ML19095B205

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W3H-IMC-2165-S-P-3

ML19095B205
Person / Time
Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
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• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2165\\W3H-IMC-216 Report Generated On : 7/6/2017 9:36:40 AM Sample Title : W3H-IMC-2165-S-P-3 Sample Description :

Sample Identification : IMC-2165-S-P-3 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 3.235E+002 grams Sample Taken On : 5/1/2017 12:00:00 AM Acquisition Started : 5/12/2017 10:13:28 AM Live Time : 1800.0 seconds Real Time : 1800.5 seconds Dead Time : 0.03 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 9:36:40 AM Page 1

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Detector Name: 8566 Sample

Title:

W3H-IMC-2165-S-P-3 Peak Analysis Performed on: 7/6/2017 9:36:36 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 98-110 103.11 25.91 0.54 4.58E+001 56.60 9.75E+001 F 2 177-194 186.71 46.83 0.57 8.04E+001 52.18 1.23E+002 F 3 209-219 212.74 53.35 0.51 4.89E+001 17.97 8.25E+001 M 4 295-315 299.44 75.04 0.60 1.52E+002 30.74 2.27E+002 m 5 295-315 308.16 77.23 0.61 9.82E+001 24.68 1.95E+002 F 6 331-343 337.70 84.62 0.84 2.09E+002 29.19 1.60E+002 F 7 355-363 359.02 89.95 0.58 7.84E+001 22.48 1.13E+002 F 8 365-382 373.59 93.60 0.62 1.60E+002 134.56 1.92E+002 F 9 431-441 436.59 109.36 0.22 4.77E+001 72.82 8.98E+001 F 10 568-579 574.42 143.86 0.73 2.06E+002 29.51 1.11E+002 F 11 645-659 652.40 163.37 0.76 1.13E+002 73.66 1.09E+002 F 12 734-749 741.68 185.71 0.93 9.62E+002 58.43 9.40E+001 F 13 813-826 819.66 205.23 0.95 8.85E+001 20.41 6.30E+001 F 14 948-960 952.72 238.52 0.85 1.76E+002 28.44 8.13E+001 F 15 1175-1186 1179.18 295.20 1.08 4.56E+001 16.47 3.60E+001 F 16 1399-1412 1404.75 351.64 1.13 7.11E+001 18.65 3.08E+001 F 17 2322-2337 2328.61 582.83 1.39 4.58E+001 55.35 2.67E+001 F 18 2425-2441 2432.48 608.83 1.57 5.11E+001 17.51 3.12E+001 F 19 3630- 3647 3639.21 910.80 1.85 4.95E+001 47.77 1.29E+001 F 20 5822-5848 5834.99 1460.29 2.74 2.05E+002 28.78 4.50E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:36:40 AM Page 2

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Sample

Title:

W3H-IMC-2165-S-P-3 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.955 1460.82* 10.66 1.04640E+001 1.65567E+000 Pb-210 0.986 46.54* 4.25 2.60708E+000 1.79746E+000 Pb-212 0.997 74.82* 10.28 1.02894E+000 2.49822E-001 77.11* 17.10 3.90801E-001 1.11124E-001 86.83 2.07 87.35 3.97 89.78* 1.46 3.37372E+000 1.05252E+000 115.18 0.60 238.63* 43.60 3.84380E-001 7.30849E-002 300.09 3.30 BI-214 0.208 76.86* 0.55 1.22618E+001 3.50403E+000 79.29 0.91 609.32* 45.49 2.78380E-001 9.77161E-002 665.45 1.53 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.11 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1583.20 0.70 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 2204.06 4.92 2447.70 1.55 PB-214 0.847 74.82* 5.80 1.82371E+000 4.71898E-001 77.11* 9.70 6.88938E-001 2.05484E-001 86.83 1.70 87.35 2.24 89.78* 0.82 6.00687E+000 1.94503E+000 241.99 7.25 258.76 0.53 295.22* 18.42 2.89808E-001 1.07855E-001

Interference Corrected Activity Report 7/6/2017 9:36:40 AM Page 3 Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty PB-214 0.847 351.93* 35.60 2.80415E-001 7.72292E-002 785.96 1.06 839.07 0.58 Ra-226 0.877 81.07 0.20 83.79* 0.32 4.16780E+001 7.88701E+000 186.21* 3.64 2.02752E+001 2.47686E+000 U-234 0.997 53.20* 0.12 4.23152E+001 1.69270E+001 120.90 0.04 U-235 0.998 89.96* 3.43 1.43603E+000 4.50352E-001 93.35* 5.54 1.79374E+000 1.52281E+000 104.82 0.69 105.60 1.31 108.58 0.50 109.19* 1.66 1.75116E+000 2.69391E+000 143.76* 10.96 1.23278E+000 2.19033E-001 163.36* 5.08 1.56166E+000 1.03211E+000 194.94 0.63 202.12 1.08 205.32* 5.02 1.46460E+000 3.71362E-001

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:36:40 AM Page 4

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Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.955 1.046396E+001 1.655672E+000 Pb-210 0.986 2.607084E+000 1.797462E+000 Pb-212 0.997 3.663189E-001 5.986343E-002 BI-214 0.208 2.748203E-001 9.767081E-002 PB-214 0.847 2.758325E-001 6.032641E-002 Ra-226 0.877 2.219656E+001 2.363071E+000 U-234 0.997 4.231519E+001 1.692701E+001 U-235 0.998 1.296065E+000 1.686934E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:36:40 AM Page 5

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Peak Locate Performed on: 7/6/2017 9:36:36 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 1 25.91 2.5420E-002 123.69 F 17 582.83 2.5418E-002 120.98 F 19 910.80 2.7519E-002 96.43 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 7/6/2017 9:36:40 AM Page 6

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W3H-IMC-2165-S-P-3 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 7.015E-001 7.01E-001 1.046E+001 2.817E-00

+ Pb-210 46.54* 4.25 2.455E+000 2.45E+000 2.607E+000 1.183E+00 BI-212 727.33 6.67 1.750E+000 1.75E+000 -6.181E-001 8.152E-00 785.37 1.10 1.187E+001 3.076E+000 5.548E+00 1078.62 0.56 2.497E+001 3.580E+000 1.148E+00 1620.50 1.47 9.110E+000 1.542E+000 4.006E+00

+ Pb-212 74.82* 10.28 4.923E-001 1.11E-001 1.029E+000 2.370E-00 77.11* 17.10 2.695E-001 3.908E-001 1.294E-00 86.83 2.07 3.002E+000 1.159E+000 1.459E+00 87.35 3.97 1.364E+000 6.025E-001 6.605E-00 89.78* 1.46 2.489E+000 3.374E+000 1.186E+00 115.18 0.60 7.003E+000 6.506E-001 3.363E+00 238.63* 43.60 1.105E-001 3.844E-001 5.232E-00 300.09 3.30 1.974E+000 2.561E-001 9.382E-00

+ BI-214 76.86* 0.55 8.457E+000 1.70E-001 1.226E+001 4.059E+00 79.29 0.91 6.840E+000 -1.081E+000 3.320E+00 609.32* 45.49 1.704E-001 2.784E-001 7.781E-00 665.45 1.53 7.549E+000 -1.754E+000 3.536E+00 768.36 4.89 2.741E+000 8.914E-001 1.285E+00 806.18 1.26 8.517E+000 2.619E+000 3.912E+00 934.06 3.11 4.395E+000 1.109E+000 2.036E+00 1120.29 14.92 1.143E+000 3.613E-001 5.322E-00 1155.21 1.63 1.080E+001 5.740E+000 5.032E+00 1238.11 5.83 2.659E+000 2.125E-001 1.220E+00 1280.98 1.43 1.161E+001 4.915E+000 5.349E+00 1377.67 3.99 3.369E+000 1.795E+000 1.509E+00 1385.31 0.79 1.733E+001 -9.798E+000 7.777E+00 1401.52 1.33 1.025E+001 2.523E+000 4.593E+00 1407.99 2.39 5.616E+000 3.646E+000 2.510E+00 1509.21 2.13 4.950E+000 1.139E+000 2.119E+00 1583.20 0.70 1.991E+001 -5.479E+000 8.836E+00 1661.27 1.05 1.208E+001 2.360E+000 5.251E+00 1729.59 2.88 5.173E+000 3.850E-001 2.289E+00 1764.49 15.30 1.055E+000 6.619E-001 4.704E-00 1847.43 2.03 6.896E+000 -1.331E-001 2.998E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 8.725E-001 1.22E-001 1.824E+000 4.200E-00 77.11* 9.70 4.751E-001 6.889E-001 2.281E-00 86.83 1.70 3.655E+000 1.411E+000 1.777E+00 87.35 2.24 2.418E+000 1.068E+000 1.171E+00

Nuclide MDA Report 7/6/2017 9:36:40 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78* 0.82 4.432E+000 1.22E-001 6.007E+000 2.112E+00 241.99 7.25 1.166E+000 1.908E-001 5.652E-00 258.76 0.53 9.782E+000 4.909E+000 4.629E+00 295.22* 18.42 2.033E-001 2.898E-001 9.303E-00 351.93* 35.60 1.222E-001 2.804E-001 5.577E-00 785.96 1.06 1.235E+001 4.288E+000 5.772E+00 839.07 0.58 2.053E+001 -1.108E+001 9.485E+00

+ Ra-226 81.07 0.20 2.556E+001 1.22E+000 5.719E+000 1.232E+00 83.79* 0.32 1.533E+001 4.168E+001 7.394E+00 186.21* 3.64 1.222E+000 2.028E+001 5.825E-00 AC-228 89.96 1.90 8.381E+013 1.85E+013 1.559E+013 4.069E+01 93.35 3.10 5.194E+013 -2.643E+013 2.523E+01 99.51 1.26 8.978E+013 -1.853E+013 4.310E+01 105.60 0.74 1.677E+014 -2.242E+013 8.080E+01 129.07 2.42 4.965E+013 1.298E+013 2.387E+01 153.98 0.72 1.790E+014 1.349E+014 8.604E+01 209.25 3.89 3.746E+013 2.882E+012 1.793E+01 214.85 0.76 1.628E+014 -3.676E+013 7.722E+01 270.24 3.46 4.469E+013 1.500E+013 2.120E+01 328.00 2.95 5.929E+013 1.505E+013 2.801E+01 338.32 11.27 1.956E+013 2.898E+013 9.338E+01 409.46 1.92 9.663E+013 -5.748E+013 4.515E+01 463.00 4.40 5.261E+013 -6.506E+013 2.474E+01 562.50 0.87 2.903E+014 -6.450E+013 1.355E+01 674.75 2.10 1.333E+014 -3.807E+012 6.186E+01 726.86 0.62 5.234E+014 -9.691E+013 2.442E+01 755.32 1.00 3.268E+014 5.933E+011 1.521E+01 772.29 1.49 2.478E+014 1.687E+014 1.162E+01 794.95 4.25 7.496E+013 1.903E+013 3.471E+01 830.49 0.54 6.033E+014 6.116E+013 2.789E+01 835.71 1.61 2.125E+014 6.958E+013 9.859E+01 840.38 0.91 3.586E+014 -8.344E+013 1.657E+01 904.20 0.77 5.634E+014 -6.383E+014 2.645E+01 911.20 25.80 1.854E+013 2.054E+013 8.752E+01 964.77 4.99 9.525E+013 6.024E+013 4.481E+01 968.97 15.80 3.069E+013 3.750E+013 1.445E+01 1247.08 0.50 7.613E+014 -6.305E+013 3.457E+01 1459.14 0.83 1.310E+015 3.655E+015 6.306E+01 1495.91 0.86 3.191E+014 -1.339E+014 1.357E+01 1588.20 3.22 1.309E+014 7.018E+013 5.876E+01 1630.63 1.51 2.036E+014 -2.380E+013 8.717E+01 TH-230 67.67 0.38 1.557E+001 1.56E+001 7.943E+000 7.514E+00 PA-234 742.81 0.11 1.092E+002 1.72E+001 -1.570E+001 5.078E+00 766.42 0.32 4.116E+001 -1.150E+001 1.926E+00 1001.03 0.84 1.723E+001 2.627E-001 7.985E+00 TH-234 63.29 3.70 1.765E+000 1.77E+000 1.007E+000 8.524E-00 92.38 2.13 3.089E+000 7.876E+000 1.505E+00 92.80 2.10 2.943E+000 3.552E-001 1.431E+00 112.81 0.21 1.944E+001 5.914E+000 9.327E+00

+ U-234 53.20* 0.12 4.590E+001 4.59E+001 4.232E+001 2.178E+00 120.90 0.04 1.284E+002 5.556E+001 6.182E+00

Nuclide MDA Report 7/6/2017 9:36:40 AM Page 8 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96* 3.43 1.060E+000 3.44E-001 1.436E+000 5.050E-00 93.35* 5.54 1.051E+000 1.794E+000 5.104E-00 104.82 0.69 6.892E+000 8.973E+000 3.325E+00 105.60 1.31 3.479E+000 -4.652E-001 1.677E+00 108.58 0.50 9.421E+000 4.875E-001 4.546E+00 109.19* 1.66 2.027E+000 1.751E+000 9.637E-00 143.76* 10.96 3.439E-001 1.233E+000 1.638E-00 163.36* 5.08 8.420E-001 1.562E+000 4.023E-00 194.94 0.63 7.550E+000 -1.660E+000 3.604E+00 202.12 1.08 5.413E+000 1.292E+000 2.604E+00 205.32* 5.02 7.617E-001 1.465E+000 3.584E-00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 9:36:41 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2165\\W3H-IMC-216 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 1.05E+001 15.823 Pb-210 46.5 ^ 2.61E+000 68.945 Pb-212 74.8 1.03E+000 24.280 2.677[30.839] 4.39 -0.785 77.1 3.91E-001 28.435 1.017[34.206] [ 0.300]

89.8 3.37E+000 31.197 8.777[36.535]

238.6 ^ 3.84E-001 19.014 1.000[26.889]

BI-214 76.9 1.23E+001 28.577 44.047[45.263] 11.72 -1.828 609.3 ^ 2.78E-001 35.102 1.000[49.641] [ 0.324]

PB-214 74.8 1.82E+000 25.876 6.504[37.790] 7.36 -1.256 77.1 6.89E-001 29.826 2.457[40.597] [ 0.266]

89.8 6.01E+000 32.380 21.421[42.509]

295.2 2.90E-001 37.216 1.033[46.298]

351.9 ^ 2.80E-001 27.541 1.000[38.949]

Ra-226 83.8 4.17E+001 18.924 2.056[22.524] 4.72 -0.902 186.2 ^ 2.03E+001 12.216 1.000[17.276] [ 0.355]

U-234 53.2 ^ 4.23E+001 40.002 U-235 90.0 1.44E+000 31.361 1.165[36.044] 0.21 -0.020 93.3 1.79E+000 84.896 1.455[86.735] [ 0.548]

109.2 1.75E+000 153.83 1.420[154.85]

143.8 ^ 1.23E+000 17.767 1.000[25.127]

163.4 1.56E+000 66.091 1.267[68.437]

205.3 1.46E+000 25.356 1.188[30.961]