ML19095B141

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W3H-ERRU-0310-S-P-2

ML19095B141
Person / Time
Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
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References
Download: ML19095B141 (10)

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• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0310\\W3H-ERRU-03 Report Generated On : 7/6/2017 9:59:53 AM Sample Title : W3H-EERU-0310-S-P-2 Sample Description :

Sample Identification : 0310-S-P-2 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 2.990E+002 grams Sample Taken On : 6/1/2017 2:00:00 PM Acquisition Started : 6/6/2017 2:41:53 PM Live Time : 1800.0 seconds Real Time : 1800.5 seconds Dead Time : 0.03 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 9:59:53 AM Page 1

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Detector Name: 8566 Sample

Title:

W3H-EERU-0310-S-P-2 Peak Analysis Performed on: 7/6/2017 9:59:48 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 208-219 213.15 53.45 0.67 7.04E+001 18.53 8.00E+001 M 2 296-313 299.94 75.17 0.71 1.49E+002 95.52 1.83E+002 m 3 296-313 308.29 77.26 0.71 8.59E+001 49.84 2.24E+002 F 4 333-345 337.15 84.48 0.84 2.29E+002 30.06 1.91E+002 F 5 356-365 359.16 89.99 0.67 1.30E+002 24.59 1.18E+002 F 6 365-381 373.01 93.45 0.78 1.54E+002 91.20 2.21E+002 F 7 429-440 435.79 109.16 0.40 3.38E+001 31.69 1.30E+002 F 8 566-581 574.32 143.83 0.83 2.95E+002 101.43 1.50E+002 F 9 647-662 652.50 163.40 0.82 1.05E+002 22.39 1.08E+002 F 10 734-750 741.82 185.75 0.91 1.48E+003 147.37 9.56E+001 F 11 813-830 819.78 205.26 0.82 1.01E+002 66.59 8.78E+001 F 12 947-959 952.67 238.51 0.83 1.29E+002 24.40 6.18E+001 F 13 1174-1183 1178.25 294.96 0.64 3.08E+001 39.59 3.40E+001 F 14 1398-1411 1405.38 351.80 0.99 5.15E+001 16.81 3.36E+001 F 15 2321-2335 2327.94 582.67 1.22 4.22E+001 15.46 2.38E+001 F 16 2426-2440 2432.57 608.85 1.15 4.87E+001 16.17 2.38E+001 F 17 5824-5850 5836.16 1460.58 2.95 1.88E+002 27.47 4.50E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:59:53 AM Page 2

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Sample

Title:

W3H-EERU-0310-S-P-2 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.991 1460.82* 10.66 1.03693E+001 1.69583E+000 Pb-212 0.995 74.82* 10.28 1.09183E+000 7.13269E-001 77.11* 17.10 3.69914E-001 2.20105E-001 86.83 2.07 87.35 3.97 89.78* 1.46 6.06614E+000 1.36674E+000 115.18 0.60 238.63* 43.60 3.03251E-001 6.51365E-002 300.09 3.30 BI-214 0.236 76.86* 0.55 1.16065E+001 6.91391E+000 79.29 0.91 609.32* 45.49 2.87072E-001 9.77913E-002 665.45 1.53 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.11 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1583.20 0.70 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 2204.06 4.92 2447.70 1.55 PB-214 0.848 74.82* 5.80 1.93517E+000 1.27601E+000 77.11* 9.70 6.52117E-001 3.92436E-001 86.83 1.70 87.35 2.24 89.78* 0.82 1.08007E+001 2.60748E+000 241.99 7.25 258.76 0.53 295.22* 18.42 2.11399E-001 2.72641E-001 351.93* 35.60 2.19739E-001 7.40832E-002

Interference Corrected Activity Report 7/6/2017 9:59:53 AM Page 3 Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty PB-214 0.848 785.96 1.06 839.07 0.58 Ra-226 0.884 81.07 0.20 83.79* 0.32 4.94456E+001 9.05804E+000 186.21* 3.64 3.37883E+001 4.91204E+000 U-234 0.992 53.20* 0.12 6.57221E+001 2.01395E+001 120.90 0.04 U-235 0.999 89.96* 3.43 2.58207E+000 5.87592E-001 93.35* 5.54 1.86990E+000 1.12938E+000 104.82 0.69 105.60 1.31 108.58 0.50 109.19* 1.66 1.34232E+000 1.28339E+000 143.76* 10.96 1.91066E+000 6.86204E-001 163.36* 5.08 1.56838E+000 3.74076E-001 194.94 0.63 202.12 1.08 205.32* 5.02 1.81690E+000 1.20808E+000

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

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Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.991 1.036930E+001 1.695833E+000 Pb-212 0.995 3.058074E-001 6.194252E-002 BI-214 0.236 2.866273E-001 9.776246E-002 PB-214 0.848 2.208897E-001 7.027824E-002 Ra-226 0.884 3.734636E+001 4.317997E+000 U-234 0.992 6.572207E+001 2.013954E+001 U-235 0.999 1.812091E+000 2.626995E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

• • • • • • • • • • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 9:59:48 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 15 582.67 2.3433E-002 36.66 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 7/6/2017 9:59:53 AM Page 5

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W3H-EERU-0310-S-P-2 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 7.591E-001 7.59E-001 1.037E+001 3.048E-00 Pb-210 46.54 4.25 2.012E+000 2.01E+000 6.757E-001 9.577E-00 BI-212 727.33 6.67 2.067E+000 2.07E+000 -4.777E-002 9.688E-00 785.37 1.10 1.194E+001 2.485E+000 5.551E+00 1078.62 0.56 2.586E+001 6.539E-001 1.184E+00 1620.50 1.47 8.555E+000 -5.269E-001 3.683E+00

+ Pb-212 74.82* 10.28 4.801E-001 1.05E-001 1.092E+000 2.301E-00 77.11* 17.10 3.112E-001 3.699E-001 1.498E-00 86.83 2.07 3.297E+000 -2.662E-001 1.603E+00 87.35 3.97 1.494E+000 -1.385E-001 7.236E-00 89.78* 1.46 2.845E+000 6.066E+000 1.360E+00 115.18 0.60 8.244E+000 -6.576E+000 3.972E+00 238.63* 43.60 1.051E-001 3.033E-001 4.935E-00 300.09 3.30 2.078E+000 -6.556E-001 9.862E-00

+ BI-214 76.86* 0.55 9.764E+000 1.58E-001 1.161E+001 4.699E+00 79.29 0.91 7.087E+000 7.974E-001 3.436E+00 609.32* 45.49 1.578E-001 2.871E-001 7.091E-00 665.45 1.53 8.717E+000 4.055E+000 4.100E+00 768.36 4.89 2.717E+000 1.322E+000 1.266E+00 806.18 1.26 9.786E+000 -5.548E-001 4.518E+00 934.06 3.11 4.546E+000 -7.732E-001 2.099E+00 1120.29 14.92 1.098E+000 -4.911E-002 5.066E-00 1155.21 1.63 9.898E+000 -6.136E+000 4.550E+00 1238.11 5.83 3.286E+000 4.214E-001 1.524E+00 1280.98 1.43 1.244E+001 -2.751E+000 5.724E+00 1377.67 3.99 3.836E+000 2.730E-001 1.728E+00 1385.31 0.79 1.875E+001 -3.941E-002 8.414E+00 1401.52 1.33 1.005E+001 -9.968E-001 4.445E+00 1407.99 2.39 5.845E+000 -7.943E-002 2.600E+00 1509.21 2.13 6.836E+000 5.216E-001 3.033E+00 1583.20 0.70 2.411E+001 1.360E+001 1.084E+00 1661.27 1.05 1.483E+001 3.405E+000 6.560E+00 1729.59 2.88 5.074E+000 1.202E+000 2.215E+00 1764.49 15.30 1.324E+000 1.293E+000 6.003E-00 1847.43 2.03 8.080E+000 -1.836E+000 3.553E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 8.509E-001 1.38E-001 1.935E+000 4.079E-00 77.11* 9.70 5.486E-001 6.521E-001 2.640E-00 86.83 1.70 4.014E+000 -3.242E-001 1.952E+00 87.35 2.24 2.648E+000 -2.454E-001 1.282E+00

Nuclide MDA Report 7/6/2017 9:59:53 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78* 0.82 5.065E+000 1.38E-001 1.080E+001 2.421E+00 241.99 7.25 1.129E+000 -8.977E-002 5.449E-00 258.76 0.53 9.949E+000 -1.297E+000 4.691E+00 295.22* 18.42 2.050E-001 2.114E-001 9.319E-00 351.93* 35.60 1.376E-001 2.197E-001 6.305E-00 785.96 1.06 1.203E+001 -2.239E+000 5.575E+00 839.07 0.58 2.137E+001 -1.448E+001 9.843E+00

+ Ra-226 81.07 0.20 2.962E+001 1.36E+000 -2.615E+001 1.432E+00 83.79* 0.32 1.804E+001 4.945E+001 8.730E+00 186.21* 3.64 1.359E+000 3.379E+001 6.489E-00 AC-228 89.96 1.90 2.900E+006 5.36E+005 4.174E+006 1.410E+00 93.35 3.10 1.765E+006 -2.856E+006 8.582E+00 99.51 1.26 3.104E+006 -1.313E+006 1.493E+00 105.60 0.74 5.676E+006 1.965E+006 2.738E+00 129.07 2.42 1.569E+006 -4.847E+005 7.530E+00 153.98 0.72 5.192E+006 -1.089E+006 2.481E+00 209.25 3.89 1.214E+006 6.451E+005 5.806E+00 214.85 0.76 4.918E+006 -1.778E+006 2.321E+00 270.24 3.46 1.466E+006 7.857E+005 6.951E+00 328.00 2.95 1.885E+006 -9.955E+004 8.885E+00 338.32 11.27 5.616E+005 4.253E+005 2.662E+00 409.46 1.92 3.620E+006 3.245E+005 1.705E+00 463.00 4.40 1.690E+006 4.092E+005 7.932E+00 562.50 0.87 1.013E+007 6.517E+005 4.743E+00 674.75 2.10 4.859E+006 2.182E+005 2.271E+00 726.86 0.62 1.860E+007 4.486E+006 8.722E+00 755.32 1.00 9.688E+006 -6.552E+006 4.473E+00 772.29 1.49 7.177E+006 -2.796E+006 3.334E+00 794.95 4.25 2.646E+006 -6.292E+004 1.231E+00 830.49 0.54 1.902E+007 -1.086E+007 8.759E+00 835.71 1.61 6.729E+006 3.411E+006 3.111E+00 840.38 0.91 1.152E+007 -4.971E+006 5.311E+00 904.20 0.77 1.702E+007 -1.519E+007 7.944E+00 911.20 25.80 5.363E+005 2.274E+005 2.511E+00 964.77 4.99 2.782E+006 1.288E+005 1.298E+00 968.97 15.80 9.422E+005 4.137E+005 4.416E+00 1247.08 0.50 2.810E+007 -3.817E+007 1.290E+00 1459.14 0.83 4.211E+007 1.220E+008 2.026E+00 1495.91 0.86 1.455E+007 4.718E+006 6.490E+00 1588.20 3.22 4.254E+006 1.511E+006 1.905E+00 1630.63 1.51 5.960E+006 -3.130E+006 2.496E+00 TH-230 67.67 0.38 1.567E+001 1.57E+001 -4.061E+000 7.541E+00 PA-234 742.81 0.11 1.252E+002 1.88E+001 -3.702E+000 5.849E+00 766.42 0.32 4.122E+001 1.440E+001 1.918E+00 1001.03 0.84 1.880E+001 2.590E+000 8.719E+00 TH-234 63.29 3.70 1.851E+000 1.85E+000 1.444E+000 8.928E-00 92.38 2.13 3.501E+000 8.743E+000 1.708E+00 92.80 2.10 3.321E+000 -1.393E+000 1.617E+00 112.81 0.21 2.349E+001 -8.024E+000 1.132E+00

+ U-234 53.20* 0.12 5.012E+001 5.01E+001 6.572E+001 2.380E+00 120.90 0.04 1.469E+002 2.576E+001 7.089E+00

Nuclide MDA Report 7/6/2017 9:59:53 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96* 3.43 1.211E+000 4.69E-001 2.582E+000 5.787E-00 93.35* 5.54 1.193E+000 1.870E+000 5.802E-00 104.82 0.69 7.157E+000 1.155E+000 3.448E+00 105.60 1.31 3.854E+000 1.334E+000 1.859E+00 108.58 0.50 1.086E+001 -2.308E+000 5.251E+00 109.19* 1.66 2.689E+000 1.342E+000 1.291E+00 143.76* 10.96 4.689E-001 1.911E+000 2.257E-00 163.36* 5.08 9.267E-001 1.568E+000 4.431E-00 194.94 0.63 7.714E+000 8.382E-001 3.672E+00 202.12 1.08 5.998E+000 -1.356E+000 2.888E+00 205.32* 5.02 1.044E+000 1.817E+000 4.976E-00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 9:59:53 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0310\\W3H-ERRU-03 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 1.04E+001 16.354 Pb-212 74.8 1.09E+000 65.328 3.600[68.768] 11.16 -2.016 77.1 3.70E-001 59.502 1.220[63.260] [ 0.385]

89.8 6.07E+000 22.531 20.004[31.129]

238.6 ^ 3.03E-001 21.479 1.000[30.376]

BI-214 76.9 1.16E+001 59.569 40.431[68.622] 11.46 -1.787 609.3 ^ 2.87E-001 34.065 1.000[48.175] [ 0.405]

PB-214 74.8 1.94E+000 65.938 8.807[74.057] 11.52 -1.947 77.1 6.52E-001 60.179 2.968[68.979] [ 0.388]

89.8 1.08E+001 24.142 49.152[41.467]

295.2 2.11E-001 128.97 0.962[133.30]

351.9 ^ 2.20E-001 33.714 1.000[47.679]

Ra-226 83.8 4.94E+001 18.319 1.463[23.387] 2.49 -0.477 186.2 ^ 3.38E+001 14.538 1.000[20.559] [ 0.390]

U-234 53.2 ^ 6.57E+001 30.643 U-235 90.0 2.58E+000 22.757 1.351[42.517] 2.38 -0.489 93.3 1.87E+000 60.398 0.979[70.269] [ 0.772]

109.2 1.34E+000 95.610 0.703[102.13]

143.8 ^ 1.91E+000 35.915 1.000[50.791]

163.4 1.57E+000 23.851 0.821[43.113]

205.3 1.82E+000 66.491 0.951[75.571]