ML19095B156

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W3H-ERRU-0310-S-P-6

ML19095B156
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Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
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• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0310\\W3H-ERRU-03 Report Generated On : 7/6/2017 10:02:03 AM Sample Title : W3H-ERRU-0310-S-P-6 Sample Description :

Sample Identification : 0310-S-P-6 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 2.800E+002 grams Sample Taken On : 6/1/2017 2:00:00 PM Acquisition Started : 6/7/2017 10:03:46 AM Live Time : 1800.0 seconds Real Time : 1800.4 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 10:02:03 AM Page 1

• • • • • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W3H-ERRU-0310-S-P-6 Peak Analysis Performed on: 7/6/2017 10:02:00 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 295-304 299.63 75.09 0.69 1.03E+002 23.05 1.13E+002 F 2 355-364 360.17 90.24 0.34 4.02E+001 34.69 5.00E+001 F 3 569-582 574.62 143.91 0.47 9.79E+001 44.77 8.58E+001 F 4 645-659 651.96 163.26 0.65 6.28E+001 45.08 7.50E+001 F 5 735-751 741.57 185.69 0.88 4.41E+002 40.44 7.65E+001 F 6 947-957 952.13 238.38 0.95 4.63E+001 16.31 3.71E+001 F 7 2427-2439 2433.38 609.05 1.09 2.43E+001 12.34 1.52E+001 F 8 5824-5847 5834.97 1460.28 2.51 1.25E+002 22.64 4.00E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 10:02:03 AM Page 2

• • • • • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W3H-ERRU-0310-S-P-6 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.954 1460.82* 10.66 7.37738E+000 1.43977E+000 Pb-212 0.628 74.82* 10.28 8.03521E-001 2.10021E-001 77.11 17.10 86.83 2.07 87.35 3.97 89.78* 1.46 1.99429E+000 1.73898E+000 115.18 0.60 238.63* 43.60 1.16363E-001 4.26692E-002 300.09 3.30 BI-214 0.996 76.86 0.55 79.29 0.91 609.32* 45.49 1.52965E-001 7.86034E-002 665.45 1.53 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.11 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1583.20 0.70 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 2204.06 4.92 2447.70 1.55 Ra-226 0.962 81.07 0.20 83.79 0.32 186.21* 3.64 1.07538E+001 1.50645E+000 U-235 0.740 89.96* 3.43 8.48874E-001 7.40701E-001 93.35 5.54 104.82 0.69 105.60 1.31 108.58 0.50 109.19 1.66

Interference Corrected Activity Report 7/6/2017 10:02:03 AM Page 3 Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty U-235 0.740 143.76* 10.96 6.76500E-001 3.17401E-001 163.36* 5.08 1.00327E+000 7.27781E-001 194.94 0.63 202.12 1.08 205.32 5.02

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 10:02:03 AM Page 4

• • • • • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.954 7.377378E+000 1.439773E+000 Pb-212 0.628 1.444684E-001 4.170069E-002 BI-214 0.996 1.529652E-001 7.860337E-002 Ra-226 0.962 1.075375E+001 1.506451E+000 U-235 0.740 7.364969E-001 2.704435E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

• • • • • • • • • • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 10:01:59 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified.

Nuclide MDA Report 7/6/2017 10:02:03 AM Page 5

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W3H-ERRU-0310-S-P-6 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 7.524E-001 7.52E-001 7.377E+000 2.964E-00 Pb-210 46.54 4.25 2.118E+000 2.12E+000 2.089E+000 1.007E+00 BI-212 727.33 6.67 1.833E+000 1.83E+000 6.376E-001 8.475E-00 785.37 1.10 1.224E+001 2.203E+000 5.671E+00 1078.62 0.56 3.003E+001 1.450E+000 1.385E+00 1620.50 1.47 1.127E+001 3.189E+000 4.999E+00

+ Pb-212 74.82* 10.28 4.678E-001 8.45E-002 8.035E-001 2.233E-00 77.11 17.10 3.771E-001 4.603E-002 1.823E-00 86.83 2.07 2.503E+000 2.132E-001 1.204E+00 87.35 3.97 1.204E+000 -1.540E+000 5.768E-00 89.78* 1.46 2.020E+000 1.994E+000 9.428E-00 115.18 0.60 6.268E+000 -4.886E+000 2.974E+00 238.63* 43.60 8.450E-002 1.164E-001 3.885E-00 300.09 3.30 1.792E+000 -2.563E+000 8.396E-00

+ BI-214 76.86 0.55 1.198E+001 1.34E-001 1.592E+000 5.793E+00 79.29 0.91 5.273E+000 1.121E+000 2.521E+00 609.32* 45.49 1.335E-001 1.530E-001 5.825E-00 665.45 1.53 8.498E+000 1.268E+000 3.973E+00 768.36 4.89 2.836E+000 1.192E+000 1.319E+00 806.18 1.26 1.055E+001 7.258E+000 4.873E+00 934.06 3.11 4.050E+000 -2.081E+000 1.839E+00 1120.29 14.92 1.138E+000 2.308E-001 5.238E-00 1155.21 1.63 1.181E+001 -3.739E-001 5.481E+00 1238.11 5.83 3.172E+000 -3.156E+000 1.459E+00 1280.98 1.43 1.087E+001 -3.721E+000 4.907E+00 1377.67 3.99 3.751E+000 -1.016E+000 1.672E+00 1385.31 0.79 1.820E+001 -3.829E+000 8.075E+00 1401.52 1.33 1.163E+001 4.156E+000 5.199E+00 1407.99 2.39 6.608E+000 -2.686E-001 2.960E+00 1509.21 2.13 6.297E+000 -1.013E-001 2.737E+00 1583.20 0.70 2.149E+001 2.128E+000 9.451E+00 1661.27 1.05 1.548E+001 2.963E+000 6.828E+00 1729.59 2.88 5.977E+000 4.156E+000 2.644E+00 1764.49 15.30 1.195E+000 8.938E-001 5.315E-00 1847.43 2.03 6.972E+000 -2.114E-001 2.966E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00 PB-214 74.82 5.80 1.198E+000 2.19E-001 1.538E+000 5.804E-00 77.11 9.70 6.649E-001 8.114E-002 3.215E-00 86.83 1.70 3.048E+000 2.596E-001 1.466E+00 87.35 2.24 2.133E+000 -2.730E+000 1.022E+00

Nuclide MDA Report 7/6/2017 10:02:03 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram PB-214 89.78 0.82 5.368E+000 2.19E-001 -7.023E+000 2.564E+00 241.99 7.25 8.767E-001 -4.908E-001 4.176E-00 258.76 0.53 1.007E+001 3.305E+000 4.733E+00 295.22 18.42 3.649E-001 2.886E-001 1.725E-00 351.93 35.60 2.191E-001 9.803E-002 1.034E-00 785.96 1.06 1.273E+001 3.550E+000 5.899E+00 839.07 0.58 2.328E+001 -1.999E+000 1.074E+00

+ Ra-226 81.07 0.20 2.175E+001 1.31E+000 -9.393E+000 1.035E+00 83.79 0.32 1.722E+001 2.995E+001 8.295E+00 186.21* 3.64 1.305E+000 1.075E+001 6.196E-00 AC-228 89.96 1.90 1.864E+007 4.47E+006 -2.057E+007 8.938E+00 93.35 3.10 1.115E+007 1.297E+007 5.342E+00 99.51 1.26 1.921E+007 -7.045E+006 9.044E+00 105.60 0.74 3.768E+007 -2.340E+007 1.789E+00 129.07 2.42 1.110E+007 2.655E+006 5.248E+00 153.98 0.72 4.179E+007 -4.606E+006 1.981E+00 209.25 3.89 9.698E+006 -1.782E+007 4.598E+00 214.85 0.76 4.420E+007 -5.452E+006 2.079E+00 270.24 3.46 1.217E+007 8.233E+006 5.726E+00 328.00 2.95 1.527E+007 -2.828E+006 7.127E+00 338.32 11.27 4.466E+006 -6.118E+005 2.095E+00 409.46 1.92 2.791E+007 2.488E+006 1.296E+00 463.00 4.40 1.533E+007 2.573E+006 7.172E+00 562.50 0.87 8.830E+007 -3.928E+006 4.111E+00 674.75 2.10 3.888E+007 -1.009E+007 1.794E+00 726.86 0.62 1.414E+008 1.012E+007 6.522E+00 755.32 1.00 8.547E+007 -3.289E+007 3.922E+00 772.29 1.49 6.743E+007 4.315E+007 3.130E+00 794.95 4.25 2.109E+007 -1.045E+007 9.676E+00 830.49 0.54 1.783E+008 -3.154E+007 8.205E+00 835.71 1.61 6.197E+007 2.052E+007 2.858E+00 840.38 0.91 1.102E+008 1.352E+007 5.083E+00 904.20 0.77 1.494E+008 -7.421E+007 6.930E+00 911.20 25.80 4.526E+006 2.589E+006 2.101E+00 964.77 4.99 2.690E+007 3.098E+007 1.257E+00 968.97 15.80 8.113E+006 6.174E+006 3.778E+00 1247.08 0.50 2.632E+008 -1.873E+007 1.207E+00 1459.14 0.83 3.345E+008 8.018E+008 1.597E+00 1495.91 0.86 1.237E+008 3.764E+007 5.437E+00 1588.20 3.22 3.482E+007 -8.791E+006 1.531E+00 1630.63 1.51 7.415E+007 -2.540E+006 3.249E+00 TH-230 67.67 0.38 1.207E+001 1.21E+001 -4.879E+000 5.720E+00 PA-234 742.81 0.11 1.191E+002 1.90E+001 6.581E+001 5.514E+00 766.42 0.32 4.195E+001 4.026E-001 1.945E+00 1001.03 0.84 1.904E+001 3.373E+000 8.788E+00 TH-234 63.29 3.70 1.431E+000 1.43E+000 7.944E-001 6.807E-00 92.38 2.13 2.416E+000 2.836E+000 1.162E+00 92.80 2.10 2.377E+000 2.542E+000 1.142E+00 112.81 0.21 1.825E+001 -1.277E+001 8.670E+00 U-234 53.20 0.12 5.502E+001 5.50E+001 2.882E+001 2.615E+00 120.90 0.04 1.040E+002 -8.405E+000 4.926E+00

Nuclide MDA Report 7/6/2017 10:02:03 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96* 3.43 8.597E-001 3.68E-001 8.489E-001 4.013E-00 93.35 5.54 8.452E-001 9.837E-001 4.051E-00 104.82 0.69 5.341E+000 -2.279E+000 2.531E+00 105.60 1.31 2.885E+000 -1.792E+000 1.370E+00 108.58 0.50 8.161E+000 -2.816E+000 3.890E+00 109.19 1.66 2.459E+000 -3.606E-001 1.172E+00 143.76* 10.96 3.677E-001 6.765E-001 1.745E-00 163.36* 5.08 8.149E-001 1.003E+000 3.858E-00 194.94 0.63 7.127E+000 2.667E+000 3.366E+00 202.12 1.08 4.876E+000 -2.041E+000 2.319E+00 205.32 5.02 1.120E+000 4.664E-001 5.341E-00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 10:02:03 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0310\\W3H-ERRU-03 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 7.38E+000 19.516 Pb-212 74.8 8.04E-001 26.138 6.905[45.031] 9.87 -1.795 89.8 1.99E+000 87.198 17.138[94.595] [ 0.582]

238.6 ^ 1.16E-001 36.669 1.000[51.858]

BI-214 609.3 ^ 1.53E-001 51.386 Ra-226 186.2 ^ 1.08E+001 14.009 U-235 90.0 8.49E-001 87.257 1.255[99.071] -0.04 0.041 143.8 ^ 6.76E-001 46.918 1.000[66.352] [ 2.106]

163.4 1.00E+000 72.541 1.483[86.391]