ML19095B078

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Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - UNC-IMC-2002-S-P-1
ML19095B078
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Site: 07000371
Issue date: 03/01/2018
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Download: ML19095B078 (10)
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          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2002\\UNC-IMC-200 Report Generated On : 5/15/2017 10:37:57 AM Sample Title : W3H-IMC-2002-S-P-1 Sample Description :

Sample Identification : IMC-2002-S-P-1 Sample Type :

Sample Geometry : cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 2.910E+002 grams Sample Taken On : 5/3/2017 12:00:00 AM Acquisition Started : 5/9/2017 9:36:51 AM Live Time : 1800.0 seconds Real Time : 1800.5 seconds Dead Time : 0.03 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 5/15/2017 Efficiency ID : H-IMC-2002-S-P-1

Peak Analysis Report 5/15/2017 10:37:57 AM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

W3H-IMC-2002-S-P-1 Peak Analysis Performed on: 5/15/2017 10:37:47 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 48-58 52.85 13.34 0.47 9.15E+001 24.24 1.62E+002 F 2 58-71 65.73 16.56 0.73 4.90E+002 40.69 1.72E+002 F 3 97-109 103.00 25.89 0.53 8.07E+001 21.59 1.24E+002 F 4 205-219 213.33 53.49 0.79 1.87E+002 78.76 1.05E+002 M 5 285-314 291.02 72.94 0.75 1.50E+002 26.16 1.69E+002 m 6 285-314 299.64 75.09 0.76 2.62E+002 32.39 2.20E+002 m 7 285-314 308.34 77.27 0.77 6.97E+001 22.06 2.10E+002 F 8 331-344 337.34 84.53 0.84 4.26E+002 39.66 2.22E+002 M 9 345-365 349.76 87.64 0.81 3.97E+001 30.46 1.39E+002 m 10 345-365 359.79 90.15 0.82 1.64E+002 92.38 1.86E+002 F 11 365-379 373.26 93.52 0.96 2.54E+002 32.97 2.43E+002 F 12 431-441 436.62 109.37 0.45 9.55E+001 73.40 1.39E+002 F 13 569-582 574.45 143.86 0.83 5.45E+002 44.78 1.14E+002 F 14 648-657 652.83 163.48 0.88 2.27E+002 30.24 8.25E+001 F 15 736-755 741.89 185.77 0.91 2.30E+003 88.80 1.00E+002 M 16 802-827 808.35 202.40 0.94 4.55E+001 15.66 3.91E+001 m 17 802-827 819.86 205.28 0.94 2.06E+002 44.40 3.68E+001 F 18 946-958 952.90 238.57 1.02 1.01E+002 67.85 5.85E+001 F 19 1400- 1411 1405.24 351.76 0.91 4.07E+001 15.52 3.00E+001 F 20 5824-5848 5835.64 1460.45 2.41 1.72E+002 26.70 9.72E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/15/2017 10:37:57 AM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

W3H-IMC-2002-S-P-1 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.978 1460.82* 10.66 1.04844E+001 1.85739E+000 Pb-212 0.996 74.82* 10.28 2.15960E+000 5.10948E-001 77.11* 17.10 3.37851E-001 1.26769E-001 86.83 2.07 87.35* 3.97 7.69694E-001 6.11222E-001 89.78* 1.46 8.58136E+000 5.11785E+000 115.18 0.60 238.63* 43.60 2.63262E-001 1.82239E-001 300.09 3.30 PB-214 0.510 74.82* 5.80 3.82770E+000 9.68208E-001 77.11* 9.70 5.95592E-001 2.29822E-001 86.83 1.70 87.35* 2.24 1.36414E+000 1.08953E+000 89.78* 0.82 1.52790E+001 9.20809E+000 241.99 7.25 258.76 0.53 295.22 18.42 351.93* 35.60 1.92420E-001 7.86240E-002 785.96 1.06 839.07 0.58 Ra-226 0.886 81.07 0.20 83.79* 0.32 1.03339E+002 2.28511E+001 186.21* 3.64 5.81922E+001 1.01079E+001 U-234 0.550 53.20* 0.12 1.98449E+002 9.63620E+001 120.90 0.04 U-235 0.997 89.96* 3.43 3.65268E+000 2.18156E+000 93.35* 5.54 3.45473E+000 8.29742E-001 104.82 0.69 105.60 1.31 108.58 0.50 109.19* 1.66 4.24239E+000 3.42703E+000 143.76* 10.96 3.92659E+000 8.40256E-001 163.36* 5.08 3.77911E+000 8.67303E-001 194.94 0.63 202.12* 1.08 4.15542E+000 1.58173E+000 205.32* 5.02 4.09473E+000 1.09597E+000

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/15/2017 10:37:57 AM Page 3

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.978 1.048444E+001 1.857394E+000 Pb-212 0.996 3.208456E-001 1.045385E-001 PB-214 0.510 1.983605E-001 7.702558E-002 Ra-226 0.886 6.558021E+001 9.243901E+000 U-234 0.550 1.984486E+002 9.636201E+001 U-235 0.997 3.798277E+000 4.138181E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/15/2017 10:37:57 AM Page 4

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 5/15/2017 10:37:47 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 1 13.34 5.0831E-002 26.50 F 2 16.56 2.7196E-001 8.31 F 3 25.89 4.4843E-002 26.74 M 5 72.94 8.3448E-002 17.41 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 5/15/2017 10:37:57 AM Page 5

          • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: cylinder Sample

Title:

W3H-IMC-2002-S-P-1 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 1.132E+000 1.13E+000 1.048E+001 4.837E-00 Pb-210 46.54 4.25 2.612E+000 2.61E+000 2.405E+000 1.251E+00 BI-212 727.33 6.67 2.064E+000 2.06E+000 2.644E-001 9.607E-00 785.37 1.10 1.201E+001 -7.293E+000 5.541E+00 1078.62 0.56 3.168E+001 -1.257E+001 1.464E+00 1620.50 1.47 1.088E+001 -1.600E+000 4.786E+00

+ Pb-212 74.82* 10.28 5.915E-001 1.14E-001 2.160E+000 2.846E-00 77.11* 17.10 3.403E-001 3.379E-001 1.636E-00 86.83 2.07 4.358E+000 -8.505E+000 2.128E+00 87.35* 3.97 1.118E+000 7.697E-001 5.327E-00 89.78* 1.46 3.456E+000 8.581E+000 1.657E+00 115.18 0.60 9.863E+000 4.738E+000 4.763E+00 238.63* 43.60 1.137E-001 2.633E-001 5.330E-00 300.09 3.30 2.170E+000 -3.677E+000 1.026E+00 BI-214 76.86 0.55 1.801E+001 3.05E-001 3.849E+001 8.797E+00 79.29 0.91 8.639E+000 2.993E-001 4.198E+00 609.32 45.49 3.045E-001 2.140E-001 1.434E-00 665.45 1.53 8.632E+000 4.943E+000 4.030E+00 768.36 4.89 3.262E+000 2.373E+000 1.528E+00 806.18 1.26 1.031E+001 -5.504E+000 4.737E+00 934.06 3.11 4.785E+000 1.372E+000 2.200E+00 1120.29 14.92 1.417E+000 2.085E-001 6.617E-00 1155.21 1.63 1.139E+001 1.976E+000 5.253E+00 1238.11 5.83 3.570E+000 1.034E+000 1.654E+00 1280.98 1.43 1.125E+001 -1.013E+000 5.077E+00 1377.67 3.99 4.437E+000 1.344E+000 2.009E+00 1385.31 0.79 2.209E+001 1.741E-001 9.984E+00 1401.52 1.33 1.110E+001 2.412E+000 4.910E+00 1407.99 2.39 5.455E+000 -3.890E+000 2.371E+00 1509.21 2.13 5.914E+000 -2.252E+000 2.532E+00 1583.20 0.70 2.276E+001 -7.152E-001 1.004E+00 1661.27 1.05 1.484E+001 3.516E+000 6.479E+00 1729.59 2.88 3.946E+000 -7.884E-002 1.617E+00 1764.49 15.30 1.542E+000 1.261E+000 7.029E-00 1847.43 2.03 7.480E+000 1.788E-001 3.202E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 1.048E+000 1.39E-001 3.828E+000 5.044E-00 77.11* 9.70 6.000E-001 5.956E-001 2.884E-00 86.83 1.70 5.307E+000 -1.036E+001 2.592E+00 87.35* 2.24 1.981E+000 1.364E+000 9.442E-00

Nuclide MDA Report 5/15/2017 10:37:57 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78* 0.82 6.153E+000 1.39E-001 1.528E+001 2.951E+00 241.99 7.25 1.162E+000 -6.512E-001 5.597E-00 258.76 0.53 1.142E+001 8.813E+000 5.395E+00 295.22 18.42 3.909E-001 7.623E-002 1.851E-00 351.93* 35.60 1.392E-001 1.924E-001 6.320E-00 785.96 1.06 1.285E+001 -6.514E+000 5.942E+00 839.07 0.58 2.435E+001 -1.381E+000 1.124E+00

+ Ra-226 81.07 0.20 3.625E+001 1.63E+000 2.580E+001 1.757E+00 83.79* 0.32 2.236E+001 1.033E+002 1.085E+00 186.21* 3.64 1.629E+000 5.819E+001 7.802E-00 AC-228 89.96 1.90 1.439E+008 2.23E+007 -2.605E+008 7.009E+00 93.35 3.10 9.451E+007 -9.867E+007 4.614E+00 99.51 1.26 1.439E+008 -2.162E+008 6.924E+00 105.60 0.74 2.876E+008 -5.590E+007 1.392E+00 129.07 2.42 7.648E+007 -3.711E+007 3.680E+00 153.98 0.72 2.764E+008 -3.941E+007 1.330E+00 209.25 3.89 5.457E+007 -1.108E+006 2.608E+00 214.85 0.76 2.317E+008 7.425E+007 1.096E+00 270.24 3.46 6.214E+007 8.834E+006 2.936E+00 328.00 2.95 7.943E+007 -2.704E+006 3.728E+00 338.32 11.27 2.235E+007 6.092E+006 1.051E+00 409.46 1.92 1.586E+008 1.028E+008 7.456E+00 463.00 4.40 7.179E+007 -1.664E+007 3.354E+00 562.50 0.87 4.752E+008 1.340E+008 2.231E+00 674.75 2.10 1.977E+008 -1.101E+007 9.168E+00 726.86 0.62 7.486E+008 -1.256E+008 3.481E+00 755.32 1.00 4.698E+008 2.927E+007 2.181E+00 772.29 1.49 3.589E+008 1.477E+008 1.679E+00 794.95 4.25 1.214E+008 2.560E+007 5.656E+00 830.49 0.54 9.493E+008 -1.237E+008 4.407E+00 835.71 1.61 3.041E+008 -1.233E+008 1.406E+00 840.38 0.91 5.408E+008 2.741E+008 2.500E+00 904.20 0.77 7.693E+008 -2.388E+008 3.590E+00 911.20 25.80 2.423E+007 -5.422E+006 1.134E+00 964.77 4.99 1.155E+008 -2.832E+007 5.354E+00 968.97 15.80 3.928E+007 4.193E+007 1.831E+00 1247.08 0.50 1.310E+009 -8.687E+007 6.025E+00 1459.14 0.83 1.818E+009 4.701E+009 8.732E+00 1495.91 0.86 5.744E+008 -2.376E+008 2.517E+00 1588.20 3.22 1.775E+008 6.773E+007 7.877E+00 1630.63 1.51 4.114E+008 1.008E+008 1.839E+00 TH-230 67.67 0.38 1.968E+001 1.97E+001 -1.702E+001 9.509E+00 PA-234 742.81 0.11 1.277E+002 2.03E+001 3.254E+001 5.927E+00 766.42 0.32 4.929E+001 1.177E+001 2.306E+00 1001.03 0.84 2.026E+001 -8.033E-001 9.375E+00 TH-234 63.29 3.70 2.109E+000 2.11E+000 -1.367E-002 1.018E+00 92.38 2.13 4.497E+000 1.380E+001 2.200E+00 92.80 2.10 4.336E+000 3.862E+000 2.119E+00 112.81 0.21 2.764E+001 -1.102E+001 1.334E+00

+ U-234 53.20* 0.12 6.991E+001 6.99E+001 1.984E+002 3.351E+00 120.90 0.04 1.788E+002 1.536E+002 8.654E+00

Nuclide MDA Report 5/15/2017 10:37:57 AM Page 7 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96* 3.43 1.471E+000 4.39E-001 3.653E+000 7.055E-00 93.35* 5.54 1.339E+000 3.455E+000 6.512E-00 104.82 0.69 9.273E+000 9.391E+000 4.490E+00 105.60 1.31 4.780E+000 -9.292E-001 2.314E+00 108.58 0.50 1.398E+001 3.539E+000 6.792E+00 109.19* 1.66 3.024E+000 4.242E+000 1.452E+00 143.76* 10.96 4.387E-001 3.927E+000 2.096E-00 163.36* 5.08 7.913E-001 3.779E+000 3.731E-00 194.94 0.63 8.897E+000 4.807E+000 4.243E+00 202.12* 1.08 2.906E+000 4.155E+000 1.329E+00 205.32* 5.02 6.154E-001 4.095E+000 2.808E-00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

5/15/2017 10:37:57 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
===================================================

Analysis using Key Line Activities

===================================================

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-2002\\UNC-IMC-200 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 1.05E+001 17.716 Pb-212 74.8 2.16E+000 23.659 8.203[73.155] 7.34 -1.297 77.1 3.38E-001 37.522 1.283[78.739] [ 0.966]

87.3 7.70E-001 79.411 2.924[105.34]

89.8 8.58E+000 59.639 32.596[91.371]

238.6 ^ 2.63E-001 69.224 1.000[97.897]

PB-214 74.8 3.83E+000 25.295 19.892[48.056] 9.66 -1.630 77.1 5.96E-001 38.587 3.095[56.201] [ 0.437]

87.3 1.36E+000 79.869 7.089[89.714]

89.8 1.53E+001 60.266 79.404[72.812]

351.9 ^ 1.92E-001 40.861 1.000[57.786]

Ra-226 83.8 1.03E+002 22.113 1.776[28.119] 3.76 -0.719 186.2 ^ 5.82E+001 17.370 1.000[24.565] [ 0.468]

U-234 53.2 ^ 1.98E+002 48.558 U-235 90.0 3.65E+000 59.725 0.930[63.443] -0.92 0.180 93.3 3.45E+000 24.018 0.880[32.168] [ 0.482]

109.2 4.24E+000 80.781 1.080[83.567]

143.8 ^ 3.93E+000 21.399 1.000[30.263]

163.4 3.78E+000 22.950 0.962[31.379]

202.1 4.16E+000 38.064 1.058[43.667]

205.3 4.09E+000 26.765 1.043[34.268]

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