ML19095B192

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W3H-IMC-000312-S-P-8

ML19095B192
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Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
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• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0312\\W3H-IMC-000 Report Generated On : 7/6/2017 9:32:57 AM Sample Title : W3H-IMC-0312-S-P-8 Sample Description :

Sample Identification : IMC-0312-S-P-8 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 4.272E+002 grams Sample Taken On : 4/18/2017 12:00:00 AM Acquisition Started : 5/4/2017 7:21:36 AM Live Time : 1800.0 seconds Real Time : 1800.6 seconds Dead Time : 0.03 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 9:32:57 AM Page 1

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Detector Name: 8566 Sample

Title:

W3H-IMC-0312-S-P-8 Peak Analysis Performed on: 7/6/2017 9:32:51 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 59-71 65.32 16.46 0.78 4.18E+002 115.86 1.95E+002 F 2 72-85 76.90 19.36 0.89 1.51E+002 101.79 1.54E+002 F 3 98-109 102.95 25.87 0.53 8.18E+001 22.63 1.44E+002 F 4 209-219 213.27 53.48 0.68 1.73E+002 26.47 1.19E+002 M 5 282-313 291.26 73.00 0.84 1.75E+002 70.56 2.67E+002 m 6 282-313 299.50 75.06 0.85 3.32E+002 121.22 2.73E+002 m 7 282-313 308.74 77.37 0.86 1.02E+002 45.06 2.80E+002 F 8 331-344 336.99 84.44 0.83 4.06E+002 40.38 2.73E+002 F 9 355-365 359.76 90.14 0.66 1.60E+002 29.84 2.18E+002 F 10 366-379 373.35 93.54 0.79 2.74E+002 155.27 2.31E+002 F 11 431-440 436.23 109.28 0.74 9.88E+001 24.39 1.42E+002 F 12 478-488 483.19 121.03 0.49 4.43E+001 76.80 1.44E+002 F 13 570- 580 574.50 143.88 0.83 5.18E+002 44.71 1.38E+002 F 14 647-659 652.88 163.49 0.84 2.00E+002 94.65 1.30E+002 F 15 735-749 741.94 185.78 0.90 2.23E+003 88.61 1.46E+002 M 16 800- 827 806.57 201.95 1.00 4.79E+001 23.69 6.68E+001 m 17 800- 827 819.88 205.28 1.00 2.02E+002 70.15 6.29E+001 F 18 947-958 953.47 238.71 0.90 1.27E+002 24.73 6.90E+001 F 19 1347-1356 1351.45 338.30 0.92 2.63E+001 14.02 2.80E+001 F 20 1398-1413 1405.50 351.83 1.03 5.71E+001 18.50 5.60E+001 F 21 2323-2338 2329.83 583.14 1.23 3.12E+001 15.31 3.60E+001 F 22 5825-5849 5836.71 1460.71 2.49 1.95E+002 28.22 8.33E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:32:57 AM Page 2

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Sample

Title:

W3H-IMC-0312-S-P-8 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.998 1460.82* 10.66 7.53253E+000 1.22195E+000 Pb-212 0.855 74.82* 10.28 1.69805E+000 6.61433E-001 77.11* 17.10 3.06208E-001 1.41583E-001 86.83 2.07 87.35 3.97 89.78* 1.46 5.21904E+000 1.16484E+000 115.18 0.60 238.63* 43.60 2.09737E-001 4.59812E-002 300.09 3.30 PB-214 0.456 74.82* 5.80 3.00965E+000 1.20286E+000 77.11* 9.70 5.39810E-001 2.54282E-001 86.83 1.70 87.35 2.24 89.78* 0.82 9.29244E+000 2.22501E+000 241.99 7.25 258.76 0.53 295.22 18.42 351.93* 35.60 1.70645E-001 5.71017E-002 785.96 1.06 839.07 0.58 Ra-226 0.888 81.07 0.20 83.79* 0.32 6.13672E+001 9.93669E+000 186.21* 3.64 3.56888E+001 4.03820E+000 U-234 0.990 53.20* 0.12 1.13040E+002 2.47372E+001 120.90* 0.04 5.91112E+001 1.04096E+002 U-235 0.997 89.96* 3.43 2.22147E+000 5.00874E-001 93.35* 5.54 2.32558E+000 1.34795E+000 104.82 0.69 105.60 1.31 108.58 0.50 109.19* 1.66 2.74787E+000 8.49719E-001 143.76* 10.96 2.34698E+000 3.19407E-001 163.36* 5.08 2.09645E+000 1.01631E+000 194.94 0.63 202.12* 1.08 2.75418E+000 1.39606E+000 205.32* 5.02 2.52920E+000 9.18954E-001

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

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Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.998 7.532526E+000 1.221946E+000 Pb-212 0.855 2.147049E-001 4.349971E-002 PB-214 0.456 1.750133E-001 5.571472E-002 Ra-226 0.888 3.932858E+001 3.741070E+000 U-234 0.990 1.101569E+002 2.406703E+001 U-235 0.997 2.337758E+000 2.269806E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:32:57 AM Page 4

• • • • • • • • • • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 9:32:51 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 1 16.46 2.3238E-001 27.70 F 2 19.36 8.3849E-002 67.44 F 3 25.87 4.5458E-002 27.66 M 5 73.00 9.7383E-002 40.25 F 19 338.30 1.4587E-002 53.38 F 21 583.14 1.7348E-002 49.04 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 7/6/2017 9:32:58 AM Page 5

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W3H-IMC-0312-S-P-8 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 6.722E-001 6.72E-001 7.533E+000 2.838E-00 Pb-210 46.54 4.25 1.657E+000 1.66E+000 5.108E-001 7.948E-00 BI-212 727.33 6.67 1.315E+000 1.32E+000 4.346E-001 6.124E-00 785.37 1.10 9.407E+000 4.643E+000 4.409E+00 1078.62 0.56 1.851E+001 1.584E+000 8.493E+00 1620.50 1.47 5.575E+000 -9.835E-001 2.371E+00

+ Pb-212 74.82* 10.28 4.077E-001 7.58E-002 1.698E+000 1.969E-00 77.11* 17.10 2.427E-001 3.062E-001 1.173E-00 86.83 2.07 2.766E+000 1.390E+000 1.351E+00 87.35 3.97 1.228E+000 7.228E-001 5.978E-00 89.78* 1.46 2.750E+000 5.219E+000 1.331E+00 115.18 0.60 6.825E+000 -4.434E+000 3.307E+00 238.63* 43.60 7.579E-002 2.097E-001 3.566E-00 300.09 3.30 1.389E+000 -2.909E+000 6.573E-00 BI-214 76.86 0.55 1.290E+001 2.02E-001 9.803E-001 6.320E+00 79.29 0.91 5.957E+000 -1.060E+000 2.903E+00 609.32 45.49 2.024E-001 1.301E-001 9.561E-00 665.45 1.53 5.457E+000 -9.174E-001 2.548E+00 768.36 4.89 2.163E+000 6.613E-001 1.017E+00 806.18 1.26 7.406E+000 4.189E+000 3.440E+00 934.06 3.11 3.548E+000 1.872E+000 1.652E+00 1120.29 14.92 9.281E-001 4.936E-001 4.343E-00 1155.21 1.63 8.058E+000 4.721E+000 3.750E+00 1238.11 5.83 2.465E+000 1.571E+000 1.150E+00 1280.98 1.43 9.224E+000 5.134E-001 4.265E+00 1377.67 3.99 3.228E+000 1.201E+000 1.481E+00 1385.31 0.79 1.684E+001 1.125E+001 7.748E+00 1401.52 1.33 8.038E+000 -8.306E-001 3.614E+00 1407.99 2.39 4.483E+000 1.399E+000 2.016E+00 1509.21 2.13 5.171E+000 1.925E+000 2.316E+00 1583.20 0.70 1.508E+001 5.753E+000 6.691E+00 1661.27 1.05 9.661E+000 4.281E+000 4.233E+00 1729.59 2.88 3.351E+000 1.116E+000 1.450E+00 1764.49 15.30 9.525E-001 7.359E-001 4.331E-00 1847.43 2.03 4.908E+000 -6.047E-001 2.113E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 7.227E-001 1.27E-001 3.010E+000 3.491E-00 77.11* 9.70 4.278E-001 5.398E-001 2.067E-00 86.83 1.70 3.368E+000 1.692E+000 1.645E+00 87.35 2.24 2.177E+000 1.281E+000 1.059E+00

Nuclide MDA Report 7/6/2017 9:32:58 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78* 0.82 4.896E+000 1.27E-001 9.292E+000 2.370E+00 241.99 7.25 8.223E-001 -8.356E-001 3.976E-00 258.76 0.53 7.571E+000 -2.356E+000 3.587E+00 295.22 18.42 2.722E-001 4.139E-002 1.296E-00 351.93* 35.60 1.267E-001 1.706E-001 5.930E-00 785.96 1.06 9.787E+000 4.831E+000 4.587E+00 839.07 0.58 1.481E+001 5.333E+000 6.814E+00

+ Ra-226 81.07 0.20 2.445E+001 1.12E+000 4.034E+000 1.188E+00 83.79* 0.32 1.542E+001 6.137E+001 7.503E+00 186.21* 3.64 1.121E+000 3.569E+001 5.388E-00 AC-228 89.96 1.90 4.296E+019 6.94E+018 5.201E+019 2.098E+01 93.35 3.10 2.691E+019 -4.626E+019 1.315E+01 99.51 1.26 4.279E+019 -5.019E+019 2.066E+01 105.60 0.74 8.738E+019 4.320E+019 4.245E+01 129.07 2.42 2.515E+019 6.444E+018 1.218E+01 153.98 0.72 8.362E+019 -2.399E+019 4.039E+01 209.25 3.89 1.711E+019 -2.484E+018 8.229E+01 214.85 0.76 7.380E+019 -1.301E+019 3.518E+01 270.24 3.46 1.912E+019 4.595E+018 9.093E+01 328.00 2.95 2.510E+019 4.444E+018 1.188E+01 338.32 11.27 7.165E+018 2.002E+018 3.402E+01 409.46 1.92 4.465E+019 -8.143E+018 2.103E+01 463.00 4.40 2.240E+019 1.078E+019 1.056E+01 562.50 0.87 1.173E+020 -2.130E+019 5.469E+01 674.75 2.10 5.943E+019 -9.990E+018 2.774E+01 726.86 0.62 2.069E+020 7.947E+018 9.626E+01 755.32 1.00 1.360E+020 -5.351E+018 6.338E+01 772.29 1.49 1.058E+020 2.600E+019 4.975E+01 794.95 4.25 3.179E+019 1.981E+018 1.476E+01 830.49 0.54 2.451E+020 -8.211E+019 1.132E+02 835.71 1.61 7.375E+019 -2.786E+019 3.373E+01 840.38 0.91 1.386E+020 -8.906E+019 6.371E+01 904.20 0.77 2.081E+020 -3.216E+020 9.699E+01 911.20 25.80 6.941E+018 5.761E+018 3.259E+01 964.77 4.99 3.169E+019 2.257E+019 1.469E+01 968.97 15.80 1.005E+019 2.346E+018 4.658E+01 1247.08 0.50 3.706E+020 4.971E+019 1.709E+02 1459.14 0.83 5.279E+020 1.549E+021 2.540E+02 1495.91 0.86 1.696E+020 3.686E+019 7.504E+01 1588.20 3.22 5.368E+019 4.480E+019 2.409E+01 1630.63 1.51 7.390E+019 -7.317E+018 3.095E+01 TH-230 67.67 0.38 1.449E+001 1.45E+001 6.624E+000 7.041E+00 PA-234 742.81 0.11 8.073E+001 1.34E+001 -2.744E+000 3.748E+00 766.42 0.32 3.275E+001 -2.797E+000 1.537E+00 1001.03 0.84 1.338E+001 -2.520E+000 6.212E+00 TH-234 63.29 3.70 1.513E+000 1.51E+000 3.856E-001 7.339E-00 92.38 2.13 2.965E+000 9.173E+000 1.453E+00 92.80 2.10 2.888E+000 2.746E+000 1.414E+00 112.81 0.21 1.977E+001 -8.810E-001 9.586E+00

+ U-234 53.20* 0.12 4.124E+001 4.12E+001 1.130E+002 1.974E+00 120.90* 0.04 8.500E+001 5.911E+001 4.069E+00

Nuclide MDA Report 7/6/2017 9:32:58 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96* 3.43 1.171E+000 2.81E-001 2.221E+000 5.665E-00 93.35* 5.54 7.970E-001 2.326E+000 3.870E-00 104.82 0.69 6.477E+000 8.558E+000 3.147E+00 105.60 1.31 3.349E+000 1.656E+000 1.627E+00 108.58 0.50 9.400E+000 -6.568E+000 4.575E+00 109.19* 1.66 1.853E+000 2.748E+000 8.890E-00 143.76* 10.96 2.815E-001 2.347E+000 1.346E-00 163.36* 5.08 6.652E-001 2.096E+000 3.184E-00 194.94 0.63 5.949E+000 -2.443E+000 2.845E+00 202.12* 1.08 2.342E+000 2.754E+000 1.093E+00 205.32* 5.02 4.965E-001 2.529E+000 2.313E-00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 9:32:58 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0312\\W3H-IMC-000 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 7.53E+000 16.222 Pb-212 74.8 1.70E+000 38.952 8.096[44.698] 11.13 -2.005 77.1 3.06E-001 46.237 1.460[51.172] [ 0.362]

89.8 5.22E+000 22.319 24.884[31.285]

238.6 ^ 2.10E-001 21.923 1.000[31.004]

PB-214 74.8 3.01E+000 39.967 17.637[52.126] 11.30 -1.898 77.1 5.40E-001 47.106 3.163[57.781] [ 0.376]

89.8 9.29E+000 23.944 54.455[41.147]

351.9 ^ 1.71E-001 33.462 1.000[47.323]

Ra-226 83.8 6.14E+001 16.192 1.720[19.754] 3.55 -0.679 186.2 ^ 3.57E+001 11.315 1.000[16.002] [ 0.318]

U-234 53.2 ^ 1.13E+002 21.884 1.000[30.948] 3.14 -0.790 120.9 5.91E+001 176.10 0.523[177.45] [ 2.194]

U-235 90.0 2.22E+000 22.547 0.947[26.336] -0.40 0.085 93.3 2.33E+000 57.962 0.991[59.538] [ 0.443]

109.2 2.75E+000 30.923 1.171[33.785]

143.8 ^ 2.35E+000 13.609 1.000[19.246]

163.4 2.10E+000 48.478 0.893[50.352]

202.1 2.75E+000 50.689 1.173[52.484]

205.3 2.53E+000 36.334 1.078[38.799]