ML19095B178

From kanterella
Jump to navigation Jump to search
Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W3H-IMC-000312-S-P-4
ML19095B178
Person / Time
Site: 07000371
Issue date: 03/01/2018
From:
Cabrera Services
To:
NRC Region 1
Shared Package
ml051740240 List: ... further results
References
Download: ML19095B178 (10)
v • d • e


Text

          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0312\\W3H-IMC-000 Report Generated On : 7/6/2017 9:30:39 AM Sample Title : UNC-IMC-000312-S-P-4 Sample Description :

Sample Identification : IMC-000312-S-P-4 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 3.072E+002 grams Sample Taken On : 4/28/2017 12:00:00 AM Acquisition Started : 5/3/2017 1:03:27 PM Live Time : 1800.0 seconds Real Time : 1800.7 seconds Dead Time : 0.04 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 9:30:39 AM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

UNC-IMC-000312-S-P-4 Peak Analysis Performed on: 7/6/2017 9:30:31 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 48-58 52.57 13.27 0.58 3.38E+002 38.43 2.67E+002 F 2 59-72 65.15 16.41 0.91 1.71E+003 206.67 4.41E+002 F 3 93-111 102.92 25.87 0.84 3.85E+002 103.73 1.95E+002 F 4 209-218 213.34 53.50 0.69 3.42E+002 35.11 1.15E+002 M 5 286-306 291.06 72.95 0.81 1.52E+002 63.91 2.78E+002 m 6 286-306 299.66 75.10 0.81 3.09E+002 114.47 3.19E+002 M 7 322-343 325.58 81.58 0.78 6.97E+001 24.32 2.00E+002 m 8 322-343 337.17 84.49 0.79 7.78E+002 52.70 2.68E+002 F 9 354-366 359.52 90.08 0.68 3.26E+002 39.81 3.16E+002 M 10 366-387 373.34 93.54 0.95 4.99E+002 140.95 2.37E+002 m 11 366-387 383.68 96.12 0.95 6.77E+001 27.65 2.54E+002 F 12 428-442 436.42 109.32 1.01 2.02E+002 126.33 3.13E+002 F 13 473-488 482.77 120.92 0.65 1.01E+002 84.56 2.46E+002 F 14 569-585 574.56 143.89 0.84 1.04E+003 60.88 1.96E+002 F 15 646-659 652.66 163.44 0.88 4.69E+002 112.21 1.38E+002 F 16 736-751 741.94 185.78 0.90 4.78E+003 127.92 1.12E+002 F 17 773-785 778.46 194.92 0.75 4.73E+001 50.97 5.53E+001 M 18 802-830 807.27 202.13 0.90 5.44E+001 22.26 4.73E+001 m 19 802-830 820.17 205.35 0.91 3.65E+002 94.97 4.42E+001 F 20 1400- 1411 1404.37 351.55 0.71 2.01E+001 12.23 2.88E+001 F 21 5826-5846 5835.62 1460.44 2.70 1.11E+002 21.84 1.05E+001 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:30:39 AM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

UNC-IMC-000312-S-P-4 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.977 1460.82* 10.66 5.97900E+000 1.25254E+000 PB-214 0.215 74.82* 5.80 3.89522E+000 1.57531E+000 77.11 9.70 86.83 1.70 87.35 2.24 89.78* 0.82 2.63122E+001 5.10093E+000 241.99 7.25 258.76 0.53 295.22 18.42 351.93* 35.60 8.36129E-002 5.12652E-002 785.96 1.06 839.07 0.58 Ra-226 0.966 81.07* 0.20 2.45884E+001 9.17949E+000 83.79* 0.32 1.63471E+002 2.36355E+001 186.21* 3.64 1.06142E+002 1.16015E+001 U-234 0.989 53.20* 0.12 3.10369E+002 5.80721E+001 120.90* 0.04 1.87577E+002 1.66721E+002 U-235 0.936 89.96* 3.43 6.29035E+000 1.10906E+000 93.35* 5.54 5.87998E+000 1.81576E+000 104.82 0.69 105.60 1.31 108.58 0.50 109.19* 1.66 7.79796E+000 5.09621E+000 143.76* 10.96 6.56089E+000 7.89902E-001 163.36* 5.08 6.83878E+000 1.78833E+000 194.94* 0.63 6.30436E+000 6.82404E+000 202.12* 1.08 4.35446E+000 1.84514E+000 205.32* 5.02 6.36474E+000 1.78677E+000

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:30:39 AM Page 3

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.977 5.978996E+000 1.252542E+000 PB-214 0.215 8.790487E-002 5.123262E-002 Ra-226 0.966 6.511170E+001 6.886349E+000 U-234 0.989 2.970835E+002 5.484055E+001 U-235 0.936 6.287923E+000 5.086982E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:30:39 AM Page 4

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 9:30:31 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 1 13.27 1.8780E-001 11.37 F 2 16.41 9.4747E-001 12.12 F 3 25.87 2.1411E-001 26.92 M 5 72.95 8.4270E-002 42.13 m 11 96.12 3.7609E-002 40.84 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 7/6/2017 9:30:39 AM Page 5

          • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

UNC-IMC-000312-S-P-4 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 9.891E-001 9.89E-001 5.979E+000 4.218E-00 Pb-210 46.54 4.25 2.836E+000 2.84E+000 2.423E+000 1.371E+00 BI-212 727.33 6.67 1.745E+000 1.74E+000 -3.255E-001 8.094E-00 785.37 1.10 1.096E+001 -7.990E-001 5.072E+00 1078.62 0.56 2.141E+001 -1.155E+001 9.643E+00 1620.50 1.47 8.045E+000 5.770E-001 3.444E+00 Pb-212 74.82 10.28 1.044E+000 1.40E-001 2.614E+000 5.124E-00 77.11 17.10 5.505E-001 4.755E-002 2.696E-00 86.83 2.07 4.568E+000 5.722E-001 2.240E+00 87.35 3.97 1.857E+000 2.976E-001 9.056E-00 89.78 1.46 5.851E+000 1.670E+001 2.864E+00 115.18 0.60 1.117E+001 4.904E+000 5.438E+00 238.63 43.60 1.404E-001 1.847E-001 6.710E-00 300.09 3.30 1.664E+000 -1.956E+000 7.804E-00 BI-214 76.86 0.55 1.756E+001 2.33E-001 2.045E+000 8.599E+00 79.29 0.91 8.047E+000 -1.281E+000 3.918E+00 609.32 45.49 2.327E-001 -3.015E-002 1.086E-00 665.45 1.53 7.039E+000 -1.329E-002 3.268E+00 768.36 4.89 2.664E+000 3.812E-001 1.242E+00 806.18 1.26 9.158E+000 -6.365E-001 4.214E+00 934.06 3.11 3.692E+000 -1.466E+000 1.676E+00 1120.29 14.92 1.099E+000 5.105E-001 5.083E-00 1155.21 1.63 9.221E+000 -2.744E+000 4.222E+00 1238.11 5.83 2.509E+000 -2.557E+000 1.139E+00 1280.98 1.43 9.755E+000 -6.247E+000 4.394E+00 1377.67 3.99 3.351E+000 -1.063E+000 1.491E+00 1385.31 0.79 1.793E+001 9.551E+000 8.031E+00 1401.52 1.33 1.118E+001 1.940E+000 5.026E+00 1407.99 2.39 5.689E+000 -7.731E-002 2.531E+00 1509.21 2.13 7.061E+000 3.461E+000 3.156E+00 1583.20 0.70 2.006E+001 -4.073E+000 8.851E+00 1661.27 1.05 1.155E+001 6.444E-001 4.946E+00 1729.59 2.88 4.802E+000 9.383E-001 2.087E+00 1764.49 15.30 1.021E+000 3.574E-001 4.502E-00 1847.43 2.03 6.825E+000 5.080E-001 2.939E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 1.083E+000 1.20E-001 3.895E+000 5.245E-00 77.11 9.70 9.705E-001 8.382E-002 4.752E-00 86.83 1.70 5.562E+000 6.967E-001 2.728E+00 87.35 2.24 3.291E+000 5.274E-001 1.605E+00

Nuclide MDA Report 7/6/2017 9:30:39 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78* 0.82 8.610E+000 1.20E-001 2.631E+001 4.196E+00 241.99 7.25 8.156E-001 3.198E-001 3.889E-00 258.76 0.53 1.021E+001 6.656E+000 4.829E+00 295.22 18.42 3.184E-001 -4.015E-002 1.501E-00 351.93* 35.60 1.199E-001 8.361E-002 5.435E-00 785.96 1.06 1.161E+001 9.436E-001 5.377E+00 839.07 0.58 2.297E+001 8.067E+000 1.066E+00

+ Ra-226 81.07* 0.20 2.416E+001 1.40E+000 2.459E+001 1.160E+00 83.79* 0.32 1.657E+001 1.635E+002 7.999E+00 186.21* 3.64 1.400E+000 1.061E+002 6.697E-00 AC-228 89.96 1.90 1.561E+007 1.73E+006 4.296E+007 7.648E+00 93.35 3.10 1.009E+007 -3.581E+007 4.949E+00 99.51 1.26 1.456E+007 -1.241E+007 7.047E+00 105.60 0.74 3.141E+007 1.453E+007 1.531E+00 129.07 2.42 7.784E+006 -2.666E+006 3.768E+00 153.98 0.72 2.694E+007 1.471E+007 1.302E+00 209.25 3.89 5.832E+006 -2.959E+006 2.813E+00 214.85 0.76 1.966E+007 -1.003E+006 9.286E+00 270.24 3.46 4.754E+006 1.638E+006 2.229E+00 328.00 2.95 7.078E+006 5.462E+005 3.328E+00 338.32 11.27 1.733E+006 -8.439E+004 8.095E+00 409.46 1.92 1.244E+007 -7.753E+006 5.810E+00 463.00 4.40 5.915E+006 -1.980E+006 2.754E+00 562.50 0.87 3.543E+007 1.208E+007 1.646E+00 674.75 2.10 1.609E+007 -5.724E+006 7.423E+00 726.86 0.62 6.336E+007 1.675E+006 2.941E+00 755.32 1.00 3.833E+007 6.766E+006 1.771E+00 772.29 1.49 2.721E+007 -1.660E+007 1.261E+00 794.95 4.25 9.544E+006 0.000E+000 4.413E+00 830.49 0.54 8.365E+007 -6.372E+006 3.888E+00 835.71 1.61 2.866E+007 1.001E+007 1.334E+00 840.38 0.91 4.774E+007 -2.144E+006 2.210E+00 904.20 0.77 5.530E+007 -5.048E+007 2.542E+00 911.20 25.80 1.779E+006 7.744E+005 8.225E+00 964.77 4.99 9.848E+006 7.555E+006 4.560E+00 968.97 15.80 2.982E+006 7.521E+005 1.376E+00 1247.08 0.50 9.161E+007 -3.813E+007 4.127E+00 1459.14 0.83 1.362E+008 3.117E+008 6.498E+00 1495.91 0.86 4.991E+007 4.813E+006 2.187E+00 1588.20 3.22 1.637E+007 1.034E+007 7.317E+00 1630.63 1.51 2.731E+007 -1.164E+007 1.176E+00 TH-230 67.67 0.38 1.934E+001 1.93E+001 -2.908E+001 9.386E+00 PA-234 742.81 0.11 1.085E+002 1.63E+001 3.836E+001 5.026E+00 766.42 0.32 4.073E+001 -2.642E+000 1.897E+00 1001.03 0.84 1.634E+001 5.380E+000 7.503E+00 TH-234 63.29 3.70 2.174E+000 2.17E+000 2.587E+000 1.055E+00 92.38 2.13 5.070E+000 2.171E+001 2.494E+00 92.80 2.10 4.800E+000 -8.729E-001 2.358E+00 112.81 0.21 3.260E+001 -1.031E+001 1.588E+00

+ U-234 53.20* 0.12 5.474E+001 5.47E+001 3.104E+002 2.614E+00 120.90* 0.04 1.710E+002 1.876E+002 8.300E+00

Nuclide MDA Report 7/6/2017 9:30:39 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96* 3.43 2.058E+000 5.29E-001 6.290E+000 1.003E+00 93.35* 5.54 8.761E-001 5.880E+000 4.221E-00 104.82 0.69 9.925E+000 1.050E+001 4.836E+00 105.60 1.31 5.295E+000 2.449E+000 2.581E+00 108.58 0.50 1.619E+001 7.701E+000 7.923E+00 109.19* 1.66 4.312E+000 7.798E+000 2.104E+00 143.76* 10.96 5.291E-001 6.561E+000 2.560E-00 163.36* 5.08 9.739E-001 6.839E+000 4.673E-00 194.94* 0.63 5.638E+000 6.304E+000 2.639E+00 202.12* 1.08 2.777E+000 4.354E+000 1.280E+00 205.32* 5.02 5.867E-001 6.365E+000 2.698E-00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 9:30:39 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
===================================================

Analysis using Key Line Activities

===================================================

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0312\\W3H-IMC-000 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 5.98E+000 20.949 PB-214 74.8 3.90E+000 40.442 46.586[73.449] 18.90 -3.181 89.8 2.63E+001 19.386 314.69[64.304] [ 0.681]

351.9 ^ 8.36E-002 61.313 1.000[86.709]

Ra-226 81.1 2.46E+001 37.333 0.232[38.900] 0.48 -0.090 83.8 1.63E+002 14.459 1.540[18.125] [ 0.280]

186.2 ^ 1.06E+002 10.930 1.000[15.458]

U-234 53.2 ^ 3.10E+002 18.711 1.000[26.461] 2.44 -0.613 120.9 1.88E+002 88.881 0.604[90.829] [ 1.152]

U-235 90.0 6.29E+000 17.631 0.959[21.350] 0.14 -0.036 93.3 5.88E+000 30.880 0.896[33.144] [ 0.346]

109.2 7.80E+000 65.353 1.189[66.453]

143.8 ^ 6.56E+000 12.040 1.000[17.026]

163.4 6.84E+000 26.150 1.042[28.788]

194.9 6.30E+000 108.24 0.961[108.91]

202.1 4.35E+000 42.373 0.664[44.051]

205.3 6.36E+000 28.073 0.970[30.546]

Retrieved from "https://kanterella.com/w/index.php?title=ML19095B178&oldid=4932776"