ML19095B219

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W3H-IMC-2165-S-P-7

ML19095B219
Person / Time
Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
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Download: ML19095B219 (11)

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• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2165\\W3H-IMC-216 Report Generated On : 7/6/2017 9:39:15 AM Sample Title : W3H-IMC-2165-S-P-7 Sample Description :

Sample Identification : IMC-2165-S-P-7 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 3.443E+002 grams Sample Taken On : 5/1/2017 12:00:00 AM Acquisition Started : 5/15/2017 9:59:03 AM Live Time : 1800.0 seconds Real Time : 1800.6 seconds Dead Time : 0.03 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 9:39:15 AM Page 1

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Detector Name: 8566 Sample

Title:

W3H-IMC-2165-S-P-7 Peak Analysis Performed on: 7/6/2017 9:39:11 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 58-70 65.13 16.41 0.95 2.33E+002 113.10 1.56E+002 F 2 95-107 102.99 25.88 0.63 7.73E+001 52.07 9.75E+001 F 3 205-219 213.43 53.52 0.64 8.85E+001 60.59 1.18E+002 M 4 295-316 299.55 75.07 0.63 1.57E+002 30.13 2.15E+002 m 5 295-316 308.29 77.26 0.64 1.25E+002 26.77 2.21E+002 F 6 332-343 336.99 84.44 0.79 2.29E+002 30.67 1.74E+002 F 7 354-364 360.19 90.25 0.83 1.35E+002 25.04 1.28E+002 F 8 366-377 373.17 93.49 0.77 1.93E+002 94.88 1.42E+002 F 9 431-444 436.16 109.26 0.85 6.42E+001 20.09 1.45E+002 F 10 566-580 574.50 143.88 0.81 2.86E+002 97.98 1.37E+002 F 11 644-660 652.49 163.39 0.88 1.42E+002 79.60 1.38E+002 F 12 734-748 741.82 185.75 0.92 1.33E+003 68.48 9.56E+001 F 13 814-825 819.89 205.28 0.89 9.65E+001 21.71 6.45E+001 F 14 947-958 952.53 238.48 1.02 1.38E+002 25.50 7.35E+001 F 15 1174-1184 1178.94 295.13 0.87 5.34E+001 17.44 3.63E+001 F 16 1344-1356 1351.11 338.22 0.89 3.00E+001 13.19 2.34E+001 F 17 1401-1414 1405.90 351.93 1.08 6.93E+001 19.41 4.34E+001 F 18 2031-2047 2038.64 510.27 1.44 6.00E+001 63.57 4.39E+001 F 19 2321-2336 2328.57 582.82 1.58 4.88E+001 16.27 2.13E+001 F 20 2424-2439 2432.04 608.72 1.32 5.06E+001 42.49 2.00E+001 F 21 5822-5852 5836.28 1460.61 2.67 2.29E+002 30.57 8.61E+000 F 22 7044-7059 7051.96 1764.83 1.41 1.56E+001 8.88 1.60E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:39:15 AM Page 2

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Sample

Title:

W3H-IMC-2165-S-P-7 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.993 1460.82* 10.66 1.09840E+001 1.67125E+000 Pb-212 0.995 74.82* 10.28 9.94779E-001 2.33614E-001 77.11* 17.10 4.66845E-001 1.17793E-001 86.83 2.07 87.35 3.97 89.78* 1.46 5.46458E+000 1.21429E+000 115.18 0.60 238.63* 43.60 2.81723E-001 5.94129E-002 300.09 3.30 BI-214 0.349 76.86* 0.55 1.46478E+001 3.71926E+000 79.29 0.91 609.32* 45.49 2.59220E-001 2.18421E-001 665.45 1.53 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.11 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1583.20 0.70 1661.27 1.05 1729.59 2.88 1764.49* 15.30 6.18705E-001 3.53683E-001 1847.43 2.03 2118.51 1.16 2204.06 4.92 2447.70 1.55 PB-214 0.851 74.82* 5.80 1.76316E+000 4.43096E-001 77.11* 9.70 8.22995E-001 2.20478E-001 86.83 1.70 87.35 2.24 89.78* 0.82 9.72962E+000 2.32082E+000 241.99 7.25 258.76 0.53 295.22* 18.42 3.18975E-001 1.07958E-001 351.93* 35.60 2.57006E-001 7.51177E-002

Interference Corrected Activity Report 7/6/2017 9:39:15 AM Page 3 Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty PB-214 0.851 785.96 1.06 839.07 0.58 Ra-226 0.885 81.07 0.20 83.79* 0.32 4.28919E+001 7.94567E+000 186.21* 3.64 2.64422E+001 3.11343E+000 U-234 0.987 53.20* 0.12 7.16219E+001 5.02819E+001 120.90 0.04 U-235 0.997 89.96* 3.43 2.32599E+000 5.22188E-001 93.35* 5.54 2.03166E+000 1.02984E+000 104.82 0.69 105.60 1.31 108.58 0.50 109.19* 1.66 2.21343E+000 8.06552E-001 143.76* 10.96 1.60866E+000 5.75910E-001 163.36* 5.08 1.84485E+000 1.05275E+000 194.94 0.63 202.12 1.08 205.32* 5.02 1.50118E+000 3.72907E-001

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:39:15 AM Page 4

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Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.993 1.098399E+001 1.671250E+000 Pb-212 0.995 3.118678E-001 5.192620E-002 BI-214 0.349 3.564880E-001 1.856501E-001 PB-214 0.851 2.957199E-001 5.915300E-002 Ra-226 0.885 2.863168E+001 2.898828E+000 U-234 0.987 7.162192E+001 5.028191E+001 U-235 0.997 1.773950E+000 2.365470E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:39:15 AM Page 5

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Peak Locate Performed on: 7/6/2017 9:39:11 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 1 16.41 1.2924E-001 48.62 F 2 25.88 4.2946E-002 67.35 F 16 338.22 1.6694E-002 43.90 F 18 510.27 3.3346E-002 105.91 F 19 582.82 2.7108E-002 33.33 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 7/6/2017 9:39:15 AM Page 6

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W3H-IMC-2165-S-P-7 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 8.940E-001 8.94E-001 1.098E+001 3.821E-00 Pb-210 46.54 4.25 1.920E+000 1.92E+000 2.179E+000 9.181E-00 BI-212 727.33 6.67 1.750E+000 1.75E+000 -2.074E-001 8.189E-00 785.37 1.10 1.160E+001 1.237E+001 5.435E+00 1078.62 0.56 2.419E+001 -2.010E+000 1.115E+00 1620.50 1.47 8.129E+000 -4.729E+000 3.549E+00

+ Pb-212 74.82* 10.28 4.510E-001 9.68E-002 9.948E-001 2.169E-00 77.11* 17.10 2.688E-001 4.668E-001 1.294E-00 86.83 2.07 2.934E+000 1.281E+000 1.428E+00 87.35 3.97 1.343E+000 6.663E-001 6.513E-00 89.78* 1.46 2.641E+000 5.465E+000 1.266E+00 115.18 0.60 7.488E+000 -3.121E+000 3.613E+00 238.63* 43.60 9.679E-002 2.817E-001 4.562E-00 300.09 3.30 1.826E+000 -1.864E+000 8.673E-00

+ BI-214 76.86* 0.55 8.435E+000 1.29E-001 1.465E+001 4.059E+00 79.29 0.91 6.984E+000 -2.770E-001 3.398E+00 609.32* 45.49 1.289E-001 2.592E-001 5.753E-00 665.45 1.53 7.357E+000 4.363E+000 3.454E+00 768.36 4.89 2.359E+000 -3.699E-001 1.099E+00 806.18 1.26 8.813E+000 -1.273E+000 4.080E+00 934.06 3.11 4.058E+000 1.203E+000 1.877E+00 1120.29 14.92 1.166E+000 8.752E-001 5.463E-00 1155.21 1.63 9.448E+000 1.136E+000 4.377E+00 1238.11 5.83 3.036E+000 6.749E-001 1.415E+00 1280.98 1.43 9.876E+000 -2.707E+000 4.507E+00 1377.67 3.99 3.331E+000 1.598E+000 1.501E+00 1385.31 0.79 1.710E+001 4.107E+000 7.717E+00 1401.52 1.33 8.528E+000 -3.998E+000 3.762E+00 1407.99 2.39 5.177E+000 -6.323E-001 2.309E+00 1509.21 2.13 6.182E+000 2.841E+000 2.757E+00 1583.20 0.70 1.748E+001 -1.670E+001 7.686E+00 1661.27 1.05 8.688E+000 2.382E+000 3.603E+00 1729.59 2.88 4.525E+000 3.514E+000 1.983E+00 1764.49* 15.30 3.284E-001 6.187E-001 1.106E-00 1847.43 2.03 7.186E+000 1.125E+000 3.170E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 7.994E-001 1.35E-001 1.763E+000 3.845E-00 77.11* 9.70 4.739E-001 8.230E-001 2.280E-00 86.83 1.70 3.572E+000 1.560E+000 1.738E+00 87.35 2.24 2.381E+000 1.181E+000 1.154E+00

Nuclide MDA Report 7/6/2017 9:39:15 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78* 0.82 4.703E+000 1.35E-001 9.730E+000 2.254E+00 241.99 7.25 1.012E+000 -7.063E-001 4.890E-00 258.76 0.53 9.513E+000 6.066E+000 4.511E+00 295.22* 18.42 1.876E-001 3.190E-001 8.574E-00 351.93* 35.60 1.345E-001 2.570E-001 6.225E-00 785.96 1.06 1.192E+001 9.241E+000 5.578E+00 839.07 0.58 2.271E+001 6.888E+000 1.062E+00

+ Ra-226 81.07 0.20 2.675E+001 1.13E+000 -2.371E+000 1.295E+00 83.79* 0.32 1.461E+001 4.289E+001 7.051E+00 186.21* 3.64 1.135E+000 2.644E+001 5.405E-00 AC-228 89.96 1.90 2.694E+017 5.02E+016 2.402E+017 1.310E+01 93.35 3.10 1.697E+017 2.267E+017 8.261E+01 99.51 1.26 2.831E+017 -4.046E+015 1.361E+01 105.60 0.74 5.446E+017 2.502E+017 2.630E+01 129.07 2.42 1.635E+017 2.835E+016 7.882E+01 153.98 0.72 5.385E+017 2.112E+017 2.587E+01 209.25 3.89 1.196E+017 -3.073E+016 5.735E+01 214.85 0.76 5.297E+017 -2.354E+017 2.520E+01 270.24 3.46 1.355E+017 7.730E+014 6.428E+01 328.00 2.95 1.838E+017 9.574E+016 8.694E+01 338.32 11.27 5.016E+016 1.742E+016 2.373E+01 409.46 1.92 3.501E+017 1.222E+017 1.654E+01 463.00 4.40 1.582E+017 9.342E+016 7.428E+01 562.50 0.87 9.994E+017 5.479E+017 4.701E+01 674.75 2.10 4.111E+017 1.087E+017 1.909E+01 726.86 0.62 1.688E+018 1.581E+017 7.908E+01 755.32 1.00 1.071E+018 2.558E+017 5.014E+01 772.29 1.49 6.999E+017 -7.334E+016 3.264E+01 794.95 4.25 2.592E+017 -1.343E+015 1.211E+01 830.49 0.54 2.137E+018 -1.467E+017 9.992E+01 835.71 1.61 7.306E+017 3.637E+017 3.418E+01 840.38 0.91 1.291E+018 7.281E+017 6.036E+01 904.20 0.77 1.702E+018 -1.855E+018 7.986E+01 911.20 25.80 5.724E+016 6.516E+016 2.704E+01 964.77 4.99 2.848E+017 1.362E+017 1.338E+01 968.97 15.80 8.978E+016 3.398E+016 4.216E+01 1247.08 0.50 2.683E+018 -8.009E+017 1.234E+01 1459.14 0.83 4.232E+018 1.352E+019 2.042E+01 1495.91 0.86 1.115E+018 -1.943E+017 4.847E+01 1588.20 3.22 4.004E+017 2.744E+017 1.797E+01 1630.63 1.51 7.240E+017 9.261E+016 3.173E+01 TH-230 67.67 0.38 1.493E+001 1.49E+001 -3.621E+000 7.209E+00 PA-234 742.81 0.11 1.049E+002 1.63E+001 3.177E+001 4.889E+00 766.42 0.32 3.580E+001 -2.089E+001 1.666E+00 1001.03 0.84 1.633E+001 1.632E+001 7.571E+00 TH-234 63.29 3.70 1.653E+000 1.65E+000 2.409E-001 7.979E-00 92.38 2.13 3.068E+000 3.634E+000 1.497E+00 92.80 2.10 3.012E+000 3.570E+000 1.468E+00 112.81 0.21 2.124E+001 -3.644E-001 1.025E+00

+ U-234 53.20* 0.12 5.617E+001 5.62E+001 7.162E+001 2.699E+00 120.90 0.04 1.330E+002 -3.480E+001 6.428E+00

Nuclide MDA Report 7/6/2017 9:39:15 AM Page 8 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96* 3.43 1.124E+000 3.82E-001 2.326E+000 5.389E-00 93.35* 5.54 7.430E-001 2.032E+000 3.572E-00 104.82 0.69 6.736E+000 4.181E+000 3.255E+00 105.60 1.31 3.472E+000 1.595E+000 1.677E+00 108.58 0.50 1.000E+001 -9.162E-001 4.847E+00 109.19* 1.66 2.586E+000 2.213E+000 1.246E+00 143.76* 10.96 3.819E-001 1.609E+000 1.833E-00 163.36* 5.08 9.235E-001 1.845E+000 4.442E-00 194.94 0.63 7.250E+000 -3.744E+000 3.464E+00 202.12 1.08 5.445E+000 -9.638E-001 2.626E+00 205.32* 5.02 6.921E-001 1.501E+000 3.250E-00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 9:39:15 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2165\\W3H-IMC-216 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 1.10E+001 15.215 Pb-212 74.8 9.95E-001 23.484 3.531[31.563] 7.02 -1.244 77.1 4.67E-001 25.232 1.657[32.884] [ 0.319]

89.8 5.46E+000 22.221 19.397[30.635]

238.6 ^ 2.82E-001 21.089 1.000[29.825]

BI-214 76.9 1.46E+001 25.391 56.507[88.004] 8.74 -1.143 609.3 ^ 2.59E-001 84.261 1.000[119.16] [ 0.419]

1764.5 6.19E-001 57.165 2.387[101.82]

PB-214 74.8 1.76E+000 25.131 6.860[38.547] 8.53 -1.439 77.1 8.23E-001 26.790 3.202[39.648] [ 0.268]

89.8 9.73E+000 23.853 37.858[37.726]

295.2 3.19E-001 33.845 1.241[44.719]

351.9 ^ 2.57E-001 29.228 1.000[41.335]

Ra-226 83.8 4.29E+001 18.525 1.622[21.950] 3.17 -0.606 186.2 ^ 2.64E+001 11.774 1.000[16.652] [ 0.345]

U-234 53.2 ^ 7.16E+001 70.205 U-235 90.0 2.33E+000 22.450 1.446[42.257] 2.63 -0.508 93.3 2.03E+000 50.690 1.263[62.057] [ 0.644]

109.2 2.21E+000 36.439 1.376[51.083]

143.8 ^ 1.61E+000 35.801 1.000[50.630]

163.4 1.84E+000 57.064 1.147[67.365]

205.3 1.50E+000 24.841 0.933[43.575]