ML19095B216

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W3H-IMC-2165-S-P-6

ML19095B216
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Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
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• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2165\\W3H-IMC-216 Report Generated On : 7/6/2017 9:38:24 AM Sample Title : W3H-IMC-2165-S-P-6 Sample Description :

Sample Identification : IMC-2165-S-P-6 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 2.667E+002 grams Sample Taken On : 5/1/2017 12:00:00 AM Acquisition Started : 5/15/2017 9:11:06 AM Live Time : 1800.0 seconds Real Time : 1800.6 seconds Dead Time : 0.03 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 9:38:24 AM Page 1

• • • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W3H-IMC-2165-S-P-6 Peak Analysis Performed on: 7/6/2017 9:38:18 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 203-217 213.59 53.56 0.66 1.40E+002 62.06 1.18E+002 M 2 295-314 299.65 75.10 0.59 2.02E+002 33.92 2.31E+002 m 3 295-314 308.51 77.31 0.60 5.48E+001 21.01 1.95E+002 F 4 332-344 337.18 84.49 0.83 3.77E+002 37.10 1.95E+002 F 5 355-365 359.82 90.15 0.70 1.28E+002 22.06 1.80E+002 F 6 365-379 373.55 93.59 0.58 2.26E+002 78.18 2.23E+002 F 7 427-443 435.80 109.17 0.94 9.82E+001 79.27 1.87E+002 F 8 478-491 483.67 121.15 0.65 6.57E+001 71.26 1.33E+002 F 9 569-584 574.45 143.86 0.79 5.10E+002 44.42 1.60E+002 F 10 645-660 652.44 163.38 0.79 2.13E+002 82.35 1.16E+002 F 11 735-750 741.84 185.75 0.91 2.28E+003 88.93 1.12E+002 F 12 812-828 819.93 205.29 0.87 1.58E+002 26.40 9.99E+001 F 13 945-958 953.03 238.60 0.90 7.82E+001 64.44 6.48E+001 F 14 1171-1184 1178.55 295.04 0.93 3.95E+001 15.67 4.34E+001 F 15 1398-1411 1405.60 351.85 0.75 6.41E+001 47.66 3.22E+001 F 16 2322-2335 2328.26 582.75 1.12 3.57E+001 14.39 1.87E+001 F 17 2425-2441 2432.29 608.78 1.29 6.16E+001 17.33 1.84E+001 F 18 5824-5849 5835.69 1460.46 2.60 1.44E+002 24.21 5.78E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:38:24 AM Page 2

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Sample

Title:

W3H-IMC-2165-S-P-6 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.979 1460.82* 10.66 8.93566E+000 1.63494E+000 Pb-212 0.997 74.82* 10.28 1.65552E+000 3.56428E-001 77.11* 17.10 2.64328E-001 1.07269E-001 86.83 2.07 87.35 3.97 89.78* 1.46 6.65594E+000 1.41222E+000 115.18 0.60 238.63* 43.60 2.06637E-001 1.71558E-001 300.09 3.30 BI-214 0.306 76.86* 0.55 8.29361E+000 3.37392E+000 79.29 0.91 609.32* 45.49 4.07297E-001 1.18647E-001 665.45 1.53 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.11 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1583.20 0.70 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 2204.06 4.92 2447.70 1.55 PB-214 0.850 74.82* 5.80 2.93427E+000 6.84122E-001 77.11* 9.70 4.65981E-001 1.93700E-001 86.83 1.70 87.35 2.24 89.78* 0.82 1.18508E+001 2.71632E+000 241.99 7.25 258.76 0.53 295.22* 18.42 3.03964E-001 1.23806E-001 351.93* 35.60 3.06709E-001 2.29533E-001

Interference Corrected Activity Report 7/6/2017 9:38:24 AM Page 3 Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty PB-214 0.850 785.96 1.06 839.07 0.58 Ra-226 0.885 81.07 0.20 83.79* 0.32 9.12255E+001 1.47116E+001 186.21* 3.64 5.82226E+001 6.57607E+000 U-234 0.982 53.20* 0.12 1.46556E+002 6.86527E+001 120.90* 0.04 1.40583E+002 1.58159E+002 U-235 0.997 89.96* 3.43 2.83309E+000 6.07899E-001 93.35* 5.54 3.07302E+000 1.12828E+000 104.82 0.69 105.60 1.31 108.58 0.50 109.19* 1.66 4.37510E+000 3.62336E+000 143.76* 10.96 3.69662E+000 5.05176E-001 163.36* 5.08 3.57363E+000 1.43253E+000 194.94 0.63 202.12 1.08 205.32* 5.02 3.17931E+000 6.27043E-001

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:38:24 AM Page 4

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Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.979 8.935661E+000 1.634937E+000 Pb-212 0.997 1.969597E-001 9.779034E-002 BI-214 0.306 4.026865E-001 1.185905E-001 PB-214 0.850 3.020279E-001 1.040804E-001 Ra-226 0.885 6.371867E+001 6.003581E+000 U-234 0.982 1.456092E+002 6.297571E+001 U-235 0.997 3.258178E+000 3.034286E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

• • • • • • • • • • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 9:38:18 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 16 582.75 1.9826E-002 40.33 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 7/6/2017 9:38:24 AM Page 5

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W3H-IMC-2165-S-P-6 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 9.333E-001 9.33E-001 8.936E+000 3.828E-00 Pb-210 46.54 4.25 2.599E+000 2.60E+000 1.197E+000 1.245E+00 BI-212 727.33 6.67 2.138E+000 2.14E+000 2.410E-001 9.967E-00 785.37 1.10 1.307E+001 -3.333E+000 6.063E+00 1078.62 0.56 2.763E+001 -1.573E+001 1.260E+00 1620.50 1.47 9.903E+000 -9.846E-002 4.285E+00

+ Pb-212 74.82* 10.28 6.021E-001 1.23E-001 1.656E+000 2.900E-00 77.11* 17.10 3.262E-001 2.643E-001 1.566E-00 86.83 2.07 4.205E+000 2.176E+000 2.052E+00 87.35 3.97 1.826E+000 1.132E+000 8.868E-00 89.78* 1.46 4.010E+000 6.656E+000 1.935E+00 115.18 0.60 1.007E+001 2.700E-001 4.868E+00 238.63* 43.60 1.232E-001 2.066E-001 5.801E-00 300.09 3.30 2.071E+000 -1.741E+000 9.763E-00

+ BI-214 76.86* 0.55 1.024E+001 1.63E-001 8.294E+000 4.913E+00 79.29 0.91 8.167E+000 3.725E-001 3.962E+00 609.32* 45.49 1.630E-001 4.073E-001 7.254E-00 665.45 1.53 7.770E+000 -1.806E+000 3.595E+00 768.36 4.89 3.068E+000 1.592E-001 1.430E+00 806.18 1.26 1.295E+001 -2.022E+000 6.054E+00 934.06 3.11 4.950E+000 -3.070E-001 2.280E+00 1120.29 14.92 1.376E+000 5.374E-001 6.403E-00 1155.21 1.63 1.220E+001 5.248E+000 5.651E+00 1238.11 5.83 3.591E+000 1.338E+000 1.663E+00 1280.98 1.43 1.275E+001 2.262E+000 5.819E+00 1377.67 3.99 4.696E+000 2.422E+000 2.135E+00 1385.31 0.79 1.870E+001 -2.258E+001 8.274E+00 1401.52 1.33 1.198E+001 -8.594E+000 5.343E+00 1407.99 2.39 6.812E+000 -3.532E+000 3.045E+00 1509.21 2.13 8.992E+000 5.901E+000 4.064E+00 1583.20 0.70 2.515E+001 1.123E+001 1.122E+00 1661.27 1.05 1.282E+001 -7.705E+000 5.454E+00 1729.59 2.88 5.023E+000 1.254E+000 2.151E+00 1764.49 15.30 1.566E+000 1.094E+000 7.138E-00 1847.43 2.03 7.596E+000 -1.372E+000 3.252E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 1.067E+000 1.51E-001 2.934E+000 5.139E-00 77.11* 9.70 5.751E-001 4.660E-001 2.760E-00 86.83 1.70 5.120E+000 2.650E+000 2.499E+00 87.35 2.24 3.237E+000 2.006E+000 1.572E+00

Nuclide MDA Report 7/6/2017 9:38:24 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78* 0.82 7.140E+000 1.51E-001 1.185E+001 3.445E+00 241.99 7.25 1.167E+000 -2.757E-001 5.619E-00 258.76 0.53 1.170E+001 -4.923E+000 5.535E+00 295.22* 18.42 2.795E-001 3.040E-001 1.293E-00 351.93* 35.60 1.514E-001 3.067E-001 6.921E-00 785.96 1.06 1.360E+001 -8.281E-001 6.307E+00 839.07 0.58 2.467E+001 -6.495E+000 1.139E+00

+ Ra-226 81.07 0.20 3.404E+001 1.61E+000 -6.121E-001 1.647E+00 83.79* 0.32 2.045E+001 9.123E+001 9.898E+00 186.21* 3.64 1.612E+000 5.822E+001 7.714E-00 AC-228 89.96 1.90 3.375E+017 5.17E+016 4.165E+017 1.644E+01 93.35 3.10 2.141E+017 -3.175E+017 1.044E+01 99.51 1.26 3.401E+017 -3.342E+017 1.636E+01 105.60 0.74 7.188E+017 5.163E+017 3.485E+01 129.07 2.42 1.879E+017 4.428E+016 9.050E+01 153.98 0.72 6.458E+017 1.984E+017 3.104E+01 209.25 3.89 1.407E+017 2.746E+016 6.748E+01 214.85 0.76 5.874E+017 -3.350E+017 2.786E+01 270.24 3.46 1.511E+017 1.794E+016 7.142E+01 328.00 2.95 2.088E+017 1.086E+017 9.851E+01 338.32 11.27 5.672E+016 2.232E+016 2.677E+01 409.46 1.92 3.887E+017 1.416E+017 1.829E+01 463.00 4.40 1.930E+017 7.812E+016 9.082E+01 562.50 0.87 1.166E+018 4.977E+017 5.480E+01 674.75 2.10 5.119E+017 8.882E+016 2.386E+01 726.86 0.62 1.875E+018 4.196E+017 8.743E+01 755.32 1.00 1.179E+018 -1.070E+017 5.489E+01 772.29 1.49 8.138E+017 1.716E+017 3.791E+01 794.95 4.25 2.704E+017 9.558E+016 1.252E+01 830.49 0.54 2.096E+018 -2.423E+017 9.660E+01 835.71 1.61 7.538E+017 2.101E+017 3.493E+01 840.38 0.91 1.317E+018 3.010E+017 6.095E+01 904.20 0.77 1.818E+018 -7.141E+017 8.468E+01 911.20 25.80 5.171E+016 -9.449E+015 2.399E+01 964.77 4.99 2.489E+017 2.857E+016 1.143E+01 968.97 15.80 8.459E+016 4.262E+016 3.908E+01 1247.08 0.50 3.559E+018 1.738E+018 1.653E+01 1459.14 0.83 4.031E+018 9.484E+018 1.929E+01 1495.91 0.86 1.195E+018 5.289E+016 5.114E+01 1588.20 3.22 4.202E+017 -2.065E+017 1.859E+01 1630.63 1.51 7.849E+017 -1.463E+017 3.397E+01 TH-230 67.67 0.38 1.948E+001 1.95E+001 -4.756E+000 9.410E+00 PA-234 742.81 0.11 1.324E+002 2.09E+001 4.321E+001 6.159E+00 766.42 0.32 4.691E+001 2.282E+001 2.185E+00 1001.03 0.84 2.090E+001 1.646E+001 9.685E+00 TH-234 63.29 3.70 2.071E+000 2.07E+000 1.506E+000 9.989E-00 92.38 2.13 4.330E+000 1.406E+001 2.117E+00 92.80 2.10 4.190E+000 4.327E+000 2.046E+00 112.81 0.21 2.732E+001 -4.939E+000 1.318E+00

+ U-234 53.20* 0.12 7.242E+001 7.24E+001 1.466E+002 3.480E+00 120.90* 0.04 1.405E+002 1.406E+002 6.733E+00

Nuclide MDA Report 7/6/2017 9:38:24 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96* 3.43 1.707E+000 5.42E-001 2.833E+000 8.235E-00 93.35* 5.54 1.284E+000 3.073E+000 6.234E-00 104.82 0.69 9.498E+000 1.180E+001 4.603E+00 105.60 1.31 5.015E+000 3.602E+000 2.431E+00 108.58 0.50 1.386E+001 -2.316E+000 6.731E+00 109.19* 1.66 4.044E+000 4.375E+000 1.962E+00 143.76* 10.96 5.424E-001 3.697E+000 2.614E-00 163.36* 5.08 1.075E+000 3.574E+000 5.148E-00 194.94 0.63 8.460E+000 4.469E+000 4.023E+00 202.12 1.08 7.884E+000 5.829E+000 3.817E+00 205.32* 5.02 1.222E+000 3.179E+000 5.837E-00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 9:38:25 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2165\\W3H-IMC-216 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 8.94E+000 18.297 Pb-212 74.8 1.66E+000 21.530 8.012[85.770] 8.04 -1.391 77.1 2.64E-001 40.582 1.279[92.411] [ 1.156]

89.8 6.66E+000 21.217 32.211[85.692]

238.6 ^ 2.07E-001 83.024 1.000[117.41]

BI-214 76.9 8.29E+000 40.681 20.363[50.035] 9.33 -1.456 609.3 ^ 4.07E-001 29.130 1.000[41.196] [ 0.313]

PB-214 74.8 2.93E+000 23.315 9.567[78.385] 8.58 -1.468 77.1 4.66E-001 41.568 1.519[85.607] [ 0.587]

89.8 1.19E+001 22.921 38.639[78.269]

295.2 3.04E-001 40.730 0.991[85.203]

351.9 ^ 3.07E-001 74.837 1.000[105.83]

Ra-226 83.8 9.12E+001 16.127 1.567[19.689] 2.94 -0.562 186.2 ^ 5.82E+001 11.295 1.000[15.973] [ 0.317]

U-234 53.2 ^ 1.47E+002 46.844 1.000[66.247] 0.20 -0.051 120.9 1.41E+002 112.50 0.959[121.86] [ 1.690]

U-235 90.0 2.83E+000 21.457 0.766[25.439] -0.86 0.152 93.3 3.07E+000 36.716 0.831[39.176] [ 0.382]

109.2 4.38E+000 82.818 1.184[83.938]

143.8 ^ 3.70E+000 13.666 1.000[19.326]

163.4 3.57E+000 40.086 0.967[42.352]

205.3 3.18E+000 19.723 0.860[23.995]