ML19095B163

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W3H-ERRU-0310-S-P-8

ML19095B163
Person / Time
Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
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References
Download: ML19095B163 (10)

Text

• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0310\\W3H-ERRU-03 Report Generated On : 7/6/2017 10:03:05 AM Sample Title : W3H-ERRU-0310-S-P-8 Sample Description :

Sample Identification : 0310-S-P-8 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 3.645E+002 grams Sample Taken On : 6/1/2017 2:00:00 PM Acquisition Started : 6/7/2017 10:46:06 AM Live Time : 1800.0 seconds Real Time : 1800.4 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 10:03:05 AM Page 1

• • • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W3H-ERRU-0310-S-P-8 Peak Analysis Performed on: 7/6/2017 10:03:00 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts M 1 296-313 299.40 75.03 0.63 1.33E+002 26.41 1.32E+002 m 2 296-313 308.27 77.25 0.64 7.14E+001 20.11 1.37E+002 F 3 332-344 337.49 84.57 1.04 1.10E+002 92.71 1.15E+002 F 4 568-578 574.34 143.84 0.68 7.17E+001 64.22 7.01E+001 F 5 644-656 651.78 163.22 0.60 3.31E+001 42.13 6.99E+001 F 6 736-748 741.53 185.68 0.97 4.01E+002 37.56 6.34E+001 F 7 815-824 819.79 205.26 0.75 3.54E+001 14.81 3.63E+001 F 8 946-958 952.56 238.48 0.80 1.08E+002 23.32 6.83E+001 F 9 1172-1184 1178.74 295.08 0.98 4.88E+001 15.52 2.47E+001 F 10 1398-1412 1405.30 351.78 1.43 8.00E+001 52.37 1.65E+001 F 11 2320- 2335 2327.58 582.58 1.03 4.22E+001 15.14 2.53E+001 F 12 2425-2438 2431.38 608.55 1.18 3.70E+001 14.57 1.98E+001 F 13 5822-5849 5834.27 1460.11 2.90 1.75E+002 26.42 1.56E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 10:03:05 AM Page 2

• • • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W3H-ERRU-0310-S-P-8 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.921 1460.82* 10.66 7.94038E+000 1.32968E+000 Pb-212 0.996 74.82* 10.28 7.98633E-001 1.91583E-001 77.11* 17.10 2.51935E-001 7.85349E-002 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 2.09669E-001 4.97913E-002 300.09 3.30 BI-214 0.246 76.86* 0.55 7.90476E+000 2.47435E+000 79.29 0.91 609.32* 45.49 1.78744E-001 7.17286E-002 665.45 1.53 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.11 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1583.20 0.70 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 2204.06 4.92 2447.70 1.55 PB-214 0.850 74.82* 5.80 1.41551E+000 3.62415E-001 77.11* 9.70 4.44133E-001 1.44107E-001 86.83 1.70 87.35 2.24 89.78 0.82 241.99 7.25 258.76 0.53 295.22* 18.42 2.75036E-001 9.08955E-002 351.93* 35.60 2.79889E-001 1.84853E-001

Interference Corrected Activity Report 7/6/2017 10:03:05 AM Page 3 Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty PB-214 0.850 785.96 1.06 839.07 0.58 Ra-226 0.873 81.07 0.20 83.79* 0.32 1.93983E+001 1.66033E+001 186.21* 3.64 7.49619E+000 1.06065E+000 U-235 0.999 89.96 3.43 93.35 5.54 104.82 0.69 105.60 1.31 108.58 0.50 109.19 1.66 143.76* 10.96 3.80404E-001 3.43091E-001 163.36* 5.08 4.05516E-001 5.18670E-001 194.94 0.63 202.12 1.08 205.32* 5.02 5.19658E-001 2.24375E-001

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 10:03:05 AM Page 4

• • • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.921 7.940378E+000 1.329685E+000 Pb-212 0.996 1.998636E-001 4.287003E-002 BI-214 0.246 1.759895E-001 7.169953E-002 PB-214 0.850 2.606609E-001 7.207101E-002 Ra-226 0.873 7.544564E+000 1.058491E+000 U-235 0.999 4.695489E-001 1.765676E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

• • • • • • • • • • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 10:03:00 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 11 582.58 2.3458E-002 35.85 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 7/6/2017 10:03:05 AM Page 5

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W3H-ERRU-0310-S-P-8 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 4.198E-001 4.20E-001 7.940E+000 1.486E-00 Pb-210 46.54 4.25 1.708E+000 1.71E+000 2.305E+000 8.145E-00 BI-212 727.33 6.67 1.576E+000 1.58E+000 1.038E+000 7.349E-00 785.37 1.10 8.730E+000 -2.202E+000 4.020E+00 1078.62 0.56 1.970E+001 3.631E+000 8.956E+00 1620.50 1.47 7.885E+000 -1.549E+000 3.455E+00

+ Pb-212 74.82* 10.28 3.376E-001 9.03E-002 7.986E-001 1.607E-00 77.11* 17.10 2.020E-001 2.519E-001 9.622E-00 86.83 2.07 2.134E+000 -2.093E-001 1.030E+00 87.35 3.97 1.029E+000 -2.910E-001 4.954E-00 89.78 1.46 2.623E+000 -3.208E+000 1.260E+00 115.18 0.60 5.138E+000 3.388E+000 2.446E+00 238.63* 43.60 9.034E-002 2.097E-001 4.255E-00 300.09 3.30 1.531E+000 -1.642E+000 7.221E-00

+ BI-214 76.86* 0.55 6.338E+000 1.17E-001 7.905E+000 3.019E+00 79.29 0.91 4.842E+000 -2.159E+000 2.333E+00 609.32* 45.49 1.174E-001 1.787E-001 5.214E-00 665.45 1.53 6.440E+000 -3.024E+000 3.008E+00 768.36 4.89 2.144E+000 1.008E+000 9.961E-00 806.18 1.26 8.953E+000 1.626E-002 4.169E+00 934.06 3.11 3.549E+000 -4.361E-001 1.631E+00 1120.29 14.92 1.037E+000 4.964E-001 4.836E-00 1155.21 1.63 7.591E+000 -2.797E+000 3.468E+00 1238.11 5.83 3.030E+000 9.293E-001 1.418E+00 1280.98 1.43 9.668E+000 2.557E+000 4.427E+00 1377.67 3.99 2.767E+000 -1.011E+000 1.228E+00 1385.31 0.79 1.306E+001 -9.019E+000 5.743E+00 1401.52 1.33 9.420E+000 5.548E+000 4.236E+00 1407.99 2.39 5.076E+000 -2.063E-001 2.274E+00 1509.21 2.13 4.837E+000 8.168E-001 2.103E+00 1583.20 0.70 1.944E+001 7.519E+000 8.726E+00 1661.27 1.05 1.040E+001 3.465E+000 4.502E+00 1729.59 2.88 3.928E+000 -1.542E+000 1.700E+00 1764.49 15.30 1.188E+000 1.323E+000 5.436E-00 1847.43 2.03 5.752E+000 2.702E+000 2.477E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 5.984E-001 8.34E-002 1.416E+000 2.848E-00 77.11* 9.70 3.561E-001 4.441E-001 1.696E-00 86.83 1.70 2.598E+000 -2.548E-001 1.254E+00 87.35 2.24 1.824E+000 -5.158E-001 8.780E-00

Nuclide MDA Report 7/6/2017 10:03:05 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78 0.82 4.670E+000 8.34E-002 -5.712E+000 2.243E+00 241.99 7.25 9.192E-001 9.131E-002 4.436E-00 258.76 0.53 7.513E+000 -9.778E-001 3.524E+00 295.22* 18.42 1.551E-001 2.750E-001 6.990E-00 351.93* 35.60 8.345E-002 2.799E-001 3.699E-00 785.96 1.06 9.173E+000 -9.468E-002 4.228E+00 839.07 0.58 1.788E+001 -3.399E+000 8.248E+00

+ Ra-226 81.07 0.20 1.788E+001 8.45E-001 -9.853E+000 8.535E+00 83.79* 0.32 1.159E+001 1.940E+001 5.555E+00 186.21* 3.64 8.447E-001 7.496E+000 3.970E-00 AC-228 89.96 1.90 1.742E+007 4.33E+006 -1.418E+007 8.392E+00 93.35 3.10 1.062E+007 -1.704E+006 5.116E+00 99.51 1.26 1.950E+007 -6.894E+006 9.282E+00 105.60 0.74 3.373E+007 -3.309E+006 1.607E+00 129.07 2.42 9.679E+006 -2.645E+006 4.590E+00 153.98 0.72 3.715E+007 3.332E+006 1.767E+00 209.25 3.89 8.459E+006 7.892E+005 4.021E+00 214.85 0.76 4.044E+007 -9.675E+006 1.913E+00 270.24 3.46 1.106E+007 8.757E+006 5.232E+00 328.00 2.95 1.580E+007 1.317E+007 7.477E+00 338.32 11.27 4.330E+006 4.113E+006 2.050E+00 409.46 1.92 2.517E+007 -5.478E+006 1.176E+00 463.00 4.40 1.258E+007 -1.561E+006 5.882E+00 562.50 0.87 8.078E+007 1.867E+006 3.786E+00 674.75 2.10 3.614E+007 -5.686E+006 1.682E+00 726.86 0.62 1.354E+008 4.207E+007 6.313E+00 755.32 1.00 8.185E+007 1.298E+007 3.800E+00 772.29 1.49 5.788E+007 1.482E+007 2.693E+00 794.95 4.25 2.177E+007 1.243E+007 1.016E+00 830.49 0.54 1.586E+008 4.373E+006 7.336E+00 835.71 1.61 5.252E+007 1.465E+007 2.427E+00 840.38 0.91 9.077E+007 -2.960E+007 4.183E+00 904.20 0.77 1.441E+008 -4.422E+007 6.759E+00 911.20 25.80 4.461E+006 -4.975E+004 2.096E+00 964.77 4.99 2.341E+007 1.414E+007 1.097E+00 968.97 15.80 7.376E+006 6.143E+006 3.456E+00 1247.08 0.50 2.354E+008 -4.800E+007 1.086E+00 1459.14 0.83 3.152E+008 8.414E+008 1.513E+00 1495.91 0.86 9.768E+007 3.920E+007 4.264E+00 1588.20 3.22 3.290E+007 4.301E+005 1.471E+00 1630.63 1.51 6.324E+007 2.071E+007 2.781E+00 TH-230 67.67 0.38 1.118E+001 1.12E+001 -1.458E+000 5.349E+00 PA-234 742.81 0.11 8.905E+001 1.50E+001 2.483E+001 4.114E+00 766.42 0.32 3.112E+001 -1.262E+001 1.439E+00 1001.03 0.84 1.503E+001 5.311E+000 6.954E+00 TH-234 63.29 3.70 1.174E+000 1.17E+000 2.969E-001 5.601E-00 92.38 2.13 2.064E+000 2.179E+000 9.970E-00 92.80 2.10 2.016E+000 3.941E-001 9.722E-00 112.81 0.21 1.460E+001 -2.379E+001 6.952E+00 U-234 53.20 0.12 4.129E+001 4.13E+001 2.626E+001 1.960E+00 120.90 0.04 8.663E+001 2.935E+001 4.120E+00

Nuclide MDA Report 7/6/2017 10:03:05 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96 3.43 1.208E+000 2.40E-001 -9.829E-001 5.819E-00 93.35 5.54 7.436E-001 -1.193E-001 3.583E-00 104.82 0.69 4.499E+000 1.448E-001 2.143E+00 105.60 1.31 2.385E+000 -2.340E-001 1.137E+00 108.58 0.50 6.836E+000 4.183E+000 3.271E+00 109.19 1.66 1.976E+000 -6.952E-001 9.438E-00 143.76* 10.96 2.396E-001 3.804E-001 1.126E-00 163.36* 5.08 5.798E-001 4.055E-001 2.733E-00 194.94 0.63 5.832E+000 -4.210E-002 2.764E+00 202.12 1.08 3.855E+000 1.096E+000 1.836E+00 205.32* 5.02 4.764E-001 5.197E-001 2.183E-00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 10:03:05 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0310\\W3H-ERRU-03 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 7.94E+000 16.746 Pb-212 74.8 7.99E-001 23.989 3.809[33.755] 4.12 -0.755 77.1 2.52E-001 31.173 1.202[39.188] [ 0.368]

238.6 ^ 2.10E-001 23.748 1.000[33.584]

BI-214 76.9 7.90E+000 31.302 44.224[50.894] 11.74 -1.830 609.3 ^ 1.79E-001 40.129 1.000[56.751] [ 0.368]

PB-214 74.8 1.42E+000 25.603 5.057[70.834] 4.35 -0.758 77.1 4.44E-001 32.447 1.587[73.585] [ 0.540]

295.2 2.75E-001 33.049 0.983[73.852]

351.9 ^ 2.80E-001 66.045 1.000[93.402]

Ra-226 83.8 1.94E+001 85.592 2.588[86.753] 6.22 -1.191 186.2 ^ 7.50E+000 14.149 1.000[20.010] [ 1.115]

U-235 143.8 ^ 3.80E-001 90.191 1.000[127.54] -4.50 0.904 163.4 4.06E-001 127.90 1.066[156.50] [ 4.421]

205.3 5.20E-001 43.177 1.366[99.994]