ML19095B084

Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - UNC-IMC-2002-S-P-3

ML19095B084
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Site:	07000371
Issue date:	03/01/2018
From:	Cabrera Services
To:	NRC Region 1
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• • • • • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2002\\UNC-IMC-200 Report Generated On : 5/15/2017 10:42:41 AM Sample Title : W3H-IMC-2002-S-P-3 Sample Description :

Sample Identification : IMC-2002-S-P-3 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 4.480E+002 grams Sample Taken On : 5/3/2017 12:00:00 AM Acquisition Started : 5/9/2017 10:59:15 AM Live Time : 1800.0 seconds Real Time : 1800.5 seconds Dead Time : 0.03 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 5/15/2017 Efficiency ID : H-IMC-2002-S-P-3

Peak Analysis Report 5/15/2017 10:42:41 AM Page 1

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Detector Name: 8566 Sample

Title:

W3H-IMC-2002-S-P-3 Peak Analysis Performed on: 5/15/2017 10:42:33 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 58-70 65.29 16.45 0.72 2.04E+002 96.19 1.07E+002 M 2 286-314 290.70 72.86 0.82 7.60E+001 39.08 1.74E+002 m 3 286-314 299.52 75.07 0.83 2.22E+002 89.10 2.33E+002 m 4 286-314 308.37 77.28 0.83 1.70E+002 68.53 2.19E+002 M 5 331-365 337.61 84.59 0.74 1.40E+002 27.91 2.14E+002 m 6 331-365 348.76 87.39 0.74 4.77E+001 20.62 2.20E+002 m 7 331-365 359.47 90.07 0.75 5.96E+001 21.65 2.09E+002 F 8 365-376 372.88 93.42 0.83 1.10E+002 82.83 1.58E+002 F 9 568-580 574.80 143.95 0.82 1.45E+002 26.39 1.43E+002 F 10 643-658 652.67 163.44 0.88 6.63E+001 70.84 1.42E+002 F 11 736-750 741.78 185.74 0.92 7.85E+002 53.79 1.05E+002 F 12 814-825 819.72 205.24 0.73 5.48E+001 19.13 8.25E+001 F 13 943-958 953.06 238.61 1.01 2.47E+002 88.43 1.10E+002 F 14 1175-1186 1179.24 295.21 0.78 3.68E+001 16.45 5.16E+001 F 15 1345-1356 1350.73 338.12 1.15 4.21E+001 16.49 3.96E+001 F 16 1399-1411 1405.55 351.84 0.99 9.96E+001 60.52 2.73E+001 F 17 2321-2337 2328.23 582.74 1.34 7.15E+001 19.95 3.83E+001 F 18 2425-2441 2433.38 609.05 1.17 8.00E+001 57.36 2.55E+001 F 19 5823-5851 5835.69 1460.46 2.67 2.42E+002 31.40 9.67E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/15/2017 10:42:41 AM Page 2

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Sample

Title:

W3H-IMC-2002-S-P-3 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.979 1460.82* 10.66 1.12720E+001 1.74696E+000 Pb-212 0.998 74.82* 10.28 1.60987E+000 7.22380E-001 77.11* 17.10 7.19112E-001 3.24481E-001 86.83 2.07 87.35* 3.97 7.95081E-001 3.79161E-001 89.78* 1.46 2.65843E+000 1.10237E+000 115.18 0.60 238.63* 43.60 5.12673E-001 2.00508E-001 300.09 3.30 BI-214 0.199 76.86* 0.55 2.25629E+001 1.02012E+001 79.29 0.91 609.32* 45.49 4.06327E-001 2.95088E-001 665.45 1.53 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.11 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1583.20 0.70 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 2204.06 4.92 2447.70 1.55 PB-214 0.849 74.82* 5.80 2.85335E+000 1.30556E+000 77.11* 9.70 1.26771E+000 5.83299E-001 86.83 1.70 87.35* 2.24 1.40914E+000 6.82680E-001 89.78* 0.82 4.73331E+000 2.00521E+000 241.99 7.25 258.76 0.53 295.22* 18.42 2.20799E-001 1.04706E-001 351.93* 35.60 3.69902E-001 2.31187E-001

Interference Corrected Activity Report 5/15/2017 10:42:41 AM Page 3 Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty PB-214 0.849 785.96 1.06 839.07 0.58 Ra-226 0.884 81.07 0.20 83.79* 0.32 2.93633E+001 8.29173E+000 186.21* 3.64 1.59304E+001 2.91065E+000 U-235 0.998 89.96* 3.43 1.13157E+000 4.70620E-001 93.35* 5.54 1.26982E+000 9.90874E-001 104.82 0.69 105.60 1.31 108.58 0.50 109.19 1.66 143.76* 10.96 8.49386E-001 2.28300E-001 163.36* 5.08 8.90493E-001 9.65872E-001 194.94 0.63 202.12 1.08 205.32* 5.02 8.68636E-001 3.33065E-001

• = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

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Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.979 1.127202E+001 1.746955E+000 Pb-212 0.998 5.861822E-001 1.521473E-001 BI-214 0.199 4.056614E-001 2.949777E-001 PB-214 0.849 2.555869E-001 9.390171E-002 Ra-226 0.884 1.740402E+001 2.746359E+000 U-235 0.998 8.641472E-001 1.690469E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/15/2017 10:42:41 AM Page 5

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Peak Locate Performed on: 5/15/2017 10:42:33 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 1 16.45 1.1347E-001 47.09 M 2 72.86 4.2200E-002 51.45 F 15 338.12 2.3369E-002 39.19 F 17 582.74 3.9711E-002 27.91 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 5/15/2017 10:42:41 AM Page 6

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Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W3H-IMC-2002-S-P-3 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 8.945E-001 8.94E-001 1.127E+001 3.843E-00 Pb-210 46.54 4.25 2.637E+000 2.64E+000 2.729E+000 1.265E+00 BI-212 727.33 6.67 1.836E+000 1.84E+000 1.208E+000 8.627E-00 785.37 1.10 1.136E+001 3.209E+000 5.319E+00 1078.62 0.56 2.584E+001 2.433E+000 1.200E+00 1620.50 1.47 6.944E+000 -2.121E+000 2.973E+00

+ Pb-212 74.82* 10.28 5.335E-001 1.30E-001 1.610E+000 2.569E-00 77.11* 17.10 3.029E-001 7.191E-001 1.457E-00 86.83 2.07 3.234E+000 -2.113E+000 1.574E+00 87.35* 3.97 1.196E+000 7.951E-001 5.752E-00 89.78* 1.46 3.121E+000 2.658E+000 1.500E+00 115.18 0.60 8.155E+000 7.280E+000 3.938E+00 238.63* 43.60 1.295E-001 5.127E-001 6.195E-00 300.09 3.30 1.948E+000 6.474E-001 9.279E-00

+ BI-214 76.86* 0.55 9.505E+000 1.45E-001 2.256E+001 4.573E+00 79.29 0.91 7.654E+000 -3.126E-001 3.721E+00 609.32* 45.49 1.449E-001 4.063E-001 6.556E-00 665.45 1.53 8.007E+000 1.208E+000 3.781E+00 768.36 4.89 2.555E+000 1.098E+000 1.198E+00 806.18 1.26 1.014E+001 7.185E+000 4.748E+00 934.06 3.11 3.909E+000 -9.263E-001 1.806E+00 1120.29 14.92 1.117E+000 4.696E-001 5.223E-00 1155.21 1.63 9.600E+000 7.117E+000 4.462E+00 1238.11 5.83 2.890E+000 1.018E+000 1.345E+00 1280.98 1.43 9.954E+000 -1.704E+000 4.558E+00 1377.67 3.99 3.889E+000 1.249E-001 1.784E+00 1385.31 0.79 1.899E+001 5.514E+000 8.687E+00 1401.52 1.33 9.837E+000 7.000E-001 4.431E+00 1407.99 2.39 5.397E+000 1.896E-001 2.427E+00 1509.21 2.13 5.372E+000 -2.792E-001 2.362E+00 1583.20 0.70 1.849E+001 -1.315E+001 8.224E+00 1661.27 1.05 1.159E+001 3.203E+000 5.079E+00 1729.59 2.88 3.623E+000 7.391E-001 1.541E+00 1764.49 15.30 1.172E+000 1.205E-001 5.342E-00 1847.43 2.03 6.256E+000 -1.283E+000 2.720E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 9.455E-001 1.07E-001 2.853E+000 4.554E-00 77.11* 9.70 5.340E-001 1.268E+000 2.569E-00 86.83 1.70 3.938E+000 -2.573E+000 1.916E+00 87.35* 2.24 2.119E+000 1.409E+000 1.020E+00

Nuclide MDA Report 5/15/2017 10:42:41 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78* 0.82 5.557E+000 1.07E-001 4.733E+000 2.671E+00 241.99 7.25 1.229E+000 -1.599E+000 5.976E-00 258.76 0.53 1.007E+001 -3.044E+000 4.789E+00 295.22* 18.42 2.268E-001 2.208E-001 1.053E-00 351.93* 35.60 1.068E-001 3.699E-001 4.840E-00 785.96 1.06 1.159E+001 3.516E+000 5.421E+00 839.07 0.58 2.277E+001 -5.215E+000 1.067E+00

+ Ra-226 81.07 0.20 2.911E+001 1.22E+000 2.143E+001 1.407E+00 83.79* 0.32 1.478E+001 2.936E+001 7.108E+00 186.21* 3.64 1.216E+000 1.593E+001 5.804E-00 AC-228 89.96 1.90 1.276E+008 2.63E+007 -1.980E+008 6.194E+00 93.35 3.10 7.742E+007 -4.262E+007 3.760E+00 99.51 1.26 1.483E+008 -4.534E+007 7.149E+00 105.60 0.74 2.701E+008 -9.055E+007 1.306E+00 129.07 2.42 8.030E+007 5.533E+007 3.877E+00 153.98 0.72 2.757E+008 -2.227E+007 1.329E+00 209.25 3.89 5.768E+007 1.896E+007 2.773E+00 214.85 0.76 2.614E+008 -2.382E+008 1.249E+00 270.24 3.46 6.698E+007 3.549E+007 3.192E+00 328.00 2.95 8.594E+007 -8.107E+007 4.073E+00 338.32 11.27 2.625E+007 -2.458E+006 1.252E+00 409.46 1.92 1.674E+008 2.780E+007 7.937E+00 463.00 4.40 8.985E+007 7.848E+007 4.278E+00 562.50 0.87 4.418E+008 2.338E+008 2.077E+00 674.75 2.10 2.301E+008 9.693E+007 1.085E+00 726.86 0.62 7.832E+008 4.542E+008 3.680E+00 755.32 1.00 4.670E+008 -7.292E+007 2.183E+00 772.29 1.49 3.464E+008 1.059E+008 1.628E+00 794.95 4.25 1.096E+008 1.303E+007 5.105E+00 830.49 0.54 9.848E+008 3.409E+008 4.618E+00 835.71 1.61 3.260E+008 -1.580E+008 1.527E+00 840.38 0.91 5.648E+008 -3.352E+008 2.640E+00 904.20 0.77 8.374E+008 -1.061E+009 3.956E+00 911.20 25.80 2.852E+007 4.203E+007 1.357E+00 964.77 4.99 1.333E+008 1.230E+008 6.288E+00 968.97 15.80 4.247E+007 4.618E+007 2.004E+00 1247.08 0.50 1.283E+009 -1.400E+008 5.948E+00 1459.14 0.83 1.878E+009 5.976E+009 9.068E+00 1495.91 0.86 6.062E+008 -1.115E+008 2.715E+00 1588.20 3.22 1.905E+008 1.324E+008 8.639E+00 1630.63 1.51 2.697E+008 -8.238E+007 1.155E+00 TH-230 67.67 0.38 1.827E+001 1.83E+001 -8.287E+000 8.835E+00 PA-234 742.81 0.11 1.088E+002 1.72E+001 2.109E+001 5.085E+00 766.42 0.32 3.813E+001 -2.053E+001 1.784E+00 1001.03 0.84 1.716E+001 9.131E+000 7.997E+00 TH-234 63.29 3.70 1.932E+000 1.93E+000 7.634E-001 9.324E-00 92.38 2.13 3.072E+000 5.436E+000 1.495E+00 92.80 2.10 2.991E+000 1.529E-001 1.454E+00 112.81 0.21 2.273E+001 -2.486E+001 1.097E+00 U-234 53.20 0.12 7.264E+001 7.26E+001 4.959E+001 3.496E+00 120.90 0.04 1.355E+002 -1.179E+002 6.535E+00

Nuclide MDA Report 5/15/2017 10:42:41 AM Page 8 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96* 3.43 1.329E+000 3.90E-001 1.132E+000 6.386E-00 93.35* 5.54 8.589E-001 1.270E+000 4.138E-00 104.82 0.69 7.400E+000 3.688E+000 3.578E+00 105.60 1.31 3.845E+000 -1.289E+000 1.859E+00 108.58 0.50 1.031E+001 -9.235E-001 4.986E+00 109.19 1.66 3.077E+000 -1.792E-001 1.489E+00 143.76* 10.96 3.897E-001 8.494E-001 1.869E-00 163.36* 5.08 9.483E-001 8.905E-001 4.560E-00 194.94 0.63 8.078E+000 -2.262E+000 3.875E+00 202.12 1.08 5.336E+000 6.736E-001 2.569E+00 205.32* 5.02 7.921E-001 8.686E-001 3.746E-00

+ = Nuclide identified during the nuclide identification

• = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

5/15/2017 10:42:41 LACE Lace v3.2.1 Page 1

• • • • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***

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Analysis using Key Line Activities

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Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2002\\UNC-IMC-200 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

• All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 1.13E+001 15.498 Pb-212 74.8 1.61E+000 44.872 3.140[59.524] 4.35 -0.784 77.1 7.19E-001 45.123 1.403[59.713] [ 0.581]

87.3 7.95E-001 47.688 1.551[61.675]

89.8 2.66E+000 41.467 5.185[57.001]

238.6 ^ 5.13E-001 39.110 1.000[55.310]

BI-214 76.9 2.26E+001 45.212 55.529[85.547] 12.44 -1.940 609.3 ^ 4.06E-001 72.623 1.000[102.70] [ 0.646]

PB-214 74.8 2.85E+000 45.755 7.714[77.458] 8.28 -1.475 77.1 1.27E+000 46.012 3.427[77.610] [ 0.513]

87.3 1.41E+000 48.447 3.809[79.078]

89.8 4.73E+000 42.364 12.796[75.504]

295.2 2.21E-001 47.421 0.597[78.454]

351.9 ^ 3.70E-001 62.499 1.000[88.388]

Ra-226 83.8 2.94E+001 28.238 1.843[33.634] 4.00 -0.766 186.2 ^ 1.59E+001 18.271 1.000[25.839] [ 0.531]

U-235 90.0 1.13E+000 41.590 1.332[49.519] 2.03 -0.391 93.3 1.27E+000 78.033 1.495[82.532] [ 0.761]

143.8 ^ 8.49E-001 26.878 1.000[38.011]

163.4 8.90E-001 108.46 1.048[111.74]

205.3 8.69E-001 38.343 1.023[46.826]