ML19095B139

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Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - W3H-ERRU-0310-S-P-1
ML19095B139
Person / Time
Site: 07000371
Issue date: 03/01/2018
From:
Cabrera Services
To:
NRC Region 1
Shared Package
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References
Download: ML19095B139 (11)
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          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0310\\W3H-ERRU-03 Report Generated On : 7/6/2017 9:59:22 AM Sample Title : W3H-EERU-0310-S-P-1 Sample Description :

Sample Identification : 0310-S-P-1 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 3.768E+002 grams Sample Taken On : 6/1/2017 2:00:00 PM Acquisition Started : 6/6/2017 1:43:54 PM Live Time : 1800.0 seconds Real Time : 1800.5 seconds Dead Time : 0.03 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 7/6/2017 Efficiency ID : H-IMC-2002-S-P-5

Peak Analysis Report 7/6/2017 9:59:22 AM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W3H-EERU-0310-S-P-1 Peak Analysis Performed on: 7/6/2017 9:59:19 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts M 1 295-320 299.85 75.15 0.71 1.73E+002 27.40 1.38E+002 m 2 295-320 308.17 77.23 0.71 1.50E+002 25.29 1.57E+002 F 3 736-749 741.99 185.79 0.96 1.89E+002 89.70 8.23E+001 F 4 947-958 952.88 238.56 0.79 1.90E+002 29.48 7.80E+001 F 5 1173-1185 1179.19 295.20 1.08 4.90E+001 17.12 4.81E+001 F 6 1346-1357 1352.03 338.45 0.54 3.26E+001 47.06 2.88E+001 F 7 1397-1411 1404.91 351.68 1.34 1.13E+002 22.00 3.45E+001 F 8 2425-2441 2433.12 608.99 1.29 7.25E+001 56.06 2.13E+001 F 9 5824-5850 5836.24 1460.60 2.46 2.40E+002 31.52 1.50E+001 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:59:22 AM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W3H-EERU-0310-S-P-1 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.992 1460.82* 10.66 1.04995E+001 1.58008E+000 Pb-212 0.997 74.82* 10.28 1.00306E+000 2.08557E-001 77.11* 17.10 5.12791E-001 1.10103E-001 86.83 2.07 87.35 3.97 89.78 1.46 115.18 0.60 238.63* 43.60 3.55917E-001 6.58108E-002 300.09 3.30 BI-214 0.216 76.86* 0.55 1.60894E+001 3.48474E+000 79.29 0.91 609.32* 45.49 3.39481E-001 2.63640E-001 665.45 1.53 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.11 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1583.20 0.70 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 2204.06 4.92 2447.70 1.55 PB-214 0.847 74.82* 5.80 1.77784E+000 4.02424E-001 77.11* 9.70 9.03992E-001 2.10471E-001 86.83 1.70 87.35 2.24 89.78 0.82 241.99 7.25 258.76 0.53 295.22* 18.42 2.67284E-001 9.64426E-002 351.93* 35.60 3.83792E-001 8.11526E-002

Interference Corrected Activity Report 7/6/2017 9:59:22 AM Page 3 Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty PB-214 0.847 785.96 1.06 839.07 0.58 Ra-226 0.976 81.07 0.20 83.79 0.32 186.21* 3.64 3.42172E+000 1.66448E+000 AC-228 0.150 89.96 1.90 93.35 3.10 99.51 1.26 105.60 0.74 129.07 2.42 153.98 0.72 209.25 3.89 214.85 0.76 270.24 3.46 328.00 2.95 338.32* 11.27 2.50207E+005 3.62058E+005 409.46 1.92 463.00 4.40 562.50 0.87 674.75 2.10 726.86 0.62 755.32 1.00 772.29 1.49 794.95 4.25 830.49 0.54 835.71 1.61 840.38 0.91 904.20 0.77 911.20 25.80 964.77 4.99 968.97 15.80 1247.08 0.50 1459.14 0.83 1495.91 0.86 1588.20 3.22 1630.63 1.51

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 7/6/2017 9:59:22 AM Page 4

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.992 1.049947E+001 1.580077E+000 Pb-212 0.997 3.753470E-001 5.493938E-002 BI-214 0.216 3.263000E-001 2.630653E-001 PB-214 0.847 3.453336E-001 5.939357E-002 Ra-226 0.976 3.421721E+000 1.664484E+000 AC-228 0.150 2.502069E+005 3.620577E+005

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 7/6/2017 9:59:18 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide All peaks were identified.

Nuclide MDA Report 7/6/2017 9:59:22 AM Page 5

          • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W3H-EERU-0310-S-P-1 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 1.002E+000 1.00E+000 1.050E+001 4.416E-00 Pb-210 46.54 4.25 1.596E+000 1.60E+000 6.068E-001 7.600E-00 BI-212 727.33 6.67 1.670E+000 1.67E+000 7.392E-001 7.838E-00 785.37 1.10 9.842E+000 5.106E-001 4.587E+00 1078.62 0.56 2.188E+001 -4.750E+000 1.008E+00 1620.50 1.47 8.718E+000 4.303E+000 3.888E+00

+ Pb-212 74.82* 10.28 3.331E-001 9.10E-002 1.003E+000 1.587E-00 77.11* 17.10 2.084E-001 5.128E-001 9.958E-00 86.83 2.07 2.245E+000 6.557E-001 1.087E+00 87.35 3.97 1.097E+000 -1.703E+000 5.298E-00 89.78 1.46 2.741E+000 -2.980E+000 1.320E+00 115.18 0.60 5.094E+000 -2.528E+000 2.428E+00 238.63* 43.60 9.098E-002 3.559E-001 4.296E-00 300.09 3.30 1.807E+000 -9.910E-001 8.615E-00

+ BI-214 76.86* 0.55 6.539E+000 1.23E-001 1.609E+001 3.124E+00 79.29 0.91 5.679E+000 8.542E-001 2.754E+00 609.32* 45.49 1.230E-001 3.395E-001 5.517E-00 665.45 1.53 6.993E+000 -4.334E-002 3.291E+00 768.36 4.89 2.187E+000 -6.255E-001 1.020E+00 806.18 1.26 8.661E+000 4.025E+000 4.033E+00 934.06 3.11 4.053E+000 -2.365E-001 1.888E+00 1120.29 14.92 1.125E+000 1.119E+000 5.286E-00 1155.21 1.63 8.852E+000 -1.828E+000 4.109E+00 1238.11 5.83 3.116E+000 2.141E+000 1.464E+00 1280.98 1.43 9.871E+000 2.910E+000 4.542E+00 1377.67 3.99 3.187E+000 1.380E+000 1.443E+00 1385.31 0.79 1.657E+001 -4.472E+000 7.522E+00 1401.52 1.33 9.113E+000 -5.989E+000 4.098E+00 1407.99 2.39 5.488E+000 -2.395E+000 2.488E+00 1509.21 2.13 5.424E+000 -3.913E+000 2.407E+00 1583.20 0.70 1.673E+001 -5.416E+000 7.403E+00 1661.27 1.05 1.150E+001 5.854E+000 5.074E+00 1729.59 2.88 3.680E+000 1.077E+000 1.584E+00 1764.49 15.30 1.036E+000 4.615E-001 4.688E-00 1847.43 2.03 6.566E+000 3.228E+000 2.896E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 5.905E-001 1.13E-001 1.778E+000 2.813E-00 77.11* 9.70 3.674E-001 9.040E-001 1.755E-00 86.83 1.70 2.734E+000 7.985E-001 1.323E+00 87.35 2.24 1.944E+000 -3.018E+000 9.390E-00

Nuclide MDA Report 7/6/2017 9:59:22 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78 0.82 4.880E+000 1.13E-001 -5.307E+000 2.351E+00 241.99 7.25 1.033E+000 -3.006E-001 5.010E-00 258.76 0.53 8.285E+000 4.231E+000 3.918E+00 295.22* 18.42 2.036E-001 2.673E-001 9.440E-00 351.93* 35.60 1.126E-001 3.838E-001 5.172E-00 785.96 1.06 1.031E+001 -3.883E+000 4.810E+00 839.07 0.58 1.811E+001 -4.420E+000 8.384E+00

+ Ra-226 81.07 0.20 1.835E+001 9.45E-001 -1.935E+001 8.786E+00 83.79 0.32 1.365E+001 1.176E+001 6.591E+00 186.21* 3.64 9.451E-001 3.422E+000 4.480E-00

+ AC-228 89.96 1.90 1.658E+006 2.21E+005 -3.080E+006 8.002E+00 93.35 3.10 1.049E+006 4.296E+005 5.072E+00 99.51 1.26 1.817E+006 -1.557E+004 8.663E+00 105.60 0.74 3.381E+006 1.697E+006 1.619E+00 129.07 2.42 1.059E+006 3.740E+005 5.072E+00 153.98 0.72 3.429E+006 -2.724E+006 1.633E+00 209.25 3.89 8.589E+005 -4.330E+005 4.106E+00 214.85 0.76 4.389E+006 1.903E+006 2.096E+00 270.24 3.46 1.106E+006 3.034E+005 5.259E+00 328.00 2.95 1.441E+006 3.542E+005 6.819E+00 338.32* 11.27 2.215E+005 2.502E+005 1.004E+00 409.46 1.92 2.707E+006 1.639E+006 1.279E+00 463.00 4.40 1.442E+006 7.416E+005 6.840E+00 562.50 0.87 7.475E+006 -4.216E+005 3.509E+00 674.75 2.10 3.528E+006 1.529E+006 1.651E+00 726.86 0.62 1.356E+007 9.730E+006 6.367E+00 755.32 1.00 8.083E+006 -9.298E+006 3.777E+00 772.29 1.49 5.189E+006 1.693E+006 2.413E+00 794.95 4.25 2.061E+006 1.109E+006 9.651E+00 830.49 0.54 1.531E+007 -2.201E+006 7.119E+00 835.71 1.61 5.083E+006 2.389E+006 2.361E+00 840.38 0.91 8.743E+006 2.437E+006 4.051E+00 904.20 0.77 1.333E+007 -7.499E+006 6.263E+00 911.20 25.80 4.233E+005 4.109E+004 1.995E+00 964.77 4.99 2.496E+006 2.145E+006 1.182E+00 968.97 15.80 7.808E+005 5.782E+005 3.694E+00 1247.08 0.50 2.500E+007 6.467E+005 1.168E+00 1459.14 0.83 3.393E+007 1.027E+008 1.640E+00 1495.91 0.86 1.036E+007 1.817E+006 4.619E+00 1588.20 3.22 3.134E+006 2.228E+006 1.409E+00 1630.63 1.51 6.491E+006 -2.164E+005 2.901E+00 TH-230 67.67 0.38 1.225E+001 1.22E+001 4.316E+000 5.889E+00 PA-234 742.81 0.11 9.799E+001 1.58E+001 -5.184E+001 4.572E+00 766.42 0.32 3.511E+001 7.599E+000 1.642E+00 1001.03 0.84 1.578E+001 -2.281E+000 7.345E+00 TH-234 63.29 3.70 1.276E+000 1.28E+000 4.148E-002 6.123E-00 92.38 2.13 2.117E+000 2.459E+000 1.024E+00 92.80 2.10 2.154E+000 2.923E+000 1.043E+00 112.81 0.21 1.505E+001 -9.655E+000 7.186E+00 U-234 53.20 0.12 4.544E+001 4.54E+001 8.592E+000 2.171E+00 120.90 0.04 9.096E+001 4.732E+001 4.343E+00

Nuclide MDA Report 7/6/2017 9:59:22 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram U-235 89.96 3.43 1.231E+000 3.45E-001 -2.287E+000 5.941E-00 93.35 5.54 7.868E-001 3.222E-001 3.804E-00 104.82 0.69 4.909E+000 3.998E+000 2.351E+00 105.60 1.31 2.559E+000 1.285E+000 1.226E+00 108.58 0.50 6.833E+000 4.500E+000 3.275E+00 109.19 1.66 2.014E+000 -2.259E-001 9.646E-00 143.76 10.96 3.447E-001 2.797E-001 1.654E-00 163.36 5.08 7.265E-001 2.805E-001 3.472E-00 194.94 0.63 6.251E+000 3.285E+000 2.979E+00 202.12 1.08 3.931E+000 5.219E-001 1.877E+00 205.32 5.02 8.567E-001 -6.078E-001 4.091E-00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

7/6/2017 9:59:22 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
===================================================

Analysis using Key Line Activities

===================================================

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0310\\W3H-ERRU-03 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 1.05E+001 15.049 Pb-212 74.8 1.00E+000 20.792 2.818[27.825] 3.43 -0.627 77.1 5.13E-001 21.471 1.441[28.336] [ 0.287]

238.6 ^ 3.56E-001 18.491 1.000[26.150]

BI-214 76.9 1.61E+001 21.659 47.394[80.623] 11.95 -1.864 609.3 ^ 3.39E-001 77.660 1.000[109.82] [ 0.658]

PB-214 74.8 1.78E+000 22.636 4.632[30.975] 5.02 -0.885 77.1 9.04E-001 23.282 2.355[31.451] [ 0.222]

295.2 2.67E-001 36.082 0.696[41.822]

351.9 ^ 3.84E-001 21.145 1.000[29.903]

Ra-226 186.2 ^ 3.42E+000 48.645

7/6/17 9:59:22 LACE - Key Line Results Page 2 Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

AC-228 338.3 2.50E+005 ******

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