Text

Rev 0 to Operations Manual PAP-1309, Shipment of Radwaste for Disposal
	ML20133H799
Person / Time
Site:	Perry
Issue date:	08/05/1985
From:	Shatman R, Shuster C, Wahath B; CLEVELAND ELECTRIC ILLUMINATING CO.
To:	;
Shared Package
ML20133H723	List: ML20133H789; ML20133H799; PY-CEI-NRR-0329, Forwards Response to 850808 & 14 Ltrs Re Radwaste Solidification Sys.Responses Incorporated Into Rev 3 of Process Control Program.Proprietary NUS Process Svcs Repts FO-013 & SS-001 Withheld (Ref 10CFR2.790(b)(1));
References
	PAP-1309, NUDOCS 8510180118
	Download: ML20133H799 (81)
	v • d • e

i ENCLOSURE D OM1A: PAP-1309 Page: i Rev.: 0 .

THE CLEVELAND ELECTRIC ILLUMINATING COMPANY PERRY NUCLEAR POWER PLANT OPERATIONS MANUAL TITLE: SHIPMENT OF RADIOACTIVE WASTE FOR DISPOSAL REVISION: 0 EFFECTIVE DATE: 9-2-85 PNpp

, PT.kRY PREPARED: C. Reiter IOEFARTMENT CONTROLLED CCay SUBMITTED: e f_ f nAc M3 71,h C PCRRY PLANT TECHNICAL DEPAR? MENT 'W' s -] ~M ,

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SUEMITTED: /V/A PERRY PLANT OPERATIONS DEPARTMENT REVIEWED: [f 7-yd-85 NUCLEAR Q.N. DEPARTMENT APPROVED: .

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MANAGER - NUCLEAR Q.A. DEPARTMENT PORC REVIEW AND RECOMMENDATION FOR APPROVAL MEETING NUMBER: 85-59

/ p J J.WALDRON APPROVED: " .' em f 8 ,

MANAGER - PERRY PLANT TECHNICAL DEPg 24Al rnate Date APPROVED: /ld a M/DiAGCR - PERRY PL$NT OP NATIONS DEPARTMENT i s hQ h par 18as! Si88ljp

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l OMIA: PAP-1309 Page: 11 Rev.: 0

. Shipment of Radioactive Waste for Disposal PAP-1309 Table of Contents Section Title Pajtje 1.0 PURPOSE 1 2.0 SCOPE 1 3.0 RESPONSIBILITY I

4.0 REFERENCES

2 5.0 DEFINITIONS 3 6.0 DETAILS 3

-6.1 Determination of Radionuclide Content and Quantity 3 6.2 Classifying Radioactive Waste As Low Specific 4 Activity 6.3 Instructions for Completing the LSA Worksheet 6 6.4 Waste Classification 8 6.5 Waste Form and Stability 11 6.6 Instructions for Completing the Waste Classifi- 13 cation Worksheet 6.7 Packaging Radioactive Waste for Shipment 14 6.8 Hazardous Material Shipping Document Requirements 17 6.9 Instructions for Completing Shipment Documents 20-6.10 Selection of Transport Vehicle for Waste 29 Shipments 6.11 Preparing a Loading Plan 30 6.12 Loading a Transport Vehicle 32 6.13 Verification of Receipt of Waste Shipments 36 6.14 Records 36 7.0 ATTACRMENTS 39 "7.1 Attachment 1 - Table of Ag and A 2

V*l"** # 4l Radionuclides 7.2 Attachment 2 - Forms PNPP No. 6604 LSA 51 Worksheet 7.3 Attachment 3 - Table I 53 7.4 Attachment 4 - Table II 54 7.5 Attachment 5 - Form: PNPP No. 6626, Waste 55 Classification Worksheet 7.6 Attachment 6 - Barnwell Waste Management Facility 56 Radioactive Shipment Manifest 2, ., c , , t, - , y *n a g .% p,(

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i OM1A: PAP-1309 i Page: iii ,

Rev.: 0 Shipment of Radioactive Waste for Disposal PAP-1309 l

Table of Contents (Cont.) ;

1

! Section Title h 7.0 ATTACHMENTS (Cont.)

7.7 Attachment 7 - U.S. Ecology Radioactive Shipment 58 Manifest ,

7.8 Attachment 8 - South Carolina Radioactive Waste 60 Shipment Prior Notification and Manifest Form. -

DHEC 802

7.9 Attachment 9 - South Carolina Radioactive Waste 61 2 Shipment Certification Form DHEC 803 1

7.10 Attachment 10 - Washington State Low-Level Radio- 62 active Waste Shipment Certification for Commercial Generator / Packages and Brokers and Carriers, RHF-31A 7.11 Attachment 11 - Form: PNPP No. 6608, Exclusive 63 ,

Use Shipment Checklist 7.12 Attachment 12 - Form: PNPP No. 6610, Vehicle 64 Inspection Form 7.13 Attachment 13 - Fo rm: PNPP No. 6675, Isotopic 65

.; Analysis Results Form t

7.14 Attachment 14 - Standard Transport Van Dimensions 66 ,

(Inside) f 7.15 Attachment 15 - Form: PNPP No. 6606, Instruc- 67 tions for Maintaining Exclusive Use Vehicle 1,

7.16 Attachment 16 - Response to Transportation 68 j: Incidents l l L l I e

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OM1A: PAP-1309 Page: iv Rev.: 0 10CFR50.59 Applicability Check Yes No Is there a change to the plant as described /

in the FSAR?

Is there a change to a procedure / instruction /

as described in the FSAR?

Is there a test or experiment not described /

in the FSAR7 Is there a change to the Technical Specifi- /

cations?

(If yes, perform a 10CFR50.59 Safety Evaluation per PAP-0305)

Applicability Check A ,

Performed by (,,m e&_ Date T.74 iST d

SCOPE OF REVISION:

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OM1A: PAP-1309 Page: 1 Rev.: 0 SHIPMENT OF RADIOACTIVE WASTE FOR DISPOSAL

1.0 DESCRIPTION

This procedur.e provides instructions and requirements for the shipment of Low Specific Activity (LSA) Radioactive Waste by exclusive ose motor carrier to a burial facility.

2.0 SCOPE The packaging and shipment of radioactive material is governed by regulations issued by the Department of Transportation (DOT) and the Nuclear Regulatory Commission (NRC). Additional regulations have been issued by various state and local agencies which must be complied with when shipping radioactive material through areas over which they have jurisdiction.

Adherence to this procedure will ensure that shipments of LSA radioactive vaste comply with Federal, State, and burial facility re gulations.

3.0 RESPONSIBILITY 3.1 General Supervising Engineer for Radiation Protection is responsible for:

3.1.1 Ensuring shipment activities are in accordance with the plant operating license and applicable government, state, and local agency regulations.

3.1.2 Implementing the Perry Nuclear Power Plant Radioactive Material Shipment Procedures. .

3.1.3 Review and signature of shipment paperwork prior to the shipment.

3.2 The Radwaste Supervisor is responsible for ensuring that radwaste material is properly processed for disposal or storage.

3.3 The Radioactive Shipment Coordinator is responsible for:

. 3.3.1 Ensuring radioactive material for.1hJpment is packaged, handled, stored and shipped in ac alI~dppficable -- r rules and regulations. :oplanceswit)h,Q[g;({

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OM1A: PAP-1309 Page: 2 Rev.: 0 1

3.3.2 Scheduling of transport vehicles and equipment.

3.3.3 Obtaining burial site allocations.

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, 3.3.4 Ensuring the PNPP Radioactive Material Shipment Procedures are in compliance with the latest federal government, state and

} local agency regulations.

4 3.4 The Chemistry Unit is responsible for providing the necessary

, chemical and isotopic analyses on radioactive waste for shipment. i 3.5 The Health Physics Unit is responsible for all surveys. ;

3.6 The Quality Assurance Department is responsible for providing the

, necessary quality controls and checks that are required in the PNPP Quality Assurance Plan.

l 3.7 The Operations Department is responsible for the operation of loading equipment.

3.8 The Maintenance Section is responsible for construction and

- installation of any necessary blocking and bracing required in a shipment.

1 i !

i ,

4.0 REFERENCES

t 4.1 Title 10, Code of Federal Regulations, Part 20. I l

4.2 Title 10, Code of Federal Regulations, Part 61.

! 4.3 Title 10, Code of Federal Regulations, Part 71.

4.4 Title 49, Code of Federal Regulations, Parts 100-199. ,

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4.5 State of South Carolina, Radioactive Materials License 097, issued f to Chem-Nuclear Systems, Inc.

! 4.6 State of Washington, Radioactive Materials License WN-1019-2, issued to U.S. Ecology, Inc. ,

4.7 Radwaste Unit Logs and Records, OAP-1703.

1 4.8 Shipment of Limited Quantity Radioactive Material, PAP-1305.

I j 4.9 Shipment of Low Specific Activity (LSA), Radioactive Material, 1 PAP-1306. ,

! 4.10 PAP-1307, Shipment of Radioactive l iateth. W N.Q.;S* ;'% & "fil r%

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OM1A: PAP-1309 Page: 3 Rev.: 0 4.11 PAP '.308, Shipment of Radioactive Empty Packages.

4.12 PAP-1304, Radioactive Shipment Criteria.

4.13 PAP-1310, Packaging Radioactive Material for Shipment.

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4.14 PAP-1311, Shipment of Highway Route Controlled. Quantity Radioactive

Material.

j 4.15 PAP-1312 Shipment of Fissile Radioactive Material.

i

. 16 South Carolina Regulation No. 61-83, Transportation of_ Radioactive l Waste Into or Within South Carolina.

i 5.0 DEFINITIONS Definitions are listed in OM1A: PAP-1304, Radioactive Shipment Criteria.

4 l 6.0 DETAILS i

I 6.1 Determination of Radionuclide Content and Quantity l' 6.1.1 To determine if the waste may be classified as Low Specific Activity it is necessary to identify and quantify the specific activity of each radionuclide present in the material.

f

6.1.2 Identifying the radionuclide content of the material is done l by one of these methods

1

a. Obtain e smear sample from the material and perform an isotopic analysis of the smear.

b. Use the isotopic analysis results of the latest resin samples to determine the radionuclides present in the mate rial.' This method can only be used if the material

became radioactive due to exposure to plant systems or components.

c. Direct isotopic analysis of the material or a representa-tive sample of the material.

6.1.3 Determination of specific activity of the material can be performed by one of two methods:

a. Direct isotopic an'alys:I~oIIlha material...or a sample of the material (provided eypt the material and the a t(ejsamplE'Asrepresentativ,gj,

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OM1A: PAP-1309 Page: 4 Rev.: O distributed throughout the material). The activity of the material is then divided by the weight of the material analyzed to determine specific activity.

b. Calculation of total activity based on radiation levels of the material. The calculated activity is then divided by the total weight of the material to determine total specific activity.

6.1.4 If calculations of total specific activity based on radiation levels are used, an isotopic analysis must be used to deter-mine the percent abundance of the radionuclides. The total specific activity of the material is then ratioed for each radionuclide based on the percent abundance of the radionu-clide.

6.1.5 In order to classify radioactive waste for disposal, in accordance with NRC requirements, it is necessary to identify and quantify certain radionuclides in the material that PNPP is not able to measure with our equipment. The use of scaling factors allows the unmeasurable radionuclides to be ratioed to the radionuclides that are identified in routine analysis.

- Complete instructions for the sampling and analysis of radio-active waste for 10CFR61 classification are contained in OM1E: RAP-1102, 10CFR61 Compliance Sampling.

6.2 Classifying Radioactive Waste As Low Specific Activity 6.2.1 Determine the 7A values for each radionuclide in the material.

The values are 5btained from the Table of Ag and A2 Values for Radionuclides. Attachment 1.

6.2.2 Once the A 2 values for the material are known, the activity limits for LSA can be determined as follows:

1. For material in which the radioactivity is essentially uniformly distributed, the average concentration of contents shall not exceed:

a. 0.0001 millicurie per gram of radionuclides for which the A quantity is not more than .05 curie (Group I); 2

b. 0.005 millicurie per gram of radionuclides for which the A, quantity is more than .05 curie, but not more than I curie (Group II); or

c. 0.3 millicurie per gram of radionuclides for which the A quantity is more than 1 curie'(Group III).

2

2. For objects of non-radioactive material externally contaminated with radioactive material, the surface contamination shall not Ex eg; 1 4 E*l. s , [ ., , j

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OM1A: PAP-1309 Page: 5 Rev.: O

a. 2.2 E7 dpm/100 cm of radionuclides for which the A 2 quantity is not agre than .05 curie; or

b. 2.2 E8 dpm/100 cm for all other radionuclides.

6.?.3 The activity present in the material is then compared to the activity limit for the material to determine if it falls' within the shipment category.

Example: A 100 lb. drum of radioactive material requires shipment. Based on radioactive levels, it is calculated that curie content is 10 curies. Iso-topic analysis shows the only radionuclide present in the material is Co-60. The activity is uniformly distributed throughout the drum.

Determine the specific activity as follows:

10 curies I lb. 1000 mci "

.022 mci / gram of Co-60 100 lbs. 454 grams 1 curie Attachment I shows the A7 limit for Co-60 is 7 curie, there-fore the LSA limit is 0.3 mci / gram.

Since 0.22 mci / gram is within the LSA limit of 0.3 mci / gram, the material qualifies as low Specific Activity.

NOTE: The Table of Aj and A 2Values for Radionuclides, Attachment 1, is a modified table from 49CFR173.435.

The LSA limit, in mci / gram, has already been calcu-lated for each radionuclide and is listed in the LSA limit column.

6.2.4 If the package contains more than one radionuclide, the unity equation must be used to determine if the material exceeds the LSA quantity limits.

6.2.5 When determining the specific activity of solidified waste, the concentration of the radionuclide mixture shall be av-eraged over the volume of the waste and the solidification agent if the waste form is a homogenous mixture.

j 6.2.6 The concentration of radionuclides in filters encapsulated with a solidification agent shall be averaged over the volume of the filter, not the solidification agent.

6.2.7 An LSA worksheet is provided to aid in classifying radioactive ,

waste as Low Specific Activity. All completed worksheets shall be filed with the corre-ruuai -shipment-documente. -

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OM1A: PAP-1309 Page: 6 Rev.: 0 NOTE: The radioactive waste shipping computer program is normally used to perform the required LSA calculations. If the computer program is used, use of the LSA worksheet is not required.

6.3 Instructions for Completing the LSA Worksheet (Attachment 2) i 6.3.1 The number preceding each of the following instructions corresponds to the applicable item on the worksheet.

2 6.3.2 The LSA worksheet consists of two parts:

a. Part 1 - used to determine the specific activity and LSA group of each radior.uclide present in the package,

b. Part 2 - used to perform the unity equation to determine if the material can be classified as LSA.

6.3.3 Instructions

.; Part 1 i

~

1. Enter the date the worksheet is calculated (Part 1 and 2).

i l 2. Enter a description of the material (Part 1 and 2),

i

3. Enter the package number (Part 1 and 2),

1 ;

4.

If the contents of the package is part of a process i batch, enter the batch number (Part 1 and 2).

1 5.

Enter the gross weight of the package (for filters enter the weight of the filter only).

k

6. Enter the total activity of the package in millicuries.

7. Enter the sample activity in millicuries. If the activity of the package is calculated based on dose rates i of the package, enter "N/A" for the sample activity and .

sample weight, i

j 8. Enter the sample weight in grams.

9. List each radionuclide present in the material.

10. List the percent abundance of each radionuclide found in the material.

11. List the activity, in m ul(curiesc-foreach.radionuclide",

The activity can be cal nul)ah4d ib'yWiiiplying

the percen t i ONLY .

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r OM1A: PAP-1309 Page: 7 Rev.: O abundance of the radionuclide (10) by the sample activity (7). If the activity of the package was determined by dose rate calculations, multiply the percent abundance by ,

the total activity'(6).

12. List the specific activity for each radionuclide in millicuries per gram. The specific activity is calculated by dividing the radionuclide activity (11) by [

the sample weight (8). If the activity of the package l was determined by dose rate calculations, divide the radionuclide activity (11) by the package weight (5).

Convert the package weight (5) to grams by multiplying by 454 grams / pound.

13. Enter the LSA group for each radionuclide. The LSA group is found by comparing the Ay quantity of the radionuclide to the following limits:

a. Group I = A., quantity is not more than .05 curies.

b. Group II = A,, quantity is more than .05 curie but not more than 1.0 curie.

c. Group III = A quantity is more than 1.0 curie.

2 The A quantity r the radionuclide is found in the 2

Table of A /A Values for Radionuclides, Attachment 1. ;

1 y Part 2

14. List each radionuclide present in the material that falls in LSA Group I.

15. List the specific activity for each of the LSA Group I radionuclides.

16. List each radionuclide present in the material that falls in LSA Group II.

17. List the specific activity for each of the LSA Group II radionuclides.

18. List each radionuclide present in the material that falls in LSA Group III.

19. List the specific activity for each of the LSA Group III radionuclides.

20. Enter the sum of the specific activities for Group I '

radionuclides.

INFORMKrSON

ONLY i i

OM1A: PAP-1309 Page: 8 Rev.: 0

21. Enter the sum of the specific activities for Group II ,

radionuclides.

22. Enter the sum of the specific activities for Group III radionuclides.

23. Enter the total specific activity calculated for each LSA group.

24. Calculate the unity factor for each LSA group by dividing the total specific activity for each group (23) by the LSA limit.

25. Enter the sum of the unity factors (24). If the total unity factor does not exceed 1.0, then the material may be classified as LSA. If .he total unity f actor exceeds 1.0, the material must be classified as Radioactive Material n.o.s. in accordance with Reference 4.10.

6.3.4 The completed LSA worksheets shall be kept on file with the applicable shipment documents.

6.4 Waste Classification 6.4.1 Determination of the classification'of radioactive waste involves two considerations. The first consideration must be given to the concentration of long-lived radionuclides and their shorter-lived precursors. The potential hazard of these radionuclides will persist long after the burial facility has ceased operation. The second consideration must be given to the concentration of shorter-lived radionuclides for which the requirements or institutional controls and disposal methods are effective.

6.4.2 Classification determined by long-lived radionuclides - If radioactive waste contains only radionuclides listed in Table I (Attachment 3), classification shall be determined as follows: .

1. If the radionuclide concentration does not exceed the value listed in Column 1 of Table I, the waste is Class A.

2. If the radionuclide concentration exceeds the values listed in Column 1 of Table I, but does not exceed the values listed in Column 2, the waste is Class C.

3. If the radionuclide concentration exceeds the value listed in Column 2 of Taht. Y,_.ths.wasta is-not-generel4' acceptable for near-sar ace $s s

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OM1A: PAP-1309 Page: 9 Rev.: 0

4. For wastes containing mixtures of radionuclides listed in Table I, the total concentration shall be determined by the unity equation. When performing the unity equation, ensure the values used in the denominator of the equation are all from the same column.

6.4.3 Classification determined by short-lived radionuclides - If radioactive waste does not contain any of the radionuclides listed in Table I (Attachment 3), classification shall be determined based on the concentrations shown in Table II (Attachment 4), as follows:

1. If the radionuclide concentration does not exceed the value in Column A of Table II, the waste is Class A.

2. If the radionuclide concentration exceeds the value in Column A of Table II, but does not exceed the value in Column B, the waste is Class B.

3. If the radionuclide concentration exceeds the value in Column B of Table II, but does not exceed the value in Column C, the waste is Class C.

4. If the radionuclide concentration exceeds the value in Column C of Table II, the waste is not generally accept-able for near-surface disposal.

5. For wastes containing mixtures of radionuclides listed in Table II, the total concentration shall be determined by the unity equation. When performing the unity equation, ensure the values used in the denominator of the equation are all from the same column.

6.4.4 Classification determined by both long-lived and short-lived radionuclides - If radioactive vaste contains a mixture of radionuclides, some of which are listed in Table I, and some of which are listed in Table II, classification shall be determined as follows:

1. If the concentration of a nuclide listed in Table I (Attachment 3) does not exceed the value listed in Column 1, the class shall be determined by the concen-tration of nuclides listed in Table II (Attachment 4).

2. If the concentration of a nuclide listed in Table I exceeds the values shown in Column 1 but does not exceed the value shown in Column 2, the waste shall be Class C, provided the concentration of nuclides listed in Table II does not exceed the valu. =haun in ca t "=n - C .

INFORMATEM3 ONLY 4

OM1A: PAP-1309 Page: 10 Rev.: 0 1 3. The unity equation must be used for mixtures of radionu-clides. The appropriate values used in the denominator of the equation must all be taken from the same column of the same table. The sum of the fractions for the column must be less than 1.0, if the vaste class is to be determined by that column.

Example: To classify a waste containing .05 uCi/cc of C-14, 0.1 uCi/cc of Tc-99, 0.9 uC1/cc of Cs-137, and 2.3 uCi/cc of Ni-63, the following steps must be taken.

1. Compare the activities of the long-lived nuclides to the values listed in Table I (Attachment 3). C-14 and Te-99 both fall within the limits listed in Column 1, therefore the unity equation is calculated for Column 1.

0.5 uCi/cc (C-14) 0.1 uCi/cc (Tc-99) = .096 0.8 uCi/cc (C-14 limit)

0.3 uCi/cc (Tc-99 limit)

, Since the unity equation is less than 1.0, these nuclides fall within the Class A limits, therefore the vaste must classified by the concentration of nuclides listed in Table II (Attachment 4).

i

2. Compare the activities of the short-lived nuclides to the values listed in Table II.

i Cs-137 and Ni-63 both fall within the limits listed in Column A, therefore the unity equa-tion is calculated for Column A.

j 0.9 uCi/cc (Cs-137)

2.3 uCi/cc (N1-63) = 1.56 1 uCi/cc (Cs-137 limit) 3.5 uCi/cc (Ni-63 limit)

. Since the unity equation is greater than 1.0, these i

nuclides do not fall within the Class A limits, therefore the nuclide concentrations must be com-pared to the Column B values.

0.9 uCi/cc (Cs-137)

2.3 uCi/cc (Ni-63) = 0.5 44 aci/cc (Cs-137 limit) 70 uCi/cc (Ni-63 limit)

Since the unity equation for Column B is less than

1.0 the waste is classified as Class B.

6.4.5 If radioactive waste does not contain any nuclides listed in either Table I or Table II, it_is Class A.

INFORMATiC.T ONLY I

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OM1A: PAP-1309 Page: 11 Rev.: 0 6.5 Waste Form and Stability 6.5.1 In addition to classifying radioactive waste by the concen-tration of nuclides present in the material, the waste must also meet the form and stability requirements set forth in Reference 4.2.

6.5.2 The NRC Technical Position on Waste Form, Rev. O, May 1983 contains the requirements and tests necessary to comply with the form and stability requirements of Reference 4.2.

6.5.3 The following requirements are minimum requirements for all classes of waste:

1. Waste must not be packaged for disposal in cardboard or fiberboard boxes.

2. Liquid waste must be shipped or packaged in sufficient absorbent material to absorb twice the volume of the liquid.

3. Solid waste containing liquid shall contain as little free standing and noncorrosive liquid as is reasonably achievable, but in no case shall the liquid exceed 0.5%

of the volume.

4. Waste shall not be readily capable of detonation or of explosive composition or reaction at normal pressures and temperatures, or of explosive reaction with water.

l S. Water must not contain, or be capable of generating l' quantities of toxic gases, vapors, or fumes harmful to persons transporting, handling, or disposing of the waste.

6. Waste must not be pyrophoric. Pyrophoric materials contained in waste shall be treated, prepared, and packaged to be nonflammable.

7. Waste in a gaseous form must be packaged at a pressure that does not exceed 1.5 atmospheres at 20*C, Total ;

activity must not exceed 100 curies per container.

8. Waste containing hazardous, biological, pathogenic, or infectious material must be treated to reduce to the maximum extent practicable the potential hazard from the non-radiological materials.

INFORMAT!ON ONLY 1

i _ . - _ _ __ ,_ _

OM1A: PAP-1309 Page: 12 Rev.: 0 6.5.4 In addition to the minimum requirements of paragraph 6.5.3, Class B and C wastes are required to have stability, in order to ensure that Class B and C waste or its container will maintain its stability, the following conditions need to be met:

1. The waste should be a solid form or in a container or structure that provides stability after disposal.

2. The waste should not contain free standing and corrosive liquids. The wastes should contain only trace amounts of drainable liquid, and in no case may the volume of free standing liquid exceed one percent of the waste volume when vastes are disposed of in containers designed to provide stability, or 0.5 percent of the vaste volume for solidified waste.

3. The vaste or container should be resistant to degradation caused by radiation effects.

4. The waste or container should be resistant to biodegrada-

,.. tion.

5. The vaste or container should remain stable under the compressive loads inherent in the disposal environment.

6. The waste or container should remain stable if exposed to moisture or water after disposal.

1

7. The as-generated waste should be compatible with the solidification media or container.

\

8 6.5.5 In order to ensure radioactive waste meets the federal re-quirements for burial, all processed radioactive waste is processed and tested in accordance with the Process Control Program (PCP), OM12E: PCP. The Process Control Program provides the requirements and tests necessary to demonstrate the final waste product meets the form and stability requirements of the applicable waste classification, p

6.5.6 An, alternative to processing some Class B or C waste streams, particularly ion exchange resins and filter sludges, is the use of a high integrity container (HIC). The high integrity container would be used to provide the long-term stability required to meet the stability requirements in Reference 4.2.

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INFORMATEON ONLY

. _ . c .

l OM1A: PAP-1309 i Page: 13 Rev.: 0 NOTE: The radioactive waste shipping computer program is ,

normally used to peform the required waste ,

i classification calculations. If the computer i program is used, use of the vaste classification l worksheet is not required.

6.6 Instructions for Completing the Waste Classification Worksheet

, (Attachment 5) ,

6.6.1 The number preceding each of the following instructions j corresponds to the applicable item on the worksheet, t l 6.6.2 Instructions:

7

1. Enter the process batch number if applicable. t Enter the type of waste (i.e, DAW, resins, etc.).

2. i

3. Enter the package numbers for which the worksheet applies.

^~

! 4. Determine the waste classification based on the ;

long-lived nuclides as follows:

a. Enter the activity of each nuclide listed in Table II in the appropriate column. If the activity ;

of any nuclide exceeds the Column 1 limit for that ;

nuclide, enter the activity of each nuclide in j Column 2. ;

.; b. If the nuclide listed in the table is not present in 4

the radioactive vaste enter "NP" in the activity block.

c. Calculate the unity factor for each nuclide by dividing the activity of the nuclide by its limit.

j

[

d. Add the unity factors in the column to obtain the ,

total unity factor. ,

e. If the Column 1 total unity factor is less than one ;

the waste is classified based on the Table II .

nuclide concentration. l f.- If the Column 1 total unity factor is one or j greater. the unity factors must be calculated using

! Column 2 limits. _ !

g. If the Column 2 total unity factor is less than one, j the waste is. Class C provided the Table II nuclide ;

concentrations do not exceed the Column C limits. !

i h. If the column 2 total unity factor is one or greater i the waste is generally not acceptable for disposal. ;

Enter "N" in the Waste Class block (16). l IN FO&.WGN !

ONLY !

4 ,

. . , . , - . . . _ - . _ , . _ _ . . .v .,_,.,,,,,,,,,,_-.__.m.,

OMIA: PAP-1309 Page: 14 Rev.: 0

5. Determine the vaste classification based on the short-

. lived nuclides as follows:

?

I a. Enter the activity of each nuclide listed in Table II in the appropriate column. If the waste was classified as Class C in Table I, enter the Table II nuclides in Column C.

b. If the nuclide listed in the table is not present in the radioactive waste, enter "NP" in the activity block.

c. Calculate the unity factor for each nuclide by dividing the activity of tha nuclide by its limit.

d. Add the unity factors in the column to obtain the total unity factor,

e. If the Column A total unity factor is less than one,

', the waste is Class A.

f. If the Column A total unity factor is one or greater, calculate the unity factors for each nuclide using Column B limits. If the Column B total unity factor is less than one, the waste is Class B.

g. If the Column B total unity factor is one or greater, calculate the unity factor for each nuclide using Column C limits. If the Column C total unity factor is less than one, the waste is Class C.

h. If the Column C total unity factor is one or greater, the waste is. generally not acceptable for

! disposal, enter "N"s in the Waste Class Block (6)..

6. Enter the appropriate waste class in the block. Enter "N" if the waste is not acceptable for disposal.

7. Enter the total activity of all nuclides in the waste with half-lives greater than five years.

8. Check the appropriate box based on the following:

a. Waste Class B and C must be STABLE.

b. Class A wastes shipped to the Barnwell disposal facility must be STABLE if the total activity of all radionuclides with half-lives greater than five years is I uCi/cc or greater.

c. All other Class A wastes may be UNSTABLE.

9. Date and sign the worksheet.

6.7 ' Packaging Radioactive Waste for Shipment 6.7.1 In addition to DOT and NRC regelations..radioac.ttvA;yaste must be packaged in accordance with b4fialp'fqcility . regulations.

Uk4E %d a'B Mrd C L w,,, ,.j ONLX

OM1A: PAP-1309 Page: 15 Rev.: 0 6.7.2 Processed radioactive vaste and dry active waste (DAW) are packaged in accordance with the applicable Radwaste solidifi-cation or compacting instruction. These packages shall then be marked, labeled, and otherwise prepared for shipment in accordance with this procedure.

6.7.3 Some requirements for packaging are based on the burial facility to which the waste will be shipped to. If a requirement for packaging the waste is specific to one burial ,

facility, the applicable burial facility is listed in parentheses next to the requirement.

6.7.4 Inspect each packaging for the following:

a. Holes or openings where radioactive contents may leak,

b. Seals and closure devices are intact and operate properly,

c. Rust or corrosion is removed and the area is repainted as necessary.

d. Large dents or dents which may affect the integrity of the package.

, e. Nails or fasteners which protrude into the package interior.

NOTE: The Radioactive Shipment Coordinator shall be informed of any package that does not meet the ,

inspection or test requirements specified in this procedure. The affected package shall not be used for shipment unless it can be satisfactorily repaired and reinspected.

6.7.5 LSA radioactive waste that is shipped in an exclusive use vehicle shall be packaged in a strong tight package such that there will be no leakage of the material under normal condi- l tions of transportation. l 6.7.6 LSA waste shall be packaged so that under conditions normally incident to transportation the radiation level does not exceed 200 mr/hr on the accessible' external surface of the package unless the shipment is made in a closed transport vehicle in which case the limit is 1000 mr/hr. ,

6.7.7 LSA waste shall be packaged so that void spaces in the package are reduced to a minimum, but in no case shall the volume of I the vaste be less than 85% of the package volume. (Barnwell) 6.7.8 The following material is prohibited from burial at the indicated disposal facility:

a. Any pyrophoric materi al" D(B'agovell, and Richla$d)'

lkgt; (chisW m 6 w w ad ONLY b

r- , - - , ,

v -- - ,-, -

9

OM1A: PAP-1309 Page: 16 Rev.: 0 b.. Toluene, xylene, dioxane, scintillation liquids, or other organic liquids or solids with similar chemical proper-ties or packaging which have at any time contained any of these liquids. (Barnwell, Richland)

c. Chelating agents with concentrations greater than 8 per-cent by weight. (Barnwell)

d. Waste containing transuranic nuclides with concentrations greater than 10 uCi/gm. (Barnwell, Richland)

e. Radioactive waste containing toxic and hazardous chemi-cals whose chemical hazard exceeds the radiological hazard. (Barnwell, Richland)

f. Waste containing oil or lubricants in concentrations greater than 1% by waste volume. (Barnwell) 6.7.9 For the purposes of this procedure, chelating agents include the following:

a. Amine polycarboxylic acids (e.g. , EDTA, DTPA);

b. Hydroxy-carboxylic acids; and

c. Polycarboxylic acids (e.g., citric acid, carbolic acid, and glucinic acid).

6.7.10 Radioactive vaste shall nct contain any detettable free standing liquid. Free standing liquid is defined as 0.5 per-cent liquid by volume per package. The Barnwell facility allows up to 1 percent liquid by volume for solidified or dewatered waste that is disposed of in a high integrity container that is approved by the South Carolina Department of Health and Environmental Control (DHEC).

6.7.11 All wooden boxes shall be banded with metal bands. Drums shall have the threads interrupted on the closure bolt so that the nuts do not come loose during transportation.

6.7.12 Each package of LSA waste shall be marked with the following:

1. " RADIOACTIVE LSA" - Must be marked on two sides of the j package (excluding the top and bottom), except that drums l require only one marking on the side of the drum.

2. Package identification number.

3. The waste class (A, B, or C).

6.7.13 Each pcckage of LSA waste should be marked with the weight of the package.

6.7.14 The waste class shall be marked or, each package, in letters greater than one-half in:h high. ma fnllows-h h.A O . ien"ur d

OM1A: PAP-1309 Page: 17 Rev.: 0

1. For shipments to Barnwell the waste class shall be marked on the top of the package as follows:

a. Class A unstable waste shall be marked " Class A".

b. Class A stable waste shall be marked " Class A-S".

c. Class B and C waste shall be marked " Class B" or

" Class C".

2. For shipments to Richland, the waste class shall be marked in close proximity (within six inches) to each radioactive marking or label. Waste marked "RADI0AC-TIVE - LSA" need only have one classification marking.

The classification markings shall appear as follows:

a. Class A unstable waste shall be marked " Class A i Unstable",

b. Class A stable waste shall be marked " Class A Stable".

c. Class B and C waste shall be marked " Class B" or

" Class C".

, 6.7.15 Contamination surveys shall be performed on the package af ter loading and closing. Contamination levels on the external surface of the package shall not exceed:

2

a. 2,200 dpm/100 gm beta-gamma contamination, and

b. 220 dpm/100 cm alpha contamination.

6.8 Hazardous Material Shipping Document Requirements 6.8.1 Shipping documents are a communication device designed to provide pertinent information about hazardous material con-tained in the shipment. For this reason it is important that 4 the documents are complete, accurate, and_ legible.

4 6.8.2 Although there is no standard form for hazardous material shipping documents, there are requirements for what informa-tion is to be entered on the documents.

6.8.3 The shipping description of a hazardous material listed on the shipment document must include:

a. The proper shipping name prescribed for the material in Reference 4.4, part 172.101, Hazardous Material Table,

b. The hazard class prescribed for the material in the Hazardous Material Table. Except for a proper shipping name that contains words describing more than one hazard class, inclusion of the hazard class is not required when the words of the proper shipping name_contain the key SUCh' word or wordssofpthe o et9 9 m_clAsa hazard O '

cf_the ONLY m

OM1A: PAP-1309 Page: 18 Rev.: O as Radioactive Material, LSA, n.o.s.

c. The identification number (preceded by "UN" or "NA" as appropriate) prescribed for the material in the Hazardous Material Table.

d. Except for empty packagings, the total quantity (by weight, volume, or as otherwise appropriate) of the hazardous material covered by the description.

e. The basic description specified in paragraphs a., b., and

c. of this section must be shown in sequence.

f. The total quantity of the material covered by one description must appear before or after, or both before and after the description of the material.

g. Abbreviations may be used to specify the type of packag-ing and weight or volume. Example: 1 Dr. Radioactive Material, LSA, n.o.s., UN2912, 100 lbs.

h. The type of packaging and destination marks may be entered in any appropriate manner before or after the basic description.

1. Technical and chemical group names may be entered in parentheses between the proper shipping name and hazard class, r

J. Each shipping document issued in connection with a shipment made under an exemption must bear the notation

" DOT-E" followed by the exemption number assigned and so located that the notation is clearly associated with the description to which the exemption applies.

k. The description for a material offered for transportation

, as " limited quantity" must include the words " Limited Quantity" or "Ltd. Quantity" following the basic descrip-tion.

6.8.4 The description for a shipment of radioactive waste to a disposal facility must also include:

a. The name, address, and telephone number of the person generating the waste.

b. The name, address, and telephone number of the person transporting the waste to the land disposal facility,

c. The name and activity of each radionuclide in the radioactive material.

d. A description of the physical and chemical form of the material, if the material is not in special form (generic chemical description is acceptable for chemical form).

2. The activity contained in each package of the shipment in

!- terms of curies, millicuries, or microcuries. Abbrevia-tions are authorized. For the shipment of a package containing a highway route controlled quantity of radio-active materials, the words " Highway Route Controlled Quantity" must be enterad_in_ association with Abe_. basic description.

.

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OM1A: PAP-1309 Page: 19 Rev.: 0

f. The total activity of the shipment.

g. The total volume of waste contained in the shipment.

h. The total quantity of the radionuclides, H-3, C-14, Tc-99 and I-129 must be shown.

i. The total amount of source material, !n pounds, must be shown.

j. The total amount of Special Nuclear Material, in grams, must be shown.

k. The type of solidification agent, if used, must be specified.

1. Waste containing more than 0.1 percent chelating agents by weight must be identified and the weight percentage of the chelating agent estimaced,

m. Wastes claasified as Class A, Class B, or Class C in accordance with Reference 4.2, must be identified.

n. The category of label applied to each package in the shipment. Example: "RADI0 ACTIVE WHITE-1".

o. The transport index assigned to each package in a ship-ment bearing RADIOACTIVE YELLOW-Il or RADI0 ACTIVE YEL-LOW-111 labels.

q. For a package approved by the U.S. Department of Energy (DOE) or U.S. Nuclear Regulatory Commission (NRC), a notation of the package identification working as pre-scribed in the applicable DOE or NRC approval.

6.8.5 Each person who offers a hazardous material for transportation shall certify that the material is offered for transportation in accordance with Reference 4.4 by printing (manually or mechanically) on the shipping document containing the required shipping description the following certification:

"This is to certify that the above-named materials are properly classified, described, packaged, marked and labeled, and are in proper condition for transportation according to the applicable regulations of the Department of Transportation".

NOTE: In line one of the certification the words "here-in-named" may be substituted for the words "above-named".

6.8.6 Shipments of radioactive waste to a disposal facility require the use of the burial facility's Radioactive Shipment Manifest (RSM). Each RSM meets the requirements of Reference 4.1 and 4.4 for radioactive waste shipping documents.

6.8.7 In addition to the radioactive shipment manifest, each ship-ment of radioactive waste requires the following state forms:

a. The South Caro n ,5 ior ONLY

OM1A: PAP-1309 Page: 20 Rev.: 0 Notification and Manifest Form, DHEC-802. (Barnwell)

b. The South Carolina Radioactive Waste Shipment Certification Form, DHEC-803. (Barnwell)

c. The Washington State Low-Level Radioactive Waste Shipment Certification Form, RHF-31A. (Richland) 6.9 Instructions for Completing Shipment Documents 6.9.1 Barnwell Waste Management Facility Radioactive Shipment Manifest (Attachment 6)

The numbers preceding each instruction correspond to the numbered item on the Barnwell RSM. Information cust be provided for all numbered items on the RSM form. Use of N/A for "Not Applicable" is authorized.

1. Indicate generator name (consignor), address, contact person and phone number of person responsible for making the shipment. Contact person is the Radioactive Shipment Coordinator.

- 2. The consignee is pre-printed.

3. Each shipment is assigned a volume allocation number by the Barnwell of fice. Write the number in this space and use this number on all continuation pages used for each shipment. Number all the pages in chronological order.

4. List the carrier, address, telephone number, shipping date, shipment type (van, cask, etc.), shipment surface exposure (highest radiation level on the exterior of the van, cask, etc.), shipment number, liner serial number, driver signature, and date.

5. Indicate the total number of packages and the total weight, in pounds, of each hazard class.

6. Record the cumulative total of all hazard classes in these blocks. Check the appropriate box for the units of activity measurements. If the stated radionuclides listed in the four columns are not present, record in the blocks as "not present" (N.P.). If the radionuclides do exist, but are in quantities less than the lower limit of detection (LLD), the quantities of the nuclides must be recorded as being less than the minimum detectable. The minimum detectable activity must te included in parenthe-ses. Isotopes U-238, Th-232, or any other material which is source material must be-recordad in source pounds.

b a

_ ONLY x

OM1A: PAP-1309 Page: 21 Rev.: 0

7. List the weight, in grams, of all special nuclear materi-al.

8. Record volume, in cubic feet, of all disposable pallets.

9. Describe briefly what the vaste is, if the material is solidified, indicate what solidification media is used.

Example: Compacted trash, non-compacted trash, dewatered resin, solidified liquid in cement, solidified resin in cement, filters in cement, compacted lab trash, building rubble, metal components, etc.

10. Record the physical form of the waste material. " Liquid" is not authorized.

11. Record the chemical form of the vaste material. If the material contains chelating agents in quantities greater than 0.1%, the names and weight percentage must be listed.

12. Check the appropriate box (es) for each waste class present in the shipment.

13. Indicate if the shipment is transported as exclusive use or not. If "yes" is checked, instructions for maintenance of exclusive use vehicles must be provided by the shipper to the carrier.

14. .A company representative of the consignor must sign the DOT certification. All signatures must be legible.

15. A company representative of the generator must sign the S.C. DHEC certification. Title, organization, and phone number must be indicated. The date must be within 48 hours5.555556e-4 days 0.0133 hours 7.936508e-5 weeks 1.8264e-5 months of the shipping date specified in block 4. All signatures must be legible.

Barnwell RSM Continuation Sheet

16. List each package separately. Item number on the dis-posal package must correspond with the_ item number listed on the RSM.

17. List the prominent radionuclides in each package. Use of MFP or MCP are not authorized. Use as many lines as necessary to describe the contents of the package. If more than one package in the shipment contains the same activity distribution of each radiopu.clide,,qa glistingeof ,~

radionuclides is required f N N fLrs P M cAag k O lg d is Subsequent packages in this series v lone x

I OM1A: PAP-1309 Page: 22 Rev.: 0 line entry with appropriate information on each. Use of the words, "See attached ...", is not an appropriate entry.

18. Record the percent abundance of each radionuclide or the activity of each radionuclide in uCi, in each package (See Item 17).

19. Record the cumulative total of all isotopes in each package, in uCi.

20. Record the physical form of the waste material. " Liquid" is not authorized.

21. Record the chemical form of the waste material. If the material contains chelating agents in quantities greater than 0.1%, the names and weight percentage must be listed.

22. Describe briefly the vaste material is. If the material is solidified, indicate what solidification media is

- - used. Example: Compacted trash, non-compacted trash, dewatered resin, solidified liquid in cement, solidified resin in cement, filters in cement, compacted lab trash or non-compacted lab trash, building rubble, metal components, etc.

23. List the vaste classification of the package, either A, B or C.

24. Indicate if the waste is stable (S) or unstable (U).

25. Weight, in grams, of the isotope U-233 or U-235 or any i other material which is special nuclear material.

26. Weight, in pounds, of the isotopes U-238, Th-232, or any other material which is source material.

27. Weight, in pounds, of each disposable container including its contents.

~

28. Record the volume, in cubic feet, of the disposable container. Boxes with attached skids must include the skids in this volume. Drum pallets or spaces inside casks are not classified as container volume. Pallet volumes is chargeable but is not included in volume allocation.

p m . # . r m. r. w u me <

29. List each type of dispo sa gn, Spgntaingrf tsuch;asgwo steel box, drum, 17H, 1 7E, fD etII'ONLY t a., a

OM1A: PAP-1309 Page: 23 Rev.: 0 ,

30. Record the highest measured radiation level for each disposable container surface. Package surface may be the same as disposable container if a cask is not used.

Transport Index (TI) equals mrem /hr at 1 meter from accessible container (s).

31. Record the results of contamination surveys performed on the disposable containers. Do not use "BKG" for back-ground levels unless the background level is indicated in this column.

32. Indicate DOT subtype such as A y , A , LSA, etc.

2

33. If fissile radioactive material is being shipped, record the fissile class of the material as appropriate.

34. Indicate what kind of DOT labels or markings are used on each container, such as RADIOACTIVE W-1, Y-ll, Y-Ill or LSA.

35. Record in the indicated blocks, the page totals for the e- column.

6.9.2 U.S. Ecology Radioactive Shipment Manifest (Attachment 7)

The numbers preceding each instruction correspond to the numbered item on the U.S. Ecology RSM. Information must be provided for all numbered items on the RSM form.

1. Generator Number and Name - In the boxes provided, enter the number assigned to PNPP by U.S. Ecology. Indicate the plant name, address, contact person, and telephone number. The contact person is the Radioactive Shipment Coordinator. The User Permit Number is assigned to PNPP by the State of Washington, and should be consistent with the consigned disposal facility (Item 4). The shipment number should agree with the " Radiation Shipment Record Number" indicated on the Washington State form RHF-31.

This number is assigned by the Radioactive Shipment Coordinator.

2. Billing Information - Indicate in this section the exact name, address, and purchase order number which should be used by U.S. Ecology for invoicing. If disposal charges are to be billed to a broker, simply write the word

" BROKER" in this section. If U.S. Ecology is the broker, all the information in this section must be completed.

3. Agent / Broker - If an agent or' broker is 4utilfzed'[c{m-plete this section lli' sting 7the','A~g'endoFBrlyke3rr ~ 8dtes s,

OM1A: PAP-1309 Page: 24 Rev.: O contact person, telephone number, and the User Permit Number assigned to the Agent or Broker by the state of Washington. The broker may sign in this area to acknowl-edge receipt of the vaste.

4. Assigned to - Check the box for the Hanford Reservation !

site. }

5. Carrier - Indicate the originating carrier name, address, phone number, and EPA hazardous waste identification I number if required. Indicate the shipping date, type of cask used (if any) and the highest cask surface exposure ['

rate.

6. Proper shipping name - Indicate the total number of [

1 packages and total weight, in pounds, of all packages in each of the proper shipping name categories. The total weight in this section should equal the total of the ,

weights recorded in column 12 of the continuation sheets, t

7. Shipment totals - Indicate the total volume, in cubic ;

' feet, and the number of packages for the entire shipment. ,

Pallets and skids are not included in pac.kage volumes.

Also indicate the total quantity of source material, in i kilograms, and special nuclear material, in grams.

Ensure the totals, in grams, for U-233, U-235, and Plutonium equals the grand total for special nuclear t material. Indicate the quantity of Tritium, C-14, Tc-99, ;

and I-129. The total activity for all isotopes in the shipment is to be indicated in the "ALL ISOTOPES" column.

Check the appropriate box for the units of activity used for these isotopes. i

8. Signature - The certification must be signed and dated by the person responsible for the packaging and labeling !

operations and who is authorized to sign on behalf of the company. r Continuation Sheet ;

A. Complete the generator number, name, and +

agent / broker name (if used) in the upper left corner of the continuation sheet.

B. Transfer the manifest number from page 1 of the i manifest to the block in the upper right corner on the continuation sheet. -Fill in the page number and total number of pages for the shipment.

1 (A, f

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OM1A: PAP-1309 Page: 25 Rev.: 0 C. Item number - Each container must be listed indi-vidually, even if each is exactly alike in all respects. The number entered is the identification number stenciled on the container.

10. Container type - Indicate the type of disposable container used, such as 55-gallon drum, wood box, etc.

11. Container Volume - Indicate the cubic footage of the outside dimensions of each disposable container to the nearest hundredth of a cubic foot. Pallets and skids attached to the container are not to be included in the container volume. Some common containers are:

55 gallon drum - 7.50 cu. ft.

30 gallon drum - 4.01 cu. ft.

5 gallon drum - 0.67 cu. ft.

12. Container weight - List the combined weight of the container plus the contents to the nearest pound.

13. Physical Form - Describe the physical form of the con-tents in the container. " Solid", " Liquid" or " Gas" are the only acceptable descriptions.

14. Watte description - Using the codes found in NOTE #1 at the bottom of the continuation sheet, indicate the single code wi.ich most specifically describes the type of waste in the centainer. If "0THER" is used, a written explana-tion must be attached to the manifest.

15. Solidification or absorbent media - Using the codes found in NOTE #2 at the bottom of the continuation sheet, indicate the single code which identifies the name of the material used to solidify or absorb the waste material.

Use of any other material or brand name must be specif-ically approved by the government authority regulating disposal of the material. Use of "0THER" in this column requires a written explanation attached to the manifest which will include a copy of the letter of approval from

.the appropriate government authority.

16. Chemical Form - As accurately as possible, list the most prevalent chemical form, such as cellulose, Na, cement, metallic oxides, toluene, xylene, etc.

Indicate the name and percentage of chelating agents which are prese'nt in amoun_ts greater than 0.,1,%,by weight __

of the waste or greate3 thang,120Laby package volume.s

Specify whether the percengAgefisJyt,vf i gi l tseri,vglygeit g

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OM1A: PAP-1309 Page: 26 Rev.: 0 If chelating agents are not present or if they represent less than 0.1% by weight, then check the column provided.

17. Radionuclide - List all radionuclides present in the container. Enter each nuclide on a separate line and use as many lines as required for each container. Listing only the most abundant radionuclides or the category

" mixed fission products" is not acceptable.

18. Activity - List the activity for each radionuclide.

Check the appropriate box at the top of the column to indicate the units used.

19. DOT sub-type - Indicate the Department of Transportation category used to determine the maximum activity allowed in the package. Categories include "A " "A,", "LSA",

"HRCQ","LimitedQuantity"(LQ),"Inschum,entaandArti-cles" (I/A), etc.

20. Special Nuclear Material - List any special nuclear material, in grams.

21. Source Material - Indicate the weight, in kilograms, of source material contained in the shipment.

22. Waste form class - Indicate the waste classification (A, B, or C) of the waste in the container.

23. Stability Class - Indicate the stability of the waste in the container. Use the codes "S" for stable waste and "U" for unstable.

24. Radiation Level - Disposal container surface - Indicate the highest radiation level, in mrem /hr, or contact with the dispcsable container. Do not enter the values for the exposure levels on the cask (if used).

25. Do not make any marks in this column.

26. Radiation level - Disposal container at 1 meter - List the highest radiation level measured at one meter from the disposable container. Do not enter values for the exposure levels on the cask (if used).

27. Transport Index - Indicate the transport index for the package, if required. If the package does not require a transport index, enter "N/A" in-the.blockr

28. Fissile Class - Indicate th e i er ihs as applicable.

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4 OM1A: PAP-1309 Page: 27 Rev.: 0 i

29. DOT label - Indicate the type of label or marking which !

appears on the package, such as " WHITE-1", " YELLOW-11",

or "LSA", etc.

30. Totals - Enter the page totals on each continuation sheet for columns 9, 11, 12 18, 20 and 21.

6.9.3 South Carolina Radioactive Raste Shipment Prior Notification and Manifest Form (Attachment 8)

The numbers preceding each instruction correspond to the numbered item on the Prior Notification Form.

1. Enter the company name and address of PNPP.

2. Enter the name, title, and telephone number of the Radioactive Shipment Coordinator.

i 3. Enter the South Carolina Waste Transport Permit number assigned to PNPP.

' ' ~

4. Enter the volume allocation number assigned to the shipment.

5. Enter " Perry Nuclear Power Plant 10 Center Road Perry, OH 44081" 4

6. Enter "Barnwell Waste Management Facility i P.O. Box 726 Barnwell, S.C. 29812"

) 7. Enter the date the shipment is expected to leave PNPP.

8. Enter the date the shipment is expected to arrive at Barnwell. This date is normally two days after shipment leaves PNPP.

9. Enter the name of the carrier.

10. Enter the trailer number and owner, if known (exclusive use vehicle only).

11. Enter the type of transport vehicle, such as " van" or ;

" flatbed" (exclusive use vehicle only).

12. List the specific routes the vehicle will take within the ;

State of South Carolina. Verif the routes listed are"upptbyr$y wWhe.. carrier-thsM g p ( g,vyq thwa p n a'f' '

ONLN a

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OM1A: PAP-1309 Page: 28 Rev.: 0 13-25 Obtain the required information pertaining to the ship-ment from the manifest and enter it in the appropriate blocks.

The notification statement shall be signed by the General Supervising Engineer, Radiation Protection Section, or designee.

6.9.4 South Carolina Radioactive Waste Shipment Certification Form (Attachment 9)

The South Carolina certification form is a two part form that is to be completed by the shipper and carrier. The informa-tion,in Part I is to be completed by the Radioactive Shipment Coordinator, or designee. The certification statement shall-be signed by the General Supervising Engineer, Radiation Protection Section, or designee. Part II is completed by the carrier upon receipt of the shipment.

6.9.5 The Washington State Low-Level Radioactive Waste Shipment Certification for Commercial Generator / Packagers, and Brokers

'~ and Carriers (Attachment 10)

The Washington State certification form is a three part form that is to be completed by the waste generator, the shipment broker, and the carrier. The information in Section A is to be completed by the Radioactive Shipment Coordinator, or designee. The General Supervising Engineer, Radiation Protection Section, or designee, shall sign the certification in Section A. Section B shall be completed by the broker. If a broker is not used, write "NO BROKER USED" in Section B.

The carrier shall complete Section C upon receipt of the shipment.

NOTE: A broker constitutes any person, company, or organi-zation who takes possession of waste from a generator and assumes responsibility for that waste.

6.9.6 Exclusive Use Shipment Checklist (Attachment 11)

The Exclusive Use Shipment Checklist shall be completed by the Radioactive Shipment Coordinator or his designee. A Quality Control Inspector shall witness the steps indicated on the checklist. Initials shall be placed in the appropriate blocks upon completion of the step. The checklist shall be signed by the appropriate personnel upon satisfactory completion.

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d OM1A: PAP-1309 Page: 29 Rev.: 0 6.9.7 Vehicle Inspection Form (Attachment 12)

The instructions for completing the Vehicle Inspection Form

, are contained on the form. The individual performing the inspection shall sign the certification statement after the vehicle has been satisfactorily inspected.

6.9.8 Isotopic Analysis Results Form (Attachment 13)

The Isotopic Analysis Results Form shall be completed for each shipment to the Barnwell disposal facility that contains resins or aqueous filter media (including filters). A computer printout may be used in lieu of Attachment 13, provided the following information is contained on the printout.

a. Radionuclides present

b. Percent abundance of each radionuclide

c. Curie Content

d. Specific activity of each radionuclide expressed in microcuries per cubic centimeter. Transuranics shall be expressed in nanocuries per gram.

6.10 Selection of Transport Vehicle for Waste Shipments 6.10.1 Whenever possible, a closed transport vehicle should be used

for radioactive shipments. A closed transport vehicle pro-vides better protection from the elements, is less conspicuous in public, and in some cases allows for higher radiation levels on the packages.

6.10.2 An open flatbed trailer may be used to ship casks and large boxes of LSA radioactive material providing the following radiation limits are not exceeded:

a. 200 mr/hr on the accessible external surfaces of the package (PNPP guide value is 180 mr/hr).

b. 200 mr/hr at any point on the vertical planes projected from the outer edges of the transport vehicle, or the upper surface of the load, and on the lower external surface of the transport vehicle (PNPP guide value is 180 mr/hr).

c. 10 mr/hr at any point 2 meters (6.6 feet) from the vertical planes projected from the outer edges of the transport vehicle (PNPP guide value is 9 mr/hr),

d. 2 mr/hr in any normally occupied position in the trans-port vehicle (this includes sleeper cabs), except that this provision does not apply to private motor carriers when personnel are operating under the radig i,op f g*

a O. Nu i

4 OM1A: PAP-1309 Page: 30 Rev.: O protection program and wear exposure devices (PNPP guide

< value is 1.8 mr/hr).

i NOTE: The General Supervising Engineer, Radiation Protection Section may authorize the PNPP Guide Values to be exceeded, but in no case shall the radiation levels exceed the DOT limits.

6.10.3 A van or shielded van may be used to ship packages of LSA radioactive material. The radiation limits for an exclusive use closed transport are as follows:

a. 1000 mr/hr as the accessible external surfaces of the package (PNPP guide value is 900 mr/hr).

b. 200 mr/hr at any point on the outer surfaces of the transport vehicle, including the upper and lower surfaces (PNPP guide value is 180 mr/hr).

c. 10 mr/hr at any point 2 meters (6.6 feet) from the vertical planes represented by the outer lateral surfaces of the transport vehicle (PNPP guide value is 9 mr/hr).

d. 2 mr/hr in any normally occupied position in the trans-port vehicle (this includes sleeper cabs), except that this provision does not apply to private motor carriers when personnel are operating under a radiation protection program and wear radiation exposure devices (PNPP guide value is 1.8 mr/hr).

6.10.4 Whenever possible, use a canvas or roll top van for drum shipments to the Barnwell disposal facility. The open top van allows the use of a crane with a suction pick-up to off-load j the drums. This eliminates the need for palletizing the drums, thereby reducing burial volume.

6.10.5 Drums and liners that exceed the radiation limits in paragraph 6.10.2 or 6.10.3, require the use of a shipping cask in order

to comply with federal radiation limits for shipments. In this case the cask becomes the package and must be marked and labeled as such. A guide for selection of a proper shipping cask is contained in Reference 4.13.

i 6.11 Preparing a Loading Plan 6.11.1 A loading plan is useful for reducing the amount of time it takes to load a shipment, reduces man-rem exposure, and reduces the possibility of having to change the load on a vehicle due to weight distribution or radiation levels.

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Rev.: 0 6.11.2 For most radioactive shipmente the loading plan need only consist of knowing which packages are to be loaded, however, a detailed loading plan is necessary if any or all of the following conditions exist:

a. Exclusive use shipments that contain packages with radiation levels at or above 200 mr/hr;

b. Non-cask shipments to a burial facility;

c. Exclusive use shipments that will have packages stacked on one another; or

d. Exclusive use shipments that approach the weight or volume limits of the vehicle.

6.11.3 A vehicle should be loaded so that the weight is distributed evenly over the trailer. If the weight cannot be distributed evenly, the heaviest portion of the load should be placed over the axle.

6.11.4 Heavier packages shall be loaded on the bottom of the ship-ment. Drums weighing in excess of 300 pounds shall be placed t

on the bottom of the shipment unless shipped in an open top van.

6.11.5 Packages (other than drums) must have a minimum clearance of three inches from the van walls. (Barnwell) 6.11.6 Packages must have a top clearance of at least twelve inches in a closed van.

6.11.7 Packages weighing more than 8000 pounds shall not be shipped in a closed top van.

6.11.8 Attachment 14 shows the inaide dimensions for standard trailers used for shipments. Also shown in the table is the number of unpalletized 55 gallon drums per layer the trailer will hold and the number of 6-drum pallets that will fit in the trailer (1 layer).

6.11.9 Unstable Class A waste must not be mixed with other waste classes on the same pallet. Unstable Class A waste should be segregated from other wastes as much as possible. Normally unstable Class A wastes are placed in the forward part of the trailer.

6.11.10 Shipments should normally be loaded so that the packages with the highest radiation levels are placed in the center of the load. Careful attention should be paid to the radiation levels on the bottom of packages that areJcaded on-the-ven1 floor, and to the radiatf5n,Aevels onyt eatop r at are loaded on the top sthcldhfhaciggbd/M%yf V p cGgs} tf ONLY

OM1A: PAP-1309 Page: 32 Rev.: 0 6.11.11 To the extent practicable packages should be arranged with the highest dose rate surfaces facing inboard when loaded in vans, and facing inboard and to the rear when loaded on flatbed trailers.

6.11.12 Boxes and unpalletized drums may be stacked but shall be segregated. Boxes should not be stacked on unpalletized drums nor unpalletized drums on boxes.

6.11.13 When a loading plan is established, the shipment should be prestaged, if possible, in such a manner so loading equipment can access the packages in the order they are to be loaded.

Prestaging the packages also allows for inspection of the shipment.

6.12 Loading a Transport Vehicle 6.12.1 Transport vehicles consigned as exclusive use shall be in-spected for road-worthiness prior to loading. The Vehicle Inspection Form, Attachment 12, shall be used to perform and record the inspection. The completed form shall be kept on file with the appropriate shipment paperwork.

6.12.2 Transport vehicles consigned for shipment to the Richland disposal facility must have a Washington State Patrol or Washington State Utilities and Transportation Commission vehicle inspection certificate, or a visible Washington State 90 day vehicle inspection seal.

6.12.3 All shipments of radioactive material consigned as exclusive use shall be inspected by the Radioactive Shipment Coordina-tor, or his designee, prior to release of the shipment. The Exclusive use Shipment Checklist, Attachment 11, shall be used to record the results of these inspections.

6.12.4 Prior to loading a transport vehicle consigned for shipment to the Barnwell disposal facility, verify that a prior notifica-tion form (Attachment 8) was completed and mailed to the South Carolina DHEC, and the Barnwell disposal facility in time so they have 72 hours8.333333e-4 days 0.02 hours 1.190476e-4 weeks 2.7396e-5 months notice before the shipment reaches South Carolina.

6.12.5 Transport vehicles that are placarded " RADIOACTIVE" shall have a photograph taken of each of the four sides of the vehicle showing the placarding, and a photograph of the load showing any bracing and shoring.

6.12.6 All exclusive use vehicles shall have radiation and contamina-tion surveys performed on them in accordance with Health, -

Physics instructions prior TtCiEe's's'iiinin the Protected Area;.

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7 OM1A: PAP-1309 Page: 33 Rev.: 0 Boundary. Results of these surveys shall be kept on file with the shipment paperwork.

6.12.7 Open flatbed trailers shall be loaded as follows:

1. The loading plan (if required) shall be used during loading operations. Any deviations from the loading plan must be approved by the Radioactive Shipment Coordinator, or designee

2. Packages, other than drums, shall have sufficient bottom clearance to allow for placement of lifting slings or forklift operations.

3. Drums weighing more than 800 pounds must be palletized and banded together on each pallet. (Barnwell)

4. Packages shall be secured to the trailer bed with chains and binders or straps and winches supplied by the carrier.

5. Additional bracing may be provided by installing toe-boards. Toeboards will normally be sections of 2 x 4's nailed to the bed of the trailer.

6. A tamper indicating seal shall be installed on the closures of Type A and Type B packages and casks.

7. The four sides of the trailer and the front of the tractor shall be placarded " RADIOACTIVE". Extra placards shall be provided to the driver as replacements in the event a placard is lost during transit.

8. A radiation and contamination survey shall be performed on the loaded trailer and tractor. The radiation levels shall not exceed the limits specified in paragraph 6.10.2 of this procedure. Results of the surveys shall be filed with the shipment paperwork.

6.12.8 Closed transport vehicles without open. cops shall be loaded as follows:

1. The loading plan (if required) shall be used during loading operations. Any deviations from the loading plan must be approved of by the Radioactive Shipment Coordina-tor, or designee.

2. Drums need not be palletized when shipped to Richland. l If drums are palletized for ease _gf. handling,;the ' pall'lie l volume is not conside" red part..of .the burial v.olume. u u- I g g;a g g y.c C M -l y u w (pAqam 9

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OMIA: PAP-1309 Page: 34 Rev.: 0

3. Drums weighing less than-600 pounds need not palletized when shipped to Barnwell, but a surcharge will be as-sessed. Drums weighing 600 pounds or more must be palletized. Pallet volume is charged as burial volume.

Drums weighing more than 1250 pounds will not be accepted.

4. Packages, other than drums, must have a minimum clearance of three inches from the van valls. (Barnwell)

5. Packages must have a top clearance of twelve inches from the van roof.

6. Packages, other than drums, shall have sufficient bottom clearance to allow for forklift operations.

7. Blocking and bracing shall be installed to prevert shifting of the load during transportation.

8. Tamper indicating seals shall be installed on the doors of the van in such a way so as to give evidence if the doors are opened.

9. The four sides of the trailer and the front of the tractor shall be placarded " RADIOACTIVE". Extra placards shall be provided to the driver as replacements in the event a placard is lost during transit.

10. A radiation and contamination survey shall be perforned on the loaded trailer and the tractor. The radiation levels shall not exceed the limits specified in paragraph 6.10.3 of this procedure. Results of the surveys shall be filed with the shipment paperwork.

6.12.9 Closed transport vehicles with open tops shall be loaded as follows:

1. The loading plan (if required) shall be used during loading operations. Any deviations from the plan must be approved by the Radioactive Shipment Coordinator, or designee.

2. Drums need not be palletized when shipped to Richland.

If drums are palletized for ease of handling, the pallet volume is not considered part of the burial volume.

3. Drums weighing less than 800 pounds should not be pal-letized when shipped to Barnwell, to permit use of a '

vacuum offloader. Drums weighing 800 pounds or.more must be palletized. Pallet volume _is_ch uged.as,-bu, rial "

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OM1A: PAP-1309 Page: 35 Rev.: 0 volume. Drums weighing more than 1250 pounds will not be accepted.

4. Packages, other than drums, must have a minimum clearance of three inches from the van valls, unless fixed slings are attached. (Barnwell)

5. Packages, other than drums, shall have sufficient bottom clearance to allow for placement of lifting slings or forklift operation.

6. Blocking and bracing should be installed to prevent shifting of the load during transportation.

7. Tamper indicating seals shall be installed on the doors of the van in such a way so as to give evidence if the doors are opened.

8. The four sides of the trailer and the front of the tractor shall be placarded " RADIOACTIVE". Extra placards shall be provided to the driver as replacement in the event a placard is lost during transit.

9. A radiation and contamination survey shall be performed on the loaded trailer and the tractor. The radiation levels shall not exceed the limits specified in para-graph 6.10.3 of this procedure. Results of the surveys shall be filed with the shipment paperwork.

6.12.10 Prior to departure, the driver shall be briefed on the follow-ing:

a. Type of material being transported;

b. Any special routing instructions (these are to be sup-plied in writing);

c. Maintenance of exclusive use vehicle. The Instructions for Maintaining Exclusive Use Vehicle, Attachment 15, shall be signed by the driver and a copy provided to him.

The original shall be placed in the shipment file;

d. Emergency response in the event of an accident. The Response to Transportation Incidents, Attachment 16 shall be supplied to the driver; and

e. Any other special instructions concerning the shipment.

6.12.11 Prior to the shipment leaving the site, notify the burial facility of the date and time of departure. Notify Barnwell at (803) 758-7806 and Richland at (509) 377-2411.

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OM1A: PAP-1309 Page: 36 Rev.: 0 6.13 Verification of Receipt of Waste Shipments 6.13.1 The disposal facility is required to acknowledge receipt of the waste shipment within one week of receipt by returning a signed copy of the manifest or equivalent documentation.

6.13.2 If receipt of the shipment has not been acknowledged within 20 days, an investigation shall be conducted as follows:

a. Contact disposal site and the carrier to determine if the shipment arrived at the disposal site, and if not, the location of the shipment and the reasons for non-delivery.

b. Within two weeks of the completion of the investigation, a written report shall be prepared and submitted to the US NRC, Region III, Office of Inspection and Enforcement, 799 Roosevelt Road, Glen Ellyn, Illinois, 60137.

6.13.3 Verification of receipt and a copy of any investigation report (if applicable) shall be filed with the shipment paperwork, r 6.14 Records 6.14.1 The following documents are generated by this procedure:

Quality Assurance Records Barnwell Waste Management Facility Radioactive Shipment Manifest South Carolina Radioactive Waste Shipment Prior Notification and Manifest Form '

South Carolina Radioactive Waste Shipment Certification Form U.S. Ecology Radioactive Shipment Manifest Washington State Low-Level Radioactive Waste Shipment Certification Carrier's Bill of Lading High. Integrity Container. Certification Instructions for Maintaining Exclusive Use Vehicle, PNPP 6606 Written statement of any unusual conditions or hazards Exclusive Use Shipment Checklist, PNPP 6608 Vehicle Inspection Form, PNPP 6610 Package Surveys Vehicle arrival surveys Vehicle departure surveys Verification of Receipt from burial facility Lost shipment investigation report to NRC Photographs of Transport vehicle showing placarding and load bracing Waste Classification Worksheet, PNPP 6626 . - . . _

Isotopic Analysis Results Form...PNPP-6675 'M_:r '"

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OMIA: PAP-1309 Page: 37 Rev.: 0 Quality Assurance Records (Cont.)

LSA Worksheet, PNPP 6604 Routing Instructions Non Quality Records None Records identification and disposition are accomplished in 4

accordance with the Records Retention / Disposition Schedule (RR/DS) and handled in accordance with PAP-1701, Plant Records Management.

l_

6.14.2 The records generated by this procedure are to be filed together in the applicable shipment docunent package.

6.14.3 The following notations are used to ind'cate the distribution of the records:

a. (Shipment) - The original document is included in the shipment package that the carrier delivers to the con-signee.

b. (Carrier) - The document is included in the package the

carrier retains for their records.

c. (File) - The document is filed with all records generated under the same shipment number in the shipment package,

d. (Mailed /DHEC) - The original document is mailed to the South Carolina Department of Health and Environmental Control at least 72 hours8.333333e-4 days 0.02 hours 1.190476e-4 weeks 2.7396e-5 months prior to shipment.

e. (Mailed /CNSI) - The document is mailed to Chem-Nuclear Systems Inc. at the Barnwell Waste Management Facility at least 72 hours8.333333e-4 days 0.02 hours 1.190476e-4 weeks 2.7396e-5 months prior to shipment.

f. (Mailed /U.S. Ecology) - The document is mailed to U.S.

. Ecology at the Richland disposal facility at the time of shipment.

6.14.4 The document package for radioactive waste shipments to the Barnwell disposal facility shall include:

a. Barnwell Waste Management Facility Radioactive Shipment Manifest, (Attachment 6).

(Shipment) (Carrier) (File)

b. South Carolina Prior Notification and Manifest Form (Attachment 8).

(Shipment) (File) (Mailed /DHEC) (Mailed /CNSI)

c. South Carolina Radioactive Waste Shipment Certification Form (Attachment 9).

(Shipment) (Carrier) (File) __

fi3h b ONLY r c.- . .

OM1A: PAP-1309 Page: 38 Rev.: O

d. Isotopic Analysis Results Form, (Attachment 13), if applicable.

(Shipment) (File)

e. Instructions for Maintaining Exclusive Use Vehicle.

(Attachment 15).

(Shipment) (Carrier) (File)

f. Carrier's Bill of Lading (if required by the carrier).

(Shipment) (Carrier) (File)

g. Response to Transportation Incidents (Attachment 16).

(Carrier)

h. High Integrity Container Certification (if applicable).

(Shipment) (File)

1. Written statement of any unusual conditions or hazards i (if applicable).

(Shipment) (Mailed /CNSI) (File)

j. LSA Worksheet (Attachment 2).

(File)

k. Waste Classification Worksheet (Attachment 5).

(File)

1. Exclusive Use Shipment Checklist (Attachment 11).

- (File)

m. Vehicle Inspection Form (Attachment 12).

, (File)

n. Package surveys.

(File)

o. Vehicle arrival surveys.

(File)

p. Vehicle departure surveys.

(File) (Shipment)

q. Routing Instructions (if applicable)

(Carrier) (File) 6.14.5 The document package for radioactive waste shipments to the Richland disposal facility shall include:

I

a. U.S. Ecology Radioactive Shipment Manifest (Attachment 7),

(Shipment)(Carrier)(File)(Mailed /U.S. Ecology)

b. Washington State Low-Level Radioactive Waste Shipment Certification (Attachment 10).

(Shipment)(Carrier)(File)

c. Instructions for Maintaining Exclusive Use Vehicle (Attachment 15).

(Shipment) (Carrier)(File)

d. Carrier's Bill of Lading (if required by carrier).

(Shipment)(Carrier) (File)

e. Response to Transportation Incidents (Attachment 16).

(Carrier) fr- a .3 rj h[h5'bYdN E d l Of-llLY a

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OM1A. PAP-1309 Page: 39 Rev.: 0

f. Written statement of any unusual conditions or hazards (if applicable).

(Shipment)(Mailed /U.S. Ecology)(File)

g. LSA Worksheet (Attachment 2).

(File)

h. Waste Classification Worksheet (Attachment 5).

(File)

1. Exclusive Use Shipment Checklist (Attachment 11).

(File)

j. Vehicle Inspection Form (Attachment 12).

(File)

k. Package Surveys (File)

1. Vehicle Arrival Surveys (File)

m. Vehicle Departure Surveys (File) (Shipment)

n. Routing Instructions (if applicable)

(Carrier) (File) 7.0 ATTACHMENTS 7.1 Attachment 1 - Table of Ag and A2 Values f r Radionuclides.

7.2 Attachment 2 - Form: PNPP No. 6604, LSA Worksheet.

7.3 Attachment 3 - Table I.

7.4 Attachment 4 - Table II.

7.5 Attachment 5 - Form: PNPP No. 6626, Waste Classification Work-sheet.

7.6 Attachment 6 - Barnwell Waste Management Facility Radioactive Shipment Manifest.

7.7 Attachment 7 - U.S. Ecology Radioactive Shipment Manifest.

7.8 Attachment 8 - South Carolina Radioactive Waste Shipment Prior Notification and Manifest Form. DHEC 802.

7.9 Attachment 9 - South Carolina Radioactive Waste Shipment Certifica- ,

tion Form, DHEC 803.

t 7.10 Attachment 10 - Washington State Low-Level Radioactive Waste Shipment Certification for Commercial Generator / Packages and 3

Brokers and Carriers *, RHF-31A.

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OM1A: PAP-1309 Page: 40 Rev.: 0 7.11 Attachment 11 - Form: PNPP No. 6608, Exclusive Use Shipment Checklist.

7.12 Attachment 12 - Form: PNPP No. 6610, Vehicle Inspection Form.

7.13 Attachment 13 - Form: PNPP No. 6675, Isotopic Analysis Results

, Form.

7' '7.14 Attachment 14 - Standard Transport Van Dimensions (Inside).

7.15 Attacheent 15 - Form: PNPP No. 6606, Instructions for Maintaining Exclusive Use Vehicle.

7.16 Attachment 16 - Response to Transportation Incidents,

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llote 1. Refer to 49 CFR 173.423. Table 7 and 173.403 (1).

to 49 CFR 173.421 for other requf rements.

value is 20 curfes 'for Americium and Plutonium contained in For shipments solely within the linf ted States the A g Note 2.

As-Be er Pu-Se neutron sources er in nuclear powered pacemakers.

ii f must be calculated in accordasce with 49 CFR 173.433 taking into account the act v ty o IIete 3. The values for A g a nd A2 the fissten predicts and of the (1-233 la addition to that of the thorium, i Refer to 49 CFR 173.423. Table 7.

meg.

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A Refer to 49 CFR 173.421 and 173.424. -

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cross state boundary en twete to a disposal site. Advente notf fication f (,,

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PNPP No. 6604 OMIA: PAP-1309 Page: 51 Rev.: 0 LSA Worksheet Attachment 2 PART I Form: PNPP No. 6604

. 1) Date

2) Description 3) Package No.

4) Batch No. 5) Package Weight Ibs

6) Total Activity mci

7) Sample Activity mC1

8) Sample Weight gms Percent Specific LSA

9) Radionuclide 10) Abundance 11) Activity 12) Activity 13) Group r

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Form: PNPP No. 6604 PART 2

1) 'Oate 2)' Description 3) Package No.

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14) 15) 16) 17) 18) 19)

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LSA Croup Activity LSA Limit Unity Factor

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25) Total Unity Factor If the total unity factor does not exceed 1.0, the maternal may be classified as Low Specific Activity.

PART 2 Calculated By 1NFORMAT!OU ONt-Y ___

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OMIA: PAP-1309 Page: 53 Rev.: 0 Attachment 3 TABLE I Radionuclide Concentration l

col.1 cor. 2 l 1

. 1 X value pCl/cc or )

of col. 2 Cl/m3 i

C-14 .3 s C-14 in activated metal 3 80 j Ni-59 in activated metal 22 220 Nb-94 in activated metal 0.02 0.2 Tc-99 0.3 3 I-129 0.008 0.08 Alpha-omitting transuranic nuclides with half-life Greater than 5 years 1 100 10 l

P u-2 41 1 350 3,500 I

Cm-2 4 2 2,000 20,000 I

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1 OMIA: PAP-1309 Page: 54 Rev.: 0 Attachment 4 i TABLE H R a dionuclid e Concentration, pcuee A B C Total of all nuclides with less than 5 700 (1) (3) year half-lif e H-3 40 (1) (j)

Co-60 700 (1) (3)

Ni-6 3 3.5 70 700 N i-6 3 in activated metal 35 700 7,o o g S r-9 0 0.04 150 7,000 C s- 13 7 1 44 4,600 1

There are no limits established for these radionuclides in Class 8 or C wastes. Practical considerations such as the ef f ects of external radiation & Internal heat generation on transportation, handling, & disposal will limit the concentrations for these wastes. These wastes shall be Class 8 unless the concentrations of other nuclides in Table 2 determine the waste to Class C independent of these nuclides

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Micii WASTE CLASSIFICATIOkWORKSHEETlMM,yJ, i ,

PACKAGE Pos.

TABLE.I._RAOIONUa ! DES.. __

WASTE CLASS COLWN I COLLDe4 2 i

MIOE ACTIVITY LIMIT WITY ACTIVITY LIMIT WITY l STABLE UNSTABLE AC1/cc AC1/cc FACTOR A C1/cc A ci/cc FACTOR C -14 0.8 8.0 C - 14 Act. Mtl. 8 80 Ni - 59 Act' Mtl 22 220 NJCLICES WITH T1/2 > SYRS PC - 94 Act. Mtl 0,02 0.2 Tc - 29 0.3 3 A C1/cc I - 129 0.008 0.08 ACTIVITY LIMIT UNITY ACTIVITY LIMIT WITY 1

nC1/CR nci/CR FACTOR nC1/CR nC1/GR FACTOR Pu - 241 350 3500 Cm - 242 7000 20000 TRANSWANICS wITH 10 100 Y 1/2 > 5 yrs TOTAL TOTAL WITY = WITY =

FACTOR FACTOR l

TABLE II RADIONUaIDES COLtDe A COLUMN B COU)e4 C 6

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OMIA: PAP-1309 Page: 60 Rev.: 0 Attachment 8 50tml CAROLINA CEPARTMENT OF BEALTH AND ENVIRONNENTAL CONTROL Radioactive Waste Shipment Frior Notification and Maalleet Form 3 [ Failure to Complete ALL Entries Will Result in Return of Form and Constitute Neocompliance.) See Re*ecae 5tde for instructione

1. Nane and Adoress at Shipper / Generators 2. Person Responsible for Waste Shipments a) Names b) Titles e) Telephones ( )

3. Radioactive Weste Transport Fer-it No. 4 Shipment Identificatica No.:

3. Location f ree which vaste will be shipped: 6.,Name and Address of Consignee:

7. Scheduled Date of Departure of Shipment: 8. Estimated Date of Arrival of Stipeents t

9. Carrier: 10. Trailer No. 6 Owner: 11. Type Transport Vehicles (if avail.)

12. Routes snipment will follow in State of South Carolina (Be Specific):

13. Type Factage or Cast (14. Typs Container in Cask l13. Fackage or Cask Spec.:

Model No.: 1 I

16. Complete Waste Description (Be Specific):

P~~

17. Physical & Chemical Tora 18. Total No. 19. Frominent Radionuc11 dest of Fackages:

20. Total Curies: 21. Weste Clase & Stability: 22. Total Canic feet

23. DCT Sub Type 26. DOT Class. & usaard Close 23. Ewy. Route Contro11ee UN No.: (tarse quantity) .

[ ] Yes [ ] No manr1 CAT 1os I hereby cartify on behalf of the above-named shipper / generator to the South Carolina Depart-ment of Realth and Environmental Control that the information provided herein is complete and correct to the best of my knowledseg and that the shipper / generator has complied with all the provisione se required by Act No. 629 of 1980, the South Carolina Radioactive Waste Transporta-tion and Disposal Act, sad Department Regulation 61-83. Date Typed Name Signature of Consignor's Authorized Representative CDNSIGMB AGNOW12DCDElff This acknowledges to the South Carolina Department of Bealth and Environmental Control that the above-described radioactive weste shipment wee received. Date of Delivery signature of Consignee's Authorized Aepresentative i newed .. i sinLud Name and title MEC 802 (Rev.10/84) . _ . _ , . . . . . . - - - - - - - - ( - e" * (Ceptes of this form any be repredemd locallj as gd}" d g ., p,,, a y d u 'd ONLY

OMlA: PAP-1309 Page: 6i Rev.: 0 Attachment 9 SC TM CAACLDEA DEPARTMnrr er uzALTH Aac ENv:RCNMrY!AL CONT 30; Sadioactive wasta shipment Cartification Foain canaral Instructions and Zaformation: This is a tw part form to be used by shipyars and carriers of radioactive waste. The certifications contair.ed herein satisfy the resizements of sec tion 13-7-150, of Act wo. 499 of 1980, the south Carolina Radioactive waste Transportation d Disposal Act. This certification along with a copy of the prior actification fera shall capaay each shi; mast of radioactive waste into and within the state of souta Cass11aa. The shipper is to complete his portion of the form and present it to the carrier as part of the shipping docwients. Upcn receipt, the carrier shall complete his portion of the fors. Cpon delivery of t!.e shipment to the consigne*, a copy of this certification form, ar.d a copy of t4e prior sectificatica and Manifest form with the consignee acknowledgunsat. shall be returned to t?e cera.r= ent. Part Ir shi;;er's Cart.afteate of C=-= ta-ce l 1. Name of sha;;er est Addressa 2. Sha; ment Idenuticauen No. J. Trar.s;crt permat No. Tele;%ome wo. t 1 In cor;1aance wata Act No. 499 of 1983, the souta Carolina Aad&cactive Waste Trans;crt.ation and Cisposal Act. I hereby certify on behalf of the above-named shipper to the south Carolina Depart ment of sealth and Environmental Control that the above-named shipper has sempiled with all pro-visions of Act No. 499 of 1980, ar.d all applicable lawe and adalaist:stive rules and regulations both state and Federal, regar$1r.g the packaging, transportation, storage, dis;ceal and delivery of such wastas. I furthe: certify that this shipment of radioactive weste has been inspected w2 thin 44 hours of the time of departure and that ne items of non-ccepliance with applicable I laws, rules or regulations were fcur4. Cata Typed Name and Tatie of Ager.t of Sr.A;;er sig .a tur e Par- 12: Carr er's Certificat;en

a. Name of Carrier ar4 A44:ess: 2. sal;=ent Idenuf acauen No.

J. Transpect Trasier No. Teletheae Me. f )

4. Scaedaled Cate of Ce;arture of shipment S. Est:aated case of Arrival of shapsents Certificat&on is neremy made to the souts Caro 11r.a cepar=ent of Healta ar.d Envir:r.zental Centre thats (a) the shipper has provided the carrier with a copy of the shipeent manifest, the certiti l case of cos;11ance, and the routing instr actions: (b) the shiprent of radioactive wasta has beer '

properly placarfed fer tresspert according to applicable U.S. Ceperment of Transpertation Rep. laticasa (c) all shi;pir4 papers originated or reproduced by the carrier have been properly executed (d) the trans;crt vehicle has been inspected accorfing to applicable state and Federa ! replations within the pres:ribed intervals and that all safety and operational c:sponents are s i good werkit.g order and seet the regairements of regulations (e) all drivers who will operate ta vehicle vitain the state of scuth Carolina are qualified to transport hasardtus materials as specified by applicable U.S. Copartment of Transportation regulations: (f) the epa.taent shall i be immediately netified of any variance, occuring after departure, fra the shi;;er's notificati et primary routes in tsuth Carolina and estimated date of arrivals (g) all applicable laws ard 7 adai.nistrative rules and reg Alations, both state and Federal, rega: ding the trar.spertatien of ; radicactive wastes will be caplied with. Da ta i

                    / ped or praated Name ar4 Tatie signature Dutc 403                                                                                           ~

(5/00) (copies of this form may be reproduced loially as ndeledl~ ]~'~^ r . U WI . / h up a. f4 M N N \&M b l l n:s - e ya ' a k L),,! r

i I l OMIA: PAP-1309 Page: 62 ~ Rev.: 0 Attachment 10 m _ un NO SOCA 6 4 A> l N - IEPA@fNT OF SOCIAL AND HDLTH SDVIGS QM1A. M94!G 13-LLIL RADION* YE h43*1 SHIPENT CIRTIFICATIN FOR C+EJCIAL GENUA *'WPAChA2RS. AND SIGTAS AND CAARIDS The following certification, completed as applicable, is made to the State of unshington: of low. level radso-Certsfication is herede made to the State of mashingten that Radiation Shipment Record No. Order datet active waste has been inspected ta accordance with reausranents of the Governor of masharaton's LascativeFurther hovecer 19,19?9. petor to its snt;rient. cogiasse with ali applacable laws, mies and replations. The tageniped shall LMeetaff and told harmless t'.e State of tenhangtcn, in anaccorrence. in tota . for each l anotr.t not to exceed $1,000.000.00 andav Aa1 =ee say be injured, provided that indavitfication shall not exceed $5.000.000.00 fran any and all cla.as. mutts, losses, damage. tnJury ard czpenses to any person neemsoever of to property arisir4 or growing out of or sa any martict conncsted with the activatses performed uWer this order. kasert for any violation of applicable existing state or federal statute of' reSulationf hashar4t respecting f n , pechaging and s'ttpment. snspection and acceptance of any stem. or contatt.er or astertal covered by this certification i by the State o of a &Alv athorsted contractor shall release the party who executed this certificate from any and all ra# rsernt o ' andartifwataan from injury or loss. ............ 5FC'10N A: ICE T 1 OCRAWFACLA2R: vWy was RA41T MICTA: RLJE O mASTE th THIS SHIP (hT: rm:1: M: TT 11: sitTHW 3: R* Tf[ SEIIR: . (Lampany m; rucelf MDeut: WUM. Or mAM IN StIS SHIPfM: SY: InAft: Tini: Art'; trim C: TUR DC CAAAILA: E-y Names vtut CF =ASTI: IN Dt!S Sitt*4M: 3Y: f>TE: TITLE: D95 RitF.31A fl9513 414 (4/80) _w

                                                                                                                                                       ~.~.._                                        . _ .

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                                                                                                                                                                                              /f 6 a           }.

ONLY

PNPP N3. 6608 OMIA: PAP-1309 Pege: 63 Rev.: 0 Attachment 11 Exclusive Use Shipment Checklist Form: PNPP No. 6608 Date Shipment Number Destination Tha following items are inspected for compliance with. DOT, NRC, and burial facility regulations as appropriate. Enter "N/A" in the initial block of items that are not

     .Ipplicable.

Initials

1. Arrival radiation and contamination surveys per-performed on vehicle. (Attach surveys to checklist) RSC

2. Vehicle inspection performed. (Attach Exclusive use Vehicle Inspection Form to checklist). ~

RSC QC

3. Driver is issued dosistry for loading (as appro-priate).

RSC

4. Packages are ' marked and labeled as indicated on shipping documents. RSC QC 5.

Packages are loaded in accordance with a loading plan. , _ . ., RSC i 6. Blocking and bracing is installed to prevent shi f ting of load. RSC QC

7. Radiation surveys performed on vehicle are within the limits of 49CFR173.441 (Attach surveys to checklist). RSC QC 8.

Contamination surveys performed in and around loading area are within site limits. (Attach surveys to RSC checklist).

9. Vehicle 18 placarded if shipment is LSA EXCLUSIVE uSE or if any of the packages bear the RA010 ACTIVE

(.h.1 .' YELLOW 111 label. RSC qg}li f3.* blY $ %C ~

10. Tamper proof seals installed on all trailer doors.

RSC

11. Photographs taken of all four sides of the vehicle (placarded vehicles only). RSC

12. Driver is provided all necessary shipment documenta.

RSC 13.censignee is notified that the shipment is leaving the site and of the expected arrival date. RSC sdioactive Shipment Coordinator (RSC) Quality Control Inspector,(QC) or Designee. , i )

                                                                ,    . g, ., g, 3 q , . , , j, 2.,  Q               3

OMIA: PAP-1309 Page: 62 ~~ Rev.: 0 Attachment 10 M3 IXX t 4A> 21C25 IEP4CfhT OF SOCIE APC HEALN SDNI:IS Q.M'1A. mASi!Wim . Icm.tntL BANCA:*nt MAS *! SHIPENT GRTIFICATim 708 OeENC;AL GDEATJi?AChA2AS. #G BAC* IRS NO CANLIERS The following certification, cogleted as applicable. is made to the State of mashir4 ton: _ et le=. level ra.ito-Certification is heree, male to the State of tast.ngten that Radiation Shipment Record No. d active waste has been tnspected in acccrdance with re3&arShents of the Governor of tashangton's k.nece hoveeer 19, 1979. prior to its snapsent. coet:4ce .ita all appticable laws. rules and resslattens. The uridctstped shall Lfutemsff and told harniets the $ tate of hashington, 55.000.000.00 in each Ln tota , for l an asetr.t ocartence, not to exceed II.000.000.00 pe andav Aal mo any be injured. preytded that indeseitiscation shall not exceed from any and all clus, sutts. losses, dansge, injury and crpenses to any person whomsoever or to property aristra er growins out of or in any marmer conncsted with the activataes performed truter this order. k.ssert for any violation of applicable existing state of federsi statute or' regalation h State of masht respecting 4 ten , packaguig and sha., mar:t, anspectaen and acceptance of any stan, or container of matertal covered by thas certif tcation by t e or a dalv authorttod contractor shall release the party who executed this certtficate frtus any and all requirement of . annouritfsutson from tajury or loss. SEC*:S A: POR M LDCHA?A/F40.A2R: tWy ms MDIT NtscTR: vt1JE 08 #ASTF IN D4:5 S11 PENT: SY: mit: TfU.1:

.. ::*.:.:*::';;;;.:*:::::::. :::::*:::~;* :::::.::::::**:::::::*::*:::::::'*:::::::::::*:::::: .: *::.

scitm n: fi)H :liL SENIJ: . twaspany % PU481T pdAeur: VM184. Or WA$lt. IN THIS SHIPT.C 37: la4Tr: TIT'J: ArctnN C: f0L TIC CAAAILA: U r ynamea vol.LM. OF mAsti: IN THIS StiMM: MTE: 3Y: TITLE: ..................... [195 4f.31A [SS 13 424 (4/80)

4. I f . . . +

L N d* t8L t ' A .% 9 avu d ONLY <

OMIA: PAP-1309 PNPP N2. 6610 Page: 64 i Rev.: 0 VEHICLE INSPECTION FORM Attachment, 12 Form: PNPP No. 6610 Prior to loading a vehicle for shipment, an inspection will be conducted to insure the vehicle is in satisfactory condition for transporting radioactive material. NOTE Initials of the inspector will be placed in the appropriate block indicating completion of each inspection point. Unsatisfactory items will be explained in the remarks. SAT UNSAT SAT UNSAT Generel Condition (1) / Lichts (4)

Body Condition (2) / Tires (5)

        /
        /        Leake              (3)                    /          Loose Material in Trailer         (6)

(1) Approaching wahicle, note general overall condition (e.g., holes, excessive rust, bent frame, etc.). (2) check for holes, proper flooring in trailer, loose body parts that could affect safety, etc. (3) Look under vehicle for leeks of oil, grease, fuel and meter (check around wheels for grease). (4) Check that headlights, clearance lights and hazard lights operate. (5) check for sort or fist tires, excessive treed weer, and treed stripping off tires. (6) No loose material in troller, such as mood, metal scraps, boxes, tires, etc.

                        -                                 Iractor No.                       Trailer No.

TRANSPORT VEHICLES CONSIGNED FOR SHIPMENT TO WASHINGTON STATE MUST HAVE A WASHINGTON STATE PATROL OR WASHINGTON STATE UTILITIES AND TRANSPORTATION COMMISSION VEHICLE INSPECTION CERTIFICATE, OR A VISIBLE WASHINGTON STATE 90 DAY VEHICLE INSPECTION SEAL, CERTIFICATE /5EAL NUMBER REMARKS: CE! Inspector Signature gpg O RRRUI P 4% f"." " "j { { Eas Ih8 1 certify, to the best of my knowledge, , that all mechanical and safety related items are in good working condition. Driver Signature l , . l

                                                             -**    x.     . '.."       , .. . s- , 2

( Nb " ,7,, yV f as *}

t l . -

OMIA: PAP-1309 Page: 65 Rev.: 0

      , ,, g3                                                                                           Attachment 13 Form:. PNPP No. 6673 ISOTOPIC ANALYSIS RESULTS (FOR PACKAES CONTAINING RESIN OR FILTER PCDIA)
        ,               APPLICAILE PACXAGES SHIPMENT NO.

DATE WASTE VOLtK PER PACKAE RADIOPCCLIOE PERCENT A8UPCANCE ACTIVITY SPECIFIC ACTIVITY JE1 / cc e-N TRANSLRANICS PERCENT A8UPCANCE ACTIVITY SPECIFIC ACTIVITY nCI / sm

                                                                  "'**'**'*W            .e   .m, CuretEfen av we r t, ,c n.u ,1,               g ps pu (NIi h .Y _. _ . . _ _;

I .

                ~ - .                                  -             -

i > 1 OM1A: PAP-1309 Page: 66 Rev.: 0 Attachment 14 Table of Standard Transport Van Dimensions (inside) TYPE OF TRAILER 40 ft. 45 ft. 48 ft. LENGTH ---- 477 in. 540 in. 576 in. WIDTH ---- 96 in. 96 in. 96 in. - s HEIGHT ---- 99 in. 103 in. 107 in. No. of ---- 76 88 96 DRUMS (4 x 19) (4 x 22) (4 x 24) . No. of ---- 1~ 14 16 PALLETS

                                                     . 6)              (2 x 7)                           (2 x 8)

NOTE - Number of 55 gallon unpalletized drums per layer. I NOTE - Number of 6-drum pallets (72 in. x 48 in.) per layer. i i 1 I t 80 h dup '% ..LL s4. # * . en W'd OniLY w-- v-,-,w-y +

OMIA: PAP-1309 PNPP No. 6606 Page: 67 Rev.: 0 Attachment IS Form: PNPP No. 6606 Instructions for Maintaining C=clusive use ventele For " Exclusive Use" shipments of Radioactive Materials Instructions to Carrier:

1. Shipment is to be delivered to Consignee without reloading.

2. Exclusive Use means this vehicle is to transport only those materials loaded by the Perry Nuclear Power Plant.

3. Material is to be shipped directly to and be unloaded by constqnee. 4 Trailer must be cleared by consignee to ensure radiation and con-tamination levels are w2 thin specification prior to releasing the trailer for other use.

5. In the event of accidents.. leaks or unusual delays, make r e q u l'r e d report to Department of Transportation and n'o t i f y the Perry Nuclear Power Plant as.soon as possible. Make notification to the Perry Plant by call.ng (216) 259-3737 day or night End tequest the indi-vidual answering the phone to call this information to the Shift Supervisor.

6. Missing placards shall be replaced tmmediately. E=tra placards w111 be provided by Perry Nuclear Power Plant. 7. Notify the Petry Nuclear Power Plant in the event a different tractor is attached to the trailer. This is necessary to determine if the different configuration will affect radiation levels in the cab. 8. Keep these instructions with the radioactive material shipping papers. E,4 T R A PLACARDS PROVIDED C PLACARDS NOT REQUIRED ~ lTriver's Signature

                                                $          h      me           .

4 U w.a s v. _. 1,

OM1A: PAP-1309 Page: 68 Rev.: 0 Attachment 16 RESPONSE TO TRANSPORTATION INCIDENTS (MAJOR HIGHWAY ACCIDENTS, VEHICLE OR DEPOT FIRE, OR MAJOR DAMAGE OR LEAKAGE OF PACKAGING) INVOLVING RADIOACTIVE MATERIALS INSTRUCTIONS TO CARRIER

1. Radioactive Potential Health Hazards: The degree of hazard to persons exposured to radioactive material will vary depending upon the type, quantity, and form of the material. The hazard may be from internal radiation caused by breathing gases, vapors, or dust from airborne materials, or from contamination of skin, open cuts and sores; or from external radiation (as from gamma rays) due to contamination on the skin or from exposure or unshielded radio-active material. Excessive exposure may be a hazard to health or life in extreme instances.

2. Immediate Action if an Incident Occurs /

a. Request radiological monitoring assistance from the nearest regional of fice of E.R.D. A. Interagency Radiological Assis-tance Plan (see attached sheet).

b. As soon as possible, obtain a copy of the shipping papers, load manifest, bill of lading, etc. Information contained on these forms will be especially valuable to persons and organi-zations rendering emergency assistance,

c. Identify and isolate the incident area.

d. Do not move any package unless neceesary for personnel rescue.

e. Keep unnecessary personnel away.

f. Avoid areas downwind from the incident area.

g. Delay cleanup until arrival of personnel qualified in radia-tion monitoring and decontamination,

h. Advise appropriate individuals and agencies of the incident (state and local police, fire department, ambulance and para-medic squads, truck dispatcher and shipper, as appropriate).

3. Spill or Leak: If a package appears to be damaged in a manner that will allow leakage or spillage 6f t yttantsp4 ke steps, as appropriate: j

                                            % dMM[lhffollecitigtk j h((g)[    ll ONLY                  _.

i OM1A: PAP-1309 5 Page: 69 Rev.: 0 Attachment 16 (Cont.)

a. Notify emergency assistance personnel (ambulance and fire crews, police, etc.) of the presence of possible radioactive contamination and avoid entry into the hazard area if at all practical until the arrival of persons qualified in radiation monitoring,

b. Notify the shipper (Cleveland Electric Illuminating Company -

(216) 259-3737). Request the person answering to relay this information immediately to the Shift Supervisor.

c. Avoid contact with all packages, particularly those that may be leaking or damaged.

7

d. Prevent the spread of loose material by diking, absorbent materials, covering, or other suitable means.

e. Limit necessary entries into the hazard areas in the ahortest possible duration.

1

f. Do not' enter the hazard area unless it is necessary to rescue persons or to retard the flow of material from massive spills or Jeaks.

g. Delay cleanup until the arrival of personnel qualified in radiation monitoring and decontamination.

                                                             ' -- u ~ L a t. - cm uvgg ONLY

OM1A: PAP-1309 Page: 70 - t,As7 Rev.: 0 Attachment 16 (Cont. ep 1

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                                        . .                                                                                                                       tNFORMATION e# 0 Y m *.ny DW/ PAP 23/E/ cap                                                                                                                    n                      -

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m ENCLOSURE E p TABLE 11.2-10 (Continued) Solids / Normal Stream Stream Normal Maximum Gallons / Batch Gal /Yr Isotopic Number Description Batches / Day Batches / Day Batch (Pounds) (Both Units) Activity (3) 24 Radioactive Chemical Waste - 1/36.5 15,360 N/A 154,000 SeeTable11.2-14!' Effluent Design Discharge (max) 25 Hot Shower and Detergent 3.0 3.0 500 - 547,000 Negligible Drains 27 Detergent Waste Effluent 1.48 2.65 1,600 - 864,000 Negligible w2 ( _ Radioac,tive Evap. Bottoms,' 1/51 1/14 5,000 - 36,000 See Tabl.e.-~11.4 .3, s ggy .- ~s 30 Floor Drains Demin. 1/30.5 1/22.35 1,455 1,970 17,000 Buildup on Spent Resins Transfer F.D. Demin.

   "A        31          Waste Demineralizar Spent     1/35           1/15.35         1,455     1,970         15,000   Buildup on Waste

Resins Transfer g Demineralizer 34-a Cond. Demin. Spent Resins 6/3.6 yrs 6/3.6 yrs 9,970 12,090 17,000 See Table 11.4-4 l

       ~
                 "                                                                                                     ~                - - ~

to,SRW' Disp ~6 sal](b{th~ units)

         -- 34-b W.D., F.D. and S.P.D.         1/83.5         1/31.6          9,980    11,700         44,000   S.e,_e_ Table.11.4-4 3      pggg g g                                                                                              . _ _ _ ,   _

Yh$ 35 Condensate Filter Backwash 1/3.0 8.0 5,200 360 1,265,000 See Note 5 (each unit) i w 4,0, Cond. Filter Sludge to 2/36.0 1/2 7,000 4,350 142,000 See Table 11.4-2(6)

                                                                                                                       '~~~~~~~~'""*
                        'SRW"DliE6331 ~ ~
                                 . ~ . ,

I y 43 Avg. CBST Decantate 1/1.5 8.0 4,610 N/A 1,122,000 S/6 5 c

m ^ e . TABLE 11.2-10 (Continued) Solids / Normal Stream Stream Normal Maximum Gallons / Batch Gal /Yr Isotopic Number Description Batches / Day Batches / Day Batch (Pounds) (Both Units) Activity (3) 45 RWCU F/D Backwash (each unit) 1/6.5 1.0 2,400 70 270,000 See Note 7 48 RWCU F 2/97.5 5/30 2,150 1,040 16,000 See Table 1.1.4-4 f8)

                 """"          DlIpT(DSludgetoSRW
                                               ~

al ** N H* *

                              <= m 51       Avg. RBST Decantate            1/3.25         1.0              2,300      N/A       258,000          M/4 53       Fuel Pool F/D Backwash         1/5.2          1/5.2            2,160       65       152,000     See Note 2 EugLPao.1,E/p Sludge to        1/348          1/30             7,000    4,350         7,000     See Table 11.4-2(9) d.L                            _
                                                                                                                                   ~- maw, SRW n_     Disposal
                                            ,y ,

65 Decantate from Fuel Pool 1/5.2 1/5.2 2,055 N/A 144,000 Negligible y y Filter Backwash jh 81 Cask Pit Draw-Down 1/20.3 - 47,000 N/A 845,000 Negligible 84 Suppression Pool - 1/10 yrs 1,000,000 N/A - Negligible Maintenance Drain (each unit) 86 Cond. Mixed Bed Demin. 6/3.6 yrs 6/3.6 yrs 4,950 5,750 16,000 See Note 4 Spent Resins Transfer (each unit) 87 Suppression Pool Cleanup 1/30 1/15 1,750 2,365 21,000 Buildup on Demin. Spent Resins Suppression Pool l,

.i                             Transfer                                                                                        Cleanup Demin.
 ?

AC x

TABLE 11.4-2 ( SOLID RADWASTE SYSTEM INFLUENT NUCLIDE ACTIVITIES Condensate D F/D Sludge (3) Radwaste((}ter Sludge Isotope pCi/cc pCi/cc Na-24 2.9-3 Negligible P-32 4.6-3 9.7-6 Cr-51 1.4-1 4.6-3 Mn-54 1.2-2 8.8-3 Co-58 1.4+0 3.7-1 Co-60 1.6-1 1.3-1 Fe-59 2.2-2 2.7-3 2n-65 6.2-4 4.0-4 Zn-69m 3.1-5 Negligible Ag-110m 1.8-2 1.2-2 Ag-110 1.8-2 1.2-2 W-187 2.0-2 Negligible TOTAL 1.8+0 5.5-1 1 NOTES:

1. Activity based on 4 days accumulation of 8 batches followed by a 2 day decay period.

2. Activity based on 100 days accumulation of 149 batches of filter sludge from the waste collector and floor drain systems followed by a 100 day decay period.

( 11.4-23

TABLE 11.4-3 { SOLID RADWASTE SYSTEM CHEMICAL WASTE CONCENTRATE Chemical Waste Chemical Waste ? Concentrate Concentrate Isotope (pCi/cc) Isotope (pCi/cc) P-32 4.0 - 6 Te-132 7.5 - 5 Cr-51 3.1 - 4 I-132 7.7 - 5 Mn-54 7.7 - 5 Cs-137 7.3 - 2 Co-58 6.7 - 3 Ba-137m 7.3 - 2 Co-60 1.1 - 3 Ba-140 4.2 - 2 Fe-59 8.0 - 5 La-140 4.8 - 2 Zn-65 3.8 - 6 Pr-143 2.1 - 4 I-131 1.6 - 1 Ce-144 8.4 - 3 Sr-89 2.8 - 1 Pr-144 8.4 - 3 ( Cs-134 4.5 - 2 Nd-147 3.5 - 5 Cs-136 5.8 - 4 Pm-147 8.2 - 6 Sr-90 7.0 - 2 Np-239 1.2 - 5 Y-90 7.0 - 2 Pu-239 1.1 - 6 Mo-99 7.6 - 6 Y-91 2.6 - 3 Tc-99m 8.4 - 6 Zr-95 4.6 - 3 Ru-103 1.3 - 3 Nb-95m 9.8 - 5 Rh-103m 1.2 - 3 Nb-95 5.9 - 3 Ru-106 6.6 - 4 Te-129m 2.0 - 3 Rh-106 6.6 - 4 Ce-141 5.0 - 3 Ag-110m 1.2 - 4 Ag-110 1.2 - 4 Total 9.1 - 1 (

  \
       .                                11.4-24

TABLE 11.4-4 ( SOLID RADWASTE SYSTEM DEMINERALIZER ACTIVITIES RWCU Filter / Demineralizer Condensate Radwaste > Sludge Demineralizer Demineralizer Isotope (pCi/cc) (pCi/cc) (pCi/cc) P-32 2.1-2 -- Cr-51 3.5+0 -- -- Ma-54 2.1+0 -- -- Co-58 1.4+2 -- -- Co-60 3.lti Fe-59 1.3+0 -- -- Zn-65 1.0-1 -- -- Br-83 -- -- 6.5-4 Br-84 -- -- 1.2-4 ( I-131 8.7-1 6.6-7 2.9-1 I-134 -- -- 1.8-3 Sr-89 7.0+1 2.2-2 4.1-1 Tc-101 -- -- 2.2-4 Cs-134 1.1+1 1.8-2 5.3-2 Cs-136 1.0-1 3.2-7 4.1-3 Cs-138 -- -- 7.0-4 Ba-139 -- -- 2.5-3 Sr-90 1.7+1 3.2-2 8.1-2 Y-90 1.7+1 3.2-2 6.5-2 Sr-92 -- -- 6.0-3 Y-92 -- -- 9.2-3 Mo-99 2.3-5 -- 1.6-1 Tc-99m 2.5-5 -- 8.1-2 11.4-25 m

                                                                            ,saup -p---- ..wsa-u---ae-

a . ( TABLE 11.4-4 (Continued) RWCU Filter / Demineralizer Condensate Radwaste Sludge Demineralizer Demineralizer Isotope (pCi/cc) (pCi/ce) (pCi/cc) Ru-103 3.0-1 5.5-5 2.1-3 Rh-103m 2.9-1 5.3-5 1.1-3 Ru-106 1.6-1 2.3-4 7.6-4 Rh-106 1.6-1 2.3-4 6.0-4 Ag-110m 2.9+0 -- -- Ag-110 2.9+0 -- -- Te-132 5.2-4 -- 3.9-1 I-132 5.2-4 -- 2.3-2 I-135 -- -- 3.8-2 Cs-137 1.8+1 3.4-2 8.1-2 Ba-137m 1.8+1 3.4-2 6.5-2 Ba-140 6.6+0 - 1.2-5 3.2-1 La-140 7.7+0 1.4-5 6.5-2 Ba-142 -- -- 2.1-4 La-142 -- -- 7.6-4 Ce-143 -- -- 1.1-4 Pr-143 3.8-2 -- 1.5-3 Ce-144 2.1+0 2.9-3 9.7-3 Pr-144 2.1+0 2.9-3 7.6-3 Nd-147 5.6-3 -- 4.2-4 Pm-147 9.4-3 3.4-6 2.5-5 Np-239 1.3-5 -- 1.4+0 ( e 11.4-26

c- , TABLE 11.4-4 (Continued) RWCU Filter / Demineralizer Condensate Radwaste Sludge Demineralizer Demineralizer t Isotope (pCi/cc) ,__(pCi/cc) (pCi/cc) Pu-239 2.2-3 4.5-7 6.5-1

                -Br-85    --                            --

9.2-6 Sr-91 -- -- 3.8-2 Y-91m -- -- 3.6-3 Y-91 1.3+0 1.9-4 2.7-1 Zr-95 1.1+0 5.3-4 6.5-3 Nb-95m 2.4-2 1.1-5 8.7-5 Nb-95 1.9+0 9.8-4 8.1-3 Zr-97 -- -- 4.2-5 4 Nb-97m -- -- 3.0-6 Nb-97 -- -- 4.9-6 Te-129m 4.9-1 o.1-5 3.8-3 Te-129 -- -- 8.7-6 I-129 -- -- 4.8-6 I-133 -- -- 1.4-1 Ba-141 -- -- 3.5-4 La-141 -- -- 2.8-3 Ce-141 1.2+0 1.4-4 2.4+0 Totals 3.6+2 1.8-1 7.1+0 ( 11.4-27 l I - -}}

ML20133H799

Text

4.0 REFERENCES

1.0 DESCRIPTION

4.0 REFERENCES

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