ML19095B145

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Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W3H-ERRU-0310-S-P-3
ML19095B145
Person / Time
Site: 07000371
Issue date: 03/01/2018
From:
Cabrera Services
To:
NRC Region 1
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Download: ML19095B145 (9)
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          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0310\\W3H-ERRU-03 Report Generated On : 7/6/2017 10:00:28 AM Sample Title : W3H-ERRU-0310-S-P-3 Sample Description :

Sample Identification : 0310-S-P-3 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 2.384E+002 grams Sample Taken On : 6/1/2017 2:00:00 PM Acquisition Started : 6/7/2017 8:06:59 AM Live Time : 1800.0 seconds Real Time : 1800.4 seconds Dead Time : 0.02 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 10:00:28 AM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W3H-ERRU-0310-S-P-3 Peak Analysis Performed on: 7/6/2017 10:00:24 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts M 1 296-315 300.09 75.21 0.68 1.09E+002 22.02 7.93E+001 m 2 296-315 308.74 77.37 0.68 5.50E+001 16.54 8.71E+001 F 3 331-341 337.73 84.63 0.74 5.99E+001 61.73 6.60E+001 F 4 568-579 574.29 143.82 0.48 4.81E+001 49.18 3.45E+001 F 5 736-748 741.68 185.71 0.87 1.84E+002 26.90 5.85E+001 F 6 947-958 953.06 238.61 0.99 6.20E+001 56.22 3.90E+001 F 7 1174-1183 1178.84 295.11 0.53 2.79E+001 12.50 2.40E+001 F 8 1399-1411 1405.60 351.85 0.84 4.35E+001 15.30 2.47E+001 F 9 2032-2045 2040.39 510.71 0.55 4.58E+001 13.27 3.62E+001 F 10 5823-5848 5836.61 1460.69 2.46 1.30E+002 23.65 1.30E+001 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 10:00:28 AM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W3H-ERRU-0310-S-P-3 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.997 1460.82* 10.66 9.01406E+000 1.76544E+000 Pb-212 0.995 74.82* 10.28 1.00233E+000 2.42713E-001 77.11* 17.10 2.96814E-001 9.75228E-002 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 1.83359E-001 1.67249E-001 300.09 3.30 PB-214 0.849 74.82* 5.80 1.77654E+000 4.58615E-001 77.11* 9.70 5.23249E-001 1.78259E-001 86.83 1.70 87.35 2.24 89.78 0.82 241.99 7.25 258.76 0.53 295.22* 18.42 2.40112E-001 1.09916E-001 351.93* 35.60 2.33059E-001 8.42103E-002 785.96 1.06 839.07 0.58 Ra-226 0.957 81.07 0.20 83.79* 0.32 1.62233E+001 1.68350E+001 186.21* 3.64 5.25743E+000 9.50253E-001 U-235 1.000 89.96 3.43 93.35 5.54 104.82 0.69 105.60 1.31 108.58 0.50 109.19 1.66 143.76* 10.96 3.90287E-001 4.01060E-001 163.36 5.08 194.94 0.63 202.12 1.08 205.32 5.02

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 10:00:28 AM Page 3

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.997 9.014057E+000 1.765445E+000 Pb-212 0.995 2.429464E-001 8.401391E-002 PB-214 0.849 2.409201E-001 6.554818E-002 Ra-226 0.957 5.292254E+000 9.487426E-001 U-235 1.000 3.902873E-001 4.010596E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 10:00:24 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 9 510.71 2.5457E-002 28.96 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 7/6/2017 10:00:28 AM Page 4

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W3H-ERRU-0310-S-P-3 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 1.473E+000 1.47E+000 9.014E+000 6.425E-00 Pb-210 46.54 4.25 2.413E+000 2.41E+000 1.762E+000 1.146E+00 BI-212 727.33 6.67 2.267E+000 2.27E+000 6.890E-001 1.052E+00 785.37 1.10 1.425E+001 1.071E+001 6.598E+00 1078.62 0.56 3.493E+001 1.867E+001 1.610E+00 1620.50 1.47 1.351E+001 2.341E+000 6.010E+00

+ Pb-212 74.82* 10.28 4.043E-001 1.04E-001 1.002E+000 1.898E-00 77.11* 17.10 2.488E-001 2.968E-001 1.171E-00 86.83 2.07 2.622E+000 -1.169E+000 1.255E+00 87.35 3.97 1.228E+000 -1.592E+000 5.845E-00 89.78 1.46 3.147E+000 -2.735E+000 1.494E+00 115.18 0.60 6.391E+000 -1.371E+000 3.007E+00 238.63* 43.60 1.040E-001 1.834E-001 4.802E-00 300.09 3.30 2.065E+000 -3.191E+000 9.662E-00 BI-214 76.86 0.55 1.414E+001 3.20E-001 3.145E+001 6.839E+00 79.29 0.91 6.373E+000 2.300E+000 3.051E+00 609.32 45.49 3.202E-001 1.184E-001 1.501E-00 665.45 1.53 9.502E+000 1.421E+000 4.427E+00 768.36 4.89 3.555E+000 1.860E+000 1.661E+00 806.18 1.26 1.180E+001 -7.158E+000 5.430E+00 934.06 3.11 5.426E+000 -1.111E-001 2.494E+00 1120.29 14.92 1.619E+000 1.178E+000 7.563E-00 1155.21 1.63 1.202E+001 -3.467E-001 5.508E+00 1238.11 5.83 3.982E+000 -3.432E-001 1.842E+00 1280.98 1.43 1.173E+001 -8.280E+000 5.243E+00 1377.67 3.99 4.572E+000 -2.152E+000 2.048E+00 1385.31 0.79 2.508E+001 6.821E+000 1.134E+00 1401.52 1.33 1.366E+001 -1.101E+000 6.106E+00 1407.99 2.39 6.870E+000 -4.333E+000 3.030E+00 1509.21 2.13 7.811E+000 -7.731E-001 3.423E+00 1583.20 0.70 2.814E+001 -5.186E+000 1.255E+00 1661.27 1.05 1.378E+001 2.135E+000 5.818E+00 1729.59 2.88 5.200E+000 -3.553E+000 2.196E+00 1764.49 15.30 1.459E+000 7.466E-001 6.520E-00 1847.43 2.03 7.163E+000 3.612E+000 2.971E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 7.166E-001 1.47E-001 1.777E+000 3.363E-00 77.11* 9.70 4.386E-001 5.232E-001 2.065E-00 86.83 1.70 3.193E+000 -1.423E+000 1.528E+00 87.35 2.24 2.176E+000 -2.821E+000 1.036E+00

Nuclide MDA Report 7/6/2017 10:00:28 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78 0.82 5.603E+000 1.47E-001 -4.870E+000 2.661E+00 241.99 7.25 1.142E+000 -2.972E-001 5.464E-00 258.76 0.53 1.114E+001 -1.993E+000 5.213E+00 295.22* 18.42 2.198E-001 2.401E-001 9.824E-00 351.93* 35.60 1.472E-001 2.331E-001 6.638E-00 785.96 1.06 1.470E+001 3.358E+000 6.799E+00 839.07 0.58 2.812E+001 1.140E+001 1.300E+00

+ Ra-226 81.07 0.20 2.290E+001 1.24E+000 1.666E+001 1.083E+00 83.79* 0.32 1.291E+001 1.622E+001 6.088E+00 186.21* 3.64 1.244E+000 5.257E+000 5.833E-00 AC-228 89.96 1.90 1.529E+007 4.31E+006 -3.002E+007 7.288E+00 93.35 3.10 9.670E+006 -3.220E+005 4.617E+00 99.51 1.26 1.792E+007 2.150E+006 8.432E+00 105.60 0.74 2.969E+007 -1.170E+007 1.395E+00 129.07 2.42 9.774E+006 7.824E+005 4.605E+00 153.98 0.72 3.667E+007 4.817E+006 1.731E+00 209.25 3.89 7.874E+006 -1.331E+006 3.701E+00 214.85 0.76 3.832E+007 -7.999E+006 1.792E+00 270.24 3.46 1.097E+007 -4.256E+006 5.146E+00 328.00 2.95 1.510E+007 2.312E+006 7.070E+00 338.32 11.27 4.312E+006 8.174E+005 2.026E+00 409.46 1.92 3.023E+007 8.075E+006 1.418E+00 463.00 4.40 1.464E+007 -5.083E+006 6.857E+00 562.50 0.87 8.452E+007 -3.916E+007 3.940E+00 674.75 2.10 4.067E+007 6.597E+006 1.891E+00 726.86 0.62 1.420E+008 3.626E+007 6.585E+00 755.32 1.00 9.129E+007 9.813E+006 4.233E+00 772.29 1.49 6.712E+007 3.410E+007 3.128E+00 794.95 4.25 2.074E+007 3.589E+006 9.551E+00 830.49 0.54 1.593E+008 -1.268E+008 7.296E+00 835.71 1.61 6.118E+007 4.600E+007 2.833E+00 840.38 0.91 1.088E+008 -2.656E+007 5.037E+00 904.20 0.77 1.455E+008 -4.023E+007 6.765E+00 911.20 25.80 4.570E+006 3.014E+006 2.132E+00 964.77 4.99 2.485E+007 1.426E+007 1.160E+00 968.97 15.80 7.536E+006 4.048E+006 3.505E+00 1247.08 0.50 2.455E+008 -5.539E+007 1.124E+00 1459.14 0.83 3.291E+008 7.908E+008 1.574E+00 1495.91 0.86 9.424E+007 3.781E+007 4.009E+00 1588.20 3.22 3.867E+007 2.650E+007 1.736E+00 1630.63 1.51 7.676E+007 1.038E+007 3.406E+00 TH-230 67.67 0.38 1.278E+001 1.28E+001 -4.821E+000 6.022E+00 PA-234 742.81 0.11 1.482E+002 2.01E+001 -3.523E+001 6.890E+00 766.42 0.32 5.286E+001 2.204E+001 2.464E+00 1001.03 0.84 2.013E+001 2.139E+000 9.208E+00 TH-234 63.29 3.70 1.545E+000 1.54E+000 2.017E-001 7.316E-00 92.38 2.13 2.617E+000 4.283E+000 1.255E+00 92.80 2.10 2.553E+000 2.089E+000 1.222E+00 112.81 0.21 1.800E+001 -7.301E+000 8.465E+00 U-234 53.20 0.12 5.647E+001 5.65E+001 1.397E+001 2.664E+00 120.90 0.04 1.048E+002 -4.039E+001 4.917E+00

Nuclide MDA Report 7/6/2017 10:00:28 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96 3.43 1.430E+000 2.70E-001 -2.807E+000 6.813E-00 93.35 5.54 9.132E-001 -3.040E-002 4.360E-00 104.82 0.69 5.597E+000 -1.409E+000 2.635E+00 105.60 1.31 2.831E+000 -1.115E+000 1.330E+00 108.58 0.50 7.287E+000 -4.052E+000 3.420E+00 109.19 1.66 2.247E+000 -6.394E-001 1.056E+00 143.76* 10.96 2.698E-001 3.903E-001 1.239E-00 163.36 5.08 9.540E-001 -1.032E-001 4.516E-00 194.94 0.63 8.530E+000 -5.514E+000 4.033E+00 202.12 1.08 5.264E+000 5.155E+000 2.493E+00 205.32 5.02 1.142E+000 8.567E-001 5.408E-00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 10:00:28 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
===================================================

Analysis using Key Line Activities

===================================================

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0310\\W3H-ERRU-03 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 9.01E+000 19.585 Pb-212 74.8 1.00E+000 24.215 5.466[94.373] 5.43 -0.998 77.1 2.97E-001 32.857 1.619[96.951] [ 1.271]

238.6 ^ 1.83E-001 91.214 1.000[128.99]

PB-214 74.8 1.78E+000 25.815 7.623[44.407] 5.89 -1.016 77.1 5.23E-001 34.068 2.245[49.661] [ 0.347]

295.2 2.40E-001 45.777 1.030[58.319]

351.9 ^ 2.33E-001 36.133 1.000[51.099]

Ra-226 83.8 1.62E+001 103.77 3.086[105.33] 7.37 -1.411 186.2 ^ 5.26E+000 18.074 1.000[25.561] [ 1.357]

U-235 143.8 ^ 3.90E-001 102.76

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