ML19095B189

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W3H-IMC-000312-S-P-7

ML19095B189
Person / Time
Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
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References
Download: ML19095B189 (11)

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• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0312\\W3H-IMC-000 Report Generated On : 7/6/2017 9:32:22 AM Sample Title : UNC-IMC-000312-S-P-7 Sample Description :

Sample Identification : IMC-000312-S-P-7 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 5.026E+002 grams Sample Taken On : 4/28/2017 12:00:00 AM Acquisition Started : 5/3/2017 3:24:03 PM Live Time : 1800.0 seconds Real Time : 1800.7 seconds Dead Time : 0.04 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 9:32:22 AM Page 1

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Detector Name: 8566 Sample

Title:

UNC-IMC-000312-S-P-7 Peak Analysis Performed on: 7/6/2017 9:32:18 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 47-58 52.57 13.27 0.52 1.14E+002 28.26 2.37E+002 F 2 58-70 65.41 16.48 0.88 4.94E+002 129.54 2.08E+002 F 3 97-109 103.16 25.92 0.62 1.37E+002 26.19 1.50E+002 F 4 205-218 213.25 53.48 0.60 1.57E+002 93.00 2.50E+002 M 5 286-314 291.64 73.09 0.83 2.01E+002 72.28 3.16E+002 m 6 286-314 299.79 75.13 0.84 3.82E+002 119.69 3.64E+002 m 7 286-314 308.68 77.36 0.85 1.03E+002 42.50 3.53E+002 F 8 321-330 324.68 81.36 0.82 8.04E+001 26.90 2.58E+002 F 9 331-343 337.25 84.51 0.89 6.09E+002 47.71 3.29E+002 F 10 355-364 359.69 90.12 0.77 2.53E+002 34.95 2.48E+002 F 11 365-378 373.07 93.47 0.84 3.33E+002 40.01 3.90E+002 F 12 429-446 435.99 109.22 1.00 1.82E+002 116.53 3.75E+002 F 13 476-487 482.73 120.91 0.70 7.95E+001 91.26 2.52E+002 F 14 567-580 574.44 143.86 0.87 7.92E+002 147.80 2.49E+002 F 15 647-659 652.86 163.49 0.93 3.15E+002 36.52 1.85E+002 F 16 734-754 741.89 185.77 0.90 3.51E+003 110.27 2.21E+002 F 17 773-784 778.56 194.94 0.66 3.50E+001 15.98 6.60E+001 M 18 800- 826 807.11 202.09 0.97 5.94E+001 17.99 6.83E+001 m 19 800- 826 820.30 205.39 0.97 2.36E+002 31.07 9.96E+001 F 20 947-959 952.97 238.59 1.03 1.54E+002 26.65 8.45E+001 F 21 1175-1184 1179.27 295.22 1.00 4.63E+001 16.28 2.80E+001 F 22 1397-1411 1404.62 351.61 1.30 6.53E+001 18.28 4.20E+001 F 23 2322-2335 2328.30 582.75 1.20 4.67E+001 16.59 2.45E+001 F 24 2426-2442 2433.84 609.17 1.38 5.62E+001 17.24 2.55E+001 F 25 5824-5852 5836.93 1460.77 3.00 2.16E+002 29.67 8.06E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:32:22 AM Page 2

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Sample

Title:

UNC-IMC-000312-S-P-7 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 1.000 1460.82* 10.66 7.10389E+000 1.10443E+000 Pb-212 0.855 74.82* 10.28 1.65979E+000 5.66431E-001 77.11* 17.10 2.63100E-001 1.14228E-001 86.83 2.07 87.35 3.97 89.78* 1.46 6.98825E+000 1.29490E+000 115.18 0.60 238.63* 43.60 2.16121E-001 4.32729E-002 300.09 3.30 BI-214 0.221 76.86* 0.55 8.25505E+000 3.59170E+000 79.29 0.91 609.32* 45.49 1.97130E-001 6.23260E-002 665.45 1.53 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.11 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1583.20 0.70 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 2204.06 4.92 2447.70 1.55 PB-214 0.788 74.82* 5.80 2.94184E+000 1.03788E+000 77.11* 9.70 4.63815E-001 2.05654E-001 86.83 1.70 87.35 2.24 89.78* 0.82 1.24425E+001 2.54552E+000 241.99 7.25 258.76 0.53 295.22* 18.42 1.89336E-001 6.87255E-002 351.93* 35.60 1.65667E-001 4.84325E-002

Interference Corrected Activity Report 7/6/2017 9:32:22 AM Page 3 Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty PB-214 0.788 785.96 1.06 839.07 0.58 Ra-226 0.966 81.07* 0.20 1.73700E+001 6.24999E+000 83.79* 0.32 7.81815E+001 1.17158E+001 186.21* 3.64 4.75829E+001 5.26003E+000 U-234 0.991 53.20* 0.12 8.69968E+001 5.33882E+001 120.90* 0.04 9.02532E+001 1.07044E+002 U-235 0.998 89.96* 3.43 2.97457E+000 5.59328E-001 93.35* 5.54 2.39768E+000 4.14935E-001 104.82 0.69 105.60 1.31 108.58 0.50 109.19* 1.66 4.30375E+000 2.86847E+000 143.76* 10.96 3.04835E+000 6.53071E-001 163.36* 5.08 2.80770E+000 4.40900E-001 194.94* 0.63 2.84624E+000 1.33776E+000 202.12* 1.08 2.90307E+000 9.37001E-001 205.32* 5.02 2.51602E+000 4.24023E-001

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:32:22 AM Page 4

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Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 1.000 7.103889E+000 1.104427E+000 Pb-212 0.855 2.161922E-001 4.019805E-002 BI-214 0.221 1.965757E-001 6.230311E-002 PB-214 0.788 1.735328E-001 3.890018E-002 Ra-226 0.966 3.960751E+001 3.806148E+000 U-234 0.991 8.764550E+001 4.777569E+001 U-235 0.998 2.677905E+000 2.002679E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:32:22 AM Page 5

• • • • • • • • • • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 9:32:18 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 1 13.27 6.3106E-002 24.88 F 2 16.48 2.7442E-001 26.23 F 3 25.92 7.6007E-002 19.14 M 5 73.09 1.1158E-001 35.99 F 23 582.75 2.5934E-002 35.55 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 7/6/2017 9:32:22 AM Page 6

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

UNC-IMC-000312-S-P-7 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 5.849E-001 5.85E-001 7.104E+000 2.480E-00 Pb-210 46.54 4.25 1.480E+000 1.48E+000 6.136E-001 7.116E-00 BI-212 727.33 6.67 1.274E+000 1.27E+000 2.415E-001 5.987E-00 785.37 1.10 7.104E+000 -7.273E+000 3.302E+00 1078.62 0.56 1.641E+001 -1.855E+000 7.555E+00 1620.50 1.47 6.536E+000 -4.833E-001 2.915E+00

+ Pb-212 74.82* 10.28 3.980E-001 7.25E-002 1.660E+000 1.931E-00 77.11* 17.10 2.305E-001 2.631E-001 1.118E-00 86.83 2.07 2.828E+000 6.170E-001 1.387E+00 87.35 3.97 1.261E+000 3.209E-001 6.167E-00 89.78* 1.46 2.417E+000 6.988E+000 1.171E+00 115.18 0.60 7.261E+000 2.347E+000 3.541E+00 238.63* 43.60 7.250E-002 2.161E-001 3.435E-00 300.09 3.30 1.280E+000 -9.937E-001 6.087E-00

+ BI-214 76.86* 0.55 7.232E+000 1.00E-001 8.255E+000 3.507E+00 79.29 0.91 5.633E+000 -2.846E-001 2.752E+00 609.32* 45.49 1.001E-001 1.971E-001 4.532E-00 665.45 1.53 5.099E+000 1.689E+000 2.396E+00 768.36 4.89 1.890E+000 4.689E-001 8.898E-00 806.18 1.26 6.962E+000 1.662E+000 3.258E+00 934.06 3.11 2.877E+000 3.402E-001 1.335E+00 1120.29 14.92 7.785E-001 3.822E-001 3.640E-00 1155.21 1.63 6.416E+000 5.284E+000 2.971E+00 1238.11 5.83 2.125E+000 1.234E+000 9.920E-00 1280.98 1.43 7.091E+000 3.600E+000 3.250E+00 1377.67 3.99 2.354E+000 1.573E+000 1.064E+00 1385.31 0.79 9.923E+000 -2.555E+000 4.390E+00 1401.52 1.33 6.359E+000 3.007E+000 2.835E+00 1407.99 2.39 3.547E+000 -9.608E-001 1.582E+00 1509.21 2.13 3.186E+000 -5.642E-001 1.364E+00 1583.20 0.70 1.504E+001 1.274E+000 6.798E+00 1661.27 1.05 6.804E+000 -2.720E+000 2.894E+00 1729.59 2.88 3.019E+000 1.982E-001 1.318E+00 1764.49 15.30 7.650E-001 5.169E-001 3.458E-00 1847.43 2.03 4.031E+000 -1.553E+000 1.726E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 7.055E-001 9.24E-002 2.942E+000 3.423E-00 77.11* 9.70 4.063E-001 4.638E-001 1.971E-00 86.83 1.70 3.443E+000 7.513E-001 1.689E+00 87.35 2.24 2.236E+000 5.687E-001 1.093E+00

Nuclide MDA Report 7/6/2017 9:32:22 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78* 0.82 4.303E+000 9.24E-002 1.244E+001 2.085E+00 241.99 7.25 7.219E-001 -4.699E-001 3.494E-00 258.76 0.53 6.154E+000 9.952E-001 2.909E+00 295.22* 18.42 1.118E-001 1.893E-001 5.035E-00 351.93* 35.60 9.241E-002 1.657E-001 4.277E-00 785.96 1.06 7.449E+000 -5.974E+000 3.464E+00 839.07 0.58 1.297E+001 1.591E+000 5.982E+00

+ Ra-226 81.07* 0.20 1.924E+001 1.30E+000 1.737E+001 9.329E+00 83.79* 0.32 1.400E+001 7.818E+001 6.825E+00 186.21* 3.64 1.299E+000 4.758E+001 6.314E-00 AC-228 89.96 1.90 1.253E+007 1.76E+006 1.884E+007 6.137E+00 93.35 3.10 7.948E+006 -1.718E+007 3.898E+00 99.51 1.26 1.277E+007 -1.345E+007 6.199E+00 105.60 0.74 2.531E+007 1.700E+007 1.234E+00 129.07 2.42 7.358E+006 -1.020E+006 3.580E+00 153.98 0.72 2.456E+007 1.290E+007 1.192E+00 209.25 3.89 4.905E+006 -9.376E+005 2.370E+00 214.85 0.76 1.813E+007 -5.508E+006 8.631E+00 270.24 3.46 4.847E+006 2.138E+006 2.306E+00 328.00 2.95 6.668E+006 9.938E+005 3.166E+00 338.32 11.27 1.759E+006 -4.030E+005 8.343E+00 409.46 1.92 1.204E+007 6.026E+006 5.691E+00 463.00 4.40 5.577E+006 5.336E+006 2.627E+00 562.50 0.87 3.390E+007 -2.957E+006 1.595E+00 674.75 2.10 1.516E+007 -5.499E+005 7.084E+00 726.86 0.62 6.079E+007 2.933E+007 2.859E+00 755.32 1.00 3.162E+007 -1.616E+007 1.465E+00 772.29 1.49 2.692E+007 7.716E+006 1.267E+00 794.95 4.25 8.563E+006 8.608E+005 3.996E+00 830.49 0.54 5.691E+007 -2.821E+007 2.611E+00 835.71 1.61 2.061E+007 5.216E+006 9.514E+00 840.38 0.91 3.595E+007 -4.155E+006 1.657E+00 904.20 0.77 5.880E+007 -2.641E+007 2.762E+00 911.20 25.80 1.931E+006 1.734E+006 9.121E+00 964.77 4.99 8.556E+006 -2.679E+004 3.988E+00 968.97 15.80 2.653E+006 1.724E+006 1.234E+00 1247.08 0.50 9.501E+007 -7.672E+007 4.390E+00 1459.14 0.83 1.390E+008 4.302E+008 6.700E+00 1495.91 0.86 4.267E+007 -4.235E+006 1.888E+00 1588.20 3.22 1.462E+007 1.732E+006 6.619E+00 1630.63 1.51 2.949E+007 1.283E+006 1.324E+00 TH-230 67.67 0.38 1.398E+001 1.40E+001 3.969E+000 6.813E+00 PA-234 742.81 0.11 6.806E+001 1.05E+001 2.228E+001 3.158E+00 766.42 0.32 2.911E+001 2.095E+001 1.371E+00 1001.03 0.84 1.050E+001 2.649E+000 4.845E+00 TH-234 63.29 3.70 1.465E+000 1.46E+000 7.727E-001 7.130E-00 92.38 2.13 2.976E+000 1.120E+001 1.463E+00 92.80 2.10 2.865E+000 1.448E+000 1.407E+00 112.81 0.21 2.069E+001 3.931E+000 1.009E+00

+ U-234 53.20* 0.12 5.419E+001 5.42E+001 8.700E+001 2.634E+00 120.90* 0.04 9.682E+001 9.025E+001 4.687E+00

Nuclide MDA Report 7/6/2017 9:32:22 AM Page 8 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96* 3.43 1.029E+000 3.41E-001 2.975E+000 4.985E-00 93.35* 5.54 8.742E-001 2.398E+000 4.274E-00 104.82 0.69 6.256E+000 5.270E+000 3.050E+00 105.60 1.31 3.276E+000 2.201E+000 1.598E+00 108.58 0.50 9.828E+000 -5.622E-001 4.808E+00 109.19* 1.66 3.075E+000 4.304E+000 1.506E+00 143.76* 10.96 3.414E-001 3.048E+000 1.655E-00 163.36* 5.08 6.702E-001 2.808E+000 3.231E-00 194.94* 0.63 3.661E+000 2.846E+000 1.720E+00 202.12* 1.08 2.012E+000 2.903E+000 9.398E-00 205.32* 5.02 5.241E-001 2.516E+000 2.476E-00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 9:32:22 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0312\\W3H-IMC-000 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 7.10E+000 15.547 Pb-212 74.8 1.66E+000 34.127 7.680[39.567] 11.73 -2.109 77.1 2.63E-001 43.416 1.217[47.811] [ 0.328]

89.8 6.99E+000 18.530 32.335[27.281]

238.6 ^ 2.16E-001 20.022 1.000[28.316]

BI-214 76.9 8.26E+000 43.509 41.876[53.783] 11.57 -1.804 609.3 ^ 1.97E-001 31.617 1.000[44.713] [ 0.338]

PB-214 74.8 2.94E+000 35.280 17.757[45.819] 12.42 -2.116 77.1 4.64E-001 44.340 2.800[53.110] [ 0.286]

89.8 1.24E+001 20.458 75.105[35.682]

295.2 1.89E-001 36.298 1.143[46.607]

351.9 ^ 1.66E-001 29.235 1.000[41.344]

Ra-226 81.1 1.74E+001 35.981 0.365[37.641] 1.19 -0.227 83.8 7.82E+001 14.985 1.643[18.622] [ 0.284]

186.2 ^ 4.76E+001 11.054 1.000[15.633]

U-234 53.2 ^ 8.70E+001 61.368 1.000[86.787] -0.18 0.045 120.9 9.03E+001 118.60 1.037[133.54] [ 1.940]

U-235 90.0 2.97E+000 18.804 0.976[28.505] -0.02 -0.016 93.3 2.40E+000 17.306 0.787[27.540] [ 0.347]

109.2 4.30E+000 66.650 1.412[70.009]

143.8 ^ 3.05E+000 21.424 1.000[30.298]

163.4 2.81E+000 15.703 0.921[26.563]

194.9 2.85E+000 47.001 0.934[51.653]

202.1 2.90E+000 32.276 0.952[38.739]

205.3 2.52E+000 16.853 0.825[27.258]