hazardous waste treatment, storage, and disposal units; and wells or springs in the area.

OUTFALL NUMBER TOTAL AREA DRAINED (PROVTDE UNrTS)

TYPES OF SURFACES (VEGETATED, STONE, PAVED, ETC)

BEST MANAGEMENT PRACTICES EMPLOYED; INCLUDE STRUCTURAL BMPS AND TREATMENT DESIGN FLOW FOR BMPS DESCRIBE HOW FLOW IS MEASURED 010 108 acres Vegetated, Paved See Attachment A, Description of Outfalls 011 425 acres Vegetated, Paved See Attachment A, Description of Outfalls 012 87 acres Vegetated, Paved See Attachment A, Description of Outfalls 014 100 acres Vegetated, Paved See Attachment A, Description of Outfalls 015 60 acres Vegetated, Paved See Attachment A, Description of Outfalls 4.2 STORMWATER FLOWS Provide the date of sampling with the flows, and how the flows were estimated.

See Attachment E, NPDES Sampling & Analysis for full description SIGNATORY REQUIREMENTS 5.0 CERTIFICATION I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.

Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.

NAME AND OFFICIAL TITLE (TYPE OR PRINT)

Fadi Diya, Senior Vice President & Chief Nuclear Officer TELEPHONE NUMBER WTH AREA CODE 573-823-6531 SIGNATURE (SEE INSTRUCTIONS)

DATE SIGNEDtzl t1 lz a"\

rvlo 780-1514 (02-19)

Page 4 of 13

2.1 FLOWS, TYPE and FREQUENCY CONTINUED 2.1 For each outfall (1) below, provide: (2) a description of all operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water, stormwater runoff, and any other process or non-process wastewater,

1. OUTFALL NO.

2. OPERATION(S) CONTRIBUTING FLOW; INCLUDE ALL PROCESSES AND SUB PROCESSES AT EACH OUTFALL

3. AVERAGE FLOW AND (MAXIMUM FLOW), INCLUDE UNITS

4. TREATMENT DESCRIPTION

5. TREATMENT CODES FROM TABLE A 003 1)Clarifier Blowdown 0.33 Flocculation 1G

2) Carbon Filter Backwash 0.004 Filtration 1Q

3) Oily Waste 0.023 Separation XX

4) Makeup Demin Plant Waste 0.0072 Neutralization 2K 007 Sanitary Waste **

0.018 (0.050) MGD Sedimentation 3G 009 Intake Electric Heaters 0 (0.000) MGD Neutralization 2K, 4A 010 Storm Water Runoff 0.08(4.6) MGD Sedimentation 1U, 4A 011 Storm Water Runoff 0.31 (19.7) MGD Sedimentation 1U, 4A 012 Storm Water Runoff 0.06(6.6) MGD Sedimentation 1U, 4A 014 Storm Water Runoff 0.04 (4.8) MGD Sedimentation 1U, 4A 015 Storm Water Runoff 0.03 (2.8) MGD Sedimentation 1U, 4A 016 Cooling Tower Bypass

2.88 (14.40) MGD Discharge 4A 017 Ultimate Heat Sink Pond 0 (0)

No Discharge NA 018 Fire Protection Test Water 0.3 (0.039 MGD Sedimentation 1U, 4A 100 Mo River combined effluent 6.66(12.6) MGD Discharge 4A

Flow is intermittent. "Average daily" flow is reported. See Section 2.20 for average for days when discharging

- No discharge in past 30 years

2

[i

MO 780-1514 (02-19)

Page 5 of 13 SEE INSTRUCTIONS; PLEASE PRINT OR TYPE.

You may report some or all of this information on separate sheet (use similar format) instead of completing these pages.

FORM C TABLE 1 FOR 3.0 - ITEMS A AND B EFFLUENT (AND INTAKE) CHARACTERISTICS THIS OUTFALL IS:

OUTFALL NO.

3.0 PART A - You must provide the results of at least one analysis for every pollutant in Part A. Complete one table for each outfall or proposed outfall. See instructions.

1. POLLUTANT

2. VALUES

3. UNITS (specify if blank)

A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS A. Biochemical Oxygen Demand, 5-day (BOD5)

B. Chemical Oxygen Demand (COD)

C. Total Organic Carbon (TOC)

D. Total Suspended Solids (TSS)

E. Ammonia as N F. Flow VALUE VALUE VALUE MILLIONS OF GALLONS PER DAY (MGD)

G. Temperature (winter)

VALUE VALUE VALUE

°F H. Temperature (summer)

VALUE VALUE VALUE

°F I. pH MINIMUM MAXIMUM AVERAGE STANDARD UNITS (SU) 3.0 PART B - Mark X in column 2A for each pollutant you know or have reason to believe is present. Mark X in column 2B for each pollutant you believe to be absent. If you mark Column 2A for any pollutant, you must provide the results for at least one analysis for the pollutant. Complete one table for each outfall (intake). Provide results for additional parameters not listed here in Part 3.0 C.

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants A. Alkalinity (CaCO3)

MINIMUM MINIMUM MINIMUM B. Bromide (24959-67-9)

C. Chloride (16887-00-6)

D. Chlorine, Total Residual E. Color F. Conductivity F. Cyanide, Amenable to Chlorination Outfall 002 - Cooling Tower Blowdown 002

<10.0

<0.50 1

mg/L lbs/d 42 2.10 1

mg/L lbs/d 16 0.80 1

mg/L lbs/d 44 2.21 1

mg/L lbs/d

<0.10

<0.005 1

mg/L lbs/d 0.006 6.4 1,34 73.4 1

8.33 1

x 200 1

mg/L lbs/d x

<5.0

<0.25 1

mg/L lbs/d x

99 4.95 1

mg/L lbs/d x

0.10 0.005 1

mg/L lbs/d x

x x

<0.005

<0.005 1

mg/L lbs/d

MO 780-1514 (02-19)

Page 6 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants (Continued)

G. E. coli H. Fluoride (16984-48-8)

I. Nitrate plus Nitrate (as N)

J. Kjeldahl, Total (as N)

K. Nitrogen, Total Organic (as N)

L. Oil and Grease M. Phenols, Total N. Phosphorus (as P), Total (7723-14-0)

O. Sulfate (as SO4)

(14808-79-8)

P. Sulfide (as S)

Q. Sulfite (as SO3)

(14265-45-3)

R. Surfactants S. Trihalomethanes, Total Subpart 2 - Metals 1M. Aluminum, Total Recoverable (7429-90-5) 2M. Antimony, Total Recoverable (7440-36-9) 3M. Arsenic, Total Recoverable (7440-38-2) 4M. Barium, Total Recoverable (7440-39-3) 5M. Beryllium, Total Recoverable (7440-41-7) 6M. Boron, Total Recoverable (7440-42-8) 7M. Cadmium, Total Recoverable (7440-43-9) 8M. Chromium III Total Recoverable (16065-83-1) 9M. Chromium VI, Dissolved (18540-29-9) 10M. Cobalt, Total Recoverable (7440-48-4) x 96 4.8 1

mpn/100ml lbs/d x

1.55 0.07 1

mg/L lbs/d x

2.6 0.13 1

mg/L lbs/d x

1.8 0.09 1

mg/L lbs/d x

1.8 0.09 1

mg/L lbs/d x

<5.0

<5.0 1

mg/L lbs/d x

0.005

<0.05 1

mg/L lbs/d x

1.4 0.07 1

mg/L lbs/d x

130 6.5 1

mg/L lbs/d x

<2.0

<0.1 1

mg/L lbs/d x

<2.0

<0.1 1

mg/L lbs/d x

0.33 0.02 1

mg/L lbs/d x

1 mg/L lbs/d x

0.88 0.04 1

mg/L lbs/d x

<0.003

<0.003 1

mg/L lbs/d x

0.019

<0.003 1

mg/L lbs/d x

0.41 0.02 1

mg/L lbs/d x

<0.001

<0.001 1

mg/L lbs/d x

0.49 0.025 1

mg/L lbs/d x

<0.001

<0.001 1

mg/L lbs/d x

<5.0

<0.25 1

ug/L lbs/d x

<0.005

<0.025 1

mg/L lbs/d x

<0.002

<0.002 1

mg/L lbs/d

MO 780-1514 (02-19)

Page 7 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 2 - Metals (Continued) 11M. Copper, Total Recoverable (7440-50-8) 12M. Iron, Total Recoverable (7439-89-6) 13M. Lead, Total Recoverable (7439-92-1) 14M. Magnesium, Total Recoverable (7439-95-4) 15M. Manganese, Total Recoverable (7439-96-5) 16M. Mercury, Total Recoverable (7439-97-6) 17M. Methylmercury (22967926) 18M. Molybdenum, Total Recoverable (7439-98-7) 19M. Nickel, Total Recoverable (7440-02-0) 20M. Selenium, Total Recoverable (7782-49-2) 21M. Silver, Total Recoverable (7440-22-4) 22M. Thallium, Total Recoverable (7440-28-0) 23M. Tin, Total Recoverable (7440-31-5) 24M. Titanium, Total Recoverable (7440-32-6) 25M. Zinc, Total Recoverable (7440-66-6)

Subpart 3 - Radioactivity 1R. Alpha Total 2R. Beta Total 3R. Radium Total 4R. Radium 226 plus 228 Total x

0.019

<0.002 1

mg/L lbs/d x

1.1 0.06 1

mg/L lbs/d x

<0.001

<0.001 1

mg/L lbs/d x

110 5.5 1

mg/L lbs/d x

0.16 0.008 1

mg/L lbs/d x

<0.0002

<0.0002 1

mg/L lbs/d x

0.143 0.007 1

ng/L lbs/d x

0.015

<0.001 1

mg/L lbs/d x

0.013

<0.001 1

mg/L lbs/d x

0.011

<0.001 1

mg/L lbs/d x

<0.005

<0.001 1

mg/L lbs/d x

<0.001

<0.001 1

mg/L lbs/d x

<0.06

<0.003 1

mg/L lbs/d x

0.013

<0.001 1

mg/L lbs/d x

0.0096

<0.001 1

mg/L lbs/d x

1.62 1

pCi/L x

0.961 1

pCi/L x

x

MO 780-1514 (02-19)

Page 5 of 13 SEE INSTRUCTIONS; PLEASE PRINT OR TYPE.

You may report some or all of this information on separate sheet (use similar format) instead of completing these pages.

FORM C TABLE 1 FOR 3.0 - ITEMS A AND B EFFLUENT (AND INTAKE) CHARACTERISTICS THIS OUTFALL IS:

OUTFALL NO.

3.0 PART A - You must provide the results of at least one analysis for every pollutant in Part A. Complete one table for each outfall or proposed outfall. See instructions.

1. POLLUTANT

2. VALUES

3. UNITS (specify if blank)

A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS A. Biochemical Oxygen Demand, 5-day (BOD5)

B. Chemical Oxygen Demand (COD)

C. Total Organic Carbon (TOC)

D. Total Suspended Solids (TSS)

E. Ammonia as N F. Flow VALUE VALUE VALUE MILLIONS OF GALLONS PER DAY (MGD)

G. Temperature (winter)

VALUE VALUE VALUE

°F H. Temperature (summer)

VALUE VALUE VALUE

°F I. pH MINIMUM MAXIMUM AVERAGE STANDARD UNITS (SU) 3.0 PART B - Mark X in column 2A for each pollutant you know or have reason to believe is present. Mark X in column 2B for each pollutant you believe to be absent. If you mark Column 2A for any pollutant, you must provide the results for at least one analysis for the pollutant. Complete one table for each outfall (intake). Provide results for additional parameters not listed here in Part 3.0 C.

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants A. Alkalinity (CaCO3)

MINIMUM MINIMUM MINIMUM B. Bromide (24959-67-9)

C. Chloride (16887-00-6)

D. Chlorine, Total Residual E. Color F. Conductivity F. Cyanide, Amenable to Chlorination Water Treatment Plant Waste 003 42 137.3 1

mg/L lb/d 28 91.5 1

mg/L lb/d 11 35.9 1

mg/L lb/d 67 219.1 1

mg/L lb/d

<0.30

<0.98 1

mg/L lb/d 0.392 1

75.4 1

7.57 1

x 300 1

mg/L x

<1.0

<3.2 1

mg/L lb/d x

25 81.7 1

mg/L lb/d x

<0.05

<0.16 1

mg/L lb/d x

x 840 1

uhmo/cm lb/d x

<0.005

<0.016 1

mg/L lb/d

MO 780-1514 (02-19)

Page 6 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants (Continued)

G. E. coli H. Fluoride (16984-48-8)

I. Nitrate plus Nitrate (as N)

J. Kjeldahl, Total (as N)

K. Nitrogen, Total Organic (as N)

L. Oil and Grease M. Phenols, Total N. Phosphorus (as P), Total (7723-14-0)

O. Sulfate (as SO4)

(14808-79-8)

P. Sulfide (as S)

Q. Sulfite (as SO3)

(14265-45-3)

R. Surfactants S. Trihalomethanes, Total Subpart 2 - Metals 1M. Aluminum, Total Recoverable (7429-90-5) 2M. Antimony, Total Recoverable (7440-36-9) 3M. Arsenic, Total Recoverable (7440-38-2) 4M. Barium, Total Recoverable (7440-39-3) 5M. Beryllium, Total Recoverable (7440-41-7) 6M. Boron, Total Recoverable (7440-42-8) 7M. Cadmium, Total Recoverable (7440-43-9) 8M. Chromium III Total Recoverable (16065-83-1) 9M. Chromium VI, Dissolved (18540-29-9) 10M. Cobalt, Total Recoverable (7440-48-4) x 404 0.89 1

mpn/100ml lb/d x

0.418 1.37 1

mg/L lb/d x

<0.02

<0.06 1

mg/L lb/d x

1.6 5.23 1

mg/L lb/d x

1.2 3.9 1

mg/L lb/d x

<5.2

<17.0 1

mg/L lb/d x

<0.005

<0.016 1

mg/L lb/d x

0.47 1.54 1

mg/L lb/d x

70 229 1

mg/L lb/d x

<2.0

<6.5 1

mg/L lb/d x

<2.0

<6.5 1

mg/L lb/d x

<1.0

<3.3 1

mg/L lb/d x

x 0.72 2.35 1

mg/L lb/d x

<0.003

<0.009 1

mg/L lb/d x

0.018 0.059 1

mg/L lb/d x

0.15 0.49 1

mg/L lb/d x

<0.001

<0.003 1

mg/L lb/d x

0.091 0.30 1

mg/L lb/d x

<0.001

<0.003 1

mg/L lb/d x

<0.005

<0.0016 1

mg/L lb/d x

<0.005

<0.016 1

mg/L lb/d x

<0.002

<0.006 1

mg/L lb/d

MO 780-1514 (02-19)

Page 7 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 2 - Metals (Continued) 11M. Copper, Total Recoverable (7440-50-8) 12M. Iron, Total Recoverable (7439-89-6) 13M. Lead, Total Recoverable (7439-92-1) 14M. Magnesium, Total Recoverable (7439-95-4) 15M. Manganese, Total Recoverable (7439-96-5) 16M. Mercury, Total Recoverable (7439-97-6) 17M. Methylmercury (22967926) 18M. Molybdenum, Total Recoverable (7439-98-7) 19M. Nickel, Total Recoverable (7440-02-0) 20M. Selenium, Total Recoverable (7782-49-2) 21M. Silver, Total Recoverable (7440-22-4) 22M. Thallium, Total Recoverable (7440-28-0) 23M. Tin, Total Recoverable (7440-31-5) 24M. Titanium, Total Recoverable (7440-32-6) 25M. Zinc, Total Recoverable (7440-66-6)

Subpart 3 - Radioactivity 1R. Alpha Total 2R. Beta Total 3R. Radium Total 4R. Radium 226 plus 228 Total x

<0.003

<0.01 1

mg/L lb/d x

0.88 2.88 1

mg/L lb/d x

<0.001

<0.003 1

mg/L lb/d x

35 114.4 1

mg/L lb/d x

2.1 6.9 1

mg/L lb/d x

<0.0002

<0.001 1

mg/L lb/d x

2.28 7.45 1

ng/L lb/d x

0.0021 0.007 1

mg/L lb/d x

<0.005

<0.016 1

mg/L lb/d x

<0.001

<0.003 1

mg/L lb/d x

<0.005

<0.016 1

mg/L lb/d x

<0.001

<0.003 1

mg/L lb/d x

<0.06

<0.19 1

mg/L lb/d x

0.0776 0.25 1

mg/L lb/d x

<0.006

<0.019 1

mg/L lb/d x

1.62 1

pCi/L x

0.961 1

pCi/L x

x

MO 780-1514 (02-19)

Page 5 of 13 SEE INSTRUCTIONS; PLEASE PRINT OR TYPE.

You may report some or all of this information on separate sheet (use similar format) instead of completing these pages.

FORM C TABLE 1 FOR 3.0 - ITEMS A AND B EFFLUENT (AND INTAKE) CHARACTERISTICS THIS OUTFALL IS:

OUTFALL NO.

3.0 PART A - You must provide the results of at least one analysis for every pollutant in Part A. Complete one table for each outfall or proposed outfall. See instructions.

1. POLLUTANT

2. VALUES

3. UNITS (specify if blank)

A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS A. Biochemical Oxygen Demand, 5-day (BOD5)

B. Chemical Oxygen Demand (COD)

C. Total Organic Carbon (TOC)

D. Total Suspended Solids (TSS)

E. Ammonia as N F. Flow VALUE VALUE VALUE MILLIONS OF GALLONS PER DAY (MGD)

G. Temperature (winter)

VALUE VALUE VALUE

°F H. Temperature (summer)

VALUE VALUE VALUE

°F I. pH MINIMUM MAXIMUM AVERAGE STANDARD UNITS (SU) 3.0 PART B - Mark X in column 2A for each pollutant you know or have reason to believe is present. Mark X in column 2B for each pollutant you believe to be absent. If you mark Column 2A for any pollutant, you must provide the results for at least one analysis for the pollutant. Complete one table for each outfall (intake). Provide results for additional parameters not listed here in Part 3.0 C.

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants A. Alkalinity (CaCO3)

MINIMUM MINIMUM MINIMUM B. Bromide (24959-67-9)

C. Chloride (16887-00-6)

D. Chlorine, Total Residual E. Color F. Conductivity F. Cyanide, Amenable to Chlorination Sanitary Waste Lagoon 007 10.0 1.67 1

mg/L lb/d 100 16.7 1

mg/L lb/d 22 3.67 1

mg/L lb/d 42 7.0 1

mg/L lb/d

<0.30

<0.05 1

mg/L lb/d 0.02 1

59 1

9.75 1

x 200 1

x

<5.0

<0.83 1

mg/L lb/d x

220 36.7 1

mg/L lb/d x

<0.10

<0.02 1

mg/L lb/d x

x 1100 1

mg/L lb/d x

<0.005

<0.005 1

mg/L lb/d

MO 780-1514 (02-19)

Page 6 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants (Continued)

G. E. coli H. Fluoride (16984-48-8)

I. Nitrate plus Nitrate (as N)

J. Kjeldahl, Total (as N)

K. Nitrogen, Total Organic (as N)

L. Oil and Grease M. Phenols, Total N. Phosphorus (as P), Total (7723-14-0)

O. Sulfate (as SO4)

(14808-79-8)

P. Sulfide (as S)

Q. Sulfite (as SO3)

(14265-45-3)

R. Surfactants S. Trihalomethanes, Total Subpart 2 - Metals 1M. Aluminum, Total Recoverable (7429-90-5) 2M. Antimony, Total Recoverable (7440-36-9) 3M. Arsenic, Total Recoverable (7440-38-2) 4M. Barium, Total Recoverable (7440-39-3) 5M. Beryllium, Total Recoverable (7440-41-7) 6M. Boron, Total Recoverable (7440-42-8) 7M. Cadmium, Total Recoverable (7440-43-9) 8M. Chromium III Total Recoverable (16065-83-1) 9M. Chromium VI, Dissolved (18540-29-9) 10M. Cobalt, Total Recoverable (7440-48-4) x

<10

<1.67 1

mg/L lb/d x

0.286 0.048 1

mg/L lb/d x

<0.02

<0.003 1

mg/L lb/d x

3.9 0.65 1

mg/L lb/d x

3.9 0.65 1

mg/L lb/d x

<5.2

<0.87 1

mg/L lb/d x

<0.005

<0.005 1

mg/L lb/d x

1.0 0.17 1

mg/L lb/d x

43 7.17 1

mg/L lb/d x

<2.0

<0.33 1

mg/L lb/d x

<2.0

<0.33 1

mg/L lb/d x

<0.5

<0.08 1

mg/L lb/d x

<0.010

<0.002 1

mg/L lb/d x

<0.003

<0.001 1

mg/L lb/d x

<0.001

<0.001 1

mg/L lb/d x

0.036 0.006 1

mg/L lb/d x

<0.001

<0.001 1

mg/L lb/d x

0.23 0.038 1

mg/L lb/d x

<0.001

<0.001 1

mg/L lb/d x

<5.0

<0.84 1

ug/L lb/d x

<0.005

<0.005 1

mg/L lb/d x

<0.002

<0.001 1

mg/L lb/d

MO 780-1514 (02-19)

Page 7 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 2 - Metals (Continued) 11M. Copper, Total Recoverable (7440-50-8) 12M. Iron, Total Recoverable (7439-89-6) 13M. Lead, Total Recoverable (7439-92-1) 14M. Magnesium, Total Recoverable (7439-95-4) 15M. Manganese, Total Recoverable (7439-96-5) 16M. Mercury, Total Recoverable (7439-97-6) 17M. Methylmercury (22967926) 18M. Molybdenum, Total Recoverable (7439-98-7) 19M. Nickel, Total Recoverable (7440-02-0) 20M. Selenium, Total Recoverable (7782-49-2) 21M. Silver, Total Recoverable (7440-22-4) 22M. Thallium, Total Recoverable (7440-28-0) 23M. Tin, Total Recoverable (7440-31-5) 24M. Titanium, Total Recoverable (7440-32-6) 25M. Zinc, Total Recoverable (7440-66-6)

Subpart 3 - Radioactivity 1R. Alpha Total 2R. Beta Total 3R. Radium Total 4R. Radium 226 plus 228 Total x

<0.003

<0.001 1

mg/L lb/d x

0.026 0.004 1

mg/L lb/d x

<0.001

<0.001 1

mg/L lb/d x

20 3.34 1

mg/L lb/d x

0.10 0.017 1

mg/L lb/d x

<0.0002

<0.001 1

mg/L lb/d x

0.342 0.057 1

ng/L lb/d x

<0.001

<0.001 1

mg/L lb/d x

<0.005

<0.001 1

mg/L lb/d x

<0.001

<0.001 1

mg/L lb/d x

<0.005

<0.001 1

mg/L lb/d x

<0.001

<0.001 1

mg/L lb/d x

<0.06

<0.01 1

mg/L lb/d x

<0.005

<0.001 1

mg/L lb/d x

<0.006

<0.001 1

mg/L lb/d x

3.08 1

pCi/L x

1.86 1

pCi/L x

x

MO 780-1514 (02-19)

Page 5 of 13 SEE INSTRUCTIONS; PLEASE PRINT OR TYPE.

You may report some or all of this information on separate sheet (use similar format) instead of completing these pages.

FORM C TABLE 1 FOR 3.0 - ITEMS A AND B EFFLUENT (AND INTAKE) CHARACTERISTICS THIS OUTFALL IS:

OUTFALL NO.

3.0 PART A - You must provide the results of at least one analysis for every pollutant in Part A. Complete one table for each outfall or proposed outfall. See instructions.

1. POLLUTANT

2. VALUES

3. UNITS (specify if blank)

A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS A. Biochemical Oxygen Demand, 5-day (BOD5)

B. Chemical Oxygen Demand (COD)

C. Total Organic Carbon (TOC)

D. Total Suspended Solids (TSS)

E. Ammonia as N F. Flow VALUE VALUE VALUE MILLIONS OF GALLONS PER DAY (MGD)

G. Temperature (winter)

VALUE VALUE VALUE

°F H. Temperature (summer)

VALUE VALUE VALUE

°F I. pH MINIMUM MAXIMUM AVERAGE STANDARD UNITS (SU) 3.0 PART B - Mark X in column 2A for each pollutant you know or have reason to believe is present. Mark X in column 2B for each pollutant you believe to be absent. If you mark Column 2A for any pollutant, you must provide the results for at least one analysis for the pollutant. Complete one table for each outfall (intake). Provide results for additional parameters not listed here in Part 3.0 C.

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants A. Alkalinity (CaCO3)

MINIMUM MINIMUM MINIMUM B. Bromide (24959-67-9)

C. Chloride (16887-00-6)

D. Chlorine, Total Residual E. Color F. Conductivity F. Cyanide, Amenable to Chlorination Stormwater 010 2.1 1.42 1

mg/L lb/d 16 5.34 21.6 14.6 1,10 mg/L lb/d 3.2 2.16 1

mg/L lb/d 9.2 3.07 10.7 7.23 1,10 mg/L lb/d

<0.5

<0.34 1

mg/L lb/d 0.04 0.081 10 63.6 1

7.8 9.4 10 x

x x

x

<0.05

<0.034 1

mg/L lb/d x

x x

MO 780-1514 (02-19)

Page 6 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants (Continued)

G. E. coli H. Fluoride (16984-48-8)

I. Nitrate plus Nitrate (as N)

J. Kjeldahl, Total (as N)

K. Nitrogen, Total Organic (as N)

L. Oil and Grease M. Phenols, Total N. Phosphorus (as P), Total (7723-14-0)

O. Sulfate (as SO4)

(14808-79-8)

P. Sulfide (as S)

Q. Sulfite (as SO3)

(14265-45-3)

R. Surfactants S. Trihalomethanes, Total Subpart 2 - Metals 1M. Aluminum, Total Recoverable (7429-90-5) 2M. Antimony, Total Recoverable (7440-36-9) 3M. Arsenic, Total Recoverable (7440-38-2) 4M. Barium, Total Recoverable (7440-39-3) 5M. Beryllium, Total Recoverable (7440-41-7) 6M. Boron, Total Recoverable (7440-42-8) 7M. Cadmium, Total Recoverable (7440-43-9) 8M. Chromium III Total Recoverable (16065-83-1) 9M. Chromium VI, Dissolved (18540-29-9) 10M. Cobalt, Total Recoverable (7440-48-4) x x

x x

<5.0

<3.37

<5.0

<3.37 10 mg/L lb/d x

x x

MO 780-1514 (02-19)

Page 7 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 2 - Metals (Continued) 11M. Copper, Total Recoverable (7440-50-8) 12M. Iron, Total Recoverable (7439-89-6) 13M. Lead, Total Recoverable (7439-92-1) 14M. Magnesium, Total Recoverable (7439-95-4) 15M. Manganese, Total Recoverable (7439-96-5) 16M. Mercury, Total Recoverable (7439-97-6) 17M. Methylmercury (22967926) 18M. Molybdenum, Total Recoverable (7439-98-7) 19M. Nickel, Total Recoverable (7440-02-0) 20M. Selenium, Total Recoverable (7782-49-2) 21M. Silver, Total Recoverable (7440-22-4) 22M. Thallium, Total Recoverable (7440-28-0) 23M. Tin, Total Recoverable (7440-31-5) 24M. Titanium, Total Recoverable (7440-32-6) 25M. Zinc, Total Recoverable (7440-66-6)

Subpart 3 - Radioactivity 1R. Alpha Total 2R. Beta Total 3R. Radium Total 4R. Radium 226 plus 228 Total x

x x

MO 780-1514 (02-19)

Page 5 of 13 SEE INSTRUCTIONS; PLEASE PRINT OR TYPE.

You may report some or all of this information on separate sheet (use similar format) instead of completing these pages.

FORM C TABLE 1 FOR 3.0 - ITEMS A AND B EFFLUENT (AND INTAKE) CHARACTERISTICS THIS OUTFALL IS:

OUTFALL NO.

3.0 PART A - You must provide the results of at least one analysis for every pollutant in Part A. Complete one table for each outfall or proposed outfall. See instructions.

1. POLLUTANT

2. VALUES

3. UNITS (specify if blank)

A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS A. Biochemical Oxygen Demand, 5-day (BOD5)

B. Chemical Oxygen Demand (COD)

C. Total Organic Carbon (TOC)

D. Total Suspended Solids (TSS)

E. Ammonia as N F. Flow VALUE VALUE VALUE MILLIONS OF GALLONS PER DAY (MGD)

G. Temperature (winter)

VALUE VALUE VALUE

°F H. Temperature (summer)

VALUE VALUE VALUE

°F I. pH MINIMUM MAXIMUM AVERAGE STANDARD UNITS (SU) 3.0 PART B - Mark X in column 2A for each pollutant you know or have reason to believe is present. Mark X in column 2B for each pollutant you believe to be absent. If you mark Column 2A for any pollutant, you must provide the results for at least one analysis for the pollutant. Complete one table for each outfall (intake). Provide results for additional parameters not listed here in Part 3.0 C.

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants A. Alkalinity (CaCO3)

MINIMUM MINIMUM MINIMUM B. Bromide (24959-67-9)

C. Chloride (16887-00-6)

D. Chlorine, Total Residual E. Color F. Conductivity F. Cyanide, Amenable to Chlorination Stormwater 011 3.2 8.3 1

mg/L lb/d 33.0 42.93 27.8 71.8 1,10 mg/L lb/d 1.2 3.1 1

mg/L lb/d 8.5 11.06 13.9 35.9 1,10 mg/L lb/d

<0.5

<1.3 1

mg/L lb/d 0.156 0.31 10 63.8 1

7.7 8.4 10 x

x x

x

<0.05

<0.13 1

ug/L lb/d x

x x

MO 780-1514 (02-19)

Page 6 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants (Continued)

G. E. coli H. Fluoride (16984-48-8)

I. Nitrate plus Nitrate (as N)

J. Kjeldahl, Total (as N)

K. Nitrogen, Total Organic (as N)

L. Oil and Grease M. Phenols, Total N. Phosphorus (as P), Total (7723-14-0)

O. Sulfate (as SO4)

(14808-79-8)

P. Sulfide (as S)

Q. Sulfite (as SO3)

(14265-45-3)

R. Surfactants S. Trihalomethanes, Total Subpart 2 - Metals 1M. Aluminum, Total Recoverable (7429-90-5) 2M. Antimony, Total Recoverable (7440-36-9) 3M. Arsenic, Total Recoverable (7440-38-2) 4M. Barium, Total Recoverable (7440-39-3) 5M. Beryllium, Total Recoverable (7440-41-7) 6M. Boron, Total Recoverable (7440-42-8) 7M. Cadmium, Total Recoverable (7440-43-9) 8M. Chromium III Total Recoverable (16065-83-1) 9M. Chromium VI, Dissolved (18540-29-9) 10M. Cobalt, Total Recoverable (7440-48-4) x x

x x

<5.0

<12.9 10 mg/L lb/d x

x x

MO 780-1514 (02-19)

Page 7 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 2 - Metals (Continued) 11M. Copper, Total Recoverable (7440-50-8) 12M. Iron, Total Recoverable (7439-89-6) 13M. Lead, Total Recoverable (7439-92-1) 14M. Magnesium, Total Recoverable (7439-95-4) 15M. Manganese, Total Recoverable (7439-96-5) 16M. Mercury, Total Recoverable (7439-97-6) 17M. Methylmercury (22967926) 18M. Molybdenum, Total Recoverable (7439-98-7) 19M. Nickel, Total Recoverable (7440-02-0) 20M. Selenium, Total Recoverable (7782-49-2) 21M. Silver, Total Recoverable (7440-22-4) 22M. Thallium, Total Recoverable (7440-28-0) 23M. Tin, Total Recoverable (7440-31-5) 24M. Titanium, Total Recoverable (7440-32-6) 25M. Zinc, Total Recoverable (7440-66-6)

Subpart 3 - Radioactivity 1R. Alpha Total 2R. Beta Total 3R. Radium Total 4R. Radium 226 plus 228 Total x

x x

MO 780-1514 (02-19)

Page 5 of 13 SEE INSTRUCTIONS; PLEASE PRINT OR TYPE.

You may report some or all of this information on separate sheet (use similar format) instead of completing these pages.

FORM C TABLE 1 FOR 3.0 - ITEMS A AND B EFFLUENT (AND INTAKE) CHARACTERISTICS THIS OUTFALL IS:

OUTFALL NO.

3.0 PART A - You must provide the results of at least one analysis for every pollutant in Part A. Complete one table for each outfall or proposed outfall. See instructions.

1. POLLUTANT

2. VALUES

3. UNITS (specify if blank)

A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS A. Biochemical Oxygen Demand, 5-day (BOD5)

B. Chemical Oxygen Demand (COD)

C. Total Organic Carbon (TOC)

D. Total Suspended Solids (TSS)

E. Ammonia as N F. Flow VALUE VALUE VALUE MILLIONS OF GALLONS PER DAY (MGD)

G. Temperature (winter)

VALUE VALUE VALUE

°F H. Temperature (summer)

VALUE VALUE VALUE

°F I. pH MINIMUM MAXIMUM AVERAGE STANDARD UNITS (SU) 3.0 PART B - Mark X in column 2A for each pollutant you know or have reason to believe is present. Mark X in column 2B for each pollutant you believe to be absent. If you mark Column 2A for any pollutant, you must provide the results for at least one analysis for the pollutant. Complete one table for each outfall (intake). Provide results for additional parameters not listed here in Part 3.0 C.

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants A. Alkalinity (CaCO3)

MINIMUM MINIMUM MINIMUM B. Bromide (24959-67-9)

C. Chloride (16887-00-6)

D. Chlorine, Total Residual E. Color F. Conductivity F. Cyanide, Amenable to Chlorination Stormwater 012 6.8 3.6 1

mg/l lb/d 7.2 3.8 10.8 5.76 1,10 mg/l lb/d 4.3 2.3 1

mg/l lb/d 3.5 1.87 3.7 1.92 1,10 mg/l lb/d

<0.5

<0.3 1

mg/l lb/d 0.032 0.064 10 68.3 1

7.62 8.39 10 x

x x

x

<0.05

<0.03 1

mg/L lb/d x

x x

MO 780-1514 (02-19)

Page 6 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants (Continued)

G. E. coli H. Fluoride (16984-48-8)

I. Nitrate plus Nitrate (as N)

J. Kjeldahl, Total (as N)

K. Nitrogen, Total Organic (as N)

L. Oil and Grease M. Phenols, Total N. Phosphorus (as P), Total (7723-14-0)

O. Sulfate (as SO4)

(14808-79-8)

P. Sulfide (as S)

Q. Sulfite (as SO3)

(14265-45-3)

R. Surfactants S. Trihalomethanes, Total Subpart 2 - Metals 1M. Aluminum, Total Recoverable (7429-90-5) 2M. Antimony, Total Recoverable (7440-36-9) 3M. Arsenic, Total Recoverable (7440-38-2) 4M. Barium, Total Recoverable (7440-39-3) 5M. Beryllium, Total Recoverable (7440-41-7) 6M. Boron, Total Recoverable (7440-42-8) 7M. Cadmium, Total Recoverable (7440-43-9) 8M. Chromium III Total Recoverable (16065-83-1) 9M. Chromium VI, Dissolved (18540-29-9) 10M. Cobalt, Total Recoverable (7440-48-4) x x

x x

<5.0

<2.7

<5.0 1,10 mg/L lb/d x

x x

MO 780-1514 (02-19)

Page 7 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 2 - Metals (Continued) 11M. Copper, Total Recoverable (7440-50-8) 12M. Iron, Total Recoverable (7439-89-6) 13M. Lead, Total Recoverable (7439-92-1) 14M. Magnesium, Total Recoverable (7439-95-4) 15M. Manganese, Total Recoverable (7439-96-5) 16M. Mercury, Total Recoverable (7439-97-6) 17M. Methylmercury (22967926) 18M. Molybdenum, Total Recoverable (7439-98-7) 19M. Nickel, Total Recoverable (7440-02-0) 20M. Selenium, Total Recoverable (7782-49-2) 21M. Silver, Total Recoverable (7440-22-4) 22M. Thallium, Total Recoverable (7440-28-0) 23M. Tin, Total Recoverable (7440-31-5) 24M. Titanium, Total Recoverable (7440-32-6) 25M. Zinc, Total Recoverable (7440-66-6)

Subpart 3 - Radioactivity 1R. Alpha Total 2R. Beta Total 3R. Radium Total 4R. Radium 226 plus 228 Total x

x x

MO 780-1514 (02-19)

Page 5 of 13 SEE INSTRUCTIONS; PLEASE PRINT OR TYPE.

You may report some or all of this information on separate sheet (use similar format) instead of completing these pages.

FORM C TABLE 1 FOR 3.0 - ITEMS A AND B EFFLUENT (AND INTAKE) CHARACTERISTICS THIS OUTFALL IS:

OUTFALL NO.

3.0 PART A - You must provide the results of at least one analysis for every pollutant in Part A. Complete one table for each outfall or proposed outfall. See instructions.

1. POLLUTANT

2. VALUES

3. UNITS (specify if blank)

A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS A. Biochemical Oxygen Demand, 5-day (BOD5)

B. Chemical Oxygen Demand (COD)

C. Total Organic Carbon (TOC)

D. Total Suspended Solids (TSS)

E. Ammonia as N F. Flow VALUE VALUE VALUE MILLIONS OF GALLONS PER DAY (MGD)

G. Temperature (winter)

VALUE VALUE VALUE

°F H. Temperature (summer)

VALUE VALUE VALUE

°F I. pH MINIMUM MAXIMUM AVERAGE STANDARD UNITS (SU) 3.0 PART B - Mark X in column 2A for each pollutant you know or have reason to believe is present. Mark X in column 2B for each pollutant you believe to be absent. If you mark Column 2A for any pollutant, you must provide the results for at least one analysis for the pollutant. Complete one table for each outfall (intake). Provide results for additional parameters not listed here in Part 3.0 C.

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants A. Alkalinity (CaCO3)

MINIMUM MINIMUM MINIMUM B. Bromide (24959-67-9)

C. Chloride (16887-00-6)

D. Chlorine, Total Residual E. Color F. Conductivity F. Cyanide, Amenable to Chlorination Stormwater 014 2.3 0.75 1

mg/L lb/d 23 6.52 24.14 7.85 1,7 mg/L lb/d 2.0 0.65 1

mg/L lb/d 6.2 1.76 14.4 4.68 1,7 mg/L lb/d

<0.05

<0.02 1

mg/L lb/d 0.034 0.039 7

62.8 1

7.5 8.16 7

x x

<0.05

<0.016 1

mg/L lb/d x

x x

MO 780-1514 (02-19)

Page 6 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants (Continued)

G. E. coli H. Fluoride (16984-48-8)

I. Nitrate plus Nitrate (as N)

J. Kjeldahl, Total (as N)

K. Nitrogen, Total Organic (as N)

L. Oil and Grease M. Phenols, Total N. Phosphorus (as P), Total (7723-14-0)

O. Sulfate (as SO4)

(14808-79-8)

P. Sulfide (as S)

Q. Sulfite (as SO3)

(14265-45-3)

R. Surfactants S. Trihalomethanes, Total Subpart 2 - Metals 1M. Aluminum, Total Recoverable (7429-90-5) 2M. Antimony, Total Recoverable (7440-36-9) 3M. Arsenic, Total Recoverable (7440-38-2) 4M. Barium, Total Recoverable (7440-39-3) 5M. Beryllium, Total Recoverable (7440-41-7) 6M. Boron, Total Recoverable (7440-42-8) 7M. Cadmium, Total Recoverable (7440-43-9) 8M. Chromium III Total Recoverable (16065-83-1) 9M. Chromium VI, Dissolved (18540-29-9) 10M. Cobalt, Total Recoverable (7440-48-4) x x

x x

<5.0

<1.6 7

mg/L lb/d x

x x

MO 780-1514 (02-19)

Page 7 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 2 - Metals (Continued) 11M. Copper, Total Recoverable (7440-50-8) 12M. Iron, Total Recoverable (7439-89-6) 13M. Lead, Total Recoverable (7439-92-1) 14M. Magnesium, Total Recoverable (7439-95-4) 15M. Manganese, Total Recoverable (7439-96-5) 16M. Mercury, Total Recoverable (7439-97-6) 17M. Methylmercury (22967926) 18M. Molybdenum, Total Recoverable (7439-98-7) 19M. Nickel, Total Recoverable (7440-02-0) 20M. Selenium, Total Recoverable (7782-49-2) 21M. Silver, Total Recoverable (7440-22-4) 22M. Thallium, Total Recoverable (7440-28-0) 23M. Tin, Total Recoverable (7440-31-5) 24M. Titanium, Total Recoverable (7440-32-6) 25M. Zinc, Total Recoverable (7440-66-6)

Subpart 3 - Radioactivity 1R. Alpha Total 2R. Beta Total 3R. Radium Total 4R. Radium 226 plus 228 Total x

x x

MO 780-1514 (02-19)

Page 5 of 13 SEE INSTRUCTIONS; PLEASE PRINT OR TYPE.

You may report some or all of this information on separate sheet (use similar format) instead of completing these pages.

FORM C TABLE 1 FOR 3.0 - ITEMS A AND B EFFLUENT (AND INTAKE) CHARACTERISTICS THIS OUTFALL IS:

OUTFALL NO.

3.0 PART A - You must provide the results of at least one analysis for every pollutant in Part A. Complete one table for each outfall or proposed outfall. See instructions.

1. POLLUTANT

2. VALUES

3. UNITS (specify if blank)

A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS A. Biochemical Oxygen Demand, 5-day (BOD5)

B. Chemical Oxygen Demand (COD)

C. Total Organic Carbon (TOC)

D. Total Suspended Solids (TSS)

E. Ammonia as N F. Flow VALUE VALUE VALUE MILLIONS OF GALLONS PER DAY (MGD)

G. Temperature (winter)

VALUE VALUE VALUE

°F H. Temperature (summer)

VALUE VALUE VALUE

°F I. pH MINIMUM MAXIMUM AVERAGE STANDARD UNITS (SU) 3.0 PART B - Mark X in column 2A for each pollutant you know or have reason to believe is present. Mark X in column 2B for each pollutant you believe to be absent. If you mark Column 2A for any pollutant, you must provide the results for at least one analysis for the pollutant. Complete one table for each outfall (intake). Provide results for additional parameters not listed here in Part 3.0 C.

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants A. Alkalinity (CaCO3)

MINIMUM MINIMUM MINIMUM B. Bromide (24959-67-9)

C. Chloride (16887-00-6)

D. Chlorine, Total Residual E. Color F. Conductivity F. Cyanide, Amenable to Chlorination Stormwater 015 2.1 0.43 1

mg/L lb/d 12 2.2 28.1 5.85 1,7 mg/L lb/d 3.0 0.62 1

mg/L lb/d 8.3 1.52 9.9 2.06 1,7 mg/L lb/d

<0.05

<0.01 1

mg/L lb/d 0.022 0.025 1,7 63.8 1

7.73 8.23 7

x x

<0.05

<0.01 1

mg/L lb/d x

x x

MO 780-1514 (02-19)

Page 6 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants (Continued)

G. E. coli H. Fluoride (16984-48-8)

I. Nitrate plus Nitrate (as N)

J. Kjeldahl, Total (as N)

K. Nitrogen, Total Organic (as N)

L. Oil and Grease M. Phenols, Total N. Phosphorus (as P), Total (7723-14-0)

O. Sulfate (as SO4)

(14808-79-8)

P. Sulfide (as S)

Q. Sulfite (as SO3)

(14265-45-3)

R. Surfactants S. Trihalomethanes, Total Subpart 2 - Metals 1M. Aluminum, Total Recoverable (7429-90-5) 2M. Antimony, Total Recoverable (7440-36-9) 3M. Arsenic, Total Recoverable (7440-38-2) 4M. Barium, Total Recoverable (7440-39-3) 5M. Beryllium, Total Recoverable (7440-41-7) 6M. Boron, Total Recoverable (7440-42-8) 7M. Cadmium, Total Recoverable (7440-43-9) 8M. Chromium III Total Recoverable (16065-83-1) 9M. Chromium VI, Dissolved (18540-29-9) 10M. Cobalt, Total Recoverable (7440-48-4) x x

x x

<5.0

<1.04

<5.0

<1.04 1,7 mg/L lb/d x

x x

MO 780-1514 (02-19)

Page 7 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 2 - Metals (Continued) 11M. Copper, Total Recoverable (7440-50-8) 12M. Iron, Total Recoverable (7439-89-6) 13M. Lead, Total Recoverable (7439-92-1) 14M. Magnesium, Total Recoverable (7439-95-4) 15M. Manganese, Total Recoverable (7439-96-5) 16M. Mercury, Total Recoverable (7439-97-6) 17M. Methylmercury (22967926) 18M. Molybdenum, Total Recoverable (7439-98-7) 19M. Nickel, Total Recoverable (7440-02-0) 20M. Selenium, Total Recoverable (7782-49-2) 21M. Silver, Total Recoverable (7440-22-4) 22M. Thallium, Total Recoverable (7440-28-0) 23M. Tin, Total Recoverable (7440-31-5) 24M. Titanium, Total Recoverable (7440-32-6) 25M. Zinc, Total Recoverable (7440-66-6)

Subpart 3 - Radioactivity 1R. Alpha Total 2R. Beta Total 3R. Radium Total 4R. Radium 226 plus 228 Total x

x x

MO 780-1514 (02-19)

Page 5 of 13 SEE INSTRUCTIONS; PLEASE PRINT OR TYPE.

You may report some or all of this information on separate sheet (use similar format) instead of completing these pages.

FORM C TABLE 1 FOR 3.0 - ITEMS A AND B EFFLUENT (AND INTAKE) CHARACTERISTICS THIS OUTFALL IS:

OUTFALL NO.

3.0 PART A - You must provide the results of at least one analysis for every pollutant in Part A. Complete one table for each outfall or proposed outfall. See instructions.

1. POLLUTANT

2. VALUES

3. UNITS (specify if blank)

A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS A. Biochemical Oxygen Demand, 5-day (BOD5)

B. Chemical Oxygen Demand (COD)

C. Total Organic Carbon (TOC)

D. Total Suspended Solids (TSS)

E. Ammonia as N F. Flow VALUE VALUE VALUE MILLIONS OF GALLONS PER DAY (MGD)

G. Temperature (winter)

VALUE VALUE VALUE

°F H. Temperature (summer)

VALUE VALUE VALUE

°F I. pH MINIMUM MAXIMUM AVERAGE STANDARD UNITS (SU) 3.0 PART B - Mark X in column 2A for each pollutant you know or have reason to believe is present. Mark X in column 2B for each pollutant you believe to be absent. If you mark Column 2A for any pollutant, you must provide the results for at least one analysis for the pollutant. Complete one table for each outfall (intake). Provide results for additional parameters not listed here in Part 3.0 C.

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants A. Alkalinity (CaCO3)

MINIMUM MINIMUM MINIMUM B. Bromide (24959-67-9)

C. Chloride (16887-00-6)

D. Chlorine, Total Residual E. Color F. Conductivity F. Cyanide, Amenable to Chlorination Cooling Tower Bypass 016

<10.0

<174.3 1

mg/L lb/d 8.4 146.4 1

mg/L lb/d 3.9 67.97 1

mg/L lb/d 13 227 13.6 237.1 1,22 mg/L lb/d

<0.3

<5.23

<0.1

<1.74 1,27 mg/L lb/d 2.09 20 62.8 1

7.8 8.48 1

x x

<1.0

<17.43 1

mg/L lb/d x

24 418.3 1

mg/L lb/d x

<0.05

<0.87

<0.05

<610 1,10 mg/L lb/d x

850 1

umho/cm lb/d x

<0.005

<0.087 1

mg/L lb/d

MO 780-1514 (02-19)

Page 6 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants (Continued)

G. E. coli H. Fluoride (16984-48-8)

I. Nitrate plus Nitrate (as N)

J. Kjeldahl, Total (as N)

K. Nitrogen, Total Organic (as N)

L. Oil and Grease M. Phenols, Total N. Phosphorus (as P), Total (7723-14-0)

O. Sulfate (as SO4)

(14808-79-8)

P. Sulfide (as S)

Q. Sulfite (as SO3)

(14265-45-3)

R. Surfactants S. Trihalomethanes, Total Subpart 2 - Metals 1M. Aluminum, Total Recoverable (7429-90-5) 2M. Antimony, Total Recoverable (7440-36-9) 3M. Arsenic, Total Recoverable (7440-38-2) 4M. Barium, Total Recoverable (7440-39-3) 5M. Beryllium, Total Recoverable (7440-41-7) 6M. Boron, Total Recoverable (7440-42-8) 7M. Cadmium, Total Recoverable (7440-43-9) 8M. Chromium III Total Recoverable (16065-83-1) 9M. Chromium VI, Dissolved (18540-29-9) 10M. Cobalt, Total Recoverable (7440-48-4) x 10 174.3 1

mg/L lb/d x

0.356 6.21 1

mg/L lb/d x

0.43 7.5 1

mg/L lb/d x

<1.0

<17.43 1

mg/L lb/d x

<1.0

<17.43 1

mg/L lb/d x

<5.0

<87.15

<5.0

<87.15 1,11 mg/L lb/d x

<0.005

<0.09 1

mg/L lb/d x

0.13 2.27 1

mg/L lb/d x

210 3660 1

mg/L lb/d x

<2.0

<34.9 1

mg/L lb/d x

<2.0

<34.9 1

mg/L lb/d x

<0.2

<3.49 1

mg/L lb/d x

x 1.0 17.43 1

mg/L lb/d x

<0.003

<0.05 1

mg/L lb/d x

0.0051 0.09 1

mg/L lb/d x

0.13 2.27 1

mg/L lb/d x

<0.001

<0.017 1

mg/L lb/d x

0.14 2.44 1

mg/L lb/d x

<0.001

<0.017 1

mg/L lb/d x

<5.0

<87.15 1

ug/L lb/d x

<0.005

<0.09 1

mg/L lb/d x

<0.002

<0.035 1

mg/L lb/d

MO 780-1514 (02-19)

Page 7 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 2 - Metals (Continued) 11M. Copper, Total Recoverable (7440-50-8) 12M. Iron, Total Recoverable (7439-89-6) 13M. Lead, Total Recoverable (7439-92-1) 14M. Magnesium, Total Recoverable (7439-95-4) 15M. Manganese, Total Recoverable (7439-96-5) 16M. Mercury, Total Recoverable (7439-97-6) 17M. Methylmercury (22967926) 18M. Molybdenum, Total Recoverable (7439-98-7) 19M. Nickel, Total Recoverable (7440-02-0) 20M. Selenium, Total Recoverable (7782-49-2) 21M. Silver, Total Recoverable (7440-22-4) 22M. Thallium, Total Recoverable (7440-28-0) 23M. Tin, Total Recoverable (7440-31-5) 24M. Titanium, Total Recoverable (7440-32-6) 25M. Zinc, Total Recoverable (7440-66-6)

Subpart 3 - Radioactivity 1R. Alpha Total 2R. Beta Total 3R. Radium Total 4R. Radium 226 plus 228 Total x

0.0035 0.061 1

mg/L lb/d x

1.5 26.15 1

mg/L lb/d x

0.0016 0.03 1

mg/L lb/d x

27 470.6 1

mg/L lb/d x

0.24 4.18 1

mg/L lb/d x

<0.0002

<0.003 1

mg/L lb/d x

0.165 2.87 1

ng/L lb/d x

0.0036 0.063 1

mg/L lb/d x

<0.005

<0.087 1

mg/L lb/d x

0.0025 0.004 1

mg/L lb/d x

<0.005

<0.087 1

mg/L lb/d x

<0.001

<0.017 1

mg/L lb/d x

<0.06

<0.105 1

mg/L lb/d x

0.016 0.03 1

mg/L lb/d x

0.0068 0.12 1

mg/L lb/d x

2.05 1

pCi/L x

0.878 1

pCi/L x

x

MO 780-1514 (02-19)

Page 5 of 13 SEE INSTRUCTIONS; PLEASE PRINT OR TYPE.

You may report some or all of this information on separate sheet (use similar format) instead of completing these pages.

FORM C TABLE 1 FOR 3.0 - ITEMS A AND B EFFLUENT (AND INTAKE) CHARACTERISTICS THIS OUTFALL IS:

OUTFALL NO.

3.0 PART A - You must provide the results of at least one analysis for every pollutant in Part A. Complete one table for each outfall or proposed outfall. See instructions.

1. POLLUTANT

2. VALUES

3. UNITS (specify if blank)

A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS A. Biochemical Oxygen Demand, 5-day (BOD5)

B. Chemical Oxygen Demand (COD)

C. Total Organic Carbon (TOC)

D. Total Suspended Solids (TSS)

E. Ammonia as N F. Flow VALUE VALUE VALUE MILLIONS OF GALLONS PER DAY (MGD)

G. Temperature (winter)

VALUE VALUE VALUE

°F H. Temperature (summer)

VALUE VALUE VALUE

°F I. pH MINIMUM MAXIMUM AVERAGE STANDARD UNITS (SU) 3.0 PART B - Mark X in column 2A for each pollutant you know or have reason to believe is present. Mark X in column 2B for each pollutant you believe to be absent. If you mark Column 2A for any pollutant, you must provide the results for at least one analysis for the pollutant. Complete one table for each outfall (intake). Provide results for additional parameters not listed here in Part 3.0 C.

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUES C. LONG TERM AVERAGE VALUES D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants A. Alkalinity (CaCO3)

MINIMUM MINIMUM MINIMUM B. Bromide (24959-67-9)

C. Chloride (16887-00-6)

D. Chlorine, Total Residual E. Color F. Conductivity F. Cyanide, Amenable to Chlorination Intake 009 37.0 1

mg/L 18 1

mg/L 4.6 1

mg/L 43 1

mg/L

<0.10 1

mg/L 19.2 1

62.8 1

8.34 1

x 160 1

mg/L x

<1.0 1

mg/L x

23 1

mg/L x

<0.05 1

mg/L x

800 1

umho/cm x

<0.005 1

mg/L

MO 780-1514 (02-19)

Page 6 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 1 - Conventional and Non-Conventional Pollutants (Continued)

G. E. coli H. Fluoride (16984-48-8)

I. Nitrate plus Nitrate (as N)

J. Kjeldahl, Total (as N)

K. Nitrogen, Total Organic (as N)

L. Oil and Grease M. Phenols, Total N. Phosphorus (as P), Total (7723-14-0)

O. Sulfate (as SO4)

(14808-79-8)

P. Sulfide (as S)

Q. Sulfite (as SO3)

(14265-45-3)

R. Surfactants S. Trihalomethanes, Total Subpart 2 - Metals 1M. Aluminum, Total Recoverable (7429-90-5) 2M. Antimony, Total Recoverable (7440-36-9) 3M. Arsenic, Total Recoverable (7440-38-2) 4M. Barium, Total Recoverable (7440-39-3) 5M. Beryllium, Total Recoverable (7440-41-7) 6M. Boron, Total Recoverable (7440-42-8) 7M. Cadmium, Total Recoverable (7440-43-9) 8M. Chromium III Total Recoverable (16065-83-1) 9M. Chromium VI, Dissolved (18540-29-9) 10M. Cobalt, Total Recoverable (7440-48-4) x 10 1

mpn/100ml x

0.44 1

mg/L x

0.32 1

mg/L x

<1.0 1

mg/L x

<1.0 1

mg/L x

<5.0 1

mg/L x

<0.005 1

mg/L x

0.14 1

mg/L x

210 1

mg/L x

<2.0 1

mg/L x

<2.0 1

mg/L x

0.31 1

mg/L 1

mg/L x

0.71 1

mg/L x

<0.003 1

mg/L x

0.0041 1

mg/L x

0.11 1

mg/L x

<0.001 1

mg/L x

0.15 1

mg/L x

<0.001 1

mg/L x

<0.005 1

mg/L x

<5.0 1

ug/L x

<0.002 1

mg/L

MO 780-1514 (02-19)

Page 7 of 13

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. VALUES

4. UNITS A. BELIEVED PRESENT B.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE C. LONG TERM AVERAGE VALUE D. NO. OF ANALYSES A. CONCEN-TRATION B. MASS CONCENTRATION MASS CONCENTRATION MASS CONCENTRATION MASS Subpart 2 - Metals (Continued) 11M. Copper, Total Recoverable (7440-50-8) 12M. Iron, Total Recoverable (7439-89-6) 13M. Lead, Total Recoverable (7439-92-1) 14M. Magnesium, Total Recoverable (7439-95-4) 15M. Manganese, Total Recoverable (7439-96-5) 16M. Mercury, Total Recoverable (7439-97-6) 17M. Methylmercury (22967926) 18M. Molybdenum, Total Recoverable (7439-98-7) 19M. Nickel, Total Recoverable (7440-02-0) 20M. Selenium, Total Recoverable (7782-49-2) 21M. Silver, Total Recoverable (7440-22-4) 22M. Thallium, Total Recoverable (7440-28-0) 23M. Tin, Total Recoverable (7440-31-5) 24M. Titanium, Total Recoverable (7440-32-6) 25M. Zinc, Total Recoverable (7440-66-6)

Subpart 3 - Radioactivity 1R. Alpha Total 2R. Beta Total 3R. Radium Total 4R. Radium 226 plus 228 Total x

<0.003 1

mg/L x

1.2 1

mg/L x

<0.001 1

mg/L x

29 1

mg/L x

0.16 1

mg/L x

<0.0002 1

mg/L x

<0.069 1

ng/L x

0.0041 1

mg/L x

<0.005 1

mg/L x

0.002 1

mg/L x

<0.005 1

mg/L x

<0.001 1

mg/L x

<0.06 1

mg/L x

0.015 1

mg/L x

<0.006 1

mg/L x

2.60 1

pCi/L x

0.66 1

pCi/L x

x

G 4 s MISSOURI DEPARTMENT OF NATURAL RESOURCES WATER PROTECTION PROGRAM, WATER POLLUTION BRANCH FORM D - APPLICATION FOR DISCHARGE PERMIT -

PRIMARY INDUSTRIES FORAGENCY USE ONLY CHECK NO.

DATE RECEIVED FEE SUBMITTED NOTE: DO NOT ATTEMPT TO COMPLETE THIS FORM BEFORE READING THE ACCOMPANYING INSTRUCTIONS 1.OO NAME OF FACILITY Ameren Missouri Callaway Energy Center 1.10 THIS FACILITY IS NOW IN OPEMTION UNDER MISSOURI OPERATING PERMIT NUMBER MO 0098001 This form is to be filled out in addition to forms A and C "Application for Discharge Permit" for the lndustries listed below:

Adhesives and sealants Aluminum forming Auto and other laundries Battery manufacturing Coal mining Coil coating Copper forming Electric and electronic compounds Electroplating Explosives man ufactu ring Foundries Gum and wood chemicals I norganic chemicals manufacturing lron and steel manufacturing Leather tanning and finishing Landfill Mechanical products man ufacturing Nonferrous metals manufacturing INDUSTRY CATEGORY Ore mining Organic chemicals manufactu ring Paint and ink formulation Pesticides Petroleum refining Pharmaceutical preparations Photographic equipment and supplies Plastic and synthetic materials manufacturing Plastic processing Porcelain enameling Printing and publishing Pulp and paperboard mills Rubber processing Soap and detergent manufacturing Steam electric power plants Textile mills Timber products processing MO 780-1s16 (06-13)

APPLICATION FOR DISCHARGE PERMIT FORM D - PRIMARY INDUSTRIES TABLE II NPDES # (IF ASSIGNED)

OUTFALL NUMBER 1.30 If you are a primary industry and this outfall contains process wastewater, refer to Table A in the instructions to determine which of the GC/MS fractions you must test for. Mark X in column 2-A for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. Mark X in column 2-B for each pollutant you know or have reason to believe is present. Mark X in column 2-C for each pollutant you believe to be absent. If you mark either columns 2-A or 2-B for any pollutant, you must provide the results of at least one analysis for that pollutant. Note that there are seven pages to this part, please review each carefully. Complete one table (all seven pages) for each outfall. See instructions for additional details and requirements.

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A.

TEST-ING REQUIRED B.

BELIEVE D

PRESENT C.

BELIEVE D

ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG. VALUE (if available)

D.

NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B.

NO OF ANALYSES (1)

CONCENTRATION (2)

MASS METALS, AND TOTAL PHENOLS 1M. Antimony, Total (7440-36-9) 2M. Arsenic, Total (7440-38-2) 3M. Beryllium, Total (7440-41-7) 4M. Cadmium, Total (7440-43-9) 5M. Chromium III (16065-83-1) 6M. Chromium VI (18540-29-9) 7M. Copper, Total (7440-50-8) 8M. Lead, Total (7439-92-1) 9M. Magnesium Total (7439-95-4) 10M. Mercury, Total (7439-97-6) 11M. Molybdenum Total (7439-98-7) 12M. Nickel, Total (7440-02-0) 13M. Selenium, Total (7782-49-2) 14M. Silver, Total (7440-22-4) 15M. Thallium, Total (7440-28-0) 16M. Tin Total (7440-31-5) 17M. Titanium Total (7440-32-6) 18M. Zinc, Total (7440-66-6)

MO 780-1516 (06-13)

PAGE 2 lbs/d

mg/L mg/L 1

lbs/d mg/L

lbs/d mg/L 1

1

<0.005 0.0047 0.144

1 mg/L lbs/d 0.227 0.0074

lbs/d mg/L 1

0.181 0.0059

1 mg/L 1

<0.031

<0.001

lbs/d mg/L 1

0.095 0.0031

lbs/d mg/L lbs/d

<0.006

<0.0002

<0.178

<0.0058 1

lbs/d mg/L 1

0.196 0.0064

lbs/d mg/L 1

<1.841

<0.06

lbs/d mg/L 1

<0.006

<0.0002

1 0.00035 1

mg/L

<0.0002 lbs/d mg/L lbs/d

<0.006 mg/L lbs/d mg/L 1

<0.015

1 0.012

0.368 lbs/d mg/L

<0.0002

0.011 mg/L lbs/d 0.218

<0.006 1

lbs/d

MO-0098001 0.00094 0.0071 002 0.0289

1

1074

lbs/d 35

CONTINUED FROM PAGE 3 19M. Cyanide, Amenable to Chlorination 20M. Phenols, Total DIOXIN 2,3,7,8 - Tetra -

chlorodibenzo-P-Dioxin (1764-01-6)

DESCRIBE RESULTS

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TES-ING RE-QUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG. VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - VOLATILE COMPOUNDS 1V. Acrolein (107-02-8) 2V. Acrylonitrile (107-13-1) 3V. Benzene (71-43-2) 4V. Bis (Chloromethyl)

Ether (542-88-1) 5V. Bromoform (75-25-2) 6V.

Carbon Tetrachloride (56-23-5) 7V. Chlorobenzene (108-90-7) 8V. Chlorodibromomethane (124-48-1) 9V. Chloroethane (75-00-3) 10V. 2-Chloroethylvinyl Ether (110-75-8) 11V. Chloroform (67-66-3) 12V. Dichlorobromomethane (75-27-4) 13V. Dichloro-difluoromethane (75-71-8) 14V. 1,1 - Dichloroethane (75-34-3) 15V. 1,2 - Dichloroethane (107-06-2) 16V. 1,1 - Dichloroethylene (75-35-4) 17V. 1,3 - Dichloropropane (78-87-5) 18V. 1,2 -Dichloropropylene (542-75-6) 19V. Ethylbenzene (100-41-4) 20V. Methyl Bromide (74-83-9) 21V. Methyl Chloride (74-87-3)

MO 780-1516 (06-13)

PAGE 3 CONTINUE ON PAGE 4

<1.53

<50

lbs/d

Testing Not Required

lbs/d mg/L 1

<1.53

<0.05

lbs/d mg/L 1

<0.08

<0.0025

ug/L

<1.53

<50 1

lbs/d ug/L 1

<0.15

<5.0

lbs/d ug/L 1

<0.15

<5.0

lbs/d ug/L 1

<0.15

<5.0

lbs/d ug/L 1

<0.15

<5.0

lbs/d ug/L 1

<0.15

<5.0

lbs/d ug/L 1

<0.15

<5.0

lbs/d ug/L 1

<0.15

<5.0

lbs/d ug/L 1

<0.15

<5.0

lbs/d ug/L 1

<0.15

<5.0

lbs/d ug/L 1

<0.15

<5.0

lbs/d ug/L 1

<0.15

<5.0

lbs/d ug/L 1

<0.15

<5.0

lbs/d ug/L 1

<0.15

<5.0

lbs/d ug/L 1

<0.15

<5.0

lbs/d ug/L 1

<0.15

<5.0

lbs/d ug/L 1

<0.15

<5.0

lbs/d ug/L 1

<0.15

<5.0

lbs/d ug/L 1

<307

<10000

lbs/d ug/L 1

<0.15

<5.0

1 ug/L lbs/d

CONTINUED FROM THE FRONT NPDES # (IF ASSIGNED)

OUTFALL NUMBER

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING RE-QUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC.MS FRACTION - VOLATILE COMPOUNDS (continued) 22V. Methylene Chloride (75-09-2) 23V. 1,1,2,2 - Tetra-chloroethane (79-34-5) 24V. Tetrachloroethylene (127-18-4) 25V. Toluene (108-88-3) 26V. 1,2 - Trans Dichloroethylene (156-60-5) 27V. 1,1,1 - Tri -

chloroethane (71-55-6) 28V. 1,1,2 - Tri-chloroethane (79-00-5) 29V. Trichloro -

ethylene (79-01-6) 30V. Trichloro -

fluoromethane (75-69-4) 31V. Vinyl Chloride (75-01-4)

GC/MS FRACTION - ACID COMPOUNDS 1A. 2 - Chlorophenol (95-57-8) 2A. 2,4 - Dichloro -

phenol (120-83-2) 3A. 2,4 - Dimethyl -

phenol (105-67-9) 4A. 4,6 - Dinitro - O-Cresol (534-52-1) 5A. 2,4 - Dinitro -

phenol (51-28-5) 6A. 2-Nitrophenol (88-75-5) 7A. 4-Nitrophenol (100-02-7) 8A. P - Chloro - M Cresol (59-50-7) 9A. Pentachloro -

phenol (87-86-5) 10A. Phenol (108-952) 11A. 2,4,6 - Trichloro-phenol (88-06-2) 12A. 2 - methyl - 4,6 dinitrophenol (534-52-1)

MO 780-1516 (06-13)

PAGE 4 CONTINUE ON PAGE 5 MO-0098001 002

<5.0

<0.15 1

ug/L lbs/d

<5.0

<0.15 1

ug/L lbs/d

<5.0

<0.15 1

ug/L lbs/d

<5.0

<0.15 1

ug/L lbs/d

<5.0

<0.15 1

ug/L lbs/d

<5.0

<0.15 1

ug/L lbs/d

<5.0

<0.15 1

ug/L lbs/d

<5.0

<0.15 1

ug/L lbs/d

<5.0

<0.15 1

ug/L lbs/d

<5.0

<0.15 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<20

<0.61 1

ug/L lbs/d

<50

<1.53 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<50

<1.53 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<50

<1.53 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<50

<1.53 1

ug/L lbs/d

<50

<1.53 1

ug/L lbs/d

CONTINUED FROM THE FRONT

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS 1B. Acenaphthene (83-32-9) 2B. Acenaphtylene (208-96-8) 3B. Anthracene (120-12-7) 4B. Benzidine (92-87-5) 5B. Benzo (a)

Anthracene (56-55-3) 6B. Benzo (a)

Pyrene (50-32-8) 7B. 3,4 -

Benzofluoranthene (205-99-2) 8B. Benzo (ghi)

Perylene (191-24-2) 9B. Benzo (k)

Fluoranthene (207-08-9) 10B. Bis (2-Chloroethoxy)

Methane (111-91-1) 11B. Bis (2-Chloroethyl)

Ether (111-44-4) 12B. Bis (2-Chloroisopropyl)

Ether (39638-32-9) 13B. Bis (2-Ethylhexyl)

Phthalate (117-81-7) 14B. 4-Bromophenyl Phenyl Ether (101-55-3) 15B. Butyl Benzyl Phthalate (85-68-7) 16B. 2-Chloronaphthalene (91-58-7) 17B. 4-Chlorophenyl Phenyl Ether (7005-72-3) 18B. Chrysene (218-01-9) 19B. Dibenzo (a.h)

Anthracene (53-70-3) 20B. 1,2 -

Dichlorobenzene (95-50-1) 21B. 1,3 -

Dichlorobenzene (541-73-1)

MO 780-1516 (02-12)

PAGE 5 CONTINUE ON PAGE 6

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<80

<2.5 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

NPDES # (IF ASSIGNED)

OUTFALL NUMBER

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS (continued) 22B. 1, 4-Dichlorobenzene (106-46-7) 23B. 3, 3-Dichlorobenzidine (91-94-1) 24B. Diethyl Phthalate (84-66-2) 25B. Dimethyl Phthalate (131-11-3) 26B. Di-N-butyl Phthalate (84-74-2) 27B. 2,4-Dinitrotoluene (121-14-2) 28B. 2,6-Dinitrotoluene (606-20-2) 29B. Di-N-Octyphthalate (117-84-0) 30B. 1,2-Diphenylhydrazine (as Azobenzene) (122 7) 31B. Fluoranthene (206-44-0) 32B. Fluorene (86-73-7) 33B. Hexachlorobenzene (87-68-3) 34B.

Hexachlorobutadiene (87-68-3) 35B. Hexachloro-cyclopentadiene (77-47-4) 36B. Hexachloroethane (67-72-1) 37B. Indeno (1,2,3-c-d)

Pyrene (193-39-5) 38B. Isophorone (78-59-1) 39B. Naphthalene (91-20-3) 40B. Nitrobenzene (98-95-3) 41B. N-Nitro-sodimethylamine (62 9)

MO 780-1516 (06-13)

PAGE 6 CONTINUE ON PAGE 7 CONTINUED FROM PAGE 5 MO-0098001 002

<10

<0.31 1

ug/L lbs/d

<20

<0.61 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

CONTINUED FROM THE FRONT

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TES-ING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS (continued) 42B. N-Nitroso N-Propylamine (621-64-7) 43B. N-Nitro-sodiphenylamine (86 6) 44B. Phenanthrene (85-01-8) 45B. Pyrene (129-00-0) 46B. 1,2,4-Tri chlorobenzene (120-82-1)

GC/MS FRACTION - PESTICIDES 1P. Aldrin (309-00-2) 2P. -BHC (319-84-6) 3P. -BHC (319-84-6) 4P. -BHC (58-89-9) 5P. -BHC (319-86-8) 6P. Chlordane (57-74-9) 7P. 4,4-DDT (50-29-3) 8P. 4,4-DDE (72-55-9) 9P. 4,4-DDD (72-54-8) 10P. Dieldrin (60-57-1) 11P. -Endosulfan (115-29-7) 12P. -Endosultan (115-29-7) 13P. Endosulfan Sulfate (1031-07-8) 14P. Endrin (72-20-8) 15P. Endrin Aldehyde (7421-93-4) 16P. Heptachlor (76-44-8)

MO 780-1516 (06-13)

PAGE 7 CONTINUED ON PAGE 8

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

<10

<0.31 1

ug/L lbs/d

NPDES # (IF ASSIGNED)

OUTFALL NUMBER

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - PESTICISES (continued) 17P. Heptachlor Epoxide (1024-57-3) 18P. PCB-1242 (53469-21-9) 19P. PBC-1254 (11097-69-1) 20P. PCB-1221 (11104-28-2) 21P. PCB-1232 (11141-16-5) 22P. PCB-1248 (12672-29-6) 23P. PCB-1260 (11096-82-5) 24P. PCB-1016 (12674-11-2) 25P. Toxaphene (8001-35-2)

J. RADIOACTIVITY (1) Alpha Total (2) Beta Total (3) Radium Total (4) Radium 226 Total MO 780-1516 (06-13)

PAGE 8 CONTINUED FROM PAGE 7

002 MO-0098001

pCi/L 1

<0.609

pCi/L 1

<0.782

pCi/L 1

<0.782

2,OO POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS A.

IS ANY POLLUTANT LISTED IN ITEM 1.30 A SUBSTANCE OR A COMPONENT OF A SUBSTANCE WHICH YOU DO OR EXPECT THAT YOU WLL OVER THE NEXT FIVE YEARS USE OR MANUFACTURE AS AN INTERMEDIATE OR FINAL PRODUCT OR BYPRODUCT?

! ves (,srALLsucHpoLLUrANrsBELow El Ho(eoroe)

B. ARE YOUR OPERATIONS SUCH THAT YOUR RAW MATERIALS, PROCESSES OR PRODUCTS CAN REASONABLE BE EXPECTED TO VARY SO THAT YOUR DISCHARGES OF POLLUTANTS MAY DURING THE NEXT FIVE YEARS EXCEED TWO TIMES THE MAXIMUM VALUES REPORTED IN ITEM 1.30?

n ves poMpLErE c BELow E rc roo ro sEcrtoN 3.oo)

C. IF YOU ANSWERED "YES" TO ITEM B, EXPLAIN BELOWAND DESCRIBE IN DETAIL THE SOURCES AND EXPECTED LEVELS OF SUCH POLLUTANTS THAT YOU ANTICIPATE WLL BE DISCHARGED FROM EACH OUTFALL OVER THE NEXT FIVE YEARS, TO THE BEST OF YOUR ABILIITY AT THIS TIME.

CONTINUE ON ADDITIONAL SHEETS IF YOU NEED MORE SPACE.

3.00 CONTRACT ANALYSIS INFORMATION WERE ANY OF THE ANALYSES REPORTED IN 1.30 PERFORMED BY A CONTRACT LABORATORY OR CONSULTING FIRM?

fl ves Lrsr rHE NAME, ADDRESS, AND TELEzHINE N:MBER oF, AND ANALrZED By, EA1H sucH LABoRAToRy oR F:RM BELow)

! Ho 1oo ro sEcrtoN 4.oo)

A. NAME B. ADDRESS C. TELEPHONE (area code and numbq)

D. POLLUTANTS ANALYZED (ns0 Pace Analytical Laboratories 944 Anglum Rd.

(314) 432-0550 See Attachment E, NPDES Hazelwood, MO 63042 Sampling & Analysis 4.OO CERTIFICATION I certify under penalty of law that I have personally examined and am familiar with the information submitted in this application and all attachments and that, based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the information is true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment.

NAME AND OFFICIAL TITLE (TYPE OR PRINT)

Fadi Diya, Chief Nuclear Officer PHONE NUMBER (AREA CODE AND NUMBER)

(573) 823-6531 SIGNATURE ry17,6 DATE SIGNED '

r rultq [?"21(

APPLICATION FOR DISCHARGE PERMIT FORM D - PRIMARY INDUSTRIES TABLE II NPDES # (IF ASSIGNED)

OUTFALL NUMBER 1.30 If you are a primary industry and this outfall contains process wastewater, refer to Table A in the instructions to determine which of the GC/MS fractions you must test for. Mark X in column 2-A for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. Mark X in column 2-B for each pollutant you know or have reason to believe is present. Mark X in column 2-C for each pollutant you believe to be absent. If you mark either columns 2-A or 2-B for any pollutant, you must provide the results of at least one analysis for that pollutant. Note that there are seven pages to this part, please review each carefully. Complete one table (all seven pages) for each outfall. See instructions for additional details and requirements.

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A.

TEST-ING REQUIRED B.

BELIEVE D

PRESENT C.

BELIEVE D

ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG. VALUE (if available)

D.

NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B.

NO OF ANALYSES (1)

CONCENTRATION (2)

MASS METALS, AND TOTAL PHENOLS 1M. Antimony, Total (7440-36-9) 2M. Arsenic, Total (7440-38-2) 3M. Beryllium, Total (7440-41-7) 4M. Cadmium, Total (7440-43-9) 5M. Chromium III (16065-83-1) 6M. Chromium VI (18540-29-9) 7M. Copper, Total (7440-50-8) 8M. Lead, Total (7439-92-1) 9M. Magnesium Total (7439-95-4) 10M. Mercury, Total (7439-97-6) 11M. Molybdenum Total (7439-98-7) 12M. Nickel, Total (7440-02-0) 13M. Selenium, Total (7782-49-2) 14M. Silver, Total (7440-22-4) 15M. Thallium, Total (7440-28-0) 16M. Tin Total (7440-31-5) 17M. Titanium Total (7440-32-6) 18M. Zinc, Total (7440-66-6)

MO 780-1516 (06-13)

PAGE 2 MO-0098001 003

<0.0006

<0.1 1

mg/L lbs/d

<0.0006

<0.1 1

0.008 0.002 1

mg/L lbs/d 0.0056 0.94 1

<0.0002

<0.001 1

mg/L lbs/d 0.00048 0.08 1

<0.0002

<0.001 1

mg/L lbs/d 0.0003 0.05 1

<0.0058

<0.001 1

mg/L lbs/d

<0.0058

<0.01 1

0.0057 0.0013 1

mg/L lbs/d 0.0053 0.89 1

<0.0006

<0.001 1

mg/L lbs/d 0.014 2.36 1

0.00028

<0.001 1

mg/L lbs/d 0.0081 1.36 1

12 2.64 1

mg/L lbs/d 17 2863 1

<0.0002

<0.001 1

mg/L lbs/d

<0.0002

<0.01 1

0.0006

<0.001 1

mg/L lbs/d 0.0024 0.404 1

<0.001

<0.001 1

mg/L lbs/d 0.015 2.53 1

<0.0002

<0.001 1

mg/L lbs/d 0.0016 2.69 1

<0.001

<0.001 1

mg/L lbs/d

<0.001

<0.01 1

<0.0002

<0.001 1

mg/L lbs/d 0.0003 0.05 1

<0.06

<0.001 1

mg/L lbs/d

<0.06

<0.01 1

<0.005

<0.001 1

mg/L lbs/d 0.071 11.96 1

0.0039

<0.001 1

mg/L lbs/d 0.038 6.40 1

CONTINUED FROM PAGE 3 19M. Cyanide, Amenable to Chlorination 20M. Phenols, Total DIOXIN 2,3,7,8 - Tetra -

chlorodibenzo-P-Dioxin (1764-01-6)

DESCRIBE RESULTS

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TES-ING RE-QUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG. VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - VOLATILE COMPOUNDS 1V. Acrolein (107-02-8) 2V. Acrylonitrile (107-13-1) 3V. Benzene (71-43-2) 4V. Bis (Chloromethyl)

Ether (542-88-1) 5V. Bromoform (75-25-2) 6V.

Carbon Tetrachloride (56-23-5) 7V. Chlorobenzene (108-90-7) 8V. Chlorodibromomethane (124-48-1) 9V. Chloroethane (75-00-3) 10V. 2-Chloroethylvinyl Ether (110-75-8) 11V. Chloroform (67-66-3) 12V. Dichlorobromomethane (75-27-4) 13V. Dichloro-difluoromethane (75-71-8) 14V. 1,1 - Dichloroethane (75-34-3) 15V. 1,2 - Dichloroethane (107-06-2) 16V. 1,1 - Dichloroethylene (75-35-4) 17V. 1,3 - Dichloropropane (78-87-5) 18V. 1,2 -Dichloropropylene (542-75-6) 19V. Ethylbenzene (100-41-4) 20V. Methyl Bromide (74-83-9) 21V. Methyl Chloride (74-87-3)

MO 780-1516 (06-13)

PAGE 3 CONTINUE ON PAGE 4

<0.011

<50

lbs/d

Testing Not Required

4

<0.01

<0.05 lbs/d mg/L 4

<0.01

<0.05

4

<0.01

<0.0025 lbs/d mg/L 4

<0.001

<0.0025

<8.5

<50 ug/L 1

<0.011

<50 1

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.004

<15

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<2K

<10000 lbs/d ug/L 1

<2.20

<10000

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1 ug/L

<50 1

lbs/d

<8.5

CONTINUED FROM THE FRONT NPDES # (IF ASSIGNED)

OUTFALL NUMBER

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING RE-QUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC.MS FRACTION - VOLATILE COMPOUNDS (continued) 22V. Methylene Chloride (75-09-2) 23V. 1,1,2,2 - Tetra-chloroethane (79-34-5) 24V. Tetrachloroethylene (127-18-4) 25V. Toluene (108-88-3) 26V. 1,2 - Trans Dichloroethylene (156-60-5) 27V. 1,1,1 - Tri -

chloroethane (71-55-6) 28V. 1,1,2 - Tri-chloroethane (79-00-5) 29V. Trichloro -

ethylene (79-01-6) 30V. Trichloro -

fluoromethane (75-69-4) 31V. Vinyl Chloride (75-01-4)

GC/MS FRACTION - ACID COMPOUNDS 1A. 2 - Chlorophenol (95-57-8) 2A. 2,4 - Dichloro -

phenol (120-83-2) 3A. 2,4 - Dimethyl -

phenol (105-67-9) 4A. 4,6 - Dinitro - O-Cresol (534-52-1) 5A. 2,4 - Dinitro -

phenol (51-28-5) 6A. 2-Nitrophenol (88-75-5) 7A. 4-Nitrophenol (100-02-7) 8A. P - Chloro - M Cresol (59-50-7) 9A. Pentachloro -

phenol (87-86-5) 10A. Phenol (108-952) 11A. 2,4,6 - Trichloro-phenol (88-06-2) 12A. 2 - methyl - 4,6 dinitrophenol (534-52-1)

MO 780-1516 (06-13)

PAGE 4 CONTINUE ON PAGE 5

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

003 MO-0098001 1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<0.9

<5.0 lbs/d ug/L 1

1

<8.5

<50 lbs/d ug/L 1

<0.003

<20

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<8.5

<50 lbs/d ug/L 1

<0.011

<50

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<8.5

<50 lbs/d ug/L 1

<0.011

<50

1

<8.5

<50 lbs/d ug/L 1

<0.011

<50

1

<8.5

<50 lbs/d ug/L 1

<0.011

<50

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<8.5

<50 lbs/d ug/L 1

<0.011

<50

CONTINUED FROM THE FRONT

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS 1B. Acenaphthene (83-32-9) 2B. Acenaphtylene (208-96-8) 3B. Anthracene (120-12-7) 4B. Benzidine (92-87-5) 5B. Benzo (a)

Anthracene (56-55-3) 6B. Benzo (a)

Pyrene (50-32-8) 7B. 3,4 -

Benzofluoranthene (205-99-2) 8B. Benzo (ghi)

Perylene (191-24-2) 9B. Benzo (k)

Fluoranthene (207-08-9) 10B. Bis (2-Chloroethoxy)

Methane (111-91-1) 11B. Bis (2-Chloroethyl)

Ether (111-44-4) 12B. Bis (2-Chloroisopropyl)

Ether (39638-32-9) 13B. Bis (2-Ethylhexyl)

Phthalate (117-81-7) 14B. 4-Bromophenyl Phenyl Ether (101-55-3) 15B. Butyl Benzyl Phthalate (85-68-7) 16B. 2-Chloronaphthalene (91-58-7) 17B. 4-Chlorophenyl Phenyl Ether (7005-72-3) 18B. Chrysene (218-01-9) 19B. Dibenzo (a.h)

Anthracene (53-70-3) 20B. 1,2 -

Dichlorobenzene (95-50-1) 21B. 1,3 -

Dichlorobenzene (541-73-1)

MO 780-1516 (02-12)

PAGE 5 CONTINUE ON PAGE 6 1

<0.9

<5.0 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<13.5

<80 lbs/d ug/L 1

<0.02

<80

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

CONTINUED FROM THE FRONT

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS 1B. Acenaphthene (83-32-9) 2B. Acenaphtylene (208-96-8) 3B. Anthracene (120-12-7) 4B. Benzidine (92-87-5) 5B. Benzo (a)

Anthracene (56-55-3) 6B. Benzo (a)

Pyrene (50-32-8) 7B. 3,4 -

Benzofluoranthene (205-99-2) 8B. Benzo (ghi)

Perylene (191-24-2) 9B. Benzo (k)

Fluoranthene (207-08-9) 10B. Bis (2-Chloroethoxy)

Methane (111-91-1) 11B. Bis (2-Chloroethyl)

Ether (111-44-4) 12B. Bis (2-Chloroisopropyl)

Ether (39638-32-9) 13B. Bis (2-Ethylhexyl)

Phthalate (117-81-7) 14B. 4-Bromophenyl Phenyl Ether (101-55-3) 15B. Butyl Benzyl Phthalate (85-68-7) 16B. 2-Chloronaphthalene (91-58-7) 17B. 4-Chlorophenyl Phenyl Ether (7005-72-3) 18B. Chrysene (218-01-9) 19B. Dibenzo (a.h)

Anthracene (53-70-3) 20B. 1,2 -

Dichlorobenzene (95-50-1) 21B. 1,3 -

Dichlorobenzene (541-73-1)

MO 780-1516 (02-12)

PAGE 5 CONTINUE ON PAGE 6 1

<0.9

<5.0 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<13.5

<80 lbs/d ug/L 1

<0.02

<80

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

NPDES # (IF ASSIGNED)

OUTFALL NUMBER

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS (continued) 22B. 1, 4-Dichlorobenzene (106-46-7) 23B. 3, 3-Dichlorobenzidine (91-94-1) 24B. Diethyl Phthalate (84-66-2) 25B. Dimethyl Phthalate (131-11-3) 26B. Di-N-butyl Phthalate (84-74-2) 27B. 2,4-Dinitrotoluene (121-14-2) 28B. 2,6-Dinitrotoluene (606-20-2) 29B. Di-N-Octyphthalate (117-84-0) 30B. 1,2-Diphenylhydrazine (as Azobenzene) (122 7) 31B. Fluoranthene (206-44-0) 32B. Fluorene (86-73-7) 33B. Hexachlorobenzene (87-68-3) 34B.

Hexachlorobutadiene (87-68-3) 35B. Hexachloro-cyclopentadiene (77-47-4) 36B. Hexachloroethane (67-72-1) 37B. Indeno (1,2,3-c-d)

Pyrene (193-39-5) 38B. Isophorone (78-59-1) 39B. Naphthalene (91-20-3) 40B. Nitrobenzene (98-95-3) 41B. N-Nitro-sodimethylamine (62 9)

MO 780-1516 (06-13)

PAGE 6 CONTINUE ON PAGE 7 CONTINUED FROM PAGE 5

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<3.4

<20 lbs/d ug/L 1

<0.003

<20

1

<0.9

<5.0 lbs/d ug/L 1

<0.003

<10

003 MO-0098001 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10 1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

CONTINUED FROM THE FRONT

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TES-ING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS (continued) 42B. N-Nitroso N-Propylamine (621-64-7) 43B. N-Nitro-sodiphenylamine (86 6) 44B. Phenanthrene (85-01-8) 45B. Pyrene (129-00-0) 46B. 1,2,4-Tri chlorobenzene (120-82-1)

GC/MS FRACTION - PESTICIDES 1P. Aldrin (309-00-2) 2P. -BHC (319-84-6) 3P. -BHC (319-84-6) 4P. -BHC (58-89-9) 5P. -BHC (319-86-8) 6P. Chlordane (57-74-9) 7P. 4,4-DDT (50-29-3) 8P. 4,4-DDE (72-55-9) 9P. 4,4-DDD (72-54-8) 10P. Dieldrin (60-57-1) 11P. -Endosulfan (115-29-7) 12P. -Endosultan (115-29-7) 13P. Endosulfan Sulfate (1031-07-8) 14P. Endrin (72-20-8) 15P. Endrin Aldehyde (7421-93-4) 16P. Heptachlor (76-44-8)

MO 780-1516 (06-13)

PAGE 7 CONTINUED ON PAGE 8

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

NPDES # (IF ASSIGNED)

OUTFALL NUMBER

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - PESTICISES (continued) 17P. Heptachlor Epoxide (1024-57-3) 18P. PCB-1242 (53469-21-9) 19P. PBC-1254 (11097-69-1) 20P. PCB-1221 (11104-28-2) 21P. PCB-1232 (11141-16-5) 22P. PCB-1248 (12672-29-6) 23P. PCB-1260 (11096-82-5) 24P. PCB-1016 (12674-11-2) 25P. Toxaphene (8001-35-2)

J. RADIOACTIVITY (1) Alpha Total (2) Beta Total (3) Radium Total (4) Radium 226 Total MO 780-1516 (06-13)

PAGE 8 CONTINUED FROM PAGE 7

003 MO-0098001

1 0.059 pCi/L 1

<0.696

1 1.30 pCi/L 1

<0.696

1 1.36 pCi/L 1

<0.696

NPDES # (IF ASSIGNED)

OUTFALL NUMBER

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS (continued) 22B. 1, 4-Dichlorobenzene (106-46-7) 23B. 3, 3-Dichlorobenzidine (91-94-1) 24B. Diethyl Phthalate (84-66-2) 25B. Dimethyl Phthalate (131-11-3) 26B. Di-N-butyl Phthalate (84-74-2) 27B. 2,4-Dinitrotoluene (121-14-2) 28B. 2,6-Dinitrotoluene (606-20-2) 29B. Di-N-Octyphthalate (117-84-0) 30B. 1,2-Diphenylhydrazine (as Azobenzene) (122 7) 31B. Fluoranthene (206-44-0) 32B. Fluorene (86-73-7) 33B. Hexachlorobenzene (87-68-3) 34B.

Hexachlorobutadiene (87-68-3) 35B. Hexachloro-cyclopentadiene (77-47-4) 36B. Hexachloroethane (67-72-1) 37B. Indeno (1,2,3-c-d)

Pyrene (193-39-5) 38B. Isophorone (78-59-1) 39B. Naphthalene (91-20-3) 40B. Nitrobenzene (98-95-3) 41B. N-Nitro-sodimethylamine (62 9)

MO 780-1516 (06-13)

PAGE 6 CONTINUE ON PAGE 7 CONTINUED FROM PAGE 5

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<3.4

<20 lbs/d ug/L 1

<0.003

<20

1

<0.9

<5.0 lbs/d ug/L 1

<0.003

<10

003 MO-0098001 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10 1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

CONTINUED FROM THE FRONT

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TES-ING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS (continued) 42B. N-Nitroso N-Propylamine (621-64-7) 43B. N-Nitro-sodiphenylamine (86 6) 44B. Phenanthrene (85-01-8) 45B. Pyrene (129-00-0) 46B. 1,2,4-Tri chlorobenzene (120-82-1)

GC/MS FRACTION - PESTICIDES 1P. Aldrin (309-00-2) 2P. -BHC (319-84-6) 3P. -BHC (319-84-6) 4P. -BHC (58-89-9) 5P. -BHC (319-86-8) 6P. Chlordane (57-74-9) 7P. 4,4-DDT (50-29-3) 8P. 4,4-DDE (72-55-9) 9P. 4,4-DDD (72-54-8) 10P. Dieldrin (60-57-1) 11P. -Endosulfan (115-29-7) 12P. -Endosultan (115-29-7) 13P. Endosulfan Sulfate (1031-07-8) 14P. Endrin (72-20-8) 15P. Endrin Aldehyde (7421-93-4) 16P. Heptachlor (76-44-8)

MO 780-1516 (06-13)

PAGE 7 CONTINUED ON PAGE 8

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<0.9

<5.0 lbs/d ug/L 1

<0.002

<5.0

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

1

<1.7

<10 lbs/d ug/L 1

<0.003

<10

NPDES # (IF ASSIGNED)

OUTFALL NUMBER

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - PESTICISES (continued) 17P. Heptachlor Epoxide (1024-57-3) 18P. PCB-1242 (53469-21-9) 19P. PBC-1254 (11097-69-1) 20P. PCB-1221 (11104-28-2) 21P. PCB-1232 (11141-16-5) 22P. PCB-1248 (12672-29-6) 23P. PCB-1260 (11096-82-5) 24P. PCB-1016 (12674-11-2) 25P. Toxaphene (8001-35-2)

J. RADIOACTIVITY (1) Alpha Total (2) Beta Total (3) Radium Total (4) Radium 226 Total MO 780-1516 (06-13)

PAGE 8 CONTINUED FROM PAGE 7

003 MO-0098001

1 0.059 pCi/L 1

<0.696

1 1.30 pCi/L 1

<0.696

1 1.36 pCi/L 1

<0.696

APPLICATION FOR DISCHARGE PERMIT FORM D - PRIMARY INDUSTRIES TABLE II NPDES # (IF ASSIGNED)

OUTFALL NUMBER 1.30 If you are a primary industry and this outfall contains process wastewater, refer to Table A in the instructions to determine which of the GC/MS fractions you must test for. Mark X in column 2-A for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. Mark X in column 2-B for each pollutant you know or have reason to believe is present. Mark X in column 2-C for each pollutant you believe to be absent. If you mark either columns 2-A or 2-B for any pollutant, you must provide the results of at least one analysis for that pollutant. Note that there are seven pages to this part, please review each carefully. Complete one table (all seven pages) for each outfall. See instructions for additional details and requirements.

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A.

TEST-ING REQUIRED B.

BELIEVE D

PRESENT C.

BELIEVE D

ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG. VALUE (if available)

D.

NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B.

NO OF ANALYSES (1)

CONCENTRATION (2)

MASS METALS, AND TOTAL PHENOLS 1M. Antimony, Total (7440-36-9) 2M. Arsenic, Total (7440-38-2) 3M. Beryllium, Total (7440-41-7) 4M. Cadmium, Total (7440-43-9) 5M. Chromium III (16065-83-1) 6M. Chromium VI (18540-29-9) 7M. Copper, Total (7440-50-8) 8M. Lead, Total (7439-92-1) 9M. Magnesium Total (7439-95-4) 10M. Mercury, Total (7439-97-6) 11M. Molybdenum Total (7439-98-7) 12M. Nickel, Total (7440-02-0) 13M. Selenium, Total (7782-49-2) 14M. Silver, Total (7440-22-4) 15M. Thallium, Total (7440-28-0) 16M. Tin Total (7440-31-5) 17M. Titanium Total (7440-32-6) 18M. Zinc, Total (7440-66-6)

MO 780-1516 (06-13)

PAGE 2 MO-0098001 007

<0.0006

<0.001 1

mg/L lbs/day

0.0007

<0.001 1

mg/L lbs/day

<0.0002

<0.001 1

mg/L lbs/day

<0.0002

<0.001 1

mg/L lbs/day

<5.8

<0.87 1

ug/L lbs/day

0.007 0.001 1

mg/L lbs/day

<0.0006

<0.001 1

mg/L lbs/day

<0.0002

<0.001 1

mg/L lbs/day

18 2.7 1

mg/L lbs/day

<0.0002

<0.001 1

mg/L lbs/day

0.00044

<0.001 1

mg/L lbs/day

<0.001

<0.001 1

mg/L lbs/day

<0.0002

<0.001 1

mg/L lbs/day

<0.0001

<0.001 1

mg/L lbs/day

<0.0002

<0.001 1

mg/L lbs/day

<0.06

<0.009 1

mg/L lbs/day

<0.005

<0.001 1

mg/L lbs/day

0.0038

<0.001 1

mg/L lbs/day

CONTINUED FROM PAGE 3 19M. Cyanide, Amenable to Chlorination 20M. Phenols, Total DIOXIN 2,3,7,8 - Tetra -

chlorodibenzo-P-Dioxin (1764-01-6)

DESCRIBE RESULTS

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TES-ING RE-QUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG. VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - VOLATILE COMPOUNDS 1V. Acrolein (107-02-8) 2V. Acrylonitrile (107-13-1) 3V. Benzene (71-43-2) 4V. Bis (Chloromethyl)

Ether (542-88-1) 5V. Bromoform (75-25-2) 6V.

Carbon Tetrachloride (56-23-5) 7V. Chlorobenzene (108-90-7) 8V. Chlorodibromomethane (124-48-1) 9V. Chloroethane (75-00-3) 10V. 2-Chloroethylvinyl Ether (110-75-8) 11V. Chloroform (67-66-3) 12V. Dichlorobromomethane (75-27-4) 13V. Dichloro-difluoromethane (75-71-8) 14V. 1,1 - Dichloroethane (75-34-3) 15V. 1,2 - Dichloroethane (107-06-2) 16V. 1,1 - Dichloroethylene (75-35-4) 17V. 1,3 - Dichloropropane (78-87-5) 18V. 1,2 -Dichloropropylene (542-75-6) 19V. Ethylbenzene (100-41-4) 20V. Methyl Bromide (74-83-9) 21V. Methyl Chloride (74-87-3)

MO 780-1516 (06-13)

PAGE 3 CONTINUE ON PAGE 4

<0.008

<50

lbs/day

lbs/day mg/L 1

<0.008

<0.05

lbs/day mg/L 1

<0.001

<0.0025

ug/L

<0.008

<50 1

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.003

<15

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<1502

<10000

lbs/day ug/L 1

<0.008

<5.0

1 ug/L lbs/day

CONTINUED FROM THE FRONT NPDES # (IF ASSIGNED)

OUTFALL NUMBER

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING RE-QUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC.MS FRACTION - VOLATILE COMPOUNDS (continued) 22V. Methylene Chloride (75-09-2) 23V. 1,1,2,2 - Tetra-chloroethane (79-34-5) 24V. Tetrachloroethylene (127-18-4) 25V. Toluene (108-88-3) 26V. 1,2 - Trans Dichloroethylene (156-60-5) 27V. 1,1,1 - Tri -

chloroethane (71-55-6) 28V. 1,1,2 - Tri-chloroethane (79-00-5) 29V. Trichloro -

ethylene (79-01-6) 30V. Trichloro -

fluoromethane (75-69-4) 31V. Vinyl Chloride (75-01-4)

GC/MS FRACTION - ACID COMPOUNDS 1A. 2 - Chlorophenol (95-57-8) 2A. 2,4 - Dichloro -

phenol (120-83-2) 3A. 2,4 - Dimethyl -

phenol (105-67-9) 4A. 4,6 - Dinitro - O-Cresol (534-52-1) 5A. 2,4 - Dinitro -

phenol (51-28-5) 6A. 2-Nitrophenol (88-75-5) 7A. 4-Nitrophenol (100-02-7) 8A. P - Chloro - M Cresol (59-50-7) 9A. Pentachloro -

phenol (87-86-5) 10A. Phenol (108-952) 11A. 2,4,6 - Trichloro-phenol (88-06-2) 12A. 2 - methyl - 4,6 dinitrophenol (534-52-1)

MO 780-1516 (06-13)

PAGE 4 CONTINUE ON PAGE 5

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

007 MO-0098001 lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.003

<20

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.008

<50

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.008

<50

lbs/day ug/L 1

<0.008

<50

lbs/day ug/L 1

<0.008

<50

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.008

<50

CONTINUED FROM THE FRONT

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS 1B. Acenaphthene (83-32-9) 2B. Acenaphtylene (208-96-8) 3B. Anthracene (120-12-7) 4B. Benzidine (92-87-5) 5B. Benzo (a)

Anthracene (56-55-3) 6B. Benzo (a)

Pyrene (50-32-8) 7B. 3,4 -

Benzofluoranthene (205-99-2) 8B. Benzo (ghi)

Perylene (191-24-2) 9B. Benzo (k)

Fluoranthene (207-08-9) 10B. Bis (2-Chloroethoxy)

Methane (111-91-1) 11B. Bis (2-Chloroethyl)

Ether (111-44-4) 12B. Bis (2-Chloroisopropyl)

Ether (39638-32-9) 13B. Bis (2-Ethylhexyl)

Phthalate (117-81-7) 14B. 4-Bromophenyl Phenyl Ether (101-55-3) 15B. Butyl Benzyl Phthalate (85-68-7) 16B. 2-Chloronaphthalene (91-58-7) 17B. 4-Chlorophenyl Phenyl Ether (7005-72-3) 18B. Chrysene (218-01-9) 19B. Dibenzo (a.h)

Anthracene (53-70-3) 20B. 1,2 -

Dichlorobenzene (95-50-1) 21B. 1,3 -

Dichlorobenzene (541-73-1)

MO 780-1516 (02-12)

PAGE 5 CONTINUE ON PAGE 6 lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.013

<80

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

NPDES # (IF ASSIGNED)

OUTFALL NUMBER

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS (continued) 22B. 1, 4-Dichlorobenzene (106-46-7) 23B. 3, 3-Dichlorobenzidine (91-94-1) 24B. Diethyl Phthalate (84-66-2) 25B. Dimethyl Phthalate (131-11-3) 26B. Di-N-butyl Phthalate (84-74-2) 27B. 2,4-Dinitrotoluene (121-14-2) 28B. 2,6-Dinitrotoluene (606-20-2) 29B. Di-N-Octyphthalate (117-84-0) 30B. 1,2-Diphenylhydrazine (as Azobenzene) (122 7) 31B. Fluoranthene (206-44-0) 32B. Fluorene (86-73-7) 33B. Hexachlorobenzene (87-68-3) 34B.

Hexachlorobutadiene (87-68-3) 35B. Hexachloro-cyclopentadiene (77-47-4) 36B. Hexachloroethane (67-72-1) 37B. Indeno (1,2,3-c-d)

Pyrene (193-39-5) 38B. Isophorone (78-59-1) 39B. Naphthalene (91-20-3) 40B. Nitrobenzene (98-95-3) 41B. N-Nitro-sodimethylamine (62 9)

MO 780-1516 (06-13)

PAGE 6 CONTINUE ON PAGE 7 CONTINUED FROM PAGE 5

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.004

<20

lbs/day ug/L 1

<0.002

<10

007 MO-0098001 lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10 lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

CONTINUED FROM THE FRONT

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TES-ING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS (continued) 42B. N-Nitroso N-Propylamine (621-64-7) 43B. N-Nitro-sodiphenylamine (86 6) 44B. Phenanthrene (85-01-8) 45B. Pyrene (129-00-0) 46B. 1,2,4-Tri chlorobenzene (120-82-1)

GC/MS FRACTION - PESTICIDES 1P. Aldrin (309-00-2) 2P. -BHC (319-84-6) 3P. -BHC (319-84-6) 4P. -BHC (58-89-9) 5P. -BHC (319-86-8) 6P. Chlordane (57-74-9) 7P. 4,4-DDT (50-29-3) 8P. 4,4-DDE (72-55-9) 9P. 4,4-DDD (72-54-8) 10P. Dieldrin (60-57-1) 11P. -Endosulfan (115-29-7) 12P. -Endosultan (115-29-7) 13P. Endosulfan Sulfate (1031-07-8) 14P. Endrin (72-20-8) 15P. Endrin Aldehyde (7421-93-4) 16P. Heptachlor (76-44-8)

MO 780-1516 (06-13)

PAGE 7 CONTINUED ON PAGE 8

lbs/day ug/LL 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.001

<5.0

lbs/day ug/L 1

<0.002

<10

lbs/day ug/L 1

<0.002

<10

NPDES # (IF ASSIGNED)

OUTFALL NUMBER

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - PESTICISES (continued) 17P. Heptachlor Epoxide (1024-57-3) 18P. PCB-1242 (53469-21-9) 19P. PBC-1254 (11097-69-1) 20P. PCB-1221 (11104-28-2) 21P. PCB-1232 (11141-16-5) 22P. PCB-1248 (12672-29-6) 23P. PCB-1260 (11096-82-5) 24P. PCB-1016 (12674-11-2) 25P. Toxaphene (8001-35-2)

J. RADIOACTIVITY (1) Alpha Total (2) Beta Total (3) Radium Total (4) Radium 226 Total MO 780-1516 (06-13)

PAGE 8 CONTINUED FROM PAGE 7 MO-0098001 007

<0.606 1

pCi/L

<0.981 1

pCi/L

<0.981 1

pCi/L

APPLICATION FOR DISCHARGE PERMIT FORM D - PRIMARY INDUSTRIES TABLE II NPDES # (IF ASSIGNED)

OUTFALL NUMBER 1.30 If you are a primary industry and this outfall contains process wastewater, refer to Table A in the instructions to determine which of the GC/MS fractions you must test for. Mark X in column 2-A for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. Mark X in column 2-B for each pollutant you know or have reason to believe is present. Mark X in column 2-C for each pollutant you believe to be absent. If you mark either columns 2-A or 2-B for any pollutant, you must provide the results of at least one analysis for that pollutant. Note that there are seven pages to this part, please review each carefully. Complete one table (all seven pages) for each outfall. See instructions for additional details and requirements.

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A.

TEST-ING REQUIRED B.

BELIEVE D

PRESENT C.

BELIEVE D

ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG. VALUE (if available)

D.

NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B.

NO OF ANALYSES (1)

CONCENTRATION (2)

MASS METALS, AND TOTAL PHENOLS 1M. Antimony, Total (7440-36-9) 2M. Arsenic, Total (7440-38-2) 3M. Beryllium, Total (7440-41-7) 4M. Cadmium, Total (7440-43-9) 5M. Chromium III (16065-83-1) 6M. Chromium VI (18540-29-9) 7M. Copper, Total (7440-50-8) 8M. Lead, Total (7439-92-1) 9M. Magnesium Total (7439-95-4) 10M. Mercury, Total (7439-97-6) 11M. Molybdenum Total (7439-98-7) 12M. Nickel, Total (7440-02-0) 13M. Selenium, Total (7782-49-2) 14M. Silver, Total (7440-22-4) 15M. Thallium, Total (7440-28-0) 16M. Tin Total (7440-31-5) 17M. Titanium Total (7440-32-6) 18M. Zinc, Total (7440-66-6)

MO 780-1516 (06-13)

PAGE 2 lbs/day

mg/L mg/L 1

lbs/day

mg/L lbs/day mg/L 1

1 0.0055 0.0037 0.089

1 mg/L lbs/day 0.062 0.0026

lbs/day mg/L 1

0.062 0.0026

1 mg/L 1

<0.024

<0.001

lbs/day mg/L 1

0.029 0.0012

lbs/day mg/L lbs/day

<0.0048

<0.0002

<139

<5.8 1

lbs/day mg/L 1

<0.12

<0.005

lbs/day mg/L 1

<1.44

<0.06

lbs/day mg/L 1

<0.0048

<0.0002

1

<0.0002 1

mg/L

<0.0002 lbs/day mg/L lbs/day

<0.0048 mg/L lbs/day mg/L 1

0.132

1 0.0021

0.05 lbs/day mg/L

<0.0002

<0.0048 mg/L lbs/day 0.062

<0.0048 1

lbs/day

MO-0098001

<0.0006 0.0026 016

<0.014 1

360.3 lbs/day 15

CONTINUED FROM PAGE 3 19M. Cyanide, Amenable to Chlorination 20M. Phenols, Total DIOXIN 2,3,7,8 - Tetra -

chlorodibenzo-P-Dioxin (1764-01-6)

DESCRIBE RESULTS

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TES-ING RE-QUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG. VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - VOLATILE COMPOUNDS 1V. Acrolein (107-02-8) 2V. Acrylonitrile (107-13-1) 3V. Benzene (71-43-2) 4V. Bis (Chloromethyl)

Ether (542-88-1) 5V. Bromoform (75-25-2) 6V.

Carbon Tetrachloride (56-23-5) 7V. Chlorobenzene (108-90-7) 8V. Chlorodibromomethane (124-48-1) 9V. Chloroethane (75-00-3) 10V. 2-Chloroethylvinyl Ether (110-75-8) 11V. Chloroform (67-66-3) 12V. Dichlorobromomethane (75-27-4) 13V. Dichloro-difluoromethane (75-71-8) 14V. 1,1 - Dichloroethane (75-34-3) 15V. 1,2 - Dichloroethane (107-06-2) 16V. 1,1 - Dichloroethylene (75-35-4) 17V. 1,3 - Dichloropropane (78-87-5) 18V. 1,2 -Dichloropropylene (542-75-6) 19V. Ethylbenzene (100-41-4) 20V. Methyl Bromide (74-83-9) 21V. Methyl Chloride (74-87-3)

MO 780-1516 (06-13)

PAGE 3 CONTINUE ON PAGE 4

<0.011

<50

lbs/day

lbs/day mg/L 1

<1.2

<0.05

lbs/day mg/L 1

<0.06

<0.0025

ug/L

<0.011

<50 1

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.004

<15

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<2.20

<10000

lbs/day ug/L 1

<0.002

<5.0

1 ug/L lbs/day

CONTINUED FROM THE FRONT NPDES # (IF ASSIGNED)

OUTFALL NUMBER

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING RE-QUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC.MS FRACTION - VOLATILE COMPOUNDS (continued) 22V. Methylene Chloride (75-09-2) 23V. 1,1,2,2 - Tetra-chloroethane (79-34-5) 24V. Tetrachloroethylene (127-18-4) 25V. Toluene (108-88-3) 26V. 1,2 - Trans Dichloroethylene (156-60-5) 27V. 1,1,1 - Tri -

chloroethane (71-55-6) 28V. 1,1,2 - Tri-chloroethane (79-00-5) 29V. Trichloro -

ethylene (79-01-6) 30V. Trichloro -

fluoromethane (75-69-4) 31V. Vinyl Chloride (75-01-4)

GC/MS FRACTION - ACID COMPOUNDS 1A. 2 - Chlorophenol (95-57-8) 2A. 2,4 - Dichloro -

phenol (120-83-2) 3A. 2,4 - Dimethyl -

phenol (105-67-9) 4A. 4,6 - Dinitro - O-Cresol (534-52-1) 5A. 2,4 - Dinitro -

phenol (51-28-5) 6A. 2-Nitrophenol (88-75-5) 7A. 4-Nitrophenol (100-02-7) 8A. P - Chloro - M Cresol (59-50-7) 9A. Pentachloro -

phenol (87-86-5) 10A. Phenol (108-952) 11A. 2,4,6 - Trichloro-phenol (88-06-2) 12A. 2 - methyl - 4,6 dinitrophenol (534-52-1)

MO 780-1516 (06-13)

PAGE 4 CONTINUE ON PAGE 5

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

016 MO-0098001 lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.002

<5.0

lbs/day ug/L 1

<0.003

<20

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.011

<50

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.011

<50

lbs/day ug/L 1

<0.011

<50

lbs/day ug/L 1

<0.011

<50

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.011

<50

CONTINUED FROM THE FRONT

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS 1B. Acenaphthene (83-32-9) 2B. Acenaphtylene (208-96-8) 3B. Anthracene (120-12-7) 4B. Benzidine (92-87-5) 5B. Benzo (a)

Anthracene (56-55-3) 6B. Benzo (a)

Pyrene (50-32-8) 7B. 3,4 -

Benzofluoranthene (205-99-2) 8B. Benzo (ghi)

Perylene (191-24-2) 9B. Benzo (k)

Fluoranthene (207-08-9) 10B. Bis (2-Chloroethoxy)

Methane (111-91-1) 11B. Bis (2-Chloroethyl)

Ether (111-44-4) 12B. Bis (2-Chloroisopropyl)

Ether (39638-32-9) 13B. Bis (2-Ethylhexyl)

Phthalate (117-81-7) 14B. 4-Bromophenyl Phenyl Ether (101-55-3) 15B. Butyl Benzyl Phthalate (85-68-7) 16B. 2-Chloronaphthalene (91-58-7) 17B. 4-Chlorophenyl Phenyl Ether (7005-72-3) 18B. Chrysene (218-01-9) 19B. Dibenzo (a.h)

Anthracene (53-70-3) 20B. 1,2 -

Dichlorobenzene (95-50-1) 21B. 1,3 -

Dichlorobenzene (541-73-1)

MO 780-1516 (02-12)

PAGE 5 CONTINUE ON PAGE 6 lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.02

<80

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

NPDES # (IF ASSIGNED)

OUTFALL NUMBER

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS (continued) 22B. 1, 4-Dichlorobenzene (106-46-7) 23B. 3, 3-Dichlorobenzidine (91-94-1) 24B. Diethyl Phthalate (84-66-2) 25B. Dimethyl Phthalate (131-11-3) 26B. Di-N-butyl Phthalate (84-74-2) 27B. 2,4-Dinitrotoluene (121-14-2) 28B. 2,6-Dinitrotoluene (606-20-2) 29B. Di-N-Octyphthalate (117-84-0) 30B. 1,2-Diphenylhydrazine (as Azobenzene) (122 7) 31B. Fluoranthene (206-44-0) 32B. Fluorene (86-73-7) 33B. Hexachlorobenzene (87-68-3) 34B.

Hexachlorobutadiene (87-68-3) 35B. Hexachloro-cyclopentadiene (77-47-4) 36B. Hexachloroethane (67-72-1) 37B. Indeno (1,2,3-c-d)

Pyrene (193-39-5) 38B. Isophorone (78-59-1) 39B. Naphthalene (91-20-3) 40B. Nitrobenzene (98-95-3) 41B. N-Nitro-sodimethylamine (62 9)

MO 780-1516 (06-13)

PAGE 6 CONTINUE ON PAGE 7 CONTINUED FROM PAGE 5

<10

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<0.003

<20

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<0.003

<10

016 MO-0098001 lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10 lbs/day ug/L 1

<0.003

<10

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<0.003

<10

lbs/day ug/L 1

<0.003

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

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<0.003

<10

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<0.003

<10

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<0.003

<10

CONTINUED FROM THE FRONT

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TES-ING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS (continued) 42B. N-Nitroso N-Propylamine (621-64-7) 43B. N-Nitro-sodiphenylamine (86 6) 44B. Phenanthrene (85-01-8) 45B. Pyrene (129-00-0) 46B. 1,2,4-Tri chlorobenzene (120-82-1)

GC/MS FRACTION - PESTICIDES 1P. Aldrin (309-00-2) 2P. -BHC (319-84-6) 3P. -BHC (319-84-6) 4P. -BHC (58-89-9) 5P. -BHC (319-86-8) 6P. Chlordane (57-74-9) 7P. 4,4-DDT (50-29-3) 8P. 4,4-DDE (72-55-9) 9P. 4,4-DDD (72-54-8) 10P. Dieldrin (60-57-1) 11P. -Endosulfan (115-29-7) 12P. -Endosultan (115-29-7) 13P. Endosulfan Sulfate (1031-07-8) 14P. Endrin (72-20-8) 15P. Endrin Aldehyde (7421-93-4) 16P. Heptachlor (76-44-8)

MO 780-1516 (06-13)

PAGE 7 CONTINUED ON PAGE 8

lbs/day ug/L 1

<0.003

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<10

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<0.002

<5.0

lbs/day ug/L 1

<0.003

<10

lbs/day ug/L 1

<0.003

<10

NPDES # (IF ASSIGNED)

OUTFALL NUMBER

1. POLLUTANT AND CAS NUMBER (if available)

2. MARK X

3. EFFLUENT

4. UNITS

5. INTAKE (optional)

A. TESTING REQUIRED B.

BELIEVED PRESENT C.

BELIEVED ABSENT A. MAXIMUM DAILY VALUE B. MAXIMUM 30 DAY VALUE (if available)

C. LONG TERM AVRG.

VALUE (if available)

D. NO. OF ANALYSES (1)

CONCENTRATION (2) MASS (1)

CONCENTRATION (2) MASS A.

CONCEN-TRATION B. MASS A. LONG TERM AVRG.

VALUE B. NO OF ANALYSES (1)

CONCENTRATION (2)

MASS GC/MS FRACTION - PESTICISES (continued) 17P. Heptachlor Epoxide (1024-57-3) 18P. PCB-1242 (53469-21-9) 19P. PBC-1254 (11097-69-1) 20P. PCB-1221 (11104-28-2) 21P. PCB-1232 (11141-16-5) 22P. PCB-1248 (12672-29-6) 23P. PCB-1260 (11096-82-5) 24P. PCB-1016 (12674-11-2) 25P. Toxaphene (8001-35-2)

J. RADIOACTIVITY (1) Alpha Total (2) Beta Total (3) Radium Total (4) Radium 226 Total MO 780-1516 (06-13)

PAGE 8 CONTINUED FROM PAGE 7

016 MO-0098001

pCi/L

<0.654

pCi/L

<0.786

pCi/L

<0.786

Attachment A Description of Outfalls 001 - Radwaste Treatment System This system serves to collect, process, store, recycle, and dispose of liquid radioactive waste generated at Callaway Energy Center. Six general sub-systems can be defined as described below:

The Boron Recycle System receives reactor coolant for the purpose of processing this waste stream for discharge. Boric acid is used as a neutron absorber in the primary system.

The boron concentration can vary substantially in Outfall 001 based on plant operation.

Also the ion exchange resin utilized in the radwaste treatment system can become rapidly saturated with boron allowing boron to pass through the treatment demineralizers. Therefore, processing of liquid radwaste by demineralization could result in up to 1000 mg/l of boron being discharged in Outfall 001. This has been noted in past NPDES Permit Reapplications for Callaway Energy Center. Although boron concentration in this Outfall may reach up to 1000 mg/L in the Discharge Monitor Tank (sample point prior to discharge), this waste stream is routed to the plant discharge line where it mixes with a minimal flow of 3,000 gpm as required by the plants Nuclear Regulatory Commission operating license. However, with administrative controls the dilution flow is maintained greater than 5,000 gpm allowing the final effluent at the point of discharge into the Missouri River to contain less than 50 mg/l of boron.

The Liquid Radwaste System collects and processes floor and equipment drains from the containment, auxiliary building, fuel building, and radwaste buildings during normal operation. However, during outages, non-radioactive drainage from equipment in these buildings may be treated by the Oily Waste System as described in Attachment C.

The Laundry and Hot Shower system collects waste generated from washing radioactively contaminated protective gear and clothing and personnel decontamination shower wastewater. These wastes are then transferred to the liquid radwaste system for treatment.

The Secondary Liquid Waste system is used to process condensate demineralizer regeneration wastes and potentially radioactive liquid waste collected from the turbine building. The condensate demineralizer regeneration waste is divided into two waste streams; High TDS waste from the acid and caustic rinses used when chemically regenerating spent resin, and low TDS waste which results from the initial back-flushing of the unregenerated resin and the final rinsing of the regenerated resin to remove acid and caustic.

Steam Generator Blowdown is normally recycled to the main condenser for reuse in the secondary cycle. Provisions also exist to discharge the treated blowdown via Outfall 001 although this has not been done in the last thirty five years.

It should be noted that the radwaste treatment system is specifically designed for flexibility to achieve Nuclear Regulatory Commission (NRC) limitations. Actual treatment for any given batch of wastewater is dictated by the following criteria:

The level of radiological contamination and the corresponding NRC mandated discharge criteria

The NPDES permit discharge limitations

The most effective waste treatment scheme that will give the smallest volume of solid radwaste.

Overall waste stream management - processing and holdup rates, volumes of other waste streams requiring treatment or storage, etc.

The need, feasibility, and economics of the recycle versus discharge options.

The following wastewater treatment systems are used as required to treat this waste stream for recycle or discharge in compliance with NRC requirements and are also available as auxiliary or backup treatment systems to treat this discharge for compliance with NPDES permit limitations: Evaporation and/or Mixing and/or Filtration and/or Carbon Absorption and/or Ion Exchange and/or Neutralization and/or Reuse/Recycle or treated Effluent. All processing in the Radwaste Treatment System is done on a batch basis except team generator blowdown. After monitoring for radioactive content, release rates are controlled administratively to ensure that radioactive discharge criteria are met.

ALPS - Advanced Liquid Processing System is a permanently installed vendor provided skid used for treatment of liquid radioactive waste. This skid consists of six vessels and a filter housing. These components may contain various resin mixtures, charcoal adsorption media and/or filter media to provide optimum treatment for the specific wastewater being processed (show on the Flow Diagram and Water Balance).

002 - Cooling Tower Blowdown A cooling tower is utilized to dissipate excess heat to the atmosphere from the Circulating and Service Water Systems. Outfall 002 is designed as the cooling tower blowdown discharge. Blowdown from the cooling tower is necessary to maintain dissolved solids concentration in the recirculating water within acceptable operating limits.

003 - Water Treatment Plant Wastes The water treatment plant (WTP) supplies clarified river water for cooling tower makeup and other plant cooling water systems. The suspended material that is removed from

the river water is drawn from the bottom of the clarifiers as sludge. This sludge is routed through a sedimentation lagoon for solids removal. A single sedimentation lagoon is utilized; sedimentation lagoon #5 was constructed in the fall of 2016. Demineralizer system waste streams and oil separator discharges are also routed to sedimentation lagoon #5. Sedimentation lagoon #5 receives water from the demineralizer waste sump with this flow cascading to lagoon #6. The demineralizer system waste stream (previously a separate discharge point, Outfall 004, which was eliminated during previous permitting) consists of wastes generated from resin regeneration, sand and carbon filter backwash, miscellaneous wastes from floor drainage, and wet well overflows. Note finally, that this lagoon also receives effluent from the Oily Waste Processing System (which also receives effluent from an oil recovery well used to remediate a historic on-site release).

The supernatant from the sedimentation lagoon is designated as Outfall 003. Outfall 003 has been recycled for more than 20 years by routing it back to the head of the water treatment plant via a supernatant pump station.

007 - Sanitary Treatment Lagoons Outfall 007 is defined as the sanitary wastewater treatment system discharge. Primary treatment is provided in a conventional three-cell stabilization pond. Effluent from the final cell is routed (in series) to two wetland basins. Both are "artificial" (constructed) wetlands created by conversion of filled WTP (sludge) sedimentation lagoons.

The supernatant from the third stabilization pond is designated as Outfall 007. The effluent then flows through two wetlands. The connection from discharge of the final wetland to the supernatant pump station was made in conjunction with the construction of an additional WTP sedimentation lagoon (as described in a previous NPDES Permit reapplication and in the construction permit application). Outfall 007 is recycled by routing it back to the head of the water treatment plant via the WTP supernatant pump station.

Outfall 009 - Intake Heater Blowdown The river intake structure contains two recirculating electric heaters, which are used to prevent ice formation on the intake bar screen during the winter months. Outfall 009 consists of discharges from the infrequent blowdown or drainage of these boilers. We have not discharged from this outfall in the past thirty years. The boilers are currently kept in a dry lay-up condition.

Outfall 010 - Storm Water Runoff Settling Pond The drainage area for the Outfall 010 Settling Pond encompasses a total of 108 acres.

Only 20% of the drainage area consists of impervious plant site area. These areas include the cooling water chemical control building, the quality control building, the

former Unit #2 area and an area plant west of the radwaste building. The remaining drainage area consists of grassy areas within the plant boundary and areas leased to the Missouri Department of Conservation (MDC). The pond has a retention time greater than 24 hours2.777778e-4 days 0.00667 hours 3.968254e-5 weeks 9.132e-6 months . Two 48-inch square overflow boxes are located at the north side of the settling pond. Flow enters the overflow boxes and goes under the earthen pond dam to the actual discharge/sampling location. Metal louvers have been installed on the top opening of the concrete overflow box to prevent large debris from entering the storm water discharge. Outfall 010 discharges to Logan Creek.

Outfall 011 - Storm Water Runoff Settling Pond The drainage area for the Outfall 011 Settling Pond encompasses a total of 425 acres.

Only 2% of the drainage area consists of the impervious area on the plant site. These areas include the water treatment plant, radwaste building, operation support facility, demineralizer potable water building and the circulating and service water pump houses. The remaining drainage area consists of grassy areas, excavation surplus storage, and areas leased to the MDC. The pond has a retention time of less than 24 hours2.777778e-4 days 0.00667 hours 3.968254e-5 weeks 9.132e-6 months . Two 48-inch square overflow boxes are located on the north side of the settling pond. Flow enters these overflow boxes and goes under the earthen pond damn to the actual discharge/sampling location. Metal louvers have been installed on the top opening of the concrete overflow box to prevent large debris from entering the storm water discharge. Outfall 011 discharges to Logan Creek.

Outfall 012 - Storm Water Runoff The drainage area for the Outfall 012 Settling Pond encompasses a total of 87 acres.

Approximately 25% of the total drainage area consists of impervious area on the plant site. This outfall collects storm water runoff from the most of the plant area including the parking lots, office buildings, part of the switchyard, the turbine building, the outage maintenance facility and the Stores I building. The remaining areas consist of grassy areas. The settling pond was closed in 2022 under MORA19240 and reconfigured to pre-pond conditions. Quarterly sampling events occur as directed by the permit. Outfall 012 discharges to Mud Creek.

Resulting sample data has shown that the ponds are in an established state that includes grass growth along with no issues of erosion or other issues. Because of the established site conditions, Ameren believes the above stormwater discharge can be removed from the NPDES permit.

Outfall 014 - Storm Water Runoff The drainage area for the Outfall 014 Settling Pond encompasses a total of 100 acres.

Only 4% of the drainage area consists of impervious areas on the plant site. These areas include, half of the construction parking lot, the Stores II building and the maintenance shop annex. The remaining drainage area consists of grassy areas and

the land leased to the MDC. The settling pond was closed in 2022 under MORA19240 and reconfigured to pre-pond conditions. Outfall 014 discharges to Auxvasse Creek.

Resulting sample data has shown that the ponds are in an established state that includes grass growth along with no issues of erosion or other issues. Because of the established site conditions, Ameren believes the above stormwater discharge can be removed from the NPDES permit.

Outfall 015 - Storm Water Runoff The drainage area for the Outfall 015 Settling Pond encompasses a total of 60 acres.

Only one percent of the drainage area consists of impervious areas, which are paved roadways. The remaining area consists of grassy areas and land leased to the MDC.

The settling pond was closed in 2022 under MORA19240 and reconfigured to pre-pond conditions. Outfall 015 discharges to Auxvasse Creek.

NOTE: The MDC uses a minor portion of the leased land for farming and the remaining land is left in its native state for wildlife habitat.

Resulting sample data has shown that the ponds are in an established state that includes grass growth along with no issues of erosion or other issues. Because of the established site conditions, Ameren believes the above stormwater discharge can be removed from the NPDES permit.

Outfall 016 - Cooling Tower Bypass This outfall consists of clarified river water and wastewater that has been recycled through the water treatment plant. It is used to moderate flow through the water treatment plant and to provide carrier water in the discharge line if needed when discharging from Outfall 001.

Outfall 017 - Ultimate Heat Sink The Ultimate Heat Sink is a cooling pond that can provide cooling water to various plant systems during abnormal plant conditions. Outfall 017 is the overflow from the Ultimate Heat Sink, to storm water runoff pond settling pond Outfall 011. It is a no discharge outfall.

Outfall 018 - Firewater Discharges Fire protection test water is an intermittent depending on the operations at the Energy Center. On a biannual basis the energy center is required to completely empty all the fire protection water from the associated tank. This amounts to 300,000 gallons total.

Other fire water discharges include annual test discharges that are 80,000 gallons total.

All fire protection test water is discharged to Outfall 011.

Outfall 100 - Discharge Point at Missouri River This outfall consists of a combined effluent discharge for Outfalls 001, 002 and 016.

These Outfalls discharge to the Missouri River through a common man-made conveyance.

Attachment B Return of River Water The Callaway Energy Center has five points at which river water is returned back to the river, none are designated as outfalls.

1. Intake Structure Stilling Basin - The stilling basin at the intake structure predominately receives water from the excess flow of the intake pumps via the free discharge valve and returns this flow to the river. Other minor contributions include the intake sump discharge and a well used to supply lube water. As this flow is not contaminated with process waste, we believe it constitutes a return of river water.

2. Intake Line Drainage - The plant has a 48-inch diameter line that carries Missouri River water from the intake structure to the plant, which is approximately five miles away. Infrequently, it is necessary to drain this line. Usually, this only occurs about two or three times per year. The line is drained by opening the free discharge valve and/or the discharge valves for the intake pumps. This allows the water in the line to flow back to the river through the free discharge valve and the de-energized intake pumps. The drainage rate is about the same as the intake rate when the pumps are operating, so it should not pick up any additional solids that may have settled out in the line. Therefore, we believe this intake line drain back flow constitutes a return of river water.

3. Raw Water Bypass - This line diverts untreated water from the head of the water treatment plant to the plant discharge line. It is used to release excess water that is pumped from the river. The flow through this line can vary from 0 to 10,000 gallons per minute based on operating requirements. Since the line diverts and returns untreated river water, we believe it constitutes a return of river water.

4. Downstream River Sampler - Approximately 1.5 miles downstream of the intake structure is an automatic river water sampler. The sampler pumps from 1 to 2.5 GPM continuously from the river, composites a small sample and returns the remaining flow to the river. No pollutants are added to this flow so it is our position that this discharge flow is a return of river water.

5. Intake River Sampler - An automatic river water sampler is located at the intake structure to provide upstream sample data. This sampler pumps from 1 to 2.5 GPM continuously from the river, composites a small sample, and returns the remaining flow to the river. No pollutants are added to this flow so it is our position that this discharge flow is a return of river water.

ATTACHMENT C Description of Intermittent Flows Five of the six conventional outfalls defined in this application can be considered to include intermittent discharges since they process and/or release wastewater intermittently. Each is described below.

ROUTINE RELEASES:

001 - Radwaste Treatment - All of the subsystems described in Attachment A, except Steam Generator Blowdown (SGB), process or release discrete batches of wastewater.

The frequency and magnitude of each is variable. The flows from the subsystems accumulate in the Discharge Monitor Tanks (DMTs). The discharge flow rate from the DMTs is relatively constant for each batch. The current system typically produces discharges flows of approximately 250 gpm, but may discharge at 450 gpm with a 2 pump operation. Only one DMT can be discharged each day during normal operation with the maximum daily discharge of less than 100,000 gallons. Only very infrequently during refueling outages is it necessary to discharge two DMTs during one day with a maximum discharge of 190,000 gallons. Approximately five tanks are discharged per month under normal plant operation. During re-fueling outages approximately eight tanks are discharged per month.

During recovery from major plant outages and other unusual transient conditions, it may be necessary to discharge Steam Generator Blowdown (SGB). The discharge flow rate varies up to 360 gpm resulting in a maximum daily discharge flow of up to 518,400 gallons. Past operation has shown that such discharges occur infrequently. SGB has not been discharged for more than 25 years. Since this discharge occurs so infrequently, the SGB flow was not included in the maximum flows shown in Form C, Item 2.2. Previous testing of SGB indicates that this waste stream is of equal or higher quality than other much more routine components of Radwaste Treatment, Outfall 001 effluent.

003 - Water Treatment Plant Wastes - For the past 20 years, this outfall has been recycled back to the head of the water treatment plant for reuse so the discharge flow is zero.

007 - Sanitary Wastewater - For more than 15 years, this outfall has been recycled back to the head of the water treatment plant so the discharge flow is zero.

009 - Intake Heater Blowdown - Discharges from this outfall would only be anticipated in the event of extremely cold weather and are thus seasonal and intermittent. If these heaters were placed in service, it is estimated that blowdown would occur approximately once per week (and amount to less than 100 gallons). At the end of an operating season they would be drained, releasing approximately 6,000 gallons of wastewater.

There has been no discharge from this outfall for more than 30 years.

016-Cooling Tower Bypass - Discharges of cooling tower bypass vary considerably. At times discharges may occur only a few times during an entire month. During some months discharges occur almost daily for approximately 3 hours3.472222e-5 days 8.333333e-4 hours 4.960317e-6 weeks 1.1415e-6 months per day and infrequently the bypass is operated continuously. Cooling tower bypass is used to control cooling tower makeup, assist in maintaining circulating and service water chemistry, and at times provide additional flow to the discharge line during releases from Outfall 001.

DISCHARGES DURING PLANT OUTAGES:

It is necessary to drain many systems during plant outages for inspections and maintenance. In order to ensure that this water is of the same quality as water that is discharged during operation, some additional/alternate monitoring is performed.

When the cooling tower basin, and/or associated lines (between the basin and the power block) are drained, a single grab sample will be obtained and analyzed to verify compliance with Outfall 002 permit limits prior to discharge. This alternate monitoring will be performed since continuous monitoring will not be possible at all times during the draining of these systems.

Various non-radioactive systems in the Auxiliary Building have been drained in the past to floor drains in the Auxiliary Building to allow for inspection and maintenance. The floor drains from the Auxiliary Building are routed to the Radwaste System for processing and treatment. Since it is not necessary to process these non-radioactive liquid wastes through the Radwaste System, at times we divert these non-radioactive drains to the Oily Waste Processing System for treatment prior to being recycled.

Recycling of this water also results in trace amounts of chemical in Outfalls 002, 003, and 016.

ATTACHMENT D Chemical Usage The various chemical compounds that may occur in the discharges from Callaway Energy Center during normal operation fall into three usage categories:

Bulk Usage This group of compounds describes chemicals that are added directly to specific water systems for treatment at a regular rate or interval. Table 1 lists these chemicals along with their predominant function and potential discharge points.

Laboratory Reagents This category consists of a group of compounds stored and used in the five on-site plant laboratories. The predominant characteristic of this group is the relatively low usage, which would result in negligible levels in the effluent. Laboratory reagents may be discharged through the radwaste treatment Outfall 001, and sanitary wastewater in Outfall 007. At the request of the Department, Ameren Missouri will provide an inventory of these chemical compounds.

Other Chemical Compounds This grouping includes other chemical compounds that may be discharged and are not included in the previous lists. General housekeeping and maintenance chemicals, and erosion/corrosion products or byproducts from the Plant's infrastructure or fuel materials are not individually assessed. However, the Form C and D analytical data should reflect any contributions from routine use of these compounds. Note that 12% sodium hypochlorite identified in Table 1 is also used to clean the intake well periodically. At times, we use 20% hydrochloric acid to clean scale in the well. Less than 1000 gallons of 12% sodium hypochlorite and 20% hydrochloric acid are used annually for intake well cleaning.

PFAS Usage Ameren has completed an extensive and thorough investigation into all chemicals used at the Callaway site. Currently, Ameren is not using any chemicals that contain PFAS or any related compounds.

Chemical Treatment Program for Callaway Cooling Water Systems:

Product Added WTP Stilling Basin or Clarifiers Service Water (Pump Bay)

Circulating Water System Other Coagulant Continuous ~55 gallons/day varies with river solids May apply further upstream of WTP Sodium hypochlorite

~15-30 min/day

~65 gal/day

~30-60 min/day

+ shock treatments

~135 gal/day Sodium bromide added with bleach ~ 15 gal/day added with bleach ~30 gal/day Molluskicide 1-2 times per year at the river intake as needed Coagulant aid 6 months a year

~ 20-30 gal/day Monochloramine, chlorine dioxide, or bromine activated chloramine Continuous feed at a target of 0.5-1.0 ppm at the clearwell as TRO Copolymer Continuously

~50 gal/day Hydroxyethylidine, diphonic acid Continuously

~ 23 gal/day Sodium tolyltriazole Continuously

~5 gal/day Biopenetrant 1-2 adds/week

~400 gal/month Shock treatments 3/year Sulfuric acid Continuously

~1550 gal/day Sodium bisulfite or ferrous chloride for dechlorination Continuous to CT Blowdown 0.4-2.5 gal/hour

BULK CHEMICAL USAGE - CALLAWAY

1.

Ammonium hydroxide - (Reboiler/Aux. boiler) - used for pH control in recirculating water systems; Outfall 001.

2.

Boric acid - used as a neutron absorber to provide reactivity control and corrosion inhibitor in the primary loop; Outfall 001

3.

Dispersants - (organic sulfonated copolymers) used to reduce solids deposition in process tanks and plant water systems; Outfalls 001, 002, and 003.

4.

Ethylene Glycol - used as freeze protection in recirculating water systems: Outfalls 001, 003, and 007.

5.

Hydrazine - used for dissolved oxygen control in recirculating water systems; Outfalls 001 and 003.

6.

Hydrogen Peroxide - used as a chemical shock and biocide treatment in water systems; Outfall 001 and 003.

7.

Lithium hydroxide - used for pH control in the primary loop; Outfall 001

8.

Nitrite/borate products (solutions) - used as corrosion inhibitors in recirculating water systems; Outfalls 001 and 003.

9.

Coagulants - proprietary organic polymers used as coagulants in the water treatment plant; Outfalls 002, 003,

& 016

10. Sodium hydroxide - used for regenerating demineralizer resins and for pH control in various plant and wastewater systems; Outfalls 001, 003, and 009.

11. Sodium hypochlorite - used as a biocide in the circulating, service, water treatment, ultimate heat sink, clarifiers, and potable water systems; Also used to generate monochloramine: Outfalls 001, 002, 003, and 016.

12. Sodium molybdate - used as a corrosion inhibitor in closed water systems; Outfalls 001 and 003.

13. Sodium tolytriazole or Benzotriazole - used as a copper corrosion inhibitor; Outfalls 001, 002, and 003

14. Sulfuric acid - used for regenerating demineralizer resins and for pH control in various water and wastewater systems; Outfalls 001, 002, 003, and 009.

15. Monoethanolamine (ETA) - used as a pH control in closed water systems; Outfalls 001 and 003.

16. Sodium bromide - used in conjunction with sodium hypochlorite as a biocide in water systems; Outfalls 001, 002, and 003.

17. Methoxypropylamine (MPA)- used as a pH control agent in closed water systems; Outfalls 001 and 003.

18. (1-Hydroxyethylidene) diphosphonic acid (HEDP) - used to inhibit calcium carbonate scale formation in water systems and the ultimate heat sink; Outfalls 001, 002, and 003.

19. Nalco Biopenetrant - used as a biopenetrant to improve the efficiency of biocides in controlling bacteria that exist under deposits in piping systems; Outfalls 001, 002, and 003.

20. Phosphoric Acid or Pyrophosphate - used as a corrosion inhibitor for mild steel in recirculating water systems; Outfalls 001, 002, and 003.

22. Proprietary Methylene Bis based biocide - used in plant water systems; Outfalls 001, 002, and 003

23. Proprietary Quatenary ammonium compound - used as a biostat in plant water systems; Outfalls 002, 003 and 016.

24. Poly Acrylic Acid-may be used as a dispersant in the secondary system: Outfall 001, 003, and 017 during emergencies.

25. Ferric Sulfate-used for hydrogen sulfide consumption in the ground water sump: Outfall 003.

26. Trisodium Phosphate-containment sumps for accident conditions: Outfall 001.

27. Molluscicide - used intermittently (twice/year) at the water treatment plant and intake: Outfalls 002, 003, and 016.

28. Triazine - a biocide used at water treatment, circulating and service water systems: Outfalls 002, 003, and 016

29. a-Ketoglutaric Acid (AKGA) - to neutralize hydrazine in secondary liquid waste water prior to discharge:

Outfall 001.

30. Oxamine 6150 - An Ammonium Sulfate based solution used to generate Monochloramine. Outfalls 002, 016.

31. Sodium Bisulfite - Used to dechlorinate Cooling Tower Bypass when continuously feeding monochloramine to the Water Treatment Plant effluent. Feed rate is typically 15 gallons per day. Outfalls 002, 016

32. Flexpro CL5689 - Added to Circ and Service Water systems for mild steel corrosion control. Approximately 200 gallons added during 1 hour1.157407e-5 days 2.777778e-4 hours 1.653439e-6 weeks 3.805e-7 months treatment. 2-3 Treatment per week.

ATTACHMENT E NPDES Sampling and Analysis The chemical analysis of the various waste streams reported in this application came from two principal sources: 1) a special sampling and analytical project conducted in the fall of 2024 and 2) discharge monitoring data as required by our existing NPDES permit.

Plant personnel conducted the entire reapplication sampling effort. Power generation at the plant averaged in excess of 99% of capacity during the sampling period for all process outfalls.

As effluent from some outfalls is released intermittently and in batches, it was necessary to modify the default sampling requirements listed in application instructions for selected outfalls. Each sample location is discussed below to clarify these details and to allow the data to be interpreted correctly.

For the sampling project, analyses were performed by Callaway Energy Center, and 1 outside commercial laboratories: Pace Analytical (Hazelwood, MO). All analyses were conducted in accordance with Standard Methods and/or EPA methodology. Specific test methods or additional details on other aspects of the sampling or analysis program are available upon request.

Outfall 001 As previously defined, routine discharges from this outfall are from one of five sources:

the Boron Recycle System, the Liquid Radwaste System, the Laundry and Hot Shower system, the Secondary Liquid Waste system, and the Steam Generator Blowdown system (no discharge in the past thirty years). While processed separately, these waste streams are normally commingled and retained in various tanks prior to discharge (excluding Steam Generator Blowdown). Thus, discrete samples of each subsystem were not obtained. Further, Steam Generator Blowdown was recycled without discharge during our sampling project schedule as it has been for the past thirty years.

Outfall 002 Cooling Tower Blowdown was sampled over a 24-hour period on September 3rd, 2024.

The discharge was maintained at a constant flow rate. Flow proportional composite and multiple grab samples were taken as appropriate. Other than the exception below, all of the data shown under the 'Maximum Daily Value' columns in Forms C and D is from this sampling event. The flow monitored during this sample event is also shown here and was used to calculate the mass discharges under this heading.

Data under the 'Maximum 30 Day Values' and 'Long Term Averages' are based on data from July 2022 through Oct 2024. Mass discharges under these headings were calculated using the appropriate long-term average flow rates.

Outfall 003 Water treatment plant wastes are routed to Sedimentation pond #5 for solids removal before the supernatant is recycled back to the head of the water treatment plant. A small waste volume from makeup demineralizer plant regenerations (the previous NPDES Outfall 004) is routed to the Water Treatment Plant sludge pump station and is also treated by the sedimentation lagoons. A 24-hour flow composite and multiple grab samples were taken from the effluent of sedimentation pond #5 during the period of September 3rd, 2024 while it was being recycled back to the head of the water treatment plant. Although there was no discharge from this outfall at the time, the water quality at the sample point for Outfall 003 would be the same as the quality of the wastewater if the Outfall had been discharging. All of the data shown under the 'Maximum Daily Value' columns in Forms C and D is from the sampling event. Note that mass discharge values were calculated based on the estimated average discharge flow rate, even though the effluent was being recycled at the time.

No data was reported under the 'Maximum 30 Day' and 'Long Term Average' columns for this outfall since it is normally recycled and thus there is no recent historical monitoring data from DMR's. Ameren would like to maintain this Outfall permitted to preserve authorization to discharge from the water treatment plant, should the need arise.

Outfall 007 As described in Attachment A, effluent from the sanitary waste stabilization lagoons is routed through two artificially constructed wetlands. For this reapplication project, a single grab sample was collected on September 3rd, 2024 from the effluent weir at the point of discharge from the third treatment lagoon as required by our NPDES permit, although this effluent stream was being recycled at the time of sample collection.

Further polishing is completed by pumping this effluent to the first wetland. Flow continues by gravity through the second wetland which is routed to the supernatant pump station for recycle to the head of the water treatment plant. As the detention time within in the lagoons and the first wetland, both exceed 24 hours2.777778e-4 days 0.00667 hours 3.968254e-5 weeks 9.132e-6 months , a single grab sample was collected. Data from this sampling event is shown under the 'Maximum Daily Value' column in Form C.

Although there was no discharge from this outfall at the time the samples were taken, the water quality at the sample point for Outfall 007 would be the same as the quality of the wastewater if the outfall had been discharging. Other than the exception mentioned below, all of the data shown under the 'Maximum Daily Value' columns in Forms C and D is from these sampling events. Note that mass discharge values were calculated based on the estimated average discharge flow rate, even though the effluent was being recycled at the time.

No data was reported under the 'Maximum 30 Day' and 'Long Term Average' columns for Outfall 007 since it is normally recycled and thus there is no recent historical monitoring data from DMR's. Ameren would like to maintain this outfall permitted.

Outfall 009 The intake electric boilers are currently in a dry lay-up condition as they have been for many years, and so it was not possible to obtain a sample from them. The last discharge from this system occurred in early 1985, so recent past discharge data are not available. We want to keep this outfall permitted in order to preserve the authorization to discharge from the electric boilers, should extreme weather or other conditions warrant their use.

Outfalls 010 - 015 As described previously, storm water runoff from all plant areas is diverted to settling ponds, prior to discharge waters of the state via the outfalls specified in the existing permit. These outfalls are described in Attachment A and are shown on the attached site maps. All five outfalls were sampled for the permit reapplication, as described below.

Grab samples were taken from the storm water runoff ponds on November 18, 2024.

The day the ponds were sampled was after a rainfall event that resulted in pond discharges. The flow rates for all outfalls are based on calculated runoff (using appropriate runoff coefficients) from the actual rainfall measurements.

All of the data shown under the 'Long Term Average Value' columns in Form C are from these sampling events April 2022 - present for each outfall. The flow, calculated for the rainfall event triggering each of these discharges, is also shown here and used to calculate the mass discharges under this heading.

Outfall 016 The cooling tower bypass was sampled over a 24 hour2.777778e-4 days 0.00667 hours 3.968254e-5 weeks 9.132e-6 months period on September 3rd 2024.

Flow proportional composite and multiple grab samples were taken as appropriate. All of the data shown under the 'Maximum Daily Value' columns in Forms C and D is from the sampling event. Average flows obtained during sampling were used to calculate the mass discharges under this heading.

Data under the 'Maximum 30 Day' and 'Long Term Average' values are based on DMR data for the three year period, July 2022 through October 2024. Mass discharges under these headings were calculated using the appropriate long-term average flow rates.

Outfall 017 This is by definition a no discharge outfall; therefore it was not sampled.

Missouri River A modified composite sample (consisting of 4 aliquots, each collected approximately 6 hours6.944444e-5 days 0.00167 hours 9.920635e-6 weeks 2.283e-6 months apart) was taken of Missouri River water being pumped to the head of the water treatment plant for a 24 hour2.777778e-4 days 0.00667 hours 3.968254e-5 weeks 9.132e-6 months period on October 23, 2024. It is believed that this modified composite sample is representative of the river over a normal 24 hour2.777778e-4 days 0.00667 hours 3.968254e-5 weeks 9.132e-6 months period.

Data available on the Missouri River indicates substantial variability over longer periods of time. This data is provided on the 'Intake' Form C.

General Notes Important note on mass discharge calculation: As described previously, mass discharges listed under the 'Maximum Daily Value' heading, represent values calculated from the analytical data and the measured flows during the special re-application, sampling event. Consequently, the values shown do not necessarily represent an actual maximum mass discharge value.

Pace Analytical Laboratories, Inc. completed all of the parameters for storm water Outfalls 010, 011, 012, 014 and 015. Pace also analyzed for all the parameters for Outfalls 001, 002, 003, 007, 016 and the river intake except for the parameters listed below:

PDC Laboratories analyzed for methylmercury for Outfalls 001, 002, 003, 007, 016 and the River Intake The Callaway Energy Center chemistry staff analyzed each outfall for the remaining parameters:

Temperature Total Residual Chlorine Flow Total Hardness pH

Attachment F Section 311 and CERCLA Exemptions The chemicals listed below are used in water treatment processes and may be discharged in amounts exceeding their 'reportable quantities' under 40 CFR 117 and 302 (1989).

Chemical Anticipated Usage (Avg lbs/day)

Reportable Quantity (lbs/day)

Typical Quantity On-Site Outfalls Sodium Hydroxide 620 1,000 300,000 001, 003 & 009 Sodium Hypochlorite 2,100 100 100,000 001, 002, 003

& 016 Sulfuric Acid 26,000 1,000 450,000 001, 002, 003, and 009 Hydrazine 80 1

26,000 001 and 003

Recycling of Outfall 003, Water Treatment Plant Supernatant, (as described in Attachment A) may also result in trace amounts of these chemicals in Outfalls 002 and 016.

Ameren Missouri requests an exclusion under the NPDES exemptions from Section 311 and Superfund reporting for these four compounds and all others that are, as reported in this application, present in continuous or anticipated intermittent discharges (See Attachment D). These and other discharges for which exclusion are requested are exempt from Section 311 liability by 40 CFR 117.12(a)(1) if they are in compliance with the permit and 117.12(a)(2) 03 (3) if they are not. Discharges that are excluded from 311 reporting are also excluded from Superfund reporting. Any discharges other than those resulting from on-site spills would either result from circumstances identified in this application and be subject to neutralization treatment (see 117.12(c)) or would be continuous or anticipated intermittent discharge originating within the operating or treatment systems at the plant (see 117.12(d)). These discharges are, therefore, excluded from Section 311 and Superfund reporting requirements.

Attachment G General Comments on Standards Setting In anticipation of conditions that may be set in this permit renewal, Ameren Missouri requests the consideration of the following comments:

1. Mass Limits - The Steam Electric Guidelines (at 40 CFR Part 423.13(g))

specifically allow the permitting authority to express the quantity of pollutants allowed to be discharged as a concentration limitation instead of a mass-based limitation. Fixed numerical mass discharge limitations necessarily impose implicit flow restrictions at the allowable concentration levels. The flow restrictions are too inflexible to cope with the flow variability conditions and the electrical reliability imperatives placed on steam electric power plants. Unlike some industries in which waste stream flow variability is the result of a single factor, like production Callaway Energy Center has no such single parameter indicative of flow. Further, as a utility whose production is dictated by public consumption, the plant must be capable of attaining and maintaining full power production for as long as necessary. Since we feel that the concentration-based limits are sufficient and more appropriate for regulation of power plant discharges, we request that you do no impose any mass limitations when reissuing this permit.

2. Net Credits - In a situation whereby a limitation might be set on the discharge of a priority pollutant, Ameren Missouri feels it should reflect an adjustment credit for pollutants in the intake water, because discharges are returned to the Missouri River. As complete removal of compounds in this category would not be achieved by the water treatment systems at the Callaway Energy Center, we hereby request an appropriate net limitation be applied as necessary. We anticipate no adverse water quality effect from net limitations.

3. WET Test Scheduling - In accordance with permit conditions (Section D, Other Requirements, Item 6), Callaway Energy Center conducts an annual acute Whole Effluent Toxicity (WET) test on composite samples taken from Outfalls 002 and 016. When attempting to collect these special composite samples, it simplifies the sampling procedure considerably by maintaining the Cooling Tower Blowdown (Outfall 002) and Cooling Tower Bypass (Outfall 016) at a constant flow rate over the 24 hour2.777778e-4 days 0.00667 hours 3.968254e-5 weeks 9.132e-6 months sampling period. This eliminates the need to adjust sample aliquots proportionally with flow. The annual WET test is completed in either the spring or fall immediately following a molluskicide treatment (and algaecide treatment if performed), and concurrently with the weekly circulating and service water system chemical addition. Callaway Energy Center has conducted an acute WET Test every year for the past 5 years on Outfall 002 and 016. All WET tests conducted during these past 5 years at Callaway have passed with no issues identified.

Attachment H Section 316(b) Demonstration Status As part of the 2019 Callaway NPDES reapplication packet, Ameren submitted an updated 316(b) study. There have been no significant modifications or changes in the construction, design, location or capacity of the cooling water intake structure.

Accordingly, Ameren hereby incorporates by reference the results and conclusions of these prior studies and requests renewal of the 316(b) approval at Callaway.

Attachment I Activities, Materials and Management Practices with the Potential to Impact Storm Water Quality As described in Attachment E, reduced monitoring of storm water outfalls was authorized by DNR for this application (acknowledging the adequacy of prior characterization of these discharges). The data was entered into Missouri Forms C, eliminating the need to complete EPA form 2F; nonetheless, we believe this Attachment and the referenced drawings provide all the required data.

Routine/Permanent Significant Materials Storage The following significant materials have been identified at the Callaway Energy Center as being in contact with storm water currently or in the last three years. They are shown on drawing NPDES-001, NPDES Storm Water Information Outfalls 010-015 and described below. Note that compass direction references are relative to 'Plant North', a standardized reference designation, which is depicted on the drawing. Where possible, each item description listed below includes a number in brackets '{}' which corresponds to the drawing legend listing.

1. Amine Storage Tank - A 6,000 gallon tank located plant NE of the turbine building was installed to house ammonia hydroxide. A lined trough is located below the tank capable of holding 110% of the tank contents. This tank is currently empty and has not been used for more than 30 years. {827}

2. Caustic Storage Tank - A 10,000 gallon storage tank containing sodium hydrazine is located plant NE of the turbine building. A lined trough is below the tank capable of holding 110% of the tank contents. Caustic is unloaded from tank truckers using air pressure. {829}

3. Sulfuric Acid Storage Tank - A 10,000 gallon storage tank containing sulfuric acid is located plant NE of the turbine building. A lined trough is below the tank capable of holding 110% of the tank contents. Acid is unloaded from tank trucks using air pressure. {828}

4. Circulating/Service Water Sulfuric Acid Tank - A 14,000 gallon storage tank containing sulfuric acid is located near the circulating and service water pump house and cooling tower basin. Containment consists of a concrete dike capable of holding 110% of the tank contents. Acid is unloaded from tank trucks using air pressure {844A}

5. Gasoline Storage Tanks - One above ground gasoline storage tank located South of the Water Treatment building has a capacity of 2,000 gallons. A second above ground gasoline storage tank with a capacity of 500 gallons is located

plant W of the Stores II building. A prefabricated metal containment exists around each of the tanks of sufficient size to contain approximately 110% of the tank capacity. Gasoline is unloaded from tank truck using onboard truck pumps. {814}

6. Security Diesel Storage Tank - A 3,000 gallon underground tank containing diesel fuel is located by the Main Access Facility. Diesel fuel oil is unloaded from tank trucks using onboard truck pumps. {814}

7. Alternate Power Emergency System (AEPS) Diesel Generators - Four APES diesel generators are located on Highway CC south of the existing COOP substation. The AEPS diesel generators were installed during 2010. Mounted under each diesel generator skid is a 3500 gallon self-contained diesel fuel oil storage tank with a secondary containment.

8. Emergency Diesel Fuel Tanks-There are two 100,000 gallon underground diesel fuel oil storage tanks located plant S of the Emergency Diesel building. Diesel fuel oil is unloaded from tank trucks using onboard truck pumps. Diesel fuel is used to power the emergency diesel generators during testing and as needed to supply plant power. {838}

9. Vehicle Diesel Fuel Storage Tanks - Two above ground vehicle diesel storage tanks re located South of the Water Treatment Buillding. There is a 300 gallon tank used to store #1 diesel and 700 gallon tank used to store #2 diesel fuel oil.

Two additional above ground vehicle diesel storage tanks are located plant W of the Stores II building for storage of #2 diesel fuel oil. Each of these two tanks has a capacity of 500 gallons. A prefabricated metal containment exists around each tank of sufficient size to contain approximately 110% of tank capacity. Diesel fuel oil is unloaded from tank trucks using onboard truck pumps. A gas station type dispenser is used to fill diesel powered vehicles from these tanks. {886}

10. Auxiliary Fuel Oil Storage Tank - The auxiliary fuel oil storage tank is a 300,000 gallon carbon steel tank located plant W of the demineralizer building. An earthen berm capable of containing 110% of the tank contents surrounds the tank. An underground transfer line from the auxiliary fuel oil transfer system fills the tank.

This tank is used to supply diesel fuel oil to the auxiliary boiler and the fire protection diesel pumps. {869}

11. Circulating Water Chemical Control System Salt Storage - Two salt storage tanks (full of rock salt) are located plant north of the circulating water chemical control system building. The storage tanks and equipment have been retired in place.

12. Transformer Oil - Thirteen large power transformers are located on site. They are the main transformers (4 at 12,000 gallons), the Unit Auxiliary transformer (8,000 gallons), the Start Up Transformer (9,700 gallons), the Station Service transformers (2 at 2,770 gallons), the Alternate Energy Power Source transformer (2,170 gallons), the Engineered Safety Features transformers (2 at 2,270 gallons) and the Safeguard transformers (9,700 and 11,500 gallons). In addition, most buildings on site have associated service transformers located outside (~20-30 transformers) which each contain approximately 400 gallons of oil. Most outside oil filled electrical transformers are situated on top of a concrete lined pit which is filled with gravel. The exception to this is the Training Annex transformer and the eight 300 series site power loop transformers which do not have any containment. Any spills from these transformers would have to be contained in the drainage ditches adjacent to the transformers.

13. Demineralized Water Tank - A 150,000 gallon stainless steel demineralized water tank is located plant southeast of the turbine building. No containment exists around this tank. The tank is filled from the demineralized water storage tank through underground piping. It is used to supply water to the steam generators when the plant is shut down and during transients. During transients the tank can also be supplied by firewater. {831}

14. Condensate Water Tank - A 466,000 gallon stainless steel condensate water tank is located plant southeast of the turbine building. No containment exists around this tank. The tank is filled from the demineralized water storage tank through underground piping. It is used to supply water to the steam generators when the plant is shut down and during transients. During transients the tank can also be supplied by firewater. {831}

15. Refueling Water Tank - A 419,000 gallon stainless steel refueling water tank is located plant southwest of the containment building. No containment exists around this tank. The tank is filled from the reactor makeup system through underground piping. It is used to supply water to the refueling pool during outages and to the reactor system during transients. The tank contains radioactive demoralized water with 2,350 to 2,500 mg/L of Boron. {839}

16. Reactor Makeup Water Tank - A 153,000 gallon stainless steel reactor makeup water tank is located plant southwest of the containment building. No containment exists around this tank. The tank is filled from the demoralized water tank trough underground piping. It is used to supply demoralized water to the reactor system and associated support systems. {840}

17. Demineralized Water Clear Well - The demineralized water clear well consists of a 50,000 gallon carbon steel tank located plant northwest of the demineralizer

building. No containment exists around this tank. Deep well water is pumped underground to the demineralized water clear well, which is then transferred underground to supply water to the makeup demineralizers. {855}

18. Fire Water Storage Tanks - Two 300,000 gallon carbon steel firewater tanks are located plant southeast of the demineralizer building. No containment exists around these tanks. These tanks are filled from the demineralizer clear well through underground piping. They are used to supply firewater to the plant for testing and fire response. {859}

19. Neutralization Tank - The neutralization tank is a 150,000 gallon open carbon steel tank with an inner protective coating. No containment exists around this tank. In the past the tank received regeneration wastewater from the makeup demineralizer system through underground transfer lines. This tank is no longer in use.

20. Discharge Monitor Tanks - Two above ground 100,000 gallon stainless steel discharge monitor tanks are located plant south of the radwaste building. The tanks are used to store plant radioactive wastewater prior to the discharge. A single concrete diked area capable of holding 110% of the contents of one tank provides spill containment. {879}

21. Water Treatment Plant Sodium Hypochlorite Storage Tank - A 6,000 gallon plastic tank previously used for sodium hypochlorite is located plant south of the water treatment plant. The tank is empty with no plans of use in the future. No containment exists around this tank. {O}

22. Gaseous Chemical Storage -

a) Carbon Dioxide (CO2): The CO2 storage tank is located in the plant gas yard, which is plant south of the radwaste building. The primary use of CO2 is to degas the main generator of hydrogen during outages. The tank has a capacity of 6 tons of liquid CO2, a maximum pressure of 350 psig at 125 F. It is constructed per section 8 of the ASME pressure vessel code. {832}

b) Hydrogen (H2): There are 12 tubes for storage of H2 with a total capacity of 83,232 cubic feet at 2,300 psig located in the plant gas yard. Hydrogen is primarily used as a cover gas for the main turbine generator and to maintain oxygen control in the reactor coolant system. The tubes are constructed per ASME UPV code 8, Code Case 125 of a material that meets ASME SA372 Class 4. {833}

c) Oxygen (O2): An oxygen storage tube trailer provides the main source of oxygen and 8 oxygen cylinders for backup. The cylinders each contain 330 standard cubic feet of O2 at 2,640 psig. They are constructed to meet DOT specification 3AA2400. The primary use of O2 at the plant is in radwaste systems, in the evolution of hydrogen recombination. {841}

d) Nitrogen (N2): Callaway has both high and low pressure N2 with storage tanks located in the plant gas yard. There are two low pressure N2 storage tanks with a liquid capacity of 1569 gallons and 3000 gallons each. They are constructed with an inner vessel of 5083 aluminum and an outer carbon steel vessel. The primary use of low-pressure nitrogen for the plant is to purge and blanket systems to exclude oxygen. High pressure nitrogen is stored in 3 tubes with a total capacity of 24,280 cubic feet at 2,300 psig. They are designed and constructed to meet ASME code for pressure vessels. The primary use of high pressure nitrogen is to provide a backup gas supply to rapidly close plant valves during transients. {892}

23. Reclaimed Oil Storage Tank - The reclaim oil tank has a capacity of 10,000 gallons. It is an above ground tank located within an earthen dike of sufficient size to contain 110% of the tank contents. The tank is filled through underground lines from the oily wastewater separator. Used oil is removed from the tank to tanker trucks by vacuum created within the trucks. {861}

24. Oily Waste Treatment Area - This area is located southeast of the demineralizer building. The area consists of a building containing the oily wastewater separator and associated piping, the reclaimed oil storage tank, the equalization basin, and a 29,000 gallon carbon steel underground process surge tank that supplies plant oily wastewater to the separator. All Oily waste system water and oil transfers in this area are underground. Separated water is transferred to WTP sedimentation lagoon #6. {870}

25. Auxiliary Oil Transfer (Loading) Area - The auxiliary oil transfer loading area is located plant south of the auxiliary fuel oil storage tank. The area consists of a building containing pumps and piping to transfer diesel fuel oil to the auxiliary fuel oil storage tank. Diesel fuel oil is unloaded from tank trucks by pumps on the trucks or using the installed plant equipment pumps. Transfer line to the auxiliary fuel oil storage tanks are underground. {864}

26. Loading Area at Stores II - The loading area at the Stores II building consists of a standard shipping/receiving dock. All chemicals and other products are unloaded from trucks in their own shipping containers. There are not facilities for unloading of any bulk chemicals, fuel oil, or gasoline through pipelines to plant bulk storage tanks. {801}

27. Misc. Materials Storage Areas - Three areas around the Stores II building exist for miscellaneous laydown areas for items such as metal, gravel piles, fill material and old concrete. One is a concrete pad and the other two are on grass/gravel covered areas. Another materials storage area exists near the outage maintenance facility. Materials stored are metal components such as pumps, and valves, structural materials made of items such as metal, wood or concrete, pipe made of materials such as carbon steel, PVC and galvanized metal, empty portable tanks and empty metal dumpsters. {801}

28. Excavation Surplus Storage - Two storage areas are located plant south of the water treatment plant sludge lagoons containing excess dirt, concrete and asphalt from plant activities.

29. Hardened Condensate Storage Tank - The 500,000 gallon tank filled with deionized water is located plant east of the Turbine Building in a large graveled area. The tank was placed in service in June 2016, as part of the FLEX strategy that would supply ample cooling water for the Steam Generators, should a beyond design basis event occur at Callaway Energy Center

30. Oxamine Tank - The 2,500 gallon double walled tank is located plant north west of the water treatment building. This tank was placed in service in 2018 as part of a biocide addition project. This tank works in conjunction with the below mentioned Sodium Hypochlorite Tank.{872}

31. Sodium Hypochlorite Tank-This 6,650 gallon double walled tank is located plant north west of the water treatment building. This tank was placed in service in 2018 as part of a biocide addition project. This tank works in conjunction with the above mentioned Oxamine Tank. {872}

Temporary Significant Materials Storage - During the Last 3 years The following significant materials were present on-site temporarily within the last three years.

Refuel & Maintenance Outages The majority of additional materials stored on-site were for large equipment and other construction materials for the two most recent refuel outages. Additional trailers to house additional staff and equipment such as scaffolding, cranes and other materials to support the refueling outages were also on-site. No other

'significant materials' were stored on site during the past two refuel outages.

Hazardous Wastes Callaway Energy Center is normally a small quantity generator of hazardous waste generating between 200 and 2200 lbs. of hazardous waste per month. At times the quantity of hazardous waste exceeds the quantity due to infrequent activities such as equipment cleanings etc. The waste is stored in a prefabricated Hazardous Waste Storage Building (HWSB) with containment sumps, designed specifically for storage of hazardous waste. Waste is stored in the HWSB for up to 180 days prior to disposal via an offsite vendor. Typical wastes generated are Chromium, Lead, Mercury, Silver and solvents. The plant also currently maintains an outside satellite accumulation area where waste paint and solvents are accumulated. These wastes are accumulated from work performed in the plant in two separate 55 gallon drums held in a prefabricated closed spill container capable of holding 110 percent of the volume in both drums.

Management Practices A Spill Prevention, Control and Countermeasure (SPCC) plan and implementing procedure is in place at the Callaway Energy Center. The plan provides plant personnel with the necessary information regarding the types, locations and quantities of no-radioactive oil present at Callaway Energy Center and offers guidance on the containment and reporting of oil spills.

A Chemical Emergency Response Plan (CERP) and implementing procedure is also in place at the plant. This plan provides guidance and information for responding to hazardous chemical and/or oil spills.

Both plans describe various materials management practices employed to minimize contact by these materials with storm water runoff.

Outdoor Vehicle Maintenance and Cleaning Areas No outdoor vehicle maintenance and cleaning areas exist on the plant site.

Fertilizers, Pesticides, Herbicides and Soil Conditioners Herbicides are spray applied to various areas in and around the plant site as shown in drawing NPDES-001 Storm Water Information Outfalls 010-015. Herbicides are also applied to small areas near the intake building, the shooting range, the met tower and the alternate emergency diesel generator yard.

The herbicides used for weed control are Esplande 200 SC, Method 240 SL, and Roundup PRO. Pesticides are not used at Callaway Energy Center. In addition, no restricted use products are utilized at the facility.

Note that fertilizers, herbicides and soil conditioners which are used by the Missouri Department of Conservation on lands leased to them (yet within the plant storm water drainage areas) are not included in this summary.

Authorization for Non-Stormwater Components In previous applications, we described numerous releases to storm water conveyances from sources not associated with precipitation. We also discussed our justification for these releases with representatives from DNR's Jefferson City Regional Office, in meetings (and during a plant inspection) preceding re-issuance of the permit. All were approved. As a result, testing was not conducted to evaluate the presence of non-stormwater discharges (as they exist and have been previously characterized and evaluated). Thus, this application does not contain the typically applicable "non-storm water source certification" (per EPA Form 2F, Item V).

We hereby request continued allowance for releases from these sources (described below), consistent with DNR's earlier interpretation. The sources include:

1. Potable water - infrequent flushing and/or drainage of potable water lines for repairs or maintenance to the system

2. Firewater - quarterly flushing from 40 connections required for testing and maintenance of the firewater system. Note that we treat the firewater system with a bio stat, a bio penetrant and a scale inhibitor. This treatment program is designed to control microbiologically influenced corrosion to ensure integrity as required by the American Nuclear Insurers and the Nuclear Regulatory Commission. Quarterly flushes will discharge less than 50,000 gallons total.

Based on the expected concentrations and aquatic toxicity data, we do not believe there are any significant effects on the storm water runoff settling ponds from these releases. Once per three years, the entire system including the tanks, must be flushed which releases 700-800,000 gallons. Treatment chemicals are not added for a time prior to these flushes in order to ensure that residuals are very low (due to consumption within the system).

3. Manhole Pump-Outs - numerous manholes (providing access to instrumentation, piping, cables, etc.) at the plant are periodically pumped out to remove accumulated storm water. In order to address questions regarding possible contamination due to galvanized metal corrosion, a testing program was conducted and the analytical results shared with DNR. The testing indicated that zinc concentrations were reduced significantly by maintaining water levels below galvanized supports (i.e. routine pump outs). During 2012 we notified DNR that automatic pumping capability would be installed in several electric manholes. Note that water is not pumped to the storm water conveyance if an oil sheen exists or if the pH is not between 6 and 9 (which would be indicative of a spill or leak).

4. Eye Wash/Safety Shower Discharges - Releases are made from routine testing and/or emergency use of these outdoor facilities.

5. Demineralizer Water/Essential Service Water - during outages and other equipment maintenance activities it is sometime necessary to provide temporary hoses to supply water to equipment. When these hoses are dissembled, residual water is released locally.

6. Air Conditioning Condensate - condensate from various building intake air cooling units is routed to building roof drains and/or to local surfaces which in turn contribute to various storm water outfalls.

The following tables provides non-storm water plant related sources potentially discharged from conventional storm water drainage:

Outfall Non-Stormwater Sources 010

Fire water test (100gal/qtr)

Manhole discharges (10,000 gal/mo)

Eye wash/showers

ESW (<500 gall/event) 011

Fire water test (24,000 gal/qtr)

Fire water tank drain (80,000gal/3 yrs)

Manhole discharges (15,000gal/mo)

Eye wash/shower

Air conditioning condensate

ESW (<500gal/event) 012

Fire water test (11,000gal/qtr)

Manhole discharges (70,000gal/mo)

Air conditioning condensate

ESW (<500gal/event) 014

Fire water test (17,000 gal/qtr)

Air conditioning condensate 015 NONE

Plant Modifications No major plant modifications have occurred in the past 5 years.

Significant Leaks and Spills No significant spills (meeting the criteria set forth in the regulations) have occurred at Callaway Energy Center in the last 5 years.

Attachment J Requests for Modification of Current Permit Conditions Addition of Water Treatment Chemicals Callaway requests the addition of various water treatment chemicals in order to implement a new biological control methodology for out Ultimate Heat Sink (UHS) pond.

An explanation of these chemicals can be found in Attachment D.

Removal of Stormwater Pond Outfalls 012, 014 and 015 Ameren requests the removal of stormwater discharges Outfall 012, 014 and 015. In Spring 2022 the three mentioned stormwater settling ponds were closed and returned to pre pond conditions. Since that time, Ameren has sampled on a quarterly basis per permit requirements. Resulting sample data has shown that the ponds are in an established state that includes grass growth along with no issues of erosion or other issues. Because of the established site conditions, Ameren believes the three above stormwater discharges can be removed from the NPDES permit.

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