ML19095A975

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Appendix E, On-Site Lab Waste Sample Data, Gamma Spec Reports - UNC-IMC-0074-S-P-3
ML19095A975
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Site: 07000371
Issue date: 03/01/2018
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Download: ML19095A975 (9)
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          • G A M M A S P E C T R U M A N A L Y S I S *****

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0074\\UNC-IMC-007 Report Generated On : 5/9/2017 9:59:49 AM Sample Title : UNC-IMC-0074-S-P-3 Sample Description :

Sample Identification : IMC-0074-S-P-3 Sample Type :

Sample Geometry : Cylinder Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 40 - 8192 Peak Area Range (in channels) : 40 - 8192 Identification Energy Tolerance : 1.000 keV Sample Size : 4.140E+002 grams Sample Taken On : 4/18/2017 12:00:00 AM Acquisition Started : 5/2/2017 9:34:52 AM Live Time : 1800.0 seconds Real Time : 1800.6 seconds Dead Time : 0.03 %

Energy Calibration Used Done On : 4/13/2017 Efficiency Calibration Used Done On : 5/9/2017 Efficiency ID : H-IMC-0074-S-P-3

Peak Analysis Report 5/9/2017 9:59:49 AM Page 1

          • P E A K A N A L Y S I S R E P O R T *****

Detector Name: 8566 Sample

Title:

UNC-IMC-0074-S-P-3 Peak Analysis Performed on: 5/9/2017 9:59:43 AM Peak Analysis From Channel: 40 Peak Analysis To Channel: 8192 Peak ROI ROI Peak Energy FWHM Net Peak Net Area Continuum No. start end centroid (keV) (keV) Area Uncert. Counts F 1 59-71 65.40 16.48 0.65 2.44E+002 32.26 1.89E+002 M 2 296-316 299.54 75.07 0.67 1.79E+002 28.90 1.40E+002 m 3 296-316 308.60 77.34 0.68 1.37E+002 25.24 1.71E+002 F 4 332-344 337.06 84.46 0.72 1.11E+002 24.95 1.91E+002 F 5 355-364 359.66 90.11 0.63 7.69E+001 21.54 1.10E+002 F 6 571-580 574.48 143.87 0.71 1.41E+002 24.87 7.38E+001 F 7 647-658 652.47 163.39 0.95 6.53E+001 19.22 8.25E+001 F 8 735-750 741.83 185.75 0.92 7.01E+002 50.53 9.60E+001 M 9 946-970 952.83 238.55 0.94 2.02E+002 29.30 7.05E+001 m 10 946-970 966.26 241.91 0.94 4.46E+001 15.43 4.20E+001 F 11 1399-1411 1405.07 351.72 1.05 8.21E+001 20.06 3.51E+001 F 12 5822-5850 5835.94 1460.52 2.74 2.88E+002 33.80 4.83E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/9/2017 9:59:49 AM Page 2

          • N U C L I D E I D E N T I F I C A T I O N R E P O R T *****

Sample

Title:

UNC-IMC-0074-S-P-3 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201

.................... IDENTIFIED NUCLIDES....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (pCi/gram) Uncertainty K-40 0.986 1460.82* 10.66 1.21122E+001 1.75390E+000 Pb-212 0.996 74.82* 10.28 1.22101E+000 3.15357E-001 77.11* 17.10 5.44140E-001 1.48618E-001 86.83 2.07 87.35 3.97 89.78* 1.46 3.20121E+000 1.10203E+000 115.18 0.60 238.63* 43.60 3.82912E-001 8.22997E-002 300.09 3.30 PB-214 0.650 74.82* 5.80 2.16413E+000 5.91534E-001 77.11* 9.70 9.59258E-001 2.75863E-001 86.83 1.70 87.35 2.24 89.78* 0.82 5.69972E+000 2.02343E+000 241.99* 7.25 5.15641E-001 1.95869E-001 258.76 0.53 295.22 18.42 351.93* 35.60 2.78084E-001 7.92680E-002 785.96 1.06 839.07 0.58 Ra-226 0.965 81.07 0.20 83.79* 0.32 2.16731E+001 6.54245E+000 186.21* 3.64 1.30676E+001 2.40533E+000 U-235 0.541 89.96* 3.43 1.36259E+000 4.71096E-001 93.35 5.54 104.82 0.69 105.60 1.31 108.58 0.50 109.19 1.66 143.76* 10.96 7.61415E-001 2.01791E-001 163.36* 5.08 8.07179E-001 2.81389E-001 194.94 0.63 202.12 1.08 205.32 5.02

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 5/9/2017 9:59:49 AM Page 3

          • I N T E R F E R E N C E C O R R E C T E D R E P O R T *****

Nuclide Wt mean Wt mean Nuclide Id Activity Activity Name Confidence (pCi/gram) Uncertainty K-40 0.986 1.211219E+001 1.753903E+000 Pb-212 0.996 4.134843E-001 7.040152E-002 PB-214 0.650 3.253637E-001 7.095678E-002 Ra-226 0.965 1.409226E+001 2.257593E+000 U-235 0.541 8.132604E-001 1.542098E-001

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis

@ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.960 sigma

                    • U N I D E N T I F I E D P E A K S **********

Peak Locate Performed on: 5/9/2017 9:59:43 AM Peak Locate From Channel: 40 Peak Locate To Channel: 8192 Peak Energy Peak Size in Peak CPS Peak Tol.

No. (keV) Counts per Second % Uncertainty Type Nuclide F 1 16.48 1.3533E-001 13.24 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.960 sigma

Nuclide MDA Report 5/9/2017 9:59:49 AM Page 4

          • N U C L I D E M D A R E P O R T *****

Detector Name: 8566 Sample Geometry: Cylinder Sample

Title:

UNC-IMC-0074-S-P-3 Nuclide Library Used: C:\\GENIE2K\\CAMFILES\\UNC 2017 NLB 0328201 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ K-40 1460.82* 10.66 6.044E-001 6.04E-001 1.211E+001 2.454E-00 Pb-210 46.54 4.25 2.510E+000 2.51E+000 2.216E+000 1.203E+00 BI-212 727.33 6.67 1.703E+000 1.70E+000 3.343E-001 8.014E-00 785.37 1.10 9.190E+000 8.089E-001 4.269E+00 1078.62 0.56 2.240E+001 -8.879E-001 1.036E+00 1620.50 1.47 6.901E+000 -9.189E+000 3.000E+00

+ Pb-212 74.82* 10.28 3.942E-001 7.93E-002 1.221E+000 1.879E-00 77.11* 17.10 2.530E-001 5.441E-001 1.211E-00 86.83 2.07 2.760E+000 2.021E+000 1.339E+00 87.35 3.97 1.311E+000 1.050E+000 6.345E-00 89.78* 1.46 2.458E+000 3.201E+000 1.173E+00 115.18 0.60 6.786E+000 -9.705E-001 3.264E+00 238.63* 43.60 7.930E-002 3.829E-001 3.708E-00 300.09 3.30 1.774E+000 -3.612E+000 8.449E-00 BI-214 76.86 0.55 1.453E+001 2.42E-001 4.665E+001 7.096E+00 79.29 0.91 6.727E+000 1.284E+000 3.264E+00 609.32 45.49 2.417E-001 1.280E-001 1.146E-00 665.45 1.53 5.775E+000 1.938E+000 2.686E+00 768.36 4.89 2.453E+000 7.525E-001 1.154E+00 806.18 1.26 8.201E+000 -8.447E-001 3.810E+00 934.06 3.11 3.939E+000 1.478E+000 1.835E+00 1120.29 14.92 1.049E+000 -3.493E-001 4.918E-00 1155.21 1.63 8.038E+000 -6.787E+000 3.714E+00 1238.11 5.83 2.729E+000 -2.592E-001 1.274E+00 1280.98 1.43 9.779E+000 -2.799E-001 4.511E+00 1377.67 3.99 2.967E+000 -1.674E+000 1.339E+00 1385.31 0.79 1.654E+001 1.542E+001 7.537E+00 1401.52 1.33 9.165E+000 -1.138E+000 4.143E+00 1407.99 2.39 5.552E+000 1.803E+000 2.531E+00 1509.21 2.13 5.406E+000 1.657E+000 2.411E+00 1583.20 0.70 1.829E+001 7.634E+000 8.223E+00 1661.27 1.05 1.124E+001 2.580E+000 4.971E+00 1729.59 2.88 4.421E+000 6.759E-001 1.967E+00 1764.49 15.30 9.435E-001 7.147E-001 4.250E-00 1847.43 2.03 5.644E+000 1.988E+000 2.453E+00

> 2118.51 1.16 0.000E+000 0.000E+000 0.000E+00

> 2204.06 4.92 0.000E+000 0.000E+000 0.000E+00

> 2447.70 1.55 0.000E+000 0.000E+000 0.000E+00

+ PB-214 74.82* 5.80 6.987E-001 1.09E-001 2.164E+000 3.330E-00 77.11* 9.70 4.460E-001 9.593E-001 2.135E-00 86.83 1.70 3.361E+000 2.461E+000 1.631E+00 87.35 2.24 2.324E+000 1.861E+000 1.124E+00

Nuclide MDA Report 5/9/2017 9:59:49 AM Page 5 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ PB-214 89.78* 0.82 4.377E+000 1.09E-001 5.700E+000 2.088E+00 241.99* 7.25 3.798E-001 5.156E-001 1.743E-00 258.76 0.53 9.459E+000 9.902E-001 4.503E+00 295.22 18.42 3.298E-001 1.641E-001 1.575E-00 351.93* 35.60 1.093E-001 2.781E-001 5.007E-00 785.96 1.06 9.713E+000 1.343E+000 4.517E+00 839.07 0.58 1.997E+001 -1.035E-001 9.331E+00

+ Ra-226 81.07 0.20 2.415E+001 1.09E+000 1.299E+001 1.162E+00 83.79* 0.32 1.637E+001 2.167E+001 7.921E+00 186.21* 3.64 1.092E+000 1.307E+001 5.207E-00 AC-228 89.96 1.90 2.440E+017 4.98E+016 -4.690E+017 1.183E+01 93.35 3.10 1.429E+017 2.430E+017 6.923E+01 99.51 1.26 2.616E+017 -1.057E+017 1.255E+01 105.60 0.74 4.890E+017 -4.005E+017 2.356E+01 129.07 2.42 1.498E+017 -1.282E+016 7.218E+01 153.98 0.72 4.965E+017 1.545E+017 2.386E+01 209.25 3.89 1.073E+017 -3.005E+016 5.147E+01 214.85 0.76 4.922E+017 -4.450E+017 2.347E+01 270.24 3.46 1.252E+017 4.202E+016 5.955E+01 328.00 2.95 1.682E+017 -3.062E+016 7.972E+01 338.32 11.27 4.977E+016 2.482E+016 2.371E+01 409.46 1.92 3.001E+017 -9.322E+015 1.417E+01 463.00 4.40 1.485E+017 6.406E+016 7.009E+01 562.50 0.87 8.424E+017 3.260E+017 3.956E+01 674.75 2.10 3.931E+017 2.643E+017 1.840E+01 726.86 0.62 1.542E+018 2.705E+017 7.252E+01 755.32 1.00 9.157E+017 -2.558E+017 4.285E+01 772.29 1.49 6.509E+017 4.554E+017 3.054E+01 794.95 4.25 2.150E+017 1.917E+017 1.003E+01 830.49 0.54 1.809E+018 1.500E+017 8.452E+01 835.71 1.61 6.141E+017 -9.588E+016 2.871E+01 840.38 0.91 1.062E+018 1.124E+016 4.957E+01 904.20 0.77 1.446E+018 -3.522E+018 6.785E+01 911.20 25.80 5.409E+016 3.727E+016 2.570E+01 964.77 4.99 2.400E+017 9.086E+016 1.127E+01 968.97 15.80 7.740E+016 2.176E+016 3.639E+01 1247.08 0.50 2.555E+018 1.043E+018 1.188E+01 1459.14 0.83 3.867E+018 1.300E+019 1.872E+01 1495.91 0.86 1.034E+018 3.522E+017 4.560E+01 1588.20 3.22 3.564E+017 1.299E+017 1.611E+01 1630.63 1.51 7.035E+017 2.704E+017 3.144E+01 TH-230 67.67 0.38 1.657E+001 1.66E+001 5.413E+000 8.002E+00 PA-234 742.81 0.11 1.074E+002 1.49E+001 1.777E+001 5.051E+00 766.42 0.32 3.758E+001 1.973E+001 1.768E+00 1001.03 0.84 1.495E+001 2.163E+000 6.948E+00 TH-234 63.29 3.70 1.872E+000 1.87E+000 6.861E-001 9.042E-00 92.38 2.13 2.753E+000 4.179E+000 1.338E+00 92.80 2.10 2.667E+000 4.163E+000 1.295E+00 112.81 0.21 1.884E+001 -2.937E+001 9.053E+00 U-234 53.20 0.12 6.928E+001 6.93E+001 7.681E+001 3.333E+00 120.90 0.04 1.150E+002 -4.274E+000 5.528E+00

Nuclide MDA Report 5/9/2017 9:59:49 AM Page 6 Nuclide Energy Yield Line MDA Nuclide MDA Activity Dec. Leve Name (keV) (%) (pCi/gram) (pCi/gram) (pCi/gram) (pCi/gram

+ U-235 89.96* 3.43 1.046E+000 2.44E-001 1.363E+000 4.992E-00 93.35 5.54 9.443E-001 1.606E+000 4.576E-00 104.82 0.69 6.337E+000 3.831E+000 3.055E+00 105.60 1.31 3.263E+000 -2.672E+000 1.572E+00 108.58 0.50 8.980E+000 -1.581E+000 4.336E+00 109.19 1.66 2.659E+000 -2.104E+000 1.283E+00 143.76* 10.96 2.438E-001 7.614E-001 1.146E-00 163.36* 5.08 6.173E-001 8.072E-001 2.919E-00 194.94 0.63 6.740E+000 -2.091E-001 3.219E+00 202.12 1.08 4.421E+000 8.019E-001 2.120E+00 205.32 5.02 9.750E-001 -4.383E-001 4.678E-00

+ = Nuclide identified during the nuclide identification

  • = Energy line found in the spectrum

> = MDA value not calculated

@ = Half-life too short to be able to perform the decay correction

5/9/2017 9:59:49 LACE Lace v3.2.1 Page 1

        • L I N E A C T I V I T Y C O N S I S T E N C Y E V A L U A T O R ***
===================================================

Analysis using Key Line Activities

===================================================

Filename: C:\\GENIE2K\\CAMFILES\\UNC 2017\\IMC Samples\\IMC-0074\\UNC-IMC-007 Equation used to calculate plot: ln(Ratio) = A + B*ln(Energy) where: Ratio = Activity/KL Activity Notes:

'^' Denotes Key Line energy

  • All uncertainties quoted at 1.96 sigma Nuclide Energy Activity Activity Ratio[%Uncert] A B (keV) (pCi/gram) %Uncert* [uncert]

K-40 1460.8 ^ 1.21E+001 14.480 Pb-212 74.8 1.22E+000 25.828 3.189[33.601] 5.04 -0.905 77.1 5.44E-001 27.312 1.421[34.755] [ 0.332]

89.8 3.20E+000 34.425 8.360[40.584]

238.6 ^ 3.83E-001 21.493 1.000[30.396]

PB-214 74.8 2.16E+000 27.334 7.782[39.493] 7.58 -1.274 77.1 9.59E-001 28.758 3.450[40.491] [ 0.288]

89.8 5.70E+000 35.501 20.496[45.528]

242.0 5.16E-001 37.986 1.854[47.492]

351.9 ^ 2.78E-001 28.505 1.000[40.312]

Ra-226 83.8 2.17E+001 30.187 1.659[35.356] 3.31 -0.634 186.2 ^ 1.31E+001 18.407 1.000[26.031] [ 0.550]

U-235 90.0 1.36E+000 34.574 1.790[43.562] 5.03 -0.995 143.8 ^ 7.61E-001 26.502 1.000[37.480] [ 0.972]

163.4 8.07E-001 34.861 1.060[43.791]

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